[go: up one dir, main page]

CN201872227U - Foam generating and property detection and evaluation device for foaming agents - Google Patents

Foam generating and property detection and evaluation device for foaming agents Download PDF

Info

Publication number
CN201872227U
CN201872227U CN 201020596974 CN201020596974U CN201872227U CN 201872227 U CN201872227 U CN 201872227U CN 201020596974 CN201020596974 CN 201020596974 CN 201020596974 U CN201020596974 U CN 201020596974U CN 201872227 U CN201872227 U CN 201872227U
Authority
CN
China
Prior art keywords
foam
generating container
foam generating
container
blowing agent
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN 201020596974
Other languages
Chinese (zh)
Inventor
霍冀川
孙成才
刘佳奇
王程
石荣铭
袁艳红
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Sichuan Huashi Green House Building Materials Co Ltd
Original Assignee
Southwest University of Science and Technology
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Southwest University of Science and Technology filed Critical Southwest University of Science and Technology
Priority to CN 201020596974 priority Critical patent/CN201872227U/en
Application granted granted Critical
Publication of CN201872227U publication Critical patent/CN201872227U/en
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Images

Landscapes

  • Preparation Of Clay, And Manufacture Of Mixtures Containing Clay Or Cement (AREA)

Abstract

一种发泡剂泡沫发生器及性能检测和评价装置,包括:泡沫发生容器,安装有搅拌叶片的搅拌器及搅拌控制装置,其特征是:搅拌器上安装的搅拌叶片为间隔的2-3组,泡沫发生容器外还设置有一个连接有恒温控制装置的水浴容器,还包括一个泡沫导出管,该泡沫导出管的一端与所述泡沫发生容器的底部相连通、另一端穿出水浴容器;泡沫发生容器内上端还可以活动套有一个上口活塞;泡沫发生容器还可以是壁上有高度标记的透明的泡沫发生容器、并在其外设置一个连接有泡沫高度检测装置的摄像头。本实用新型,既可用作建筑材料制造领域中生产泡沫混凝土发泡剂的泡沫发生器,也可用于发泡剂产品性能的检测和评价,结构简单,实用性强。

Figure 201020596974

A blowing agent foam generator and a performance testing and evaluation device, comprising: a foam generating container, a stirrer equipped with stirring blades and a stirring control device, characterized in that: the stirring blades installed on the stirrer are spaced at intervals of 2-3 group, a water bath container connected with a constant temperature control device is arranged outside the foam generating container, and also includes a foam outlet pipe, one end of the foam outlet pipe communicates with the bottom of the foam generating container, and the other end passes through the water bath container; The upper end of the foam generating container can also be movably covered with an upper piston; the foam generating container can also be a transparent foam generating container with a height mark on the wall, and a camera connected with a foam height detection device is arranged outside it. The utility model can not only be used as a foam generator for producing foam concrete foaming agent in the field of building material manufacturing, but also can be used for detecting and evaluating the performance of foaming agent products, and has simple structure and strong practicability.

