CN201402258Y - Flame photometric detector - Google Patents
Flame photometric detector Download PDFInfo
- Publication number
- CN201402258Y CN201402258Y CN2009201069193U CN200920106919U CN201402258Y CN 201402258 Y CN201402258 Y CN 201402258Y CN 2009201069193 U CN2009201069193 U CN 2009201069193U CN 200920106919 U CN200920106919 U CN 200920106919U CN 201402258 Y CN201402258 Y CN 201402258Y
- Authority
- CN
- China
- Prior art keywords
- photometry
- photometric detector
- flame photometric
- optical filter
- luminous component
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- 238000005375 photometry Methods 0.000 claims abstract description 23
- 230000003287 optical effect Effects 0.000 claims abstract description 18
- 238000010438 heat treatment Methods 0.000 claims abstract description 13
- 238000005070 sampling Methods 0.000 claims abstract description 11
- 150000002894 organic compounds Chemical class 0.000 claims abstract description 10
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 claims abstract description 9
- 230000002146 bilateral effect Effects 0.000 claims abstract description 6
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims abstract description 5
- 239000012159 carrier gas Substances 0.000 claims abstract description 5
- 229910052739 hydrogen Inorganic materials 0.000 claims abstract description 5
- 239000001257 hydrogen Substances 0.000 claims abstract description 5
- 229920000742 Cotton Polymers 0.000 claims abstract description 4
- 239000010453 quartz Substances 0.000 claims abstract description 4
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N silicon dioxide Inorganic materials O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims abstract description 4
- 229910052717 sulfur Inorganic materials 0.000 claims description 4
- 239000011593 sulfur Substances 0.000 claims description 4
- 150000002903 organophosphorus compounds Chemical class 0.000 claims description 3
- 238000012946 outsourcing Methods 0.000 claims description 3
- 238000004321 preservation Methods 0.000 claims description 3
- 239000005864 Sulphur Substances 0.000 abstract description 5
- 239000007789 gas Substances 0.000 abstract description 5
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 abstract description 3
- 229910052698 phosphorus Inorganic materials 0.000 abstract description 3
- 239000011574 phosphorus Substances 0.000 abstract description 3
- 238000012360 testing method Methods 0.000 abstract description 2
- 238000009413 insulation Methods 0.000 abstract 1
- AJLFOPYRIVGYMJ-INTXDZFKSA-N mevastatin Chemical group C([C@H]1[C@@H](C)C=CC2=CCC[C@@H]([C@H]12)OC(=O)[C@@H](C)CC)C[C@@H]1C[C@@H](O)CC(=O)O1 AJLFOPYRIVGYMJ-INTXDZFKSA-N 0.000 abstract 1
- BHEPBYXIRTUNPN-UHFFFAOYSA-N hydridophosphorus(.) (triplet) Chemical compound [PH] BHEPBYXIRTUNPN-UHFFFAOYSA-N 0.000 description 4
- 230000007613 environmental effect Effects 0.000 description 2
- 238000012544 monitoring process Methods 0.000 description 2
- UCKMPCXJQFINFW-UHFFFAOYSA-N Sulphide Chemical compound [S-2] UCKMPCXJQFINFW-UHFFFAOYSA-N 0.000 description 1
- 239000003905 agrochemical Substances 0.000 description 1
- 238000004458 analytical method Methods 0.000 description 1
- 238000002485 combustion reaction Methods 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000013461 design Methods 0.000 description 1
- 238000001514 detection method Methods 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 229940079593 drug Drugs 0.000 description 1
- 230000002265 prevention Effects 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 230000000171 quenching effect Effects 0.000 description 1
- 230000035945 sensitivity Effects 0.000 description 1
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- Investigating, Analyzing Materials By Fluorescence Or Luminescence (AREA)
Abstract
A flame photometric detector comprises a heating device, a sampling device, a luminous component, a photometry component and an auxiliary electronic component. The sampling device is a lateral-surfacesampling device, the heating device is a double-stick heating device coated with heat insulation cotton, the luminous component comprises an internal nozzle and an external nozzle, the internal nozzle is connected with a carrier gas inlet passage and a hydrogen inlet passage, the external nozzle is connected with an air inlet passage, the photometry component is in bilateral window photometry, two sides of the luminous component are respectively equipped with two sets of photometry components consisting of quartz windows, optical filters, lenses and photomultipliers, and the two optical filters are respectively an optical filter measuring organic compounds containing phosphorus and an optical filter measuring organic compounds containing sulphur. The flame photometric detector is compactin structure, reduces space structures via lateral sampling, guarantees stability of burning via double nozzles, does not need to replace the optical filters via bilateral window photometry, can simultaneously detect the organic compounds containing phosphorus and the organic compounds containing sulphur, is convenient for being mounted in a gas chromatograph of a moving testing vehicle, and is simple, convenient and easy in operation.
Description
Technical field
The utility model relates to a kind of checkout equipment, and is particularly a kind of to organic compound and the responsive especially flame photometric detector (FPD) of gas sulfide phosphorous, sulphur.
Background technology
Flame photometric detector (FPD) (FPD) is a kind of high sensitivity, the detecting device of high selectivity.Be particularly useful for generally speaking to H
2The environmental monitoring of S and sulfurous gas, and when carrying out the analysis of agricultural drugs trace organic phosphorus compound of monitoring in the agricultural chemicals.In recent years, needs along with unexpected incidents strick precaution and processing, all kinds of emergent laboratories (nigration car) occurred, departments such as environmental protection, food supervision, health and epidemic prevention are detected for reply is on-the-spot to be needed, and gas chromatograph is installed in takes love scene on the nigration car and carry out testing.Existing chromatogram flame photometric detector (FPD) only is applicable to the common lab chromatogram, and need dismantle the photometry parts and change optical filter at survey organic compound phosphorous or sulfur-bearing, and is not too convenient.And vehicle-mounted chromatograph box mostly is horizontal post case design.
