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CN201408054Y - Calibration device for solid mass flowmeter and system including same - Google Patents

Calibration device for solid mass flowmeter and system including same Download PDF

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Publication number
CN201408054Y
CN201408054Y CN2009200718967U CN200920071896U CN201408054Y CN 201408054 Y CN201408054 Y CN 201408054Y CN 2009200718967 U CN2009200718967 U CN 2009200718967U CN 200920071896 U CN200920071896 U CN 200920071896U CN 201408054 Y CN201408054 Y CN 201408054Y
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solid mass
pipeline
feeding
mass flowmeter
outlet
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龚欣
郭晓镭
刘海峰
代正华
梁钦锋
李伟锋
陈雪莉
于广锁
王辅臣
王亦飞
王兴军
许建良
郭庆华
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East China University of Science and Technology
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East China University of Science and Technology
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Abstract

本实用新型公开了一种固体质量流量计标定装置,其包括一称重装置,一阻力部件及一设于该称重装置的入口与该阻力部件的出口间的第一管道和一与该阻力部件的入口相连的第二管道,第二管道还设一压力调节装置。本实用新型还提供一干法进料和反应的系统,其包括一进料系统和一反应装置,一上述固体质量流量计标定装置,及一路或多路输料管道,各输料管道均连接一转换装置,各输料管道均连接有至少一固体质量流量计。采用本实用新型可显著提高固体质量流量计的标定精度,能满足化工、发电、冶金等行业对固体质量流量计准确计量,且在线标定的要求。

Figure 200920071896

The utility model discloses a calibration device for a solid mass flowmeter, which comprises a weighing device, a resistance component, a first pipeline arranged between the inlet of the weighing device and the outlet of the resistance component, and a resistance component. The inlet of the component is connected to the second pipeline, and the second pipeline is also provided with a pressure regulating device. The utility model also provides a dry feeding and reaction system, which includes a feeding system and a reaction device, a calibration device for the above-mentioned solid mass flowmeter, and one or more feeding pipelines, each feeding pipeline is connected to A conversion device, each feeding pipeline is connected with at least one solid mass flowmeter. The utility model can significantly improve the calibration accuracy of the solid mass flowmeter, and can meet the requirements of the chemical industry, power generation, metallurgy and other industries for accurate measurement of the solid mass flowmeter and on-line calibration.

Figure 200920071896

Description

Calibration device for solid mass flow meter and contain its system
Technical field
The utility model relates to a kind of flowmeter prover and contains the charging reaction unit of this caliberating device, particularly a kind of online calibration device for solid mass flow meter, and contain the dry feed of this calibration device for solid mass flow meter and the system of reaction.
Background technology
Pneumatic Conveying Technology has been widely used among the commercial production such as chemical industry, generating and metallurgy, and wherein, the mass flowrate of solid material is important process operation parameter, and can it accurately measure the stability and safety operation that has directly influenced process units.Weight method is the most simple and reliable method of metering mass flowrate, but can't satisfy the operation with high pressure and the on-line measurement requirement of some technology.Therefore, based on understanding to the solid feed physical property, produced many based on different principle, can be used for the solid mass flow meter of high pressure, on-line measurement solid masses flow rate, have based on the macroscopic property of solid in the course of conveying and electrical property; The technology that needs external energy when measuring is also arranged, for example adopt the principle of energy absorption and sound vibrations, but because Gas-solid Two-phase Flow complexity in the pipeline, for example under different convey materials and operating conditions particularly the unevenness that distributes of pipeline section solid concentration give accurately to measure and brought many challenges, therefore, such measurement instrument needs to utilize weight method to demarcate or verify bar none.