Figure 201020596974

Description

A kind of blowing agent foam maker and Performance Detection and evaluating apparatus
Technical field
Foam maker and foam performance that the utility model belongs to the blowing agent that is specially adapted for producing foam concrete detect and evaluating apparatus, relate to a kind of blowing agent foam maker and Performance Detection and evaluating apparatus.The foam that is applicable to blowing agent takes place and the foam performance detection.
Background technology
High-performance quick generator for foam is a kind of mechanical device of producing the required foams of construction material such as preparation foam concrete block or foam concrete insulating, after the foam that high-performance quick generator for foam is made and the cement slurry of cement slurry or spikes such as concrete mortar or mixed powder coal ash evenly stir, make foamed cement slurry or foam concrete mortar or foam pulverized fuel ash cement slurry, its moulding by casting is promptly obtained foam concrete block or foam concrete insulating.Above-mentioned building materials quality quality depends on all multifactor, comprises the density of foam concrete, the performance of blowing agent, the uniformity of foam slurry, the factors such as compatibility of foam aperture and foam and cement slurry.And the performance and the foaming mode of the uniformity of foam slurry and foam aperture size and foam maker have direct relation, and the quality of foam concrete performance is played conclusive effect.
The present stage development comparatively production method of ripe cellular concrete product mainly contains two kinds.First method is a high-speed mixing method, and this method can be divided into two kinds of foaming modes again: a kind of mode is that foaming agent solution is poured in the homogenizer, and the adding concrete fully stirred after the high-speed stirred expanding foam solution was produced foam then.This method is easy to operate, and favorable reproducibility can reflect the foamability and the foam stability of blowing agent more exactly, is the method for testing that domestic system bubble technology generally adopts; But the shortcoming of a maximum of this method: fully need foam is transferred in the cement slurry after the foaming, in this process, may cause that the fragmentation of part foam and foam size to inhomogeneous variation, finally cause the performance of cellular concrete product to reduce.Another kind of mode be first with foaming agent solution with after concrete mortar mixes, foam with homogenizer again, directly make gas-liquid-solid foam concrete slurry; This method is compared with first kind of foaming mode, though can improve production efficiency to a certain extent, cause the pore-size distribution of cellular concrete product to broaden, have influence on the intensity of foamed concrete material, and blowing agent can not fully be foamed, reduced its utilization rate.The another kind of method that is used to make cellular concrete product is an air-compressing, this method is that foaming agent solution is pressurized to certain pressure, mix with pattern and pressure-air at foam chamber mesohigh water then, directly be added in the concrete mortar, make concrete product; Perhaps add to concrete mortar again after with foaming agent solution and compressed air mixed foaming, make the foam concrete slurry at last by blowing agent.Compare with high-speed mixing method, pneumatic plant is than homogenizer complexity, though system bubble technology is advanced, foaming efficient is higher, and the quality of foam is better relatively, but its foaming machine is expensive, make the cellular concrete product cost improve greatly, be unfavorable for large-scale production.
The application difference of foam, also inequality to the requirement of foaming properties, but majority is with the foam performance of foam and the foam stability index as the blowing agent performance in the practical application.Continuous development along with monitoring means, the researcher has developed various foaming properties evaluation methods both at home and abroad, but these methods mostly are independent development, lack corresponding country and industry standard, the comparativity of foaming substance detection and evaluation result is poor, demands the accurate more and higher Comprehensive Assessment Technology of standardized degree of development and operation urgently.
Summary of the invention
The purpose of this utility model is intended to overcome deficiency of the prior art, provide a kind of simple in structure, can intelligent detect the blowing agent foaming properties, can provide blowing agent foam maker and the Performance Detection and the evaluating apparatus of technical guarantee for the foam preparation in the foam concrete preparation process again.
Content of the present utility model is: a kind of blowing agent foam maker and Performance Detection and evaluating apparatus comprise: the foam generation container, and the agitator of stirring vane is installed and stirs control device, it is characterized in that:
It is that 2-3 at interval organizes that described agitator (5) is gone up the stirring vane of installing (4);
Also be provided with a water bath containers (6) that is connected with thermostatically-controlled equipment (11) outside the described foam generation container (1); So that eliminate ambient temperature to the influence of foaming properties, be beneficial to of the influence of research temperature to foaming properties;
Also comprise a foam delivery line (3), an end of this foam delivery line (3) is connected with the bottom of described foam generation container (1), the other end passes water bath containers (6) (being connected with concrete mortar or cement pulping system 12).
In the content of the present utility model: the upper end activity of going back is with a piston suitable for reading (2) (adopting light foam material to make) in the described foam generation container (1), so that foam generation container (1) inner foam is smooth.
In the content of the present utility model: described foam generation container (1) also is provided with a camera (8) that is connected with foam height checkout gear (9) for the transparent foam generation container (1) of the number of altitude is arranged on the wall outside the foam generation container (1).So that monitoring foam characteristic aspect both macro and micro.
In the content of the present utility model: in the described 2-3 group stirring vane (4), each organizes stirring vane (4) all is to adopt pawl type structure, promptly preferably: is connected also symmetrically arranged blade formation with agitator (5) by a 2-3 end; So that on the blowing agent certain basis, can produce the foam of better quality; Blade is preferably replaceable blade.
Compared with prior art, the utlity model has following characteristics and beneficial effect:
(1) adopts the utility model, be to be used for the high performance high speed foam maker of building material manufacture field concrete foamer, also can be used as the blowing agent industry produces in the surfactant product experiment, intelligent, precision, standardization detects the foam performance of blowing agent, both can be from the foaming properties of macroscopic view monitoring foaming substance, again can be from microcosmic monitoring foam formation and the course of reaction of eliminating, and then the foam of understanding various foaming substances forms and eliminates mechanism, the integration of realization scientific research resource and shared further promotes the research of the complicated frothing in this field;