The utility model content
In order to overcome above-mentioned deficiency, the utility model provide a kind of and adopt the photometry of bilateral window, need not dismantle photomultiplier change optical filter, can the side sample introduction, adapt to the flame photometric detector (FPD) of vehicle-mounted chromatogram.
The utility model flame photometric detector (FPD) comprises heating arrangement, sampling device, luminous component, photometry parts and auxiliary electrical components, and wherein: described sampling device is the side sampling device, and described heating arrangement is the double stick heating arrangement of outsourcing heat-preservation cotton.
The utility model flame photometric detector (FPD), wherein: described luminous component comprises inner nozzle and outer nozzle, and described inner nozzle connects carrier gas access and hydrogen access, and described outer nozzle connects the air access.
The utility model flame photometric detector (FPD), wherein: described photometry parts are the photometry of bilateral window, adorning the two cover photometry parts of being made up of quartz window, optical filter, lens and photomultiplier respectively in the both sides of luminous component, described two tablet filters are respectively the organic compound optical filter of surveying the organic phosphorus compound optical filter and surveying sulfur-bearing.
The utility model flame photometric detector (FPD), wherein: described electronic unit mainly comprises: high-voltage power supply, micro current amplifier etc.
The utility model flame photometric detector (FPD), compact conformation, the side sample introduction has reduced space structure, twin-jet nozzle guarantees the stable of burning, bilateral reveal light need not to change optical filter, can detect the organic compound of phosphorous or sulfur-bearing simultaneously, be convenient to be installed in the mobile instruction carriage gas chromatograph, easy to operation.
Description of drawings
Fig. 1 is the utility model flame photometric detector (FPD) structural representation;
Fig. 2 is the luminous and photometry parts sectional view of the utility model flame photometric detector (FPD).
Embodiment
For further setting forth the utility model flame photometric detector (FPD), do more detailed explanation below in conjunction with embodiment.
Fig. 1 is a novel flame photometric detector structural representation, and the utility model flame photometric detector (FPD) comprises heating arrangement A1, sampling device A2, luminous component A3, photometry parts A4 and auxiliary electrical components A5 five major parts.
Heating arrangement A1 installs 2 75W heating rod outsourcing high-quality heat-preservation cotton, and overall volume reduces, and heating rate is faster, and it is higher good to be incubated.Sampling device A2 directly inserts in the horizontal post case.Ignition part A3 is designed to twin-jet nozzle and has eliminated quenching effect.The photometry parts A4 of two symmetries can dismantle that photomultiplier transit light is changed optical filter and the organic compound of surveying phosphorous or sulphur respectively.
It in Fig. 2 the sectional view of luminous component and photometry parts.
The luminous component air directly enters outer nozzle 9 by air access 6, and hydrogen fully mixes after inner nozzle 10 enters the photometry parts by carrier gas access 8 by hydrogen access 7 and carrier gas, is lighted by portfire 3.Pressure dome presents outer fired state in the combustion flame periphery, has concurrently to be difficult for fire extinguishing and highly sensitive advantage.
The photometry parts mainly comprise quartz window 4, optical filter 2, lens 5 and photomultiplier 1, a cover in each photometry parts, and optical filter difference wherein is respectively and surveys phosphorus and survey the sulphur optical filter, and two cover photometry parts are finished the content detection to p and s simultaneously.
Claims (3)
1. a flame photometric detector (FPD) comprises heating arrangement, sampling device, luminous component, photometry parts and auxiliary electrical components, it is characterized in that: described sampling device is the side sampling device, and described heating arrangement is the double stick heating arrangement of outsourcing heat-preservation cotton.
2. flame photometric detector (FPD) according to claim 1 is characterized in that: described luminous component comprises inner nozzle and outer nozzle, and described inner nozzle connects carrier gas access and hydrogen access, and described outer nozzle connects the air access.
3. flame photometric detector (FPD) according to claim 2, it is characterized in that: described photometry parts are the photometry of bilateral window, adorning the two cover photometry parts of being made up of quartz window, optical filter, lens and photomultiplier respectively in the both sides of luminous component, described two tablet filters are respectively the organic compound optical filter of surveying the organic phosphorus compound optical filter and surveying sulfur-bearing.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2009201069193U CN201402258Y (en) | 2009-04-02 | 2009-04-02 | Flame photometric detector |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2009201069193U CN201402258Y (en) | 2009-04-02 | 2009-04-02 | Flame photometric detector |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN201402258Y true CN201402258Y (en) | 2010-02-10 |
Family
ID=41662054
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN2009201069193U Expired - Fee Related CN201402258Y (en) | 2009-04-02 | 2009-04-02 | Flame photometric detector |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN201402258Y (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105067729A (en) * | 2015-07-30 | 2015-11-18 | 安徽中杰信息科技有限公司 | Flame photometric detector for measuring phosphor-containing compounds and sulfur-containing compounds |
| CN106990197A (en) * | 2016-01-20 | 2017-07-28 | 株式会社岛津制作所 | Dual channel flame photometric detector |
-
2009
- 2009-04-02 CN CN2009201069193U patent/CN201402258Y/en not_active Expired - Fee Related
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105067729A (en) * | 2015-07-30 | 2015-11-18 | 安徽中杰信息科技有限公司 | Flame photometric detector for measuring phosphor-containing compounds and sulfur-containing compounds |
| CN106990197A (en) * | 2016-01-20 | 2017-07-28 | 株式会社岛津制作所 | Dual channel flame photometric detector |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| C17 | Cessation of patent right | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20100210 Termination date: 20130402 |