Adopt the fine coal forced air bed gasification technology of dry feed to have advantages such as coal adaptability is wide, service life of equipment length, efficiency of carbon conversion height, become numerous enterprises and selected one of mainstream technology of gasifying process.At present, can realize that the solid mass flow meter of on-line measurement solid masses flow rate has been applied to the fine coal forced air bed gasifying apparatus of 1000~2000 tons in day processing coal, but in operational process, expose fine coal actual flow and solid mass flow meter and show the bigger problem of flow deviation, so that operating the oxygen coal causes gasification temperature low excessively than distortion then, cause cinder notch to block up problems such as slag, the too high scaling loss water-cooling wall of gasification temperature internals, greatly influenced the safety and the cycle of operation of device.Practice shows that there is following point in the fine coal solid mass flow meter calibration technique that industrialized gasifying powder coal device had adopted at present in the through engineering approaches application facet:
(1) stated accuracy is not high.The normal pressure warehouse weighing system range that is used for the solid mass flow meter demarcation at present on the commercial plant is excessive, and timing signal not only needs the long nominal time, more gives and demarcates introducing than mistake, is difficult to satisfy the accurate calibration request of fine coal mass flowmeter.
(2) do not possess the on-line proving function.The calibration system that adopts on the commercial plant does not possess the on-line proving function at present; When reaction unit was in running status, the normal pressure warehouse that is used for the solid mass flow meter demarcation was also being born the function to other storage bin feed, thereby can't weighed to the material from calibration system when accepting from the coal mill system material.Therefore, demand developing a kind of high pressure strength conveying caliberating device that can carry out on-line proving and checking at short notice urgently to solid mass flow meter.
The utility model content
Technical problem to be solved in the utility model is to exist stated accuracy not high at present in the Pneumatic Conveying Technology of dry feed on the solid mass flow meter calibration technique in order to overcome prior art, defective that can't on-line proving, a kind of stated accuracy that significantly improves solid mass flow meter is provided, can satisfies chemical industry, generating, industries such as metallurgy to solid mass flow meter accurately metering and service requirement that can on-line proving a kind of calibration device for solid mass flow meter and comprise a dry feed of calibration device for solid mass flow meter of the present utility model and the system of reaction.
The utility model solves above-mentioned technical matters by following technical proposals: a kind of calibration device for solid mass flow meter, it is characterized in that it comprises that one is exclusively used in the weighing device that material is demarcated in weighing, resistance parts and one first pipeline and one second pipeline; This first pipeline is located between the outlet of the inlet of this weighing device and these resistance parts; This second pipeline links to each other with the inlet of these resistance parts, also is provided with a pressure adjustment assembly on this second pipeline.
Preferably, this pressure adjustment assembly comprises that at least wherein, this pipeline making-up air device also connects a gas flow adjusting means by this second pipeline be connected with each other logical a pipeline making-up air device and a pressure monitoring device.
Preferably, this weighing device is a gravimetric tank.
Preferably, the volume of this gravimetric tank is under this solid mass flow meter biggest quality flow rate of being demarcated per hour 0.2~4 times of the solid accumulation volume.
Preferably, the volume of this gravimetric tank is under this solid mass flow meter biggest quality flow rate of being demarcated per hour 0.4~2 times of the solid accumulation volume.
Preferably, this gravimetric tank is established a filtration unit in also, and this gravimetric tank comprises gravimetric tank inlet, a gravimetric tank gas vent and gravimetric tank solid material outlet, and this filtration unit is connected with the gas vent of this gravimetric tank.
Preferably, the pressure drop between the inlet of these resistance parts and outlet is 0~5MPa.
Preferably, these resistance parts are any one in orifice plate, reducer pipe, the throttling valve.
The utility model also provides the system of a kind of dry feed and reaction, it comprises a feed system and a reaction unit, it is characterized in that it also comprises: an above-mentioned calibration device for solid mass flow meter, and one or more feeding pipe, each feeding pipe all connects a conversion equipment; Wherein, this feed system is by this feeding pipe and the corresponding conversion equipment that is connected with it, be connected with this calibration device for solid mass flow meter with this reaction unit respectively, the outlet of the weighing device of this calibration device for solid mass flow meter is connected with the inlet of this feed system by an operation valve, and each feeding pipe all is connected with at least one solid mass flow meter.