(2) simple in structure, make easily, it is easy to use to produce fitting operation, and foaming is quick, and foam quality is good, and is practical.
Description of drawings
Fig. 1 is the utility model embodiment theory structure schematic diagram.
Among the figure: 1-foam generation container, 2-piston suitable for reading (adopting light foam material to make), 3-foam delivery line, 4-stirring vane, 5-(steel) agitator, 6-water bath containers (for example water-bath), 7-water, 8-camera, 9-foam height checkout gear, 10-stir control device, 11-thermostatically-controlled equipment, 12-concrete mortar or cement pulping system; I is that control section, II are for implementing part.
The specific embodiment
The utility model is described in further detail by embodiment below in conjunction with accompanying drawing.
Embodiment 1: referring to accompanying drawing.
A kind of blowing agent foam maker and Performance Detection and evaluating apparatus, composition mainly contains: foam generation container 1 is equipped with the agitator 5 (one section agitator 5 that stirring vane 4 is installed is positioned at foam generation container 1) of stirring vane 4 and stirs control device 10;
The stirring vane of installing on the described agitator 54 is at interval 3 groups;
Described foam generation container 1 is outside equipped with a water bath containers 6 that is connected with thermostatically-controlled equipment (same prior art) 11;
A foam delivery line 3, an end of this foam delivery line 3 is connected with the bottom of described foam generation container 1, the other end passes water bath containers 6 and be connected with concrete mortar or cement pulping system 12;
The upper end activity is with a piston 2 suitable for reading (adopting light foam material to make) in the foam generation container 1.
During use, inject certain amount of foaming agent solution in the foam generation container 1, take off piston 2 suitable for reading, (steel) agitator 5 is inserted in the solution, makes stirring vane 4 all immerse in the solution, rotating speed and time are set, start and stir control device 10, fully shift out agitator 5 after the foaming, socket piston 2 suitable for reading is introduced into concrete mortar or cement pulping system 12 with foam in the foam maker 1 rapidly.
Advantages such as this embodiment has simple in structure, and is easy to operate, and foaming is quick, and foam quality is good make foams foam size uniform and smooth by this embodiment, and foam stability is higher, and bleeding quantity is low.The special foam transfer organization of this embodiment device has guaranteed the LB rate of its foam, foams and concrete mortar rapid mixing, and the foam concrete that obtains slurry is poured in the mould, makes foam concrete brick or foam concrete block after the maintenance.Table 1 and table 2 are high unit weight and low unit weight foam concrete performance test data of utilizing this embodiment to prepare:
Table 1: high unit weight foam concrete physical property
Figure BSA00000338202300051
Table 2: low unit weight foam concrete physical property
Figure BSA00000338202300052
Embodiment 2: referring to accompanying drawing.
A kind of blowing agent foam maker and Performance Detection and evaluating apparatus, composition mainly contains: foam generation container 1 is equipped with the agitator 5 (one section agitator 5 that stirring vane 4 is installed is positioned at foam generation container 1) of stirring vane 4 and stirs control device 10;
The stirring vane of installing on the agitator 54 is at interval 3 groups;
Foam generation container 1 is outside equipped with a water bath containers 6 that is connected with thermostatically-controlled equipment 11; So that eliminate ambient temperature to the influence of foaming properties, be beneficial to of the influence of research temperature to foaming properties;
A foam delivery line 3, an end of this foam delivery line 3 is connected with the bottom of described foam generation container 1, the other end passes water bath containers 6 (being connected with concrete mortar or cement pulping system 12);
The upper end activity is with a piston 2 suitable for reading (adopting light foam material to make) in the foam generation container 1;
Foam generation container 1 is for there being the transparent foam generation container 1 (being made by transparent plastic material) of the number of altitude on the wall, foam generation container 1 is outside equipped with a camera 8 that is connected with foam height checkout gear 9, so that monitor foam characteristic aspect both macro and micro.
This embodiment not only can be used as the high performance high speed foam maker of concrete foamer in the building material manufacture field, also can intelligence, standard, accurately detect the foam performance of blowing agent.During detection, the piston suitable for reading 2 in the foam generation container 1 is removed, injects certain amount of foaming agent solution, agitator 5 is inserted in the solution, guarantees that stirring vane 4 all immerses; The embodiment blowing agent is adopted water-bath 7 heating, start whole controllers, promptly start thermostatically-controlled equipment 11, foam height checkout gear 9, camera 8, finish the blowing agent performance detection.Table 3 is one group of two kinds of blowing agent performance data utilizing this embodiment test:
Table 3: the performance of two kinds of types type blowing agent relatively
Figure BSA00000338202300061
This embodiment detects different blowing agent foaming properties, utilizes the high-speed stirred mode fully to foam, and is easy to operate, favorable reproducibility, and foaming is fast.The thermostatic control structure that is provided with, can accurately investigate the foaming properties of (0~100 ℃) under the different temperatures, also can investigate the foaming properties under a certain specified temp, both can eliminate the influence of ambient temperature, and can summarize the relation of different temperatures and foam froth breaking amount foaming properties.Also can satisfy simultaneously the needs of special dimension, different additive is investigated surfactant materials foam high temperature resistant property.Foam generation container 1 an outer camera 8 that is connected with foam height checkout gear 9 that is provided with, be used in the variation of dynamic monitoring foam inside structure in the foaming process, whole blowing agent foaming process is implemented to follow the tracks of detection, more accurately obtain the froth breaking situation of foam, help to explore the froth breaking mechanism of various foaming substances, all provide bigger help for foam forms theoretical research and improves the blowing agent detection level.
In the foregoing description, in the described stirring vane 4, each organizes stirring vane 4 all is to adopt pawl type structure, promptly preferably: is connected also symmetrically arranged blade formation with agitator 5 by a 2-3 end; So that on the blowing agent certain basis, can produce the foam of better quality; Blade is preferably replaceable blade.
In the foregoing description, described camera 8 can be that digital micro-analysis camera, described foam height checkout gear 9 can be that Computerized examination device, described stirring control device 10 can be the digital display homogenizers, and its structure is formed and all same prior art of using method.The digital display homogenizer can accurately be controlled velocity of rotation and mixing time, and (0~5000r/min) can carry out digitlization at any time sets, and forms trend so that observe foam better in the range of speeds.
The utility model is not limited to the foregoing description, and the utility model content is described all can implement and have described good result.

