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CN203881849U - System for measuring surface resistivity of material under high-temperature condition - Google Patents

System for measuring surface resistivity of material under high-temperature condition Download PDF

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Publication number
CN203881849U
CN203881849U CN201420166673.XU CN201420166673U CN203881849U CN 203881849 U CN203881849 U CN 203881849U CN 201420166673 U CN201420166673 U CN 201420166673U CN 203881849 U CN203881849 U CN 203881849U
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temperature
high temperature
electrode
surface resistivity
test
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魏明
胡小锋
荣利霞
王雷
刘鹤楠
兰敬辉
刘卫东
曹娟娟
潘明健
李彬
王斌
潘红九
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Ordnance Engineering College of PLA
Beijing Institute of Near Space Vehicles System Engineering
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Ordnance Engineering College of PLA
Beijing Institute of Near Space Vehicles System Engineering
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Abstract

本实用新型公开了一种高温条件下材料表面电阻率测试系统,其由定位以及传输系统、电阻测试系统组成。高温环境由高温加热炉来实现,利用红外测温仪监测材料表面温度变化,依据两电极法设计耐高温的测试电极,高温电极采用耐高温的石墨电极,高温传输线采用石墨线。测试时,首先对受试材料在高温炉内加热至一定的温度,然后迅速取出材料,放在耐高温绝缘底座上,在其自然冷却过程中连续监测材料在高温条件下的表面电阻率。本实用新型整体结构简单,并在操作控制方便。将材料加热后,在高温炉外部测试材料表面电阻率,由耐高温的石墨电极与高温材料接触,同时采用石墨线与测试仪器相连,避免了高温对测试系统的影响,保证了测量的可操作性。

The utility model discloses a material surface resistivity test system under high temperature conditions, which is composed of a positioning and transmission system and a resistance test system. The high-temperature environment is realized by a high-temperature heating furnace. The infrared thermometer is used to monitor the temperature change of the material surface, and the high-temperature-resistant test electrode is designed according to the two-electrode method. The high-temperature electrode adopts a high-temperature resistant graphite electrode, and the high-temperature transmission line adopts a graphite wire. During the test, the test material is first heated to a certain temperature in a high-temperature furnace, and then the material is quickly taken out, placed on a high-temperature insulating base, and the surface resistivity of the material under high-temperature conditions is continuously monitored during the natural cooling process. The utility model has a simple overall structure and is convenient in operation and control. After the material is heated, the surface resistivity of the material is tested outside the high-temperature furnace. The high-temperature-resistant graphite electrode is in contact with the high-temperature material. At the same time, the graphite wire is connected to the test instrument to avoid the impact of high temperature on the test system and ensure the operability of the measurement. sex.

Description

一种高温条件下材料表面电阻率测试系统A material surface resistivity test system under high temperature conditions

技术领域 technical field

本实用新型涉及一种高温条件下材料表面电阻率的测试系统,尤其是飞行器表面隔热材料在高温环境下的表面电阻率。 The utility model relates to a test system for the surface resistivity of materials under high temperature conditions, in particular to the surface resistivity of aircraft surface heat insulation materials under high temperature environments.

背景技术 Background technique

飞行器在空中飞行时因为各种原因产生的静电放电可能导致其油箱的起火爆炸,静电放电产生的辐射还会对飞行器的通讯和导航系统造成干扰,这就需要飞行器的表面材料具有一定的防静电性能。同时,飞行器在空中高速运动过程中会因与大气摩擦而产生很高的热量,尤其是在临近空间的环境下飞行器表面温度可达上千度,为此飞行器表面会覆盖隔热层。对于隔热层的防静电性能如何,尤其是在高温条件下的防静电性能是否达标,这就需要一个重要的参数来衡量,即材料的表面电阻率。然而,材料的表面电阻率会随着温度的变化而发生改变,因此,测量材料的表面电阻率以及高温条件下材料的表面电阻率尤为重要。 When the aircraft is flying in the air, the electrostatic discharge due to various reasons may cause the fuel tank to catch fire and explode. The radiation generated by the electrostatic discharge will also interfere with the communication and navigation system of the aircraft. This requires the surface material of the aircraft to have certain anti-static properties. performance. At the same time, during the high-speed movement of the aircraft in the air, high heat will be generated due to friction with the atmosphere, especially in the environment near space, the surface temperature of the aircraft can reach thousands of degrees, so the surface of the aircraft will be covered with a heat insulation layer. For the antistatic performance of the heat insulation layer, especially whether the antistatic performance under high temperature conditions is up to standard, this requires an important parameter to measure, that is, the surface resistivity of the material. However, the surface resistivity of materials will change with the change of temperature, so it is particularly important to measure the surface resistivity of materials and the surface resistivity of materials under high temperature conditions.