Preferably, this conversion equipment is a T-valve, this T-valve tool one inlet, one first outlet and one second outlet, wherein, the inlet of this T-valve is connected with the outlet of this feed system by the feeding pipe that correspondingly connects, first outlet of this T-valve is connected with second entrance of this calibration device for solid mass flow meter, and second outlet of this T-valve is connected with this reaction unit by a connecting pipe, also connects a carrier gas input media on this feeding pipe.
Preferably, this feed system comprises a continuous normal pressure warehouse, an intermittent blanking device and the issuance of materials jar of order successively.
Preferably, this intermittent blanking device is a lock hopper system or a high-pressure rotary dispenser.
Preferably, on this normal pressure warehouse, this intermittent blanking device and this issuance of materials jar carrier gas input media is housed all.
Positive progressive effect of the present utility model is:
1, the system of dry feed of the present utility model and reaction, can significantly improve the stated accuracy of solid mass flow meter, shorten the service requirement of nominal time and on-line proving, can satisfy of the accurate metering of industries such as chemical industry, generating, metallurgy solid mass flow meter.
2, the utility model employing two-way or the above conveyance conduit of two-way are the reaction unit feed, can be according to demarcating needs, by the T-valve on the feeding pipe of arbitrary road the issuance of materials jar is communicated with gravimetric tank, solid mass flow meter is demarcated, keep the operation of reaction unit simultaneously.
3, calibration device for solid mass flow meter of the present utility model, therefore accept the required material of timing signal separately by the weighing device in the on-line proving device, can solve the adverse effect that raw material variety variation etc. brings the solid mass flow meter metering accuracy by on-line proving.
4, the utility model is selected the gravimetric tank of low capacity, little range, high-precision weighing instrument can be set thereon, to improve the stated accuracy of solid mass flow meter, shorten the nominal time, online and off-line calibration and realize that the quick online switching of multiple solid material lays the foundation for the solid material mass flowrate.
Description of drawings
Fig. 1 is the calibration device for solid mass flow meter structural drawing of the utility model one preferred embodiment.
Fig. 2 is the structural drawing of the system of the dry feed of the utility model one preferred embodiment and reaction.
Embodiment
Lift a preferred embodiment below, and come the clearer the utility model that intactly illustrates in conjunction with the accompanying drawings.
As depicted in figs. 1 and 2, the utility model provides a kind of calibration device for solid mass flow meter 1, and it comprises that mainly one is exclusively used in weighing and demarcates the weighing device 11 of material ' and resistance parts 12, and first pipeline 18 that is used to connect and second pipeline 19.Wherein, be exclusively used in weighing and demarcate the weighing device 11 of material ' only be used for unique demarcation material of accepting the required weighing of calibration process, and show real-time weight, thereby solid mass flow meter is proofreaied and correct demarcation according to these data.Therefore weighing device 11 ' do not bear acceptance be not subjected to the influence of other system from the coal mill system charging and to the function of issuance of materials jar feed.When being in non-calibration process, weighing device 11 ' only have connection effect.First pipeline 18 be located at weighing device 11 ' inlet and resistance knockdown export 122 between; Second pipeline 19 links to each other with resistance component entry 121, also is equiped with a pressure adjustment assembly 5 on second pipeline 19.Referring to Fig. 2, pressure adjustment assembly 5 comprises a pipeline making-up air device and a pressure monitoring device 15 that communicates with each other by second pipeline 19 at least.The pipeline making-up air device can be known pipeline air compensation device 13, and it can be used for make-up carrier gas flow in second pipeline 19, thus the flow velocity when improving solid material and carrier gas mixture