Claims (3)

1.一种发泡剂泡沫发生器及性能检测和评价装置,包括:泡沫发生容器,安装有搅拌叶片的搅拌器及搅拌控制装置,其特征是:1. A blowing agent foam generator and a performance detection and evaluation device, comprising: a foam generating container, an agitator and a stirring control device that a stirring blade is installed, and is characterized in that: 所述搅拌器(5)上安装的搅拌叶片(4)为间隔的2-3组;The agitating blades (4) installed on the agitator (5) are 2-3 groups at intervals; 所述泡沫发生容器(1)外还设置有一个连接有恒温控制装置(11)的水浴容器(6);The foam generating container (1) is also provided with a water bath container (6) connected with a thermostatic control device (11); 还包括一个泡沫导出管(3),该泡沫导出管(3)的一端与所述泡沫发生容器(1)的底部相连通、另一端穿出水浴容器(6)。It also includes a foam outlet pipe (3), one end of the foam outlet pipe (3) communicates with the bottom of the foam generating container (1), and the other end passes through the water bath container (6). 2.按权利要求1所述的发泡剂泡沫发生器及性能检测和评价装置,其特征是:所述泡沫发生容器(1)内上端还活动套有一个上口活塞(2)。2. The blowing agent foam generator and performance testing and evaluation device according to claim 1, characterized in that: an upper piston (2) is movably sleeved on the inner upper end of the foam generating container (1). 3.按权利要求1或2所述的发泡剂泡沫发生器及性能检测和评价装置,其特征是:所述泡沫发生容器(1)为壁上有高度标记的透明的泡沫发生容器(1),泡沫发生容器(1)外还设置有一个连接有泡沫高度检测装置(9)的摄像头(8)。3. blowing agent foam generator and performance detection and evaluation device according to claim 1 or 2, characterized in that: the foam generating container (1) is a transparent foam generating container (1) with a height mark on the wall ), a camera (8) connected to a foam height detection device (9) is also provided outside the foam generating container (1).
CN 201020596974 2010-11-09 2010-11-09 Foam generating and property detection and evaluation device for foaming agents Expired - Fee Related CN201872227U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN 201020596974 CN201872227U (en) 2010-11-09 2010-11-09 Foam generating and property detection and evaluation device for foaming agents