目前,对于常温态下材料的表面电阻率的测试有三电极法、两电极法等测试方法。但是,对于高温条件下材料表面电阻率的测试,由于受加热条件和测试仪器本身的限制,现在还没有很好的测试方法。 At present, there are three-electrode method, two-electrode method and other test methods for testing the surface resistivity of materials at normal temperature. However, due to the limitations of the heating conditions and the testing instrument itself, there is no good testing method for testing the surface resistivity of materials under high temperature conditions.

实用新型内容 Utility model content

本实用新型要解决的技术问题是提供一种结构简单、操作切实可行、测量结果准确的高温条件下材料表面电阻率测试系统。 The technical problem to be solved by the utility model is to provide a material surface resistivity testing system under high temperature conditions with simple structure, practical operation and accurate measurement results.

为解决上述技术问题,本实用新型所采取的技术方案是:一种高温条件下材料表面电阻率测试系统,其关键技术在于:包括定位以及传输系统和电阻测试系统; In order to solve the above technical problems, the technical solution adopted by the utility model is: a material surface resistivity test system under high temperature conditions, the key technology of which is: including positioning and transmission system and resistance test system;

所述定位以及传输系统包括绝缘底座,所述绝缘底座上放置有测试样品,所述测试样品上方设置有两个高温电极,每个高温电极上面设有重锤; The positioning and transmission system includes an insulating base, a test sample is placed on the insulating base, two high-temperature electrodes are arranged above the test sample, and a weight is arranged on each high-temperature electrode;

所述电阻测试系统包括静电电阻测试仪,所述高温电极经高温传输线接静电电阻测试仪的转换接头。 The resistance testing system includes a static resistance tester, and the high-temperature electrode is connected to a conversion joint of the static resistance tester through a high-temperature transmission line.

优选的,所述高温电极为石墨电极,其形状为长条形。 Preferably, the high-temperature electrode is a graphite electrode, and its shape is elongated.

进一步优选的,所述电极长度为12cm,高和宽均为1cm。 Further preferably, the length of the electrode is 12 cm, and the height and width are both 1 cm.

优选的,所述绝缘底座由高温砖和用于增加绝缘性能的聚四氟乙烯板组成,所述聚四氟乙烯板设置于下方,所述高温砖设于聚四氟乙烯板上面,所述高温砖设置两块、且两块之间相隔一定距离;所述测试样品位于高温砖上。 Preferably, the insulating base is composed of high-temperature bricks and polytetrafluoroethylene plates for increasing insulation performance, the polytetrafluoroethylene plates are arranged below, the high-temperature bricks are arranged on the top of the polytetrafluoroethylene plates, and the Two high-temperature bricks are arranged with a certain distance between them; the test sample is located on the high-temperature bricks.

优选的,所述重锤为钢制圆柱体,该圆柱体上设置有一个与高温电极大小一致的凹槽,所述高温电极卡于凹槽内。 Preferably, the weight is a steel cylinder, and a groove with the same size as the high-temperature electrode is arranged on the cylinder, and the high-temperature electrode is stuck in the groove.

优选的,所述高温传输线为石墨线。 Preferably, the high-temperature transmission line is a graphite line.

还包括用于测量测试样品温度的红外测温仪和/或用于加热测试样品的高温炉。 Also included is an infrared thermometer for measuring the temperature of the test sample and/or a high temperature furnace for heating the test sample.

采用上述技术方案所产生的有益效果在于: The beneficial effects produced by adopting the above-mentioned technical scheme are:

1、本实用新型整体结构简单,并且操作控制方便。将材料加热后,在高温炉外部测试材料表面电阻率,由耐高温的石墨电极与高温材料接触,同时采用石墨线与测试仪器相连,避免了高温对测试系统的影响,保证了测量的可操作性。 1. The overall structure of the utility model is simple, and the operation and control are convenient. After the material is heated, the surface resistivity of the material is tested outside the high-temperature furnace, and the high-temperature-resistant graphite electrode is in contact with the high-temperature material. At the same time, the graphite wire is connected to the test instrument to avoid the impact of high temperature on the test system and ensure the operability of the measurement. sex.

2、本实用新型采用红外线测温仪监测材料表面温度,同时利用重锤压住电极增加电极与材料的接触,保证了测量结果的准确性。 2. The utility model uses an infrared thermometer to monitor the surface temperature of the material, and at the same time uses a heavy hammer to press the electrode to increase the contact between the electrode and the material, ensuring the accuracy of the measurement result.