by resistance parts 12, and then the pressure at controlled pressure monitoring device 15 places.Pipeline air compensation device 13 has the inlet 133 of the mixture inlet 131 of a solid material and carrier gas, solid material and 132, make-up carrier gass of carrier gas mixture outlet.Inlet 133 places of make-up carrier gas also are connected to a gas flow adjusting means, such as a pressure-regulating valve 14.Pressure monitoring device 15 can be known tensimeter.Resistance parts 12 can be selected in orifice plate, reducer pipe, the throttling valve any one for use, and the potpourri that is used to make solid material and carrier gas produces a constant pressure drop during by this equipment, thereby improves the pressure at pressure monitoring device 15 places.The pressure of weighing device 11 ' porch is normal pressure, resistance parts porch 121 pressure are controlled, at normal pressure to the scope of 5MPa, preferred 1MPa to 4MPa, by the pressure drop between resistance component entry 121 and the resistance knockdown export 122 is 0~5MPa, like this can simulation reaction device conveying operating mode during 2 normal operations, realize the demarcation of solid mass flow meter 17 under the high-pressure delivery state can realizing the on-line proving of solid mass flow meter 17 on the other hand on the one hand.Above-mentioned weighing device 11 ' can adopt a gravimetric tank 11, gravimetric tank 11 is provided with three passwaies, that is: be used to receive the mixture of carrying carrier gas secretly gravimetric tank inlet 111, be used to discharge the gravimetric tank gas vent 112 of carrier gas, and be used for the gravimetric tank solid material outlet 113 of convey materials.In order to prevent too much solid material, such as solid fuel, to be taken out of by carrier gas, gravimetric tank 11 is established a filtration unit in going back, and filtration unit is connected with the gas vent 112 of gravimetric tank.Filtration unit can be known cloth bag filtration.For slot milling is used for the sedimentation of solid material, the volume of gravimetric tank 11 is under solid mass flow meter 17 biggest quality flow rates of being demarcated per hour 0.2~4 times of material nature stacking volume, preferred 0.4~2 times.
As depicted in figs. 1 and 2, the utility model also provides the system of a kind of dry feed and reaction, it is mainly by a feed system 3 and a reaction unit 2, one as mentioned above the calibration device for solid mass flow meter that has gravimetric tank 11 1, and one or more feeding pipe 20, each feeding pipe 20 all connects a conversion equipment; Feed system 3 is by each road feeding pipe 20 and the corresponding conversion equipment that is connected with it, be connected with calibration device for solid mass flow meter 1 with reaction unit 2 respectively, when each conversion equipment with form a feed stream after reaction unit 2 is connected, and when conversion equipment is connected with calibration device for solid mass flow meter 1, then desirable demarcation material, weigh by 11 pairs of materials of getting of gravimetric tank, thereby realize on-line proving.Each feeding pipe 20 all is connected with at least one solid mass flow meter 17.The weighing device 11 of calibration device for solid mass flow meter 1 ' outlet be connected with the inlet of feed system 3 by an operation valve 4.Reaction unit 2 can be gasification furnace or high-pressure gasified reactor.Conversion equipment in the present embodiment is a T-valve 16, all connects a carrier gas input media G and an operation valve 4 on each feeding pipe 20.T-valve 16 has an inlet 162,1 first outlet 161 and 1 second outlet 163.The inlet 162 of T-valve is connected with the outlet of feed system 3 by the feeding pipe 20 that correspondingly connects, first outlet 161 of T-valve is connected with the inlet of second pipeline 19 of this calibration device for solid mass flow meter 1, second outlet 163 of T-valve is connected with reaction unit 2 by a connecting pipe, installs one or more solid mass flow meters 17 on each feeding pipe 20.Solid mass flow meter 17 in the present embodiment be meant can online demonstration process of pneumatic transmission in the instrument of solid material mass flowrate, comprise all instrument that need demarcate by weight method such as capacitance principle measurement, the measurement of ray principle, electrostatic principle measurement.