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN 201020596974 CN201872227U (en) 2010-11-09 2010-11-09 Foam generating and property detection and evaluation device for foaming agents

Publications (1)

Publication Number Publication Date
CN201872227U true CN201872227U (en) 2011-06-22

Family

ID=44160160

Family Applications (1)

Application Number Title Priority Date Filing Date
CN 201020596974 Expired - Fee Related CN201872227U (en) 2010-11-09 2010-11-09 Foam generating and property detection and evaluation device for foaming agents

Country Status (1)

Country Link
CN (1) CN201872227U (en)

Cited By (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102584317A (en) * 2012-03-13 2012-07-18 邓安仲 Method for preparing foam concrete by using physical self-foaming
CN102854286A (en) * 2011-06-27 2013-01-02 中国石油大学(北京) Measuring method for performance of foaming agent
CN103575616A (en) * 2013-11-18 2014-02-12 中南大学 Foaming performance testing device for shield muck-improving foaming agent and using method of foaming performance testing device
CN103660009A (en) * 2012-09-20 2014-03-26 昆山尚达智机械有限公司 Cement foaming machine
CN105467076A (en) * 2015-11-12 2016-04-06 中国石油化工股份有限公司 Apparatus for testing foam fire extinguishing agent performance and usage method thereof
CN105699610A (en) * 2016-04-25 2016-06-22 中国科学院武汉岩土力学研究所 Device for testing performance of soil body foam modifier in soil pressure shield construction
CN106770283A (en) * 2016-11-28 2017-05-31 中国石油天然气股份有限公司 Chemical agent foaming effect evaluation device and evaluation method
CN109564149A (en) * 2016-05-17 2019-04-02 索理思科技公司 Effluent foam Monitoring and control system
CN111521734A (en) * 2020-04-14 2020-08-11 中铁建华南建设有限公司 Foaming agent foaming capacity detection device and detection method thereof
CN112557603A (en) * 2020-12-28 2021-03-26 中国科学技术大学先进技术研究院 Testing device for surfactant
CN113945685A (en) * 2021-10-14 2022-01-18 西安热工研究院有限公司 Bubbling measuring device and measuring method