3、本实用新型可灵活用于各种绝缘材料在高温条件下表面电阻率的测试。 3. The utility model can be flexibly used for testing the surface resistivity of various insulating materials under high temperature conditions.

附图说明 Description of drawings

图1是本实用新型的原理框图。 Fig. 1 is a functional block diagram of the utility model.

具体实施方式 Detailed ways

下面结合附图和具体实施方式对本实用新型作进一步详细的说明。 Below in conjunction with accompanying drawing and specific embodiment, the utility model is described in further detail.

参见附图1,本实用新型由定位以及传输系统和常温电阻测试系统组成。本实用新型涉及到的高温炉、红外测温仪和静电电阻测试仪等仪器均采用现有市售产品即可。其中电阻测试系统由转换接头和ACL800表面电阻测试仪组成。 Referring to accompanying drawing 1, the utility model is made up of positioning and transmission system and normal temperature resistance test system. The instruments such as the high-temperature furnace, the infrared thermometer and the electrostatic resistance tester involved in the utility model all adopt existing commercially available products. Among them, the resistance test system consists of a conversion joint and an ACL800 surface resistance tester.

 高温炉的加热温度可达1000℃;高温传输线采用石墨线制作,长度为1m,确保高温不传递给测试仪器;高温电极采用石墨材料制作,制成长条型,长度为12cm,高和宽均为1cm;按压重锤用钢制作成圆柱体,直径10cm,高10cm,其底部挖出一个大小与电极一致的凹槽,使电极恰好卡于凹槽内;绝缘底座由高温砖和聚四氟乙烯板组成,将两块高温砖放置在聚四氟乙烯板上,两块高温砖之间保持一定距离,但要使材料能安放在砖上,这样保障了与所测材料接触的绝缘底座的耐高温性能和其高绝缘性能;转换接头用来连接高温传输线和静电电阻测试仪器,确保测试方便。 The heating temperature of the high-temperature furnace can reach 1000°C; the high-temperature transmission line is made of graphite wire with a length of 1m to ensure that the high temperature is not transmitted to the test instrument; the high-temperature electrode is made of graphite material and is made into a long strip with a length of 12cm and a height and width of 1cm; the pressing weight is made of steel into a cylinder with a diameter of 10cm and a height of 10cm. A groove of the same size as the electrode is dug out at the bottom, so that the electrode is just stuck in the groove; the insulating base is made of high-temperature bricks and polytetrafluoroethylene Two high-temperature bricks are placed on the Teflon board, and a certain distance is kept between the two high-temperature bricks, but the material can be placed on the bricks, so as to ensure the resistance of the insulating base in contact with the material to be tested. High temperature performance and its high insulation performance; the conversion joint is used to connect the high temperature transmission line and the electrostatic resistance testing instrument to ensure convenient testing.

  测试时,将待测材料在高温炉内加热半小时,确保材料充分受热,并加热到指定温度;然后迅速取出材料,将材料放置在事先放置好的绝缘底座的高温砖上;将石墨电极放在绝缘材料的边缘,利用重锤压住石墨电极,凹槽卡住电极,石墨传输线连接测试电极并通过转换接头连接至表面电阻测试仪;同时利用红外测温仪监测材料表面的温度,在其自然冷却过程中连续监测材料在不同温度条件下的表面电阻率。 During the test, heat the material to be tested in a high-temperature furnace for half an hour to ensure that the material is fully heated and heated to the specified temperature; then quickly take out the material and place it on the high-temperature brick on the insulating base that has been placed in advance; place the graphite electrode on the On the edge of the insulating material, use a heavy hammer to press the graphite electrode, the groove clamps the electrode, the graphite transmission line connects the test electrode and connects to the surface resistance tester through the conversion joint; at the same time, the infrared thermometer is used to monitor the temperature of the material surface, and the The surface resistivity of the material under different temperature conditions is continuously monitored during natural cooling.