When needs on-line proving solid mass flow meter 17, feed system 3 is connected with the inlet 162 of T-valve through feeding pipe 20, first outlet 161 of T-valve 16 is with after second pipeline 19 is connected, behind pipeline air compensation device 13, resistance parts 12 and first pipeline 18, be connected, then can pass through weight method on-line proving solid mass flow meter 17 with gravimetric tank inlet 111.The outlet of solid flowmeter caliberating device 1, i.e. gravimetric tank outlet 113 also are that the inlet 311 of normal pressure warehouse 31 connects by the inlet of an operation valve 4 with feed system 3.Feed system 3 can be made up of the normal pressure warehouse 31, an intermittent blanking device 32 and the issuance of materials jar 33 that link to each other in proper order successively.Normal pressure warehouse 31 be used to accept and store from gravimetric tank 11 or other weighing device 11 ' the demarcation material.Be connected with weighing instrument on the normal pressure warehouse 31, when issuance of materials jar 33 internal solid stocks are not enough, adopt as intermittent blanking devices 32 such as lock hopper system, high-pressure rotary dispensers, off and on the solid material in the normal pressure warehouse 31 is transported in the issuance of materials jar 33 under the high pressure conditions.Gravimetric tank 11 is installed in normal pressure warehouse 31 tops, is used to accept from the demarcation material of issuance of materials jar 33 and shows real-time weight, thereby solid mass flow meter 17 is demarcated.Gravimetric tank 11 is connected with normal pressure warehouse 31, is provided with operation valve 4 between gravimetric tank 11 and the normal pressure warehouse 31.Issuance of materials jar 33 is mainly used in the mode of under certain pressure the solid material of its storage being carried with strength and is transported to reaction unit 2 by feeding pipe 20.When issuance of materials jar 33 needed material feeding, the solid material in the normal pressure warehouse 31 can turn back in the issuance of materials jar 33 high pressure conditions under by intermittent blanking device 32, thereby formed the circulation conveying of solid material.Intermittent blanking device 32 can adopt a known lock hopper system or a high-pressure rotary dispenser.The one carrier gas input media that is used for delivery of carrier gas all is housed on normal pressure warehouse 31, intermittent blanking device 32 and the issuance of materials jar 33.
Solid material in the present embodiment can be any one or other similar solid fuel etc. in fine coal, petroleum coke, living beings, solid-state castoff or its potpourri.Carrier gas can be selected from nitrogen, carbon dioxide, water vapour, synthetic gas or its combination gas any one.
When demarcating solid mass flow meter 17, close the operation valve 4 between gravimetric tank 11 and the normal pressure warehouse 31; Control issuance of materials jar 33 pressure between 1MPa~6MPa, preferred 2~5MPa, and keep issuance of materials jar 33 pressure stabilitys; Adjust transportation parameters, the mode that solid fuel is carried by strength flows out from 33 outlets of issuance of materials jar, the potpourri of solid fuel and carrier gas enters conveyance conduit 20, successively by one or more solid mass flow meters 17, T-valve 16, pipeline air compensation device 13, after resistance part part 12, enter the gravimetric tank 11 of normal pressure after the decompression, carrier gas then enters dust pelletizing system through the gas vent 112 of gravimetric tank 11.When gravimetric tank 11 internal solid fuel reach required semi-invariant or timing signal not, operation valve 4 is often opened and is made gravimetric tank 11 keep being communicated with normal pressure warehouse 31, and solid fuel enters normal pressure warehouse 31 from gravimetric tank 11, does not store solid fuel in the gravimetric tank 11.Be coal dust below with the transferring raw material, carrier gas is that nitrogen is example, and the system work process that specifically describes dry feed of the present utility model and reaction is as follows:
Issuance of materials jar 33 communicates with gasification furnace by four fine coal outlets that connect one road feeding pipe 20 respectively on it, passes through four road feeding pipe 20A, 20B, 20C, 20D respectively to the gasification furnace feed.Four road feeding pipe 20A, 20B, 20C, 20D can be in twos be connected with gasification furnace from the both sides of gasification furnace opposed to each other, also can insert from the top of gasification furnace.When two solid mass flow meters 17 on the demarcation feeding pipe 20A, control issuance of materials jar 33 pressure 4.7MPa, and keep issuance of materials jar 33 pressure stabilitys.Opening controlling valve 4, the potpourri of solid material and carrier gas enters feeding pipe 20A, under the effect of carrier gas G, successively through two solid mass flow meters 17, T-valve 16, and pipeline air compensation device 13, after 12 decompressions of resistance parts, enter into normal pressure gravimetric tank 11 again.Pressure in 121 pipelines of resistance component entry is by pressure-regulating valve 14 controls, and the pressure in 121 pipelines of pressure-regulating valve 14 may command resistance component entries is to demarcating desired value.When need not timing signal, to open with the solid material of gravimetric tank 11 and export 113 operation valves that are connected 4, solid material flows in the normal pressure warehouse 31.When issuance of materials jar 33 internal solid stocks are not enough, off and on the solid materials in the normal pressure warehouse 31 are transported in the issuance of materials jar 33 under the high pressure conditions by lock hopper.