Cited By (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102854286A (en) * 2011-06-27 2013-01-02 中国石油大学(北京) Measuring method for performance of foaming agent
CN102854286B (en) * 2011-06-27 2014-10-15 中国石油大学(北京) Measuring method for performance of foaming agent
CN102584317A (en) * 2012-03-13 2012-07-18 邓安仲 Method for preparing foam concrete by using physical self-foaming
CN103660009A (en) * 2012-09-20 2014-03-26 昆山尚达智机械有限公司 Cement foaming machine
CN103575616A (en) * 2013-11-18 2014-02-12 中南大学 Foaming performance testing device for shield muck-improving foaming agent and using method of foaming performance testing device
CN103575616B (en) * 2013-11-18 2015-07-08 中南大学 A foaming performance identification device for shield dregs improved foam agent and its application method
CN105467076A (en) * 2015-11-12 2016-04-06 中国石油化工股份有限公司 Apparatus for testing foam fire extinguishing agent performance and usage method thereof
CN105699610A (en) * 2016-04-25 2016-06-22 中国科学院武汉岩土力学研究所 Device for testing performance of soil body foam modifier in soil pressure shield construction
CN109564149A (en) * 2016-05-17 2019-04-02 索理思科技公司 Effluent foam Monitoring and control system
CN106770283A (en) * 2016-11-28 2017-05-31 中国石油天然气股份有限公司 Chemical agent foaming effect evaluation device and evaluation method
CN106770283B (en) * 2016-11-28 2020-02-14 中国石油天然气股份有限公司 Device and method for evaluating foaming effect of chemical agent
CN111521734A (en) * 2020-04-14 2020-08-11 中铁建华南建设有限公司 Foaming agent foaming capacity detection device and detection method thereof
CN112557603A (en) * 2020-12-28 2021-03-26 中国科学技术大学先进技术研究院 Testing device for surfactant
CN113945685A (en) * 2021-10-14 2022-01-18 西安热工研究院有限公司 Bubbling measuring device and measuring method

Similar Documents

Publication Publication Date Title
CN201872227U (en) Foam generating and property detection and evaluation device for foaming agents
CN202105611U (en) Heating and mixing paddle of polymerization reactor
CN100566961C (en) A kind of foaming machine of making foamed bricks
CN104203867A (en) Thermally insulating mineral foam
CN104227846B (en) A kind of foam slurry device for formulating and application thereof
CN105330196A (en) Foam concrete foaming agent and application thereof
CN103011880A (en) Preparation method of inorganic foamed cement insulation board
CN206740496U (en) A kind of During Geotechnical Tests test specimen intelligence dispensing mixed stirring device
CN104264497A (en) Preparation method of water-based polyurethane foam slurry for synthetic leather
CN106835900A (en) A kind of multistage foam asphalt generation apparatus and method
CN115157443A (en) A device suitable for preparing water-based foam and mixing it with cement slurry
CN205704721U (en) A kind of mixer with automatic charging function
CN204826665U (en) Physical blowing foam concrete pumping system that foams
CN109203244A (en) A kind of method and device preparing foam concrete based on aeration method
CN103317591B (en) A kind of chemical method prepares the device of foam cement
CN102514098B (en) A new type of foam concrete slurry production and transportation machine
CN102584317A (en) Method for preparing foam concrete by using physical self-foaming
KR20160015475A (en) Control system of materials inputs for production of lightweight foamed concrete, flooring cement mortar and construction process thereof
CN203156934U (en) Stereoscopic mixed material stirring mechanism for cement foamed insulation boards
CN103030356A (en) Sand-lime brick production method and its process flow
CN203344185U (en) Automatic production line of light wall material
KR20090050385A (en) Mobile Foamed Concrete Manufacturing Equipment
CN104064733B (en) A kind of storage battery lead plaster closes cream device and adopts the conjunction cream technique of this device
CN206870131U (en) A kind of gypsum sheet material raw material agitator mixed slurry outlet device
CN212471950U (en) Foaming cement agitator tank

Legal Events

Date Code Title Description
C14 Grant of patent or utility model
GR01 Patent grant
ASS Succession or assignment of patent right

Owner name: SICHUAN HUASHI GREEN HOUSE BUILDING MATERIALS CO.,

Free format text: FORMER OWNER: XINAN SCIENCE AND TECHNOLOGY UNIV.

Effective date: 20140327

C41 Transfer of patent application or patent right or utility model
COR Change of bibliographic data

Free format text: CORRECT: ADDRESS; FROM: 621010 MIANYANG, SICHUAN PROVINCE TO: 610000 CHENGDU, SICHUAN PROVINCE

TR01 Transfer of patent right

Effective date of registration: 20140327

Address after: Chenghua District Chenghua road in Chengdu city of Sichuan province 610000 two No. 298

Patentee after: Sichuan Huashi Green House Building Materials Co., Ltd.

Address before: 621010 Sichuan, Fucheng, Qinglong District, Mianyang Road, No. 59

Patentee before: Southwest University of Science and Technology

CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20110622

Termination date: 20181109

CF01 Termination of patent right due to non-payment of annual fee