 本实用新型实现了在高温条件下对材料表面电阻率的测试,利用高温加热炉将材料加热到指定温度,利用红外测温仪监测材料表面温度变化,依据两电极法设计耐高温的石墨测试电极,使用带凹槽的重锤使电极与材料表面充分的接触,所述重锤底部设有凹槽,凹槽与电极的大小一致,使电极恰好卡于凹槽内。采用石墨线作为高温传输线。测试时,首先将受试材料在高温炉内加热至一定的温度,然后迅速取出材料,放在耐高温绝缘底座上,在其自然冷却过程中连续监测材料在高温条件下的表面电阻率,同时利用红外测温仪监测材料表面温度。 The utility model realizes the test of material surface resistivity under high temperature conditions, uses a high-temperature heating furnace to heat the material to a specified temperature, uses an infrared thermometer to monitor the temperature change of the material surface, and designs a high-temperature-resistant graphite test electrode according to the two-electrode method , use a heavy hammer with a groove to make the electrode fully contact with the surface of the material, the bottom of the weight is provided with a groove, the size of the groove is consistent with the size of the electrode, so that the electrode is just stuck in the groove. A graphite wire is used as the high temperature transmission line. During the test, first heat the test material to a certain temperature in a high-temperature furnace, then quickly take out the material, place it on a high-temperature-resistant insulating base, and continuously monitor the surface resistivity of the material under high-temperature conditions during its natural cooling process. The surface temperature of the material is monitored with an infrared thermometer.

对所公开的实施例的上述说明,使本领域专业技术人员能够实现或使用本实用新型。对这些实施例的多种修改对本领域的专业技术人员来说将是显而易见的,本文中所定义的一般原理可以在不脱离本实用新型的精神或范围的情况下,在其它实施例中实现。因此,本实用新型将不会被限制于本文所示的这些实施例,而是要符合与本文所公开的原理和新颖特点相一致的最宽的范围。 The above description of the disclosed embodiments enables those skilled in the art to realize or use the utility model. Various modifications to these embodiments will be readily apparent to those skilled in the art, and the general principles defined herein may be implemented in other embodiments without departing from the spirit or scope of the invention. Therefore, the present invention will not be limited to these embodiments shown herein, but will conform to the widest scope consistent with the principles and novel features disclosed herein.

Claims (7)

1. a material surface resistivity test macro under hot conditions, is characterized in that: comprise location and transmission system and resistance test system;
Described location and transmission system comprise insulator foot, are placed with test sample on described insulator foot, and described test sample top is provided with two high temperature electrodes, above each high temperature electrode, is provided with weight;
Described resistance test system comprises static resistance meter, and described high temperature electrode connects the X-over of static resistance meter through high temperature transmission line.
2. material surface resistivity test macro under hot conditions according to claim 1, is characterized in that: described high temperature electrode is graphite electrode, and it is shaped as strip.
3. material surface resistivity test macro under hot conditions according to claim 2, is characterized in that: described electrode length is 12cm, and height and width are 1cm.
4. material surface resistivity test macro under hot conditions according to claim 1, it is characterized in that: described insulator foot forms by high temperature brick with for increasing the polyfluortetraethylene plate of insulating property, described polyfluortetraethylene plate is arranged at below, described high temperature brick is located at above polyfluortetraethylene plate, and described high temperature brick arranges between two and two separated by a distance; Described test specimens product are positioned on high temperature brick.
5. material surface resistivity test macro under hot conditions according to claim 1, is characterized in that: described weight is steel cylinder, is provided with one and high temperature electrode groove of the same size on this right cylinder, and described high temperature electrode is stuck in groove.
6. material surface resistivity test macro under hot conditions according to claim 1, is characterized in that: described high temperature transmission line is graphite line.
7. according to material surface resistivity test macro under the hot conditions described in claim 1-6 any one, it is characterized in that: also comprise for measure test sample temperature infrared thermometer and/or for heat test sample high temperature furnace.
CN201420166673.XU 2014-04-08 2014-04-08 System for measuring surface resistivity of material under high-temperature condition Expired - Lifetime CN203881849U (en)

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103913635A (en) * 2014-04-08 2014-07-09 中国人民解放军军械工程学院 System for measuring surface resistivity of material on high-temperature condition
CN106771623A (en) * 2017-01-19 2017-05-31 西安交通大学 The test device of insulating materials resistance and resistivity under a kind of hot environment
CN114355042A (en) * 2018-12-24 2022-04-15 深圳御烟实业有限公司 Resistance detection system and method

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103913635A (en) * 2014-04-08 2014-07-09 中国人民解放军军械工程学院 System for measuring surface resistivity of material on high-temperature condition
CN106771623A (en) * 2017-01-19 2017-05-31 西安交通大学 The test device of insulating materials resistance and resistivity under a kind of hot environment
CN106771623B (en) * 2017-01-19 2019-10-11 西安交通大学 A test device for the resistance and resistivity of insulating materials under high temperature environment
CN114355042A (en) * 2018-12-24 2022-04-15 深圳御烟实业有限公司 Resistance detection system and method

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