When gasification furnace is in running status, can carry out on-line proving to the solid mass flow meter 17 on the way of appointing among four road feeding pipe 20A, 20B, 20C, the 20D.Needing to stop the feed of the feeding pipe 20 of demarcation, this road feeding pipe is communicated with gravimetric tank 11, keep gasification furnace to be in the safe operation state simultaneously by T-valve 16 to gasification furnace.After demarcating end, after the pressure at controlled pressure monitoring device 15 places is slightly larger than the gasification furnace internal pressure, by T-valve 16 feed system 3 is communicated with gasification furnace, the potpourri of solid material and carrier gas enters gasification furnace by a connecting pipe.Simultaneously, unlatching carrier gas F is used for feeding pipe 20 purgings when conveying stops.Thus, finished the on-line proving process of solid mass flow meter 17.
The utility model is by being provided with resistance parts 12 on first pipeline 18 of gravimetric tank inlet 111, improve the mode of the flow velocity of resistance parts 12 gas-solid two-phase mixtures of flowing through, increase the pressure drop at resistance parts 12 two ends, thereby improve the pressure in second pipeline 19 before the resistance component entry 121, form solid mass flow meter 17 declared working conditions under the high pressure, provide the basis for accurately demarcating.Under the effect of resistance parts 12, the port pressure of T-valve first outlet 161 can be increased to reaction unit 2 pressure, and this just passes through T-valve 16 directly from high pressure reaction assembly 2, such as high-pressure gasified stove for solid material, switch to gravimetric tank 11 condition is provided, thereby realize online accurate demarcation.In addition, little range, high-precision weighing instrument are set on the gravimetric tank 11 of the utility model low capacity, can also improve the stated accuracy of solid mass flow meter 17, shorten the nominal time, online and off-line calibration and realize that the quick online switching of multiple solid fuel lays the foundation for the fine coal mass flowrate.It is reaction unit 2 feed that the utility model adopts two-way or the above conveyance conduit 20 of two-way, can be according to demarcating needs, by the T-valve 16 on arbitrary road feeding pipe 20 issuance of materials jar 33 is communicated with gravimetric tank 11, solid mass flow meter 17 is demarcated, kept the operation of reaction unit 2 simultaneously.After demarcating end, feed system 3 is communicated with reaction unit 2 through T-valve 16 by feeding pipe 20, makes solid material enter reaction unit 2.
Though more than described embodiment of the present utility model, but those skilled in the art is to be understood that, these only illustrate, and under the prerequisite that does not deviate from principle of the present utility model and essence, can make numerous variations or modification to these embodiments.Therefore, protection domain of the present utility model is limited by appended claims.

Claims (13)

1、一种固体质量流量计标定装置,其特征在于其包括一专用于称量标定物料的称重装置,一阻力部件及一第一管道和一第二管道;该第一管道设于该称重装置的入口与该阻力部件的出口之间;该第二管道与该阻力部件的入口相连,该第二管道上还设有一压力调节装置。1. A calibration device for a solid mass flowmeter, characterized in that it includes a weighing device dedicated to weighing calibration materials, a resistance component, a first pipeline and a second pipeline; the first pipeline is located on the scale Between the inlet of the heavy device and the outlet of the resistance component; the second pipeline is connected with the inlet of the resistance component, and a pressure regulating device is also arranged on the second pipeline. 2、如权利要求1所述的固体质量流量计标定装置,其特征在于,该压力调节装置至少包括通过该第二管道彼此相连通的一管道补气装置和一压力监测装置,其中,该管道补气装置还连接一气体流量调节装置。2. The solid mass flowmeter calibration device according to claim 1, characterized in that, the pressure regulating device at least includes a pipeline gas supply device and a pressure monitoring device communicated with each other through the second pipeline, wherein the pipeline The gas supply device is also connected with a gas flow regulating device. 3、如权利要求1所述的固体质量流量计标定装置,其特征在于,该称重装置为一称重罐。3. The calibration device for solid mass flowmeter according to claim 1, characterized in that the weighing device is a weighing tank. 4、如权利要求3所述的固体质量流量计标定装置,其特征在于,该称重罐的体积为所标定的该固体质量流量计最大质量流率下每小时物料堆积体积的0.2~4倍。4. The calibration device for solid mass flowmeters according to claim 3, characterized in that the volume of the weighing tank is 0.2 to 4 times the accumulated volume of materials per hour at the calibrated maximum mass flow rate of the solid mass flowmeter . 5、如权利要求3所述的固体质量流量计标定装置,其特征在于,该称重罐的体积为所标定的该固体质量流量计最大质量流率下每小时物堆积料体积的0.4~2倍。5. The calibration device for solid mass flowmeter according to claim 3, characterized in that the volume of the weighing tank is 0.4 to 2% of the volume of material accumulation per hour at the calibrated maximum mass flow rate of the solid mass flowmeter. times. 6、如权利要求3所述的固体质量流量计标定装置,其特征在于,该称重罐还内设一过滤装置,该称重罐包含一称重罐入口、一称重罐气体出口及一称重罐固体物料出口,该过滤装置与该称重罐的气体出口相连接。6. The calibration device for solid mass flowmeter according to claim 3, characterized in that, the weighing tank is also provided with a filtering device, and the weighing tank includes a weighing tank inlet, a weighing tank gas outlet and a The solid material outlet of the weighing tank, the filter device is connected with the gas outlet of the weighing tank. 7、如权利要求1所述的固体质量流量计标定装置,其特征在于,该阻力部件的入口与出口间的压降为0~5MPa。7. The calibration device for solid mass flowmeter according to claim 1, characterized in that the pressure drop between the inlet and outlet of the resistance member is 0-5 MPa. 8、如权利要求1至7中任意一项所述的固体质量流量计标定装置,其特征在于,该阻力部件为孔板、变径管、节流阀中的任意一种。8. The solid mass flowmeter calibration device according to any one of claims 1 to 7, characterized in that the resistance component is any one of an orifice plate, a variable diameter tube, and a throttle valve. 9、一种干法进料和反应的系统,其包括一进料系统和一反应装置,其特征在于,其还包括:一如权利要求1所述的固体质量流量计标定装置,及一路或多路输料管道,各输料管道均连接一转换装置;其中,该进料系统通过该输料管道及与其相应连接的转换装置,分别与该反应装置和该固体质量流量计标定装置相连接,该固体质量流量计标定装置的称重装置的出口通过一控制阀与该进料系统的入口相连接,各输料管道均连接有至少一固体质量流量计。9. A dry feed and reaction system, which includes a feed system and a reaction device, characterized in that it also includes: a solid mass flow meter calibration device as claimed in claim 1, and one or Multiple feeding pipelines, each feeding pipeline is connected to a conversion device; wherein, the feed system is respectively connected to the reaction device and the solid mass flowmeter calibration device through the feeding pipeline and the corresponding conversion device connected thereto The outlet of the weighing device of the solid mass flowmeter calibration device is connected with the inlet of the feed system through a control valve, and each feed pipeline is connected with at least one solid mass flowmeter. 10、如权利要求9所述的干法进料和反应的系统,其特征在于,该转换装置为一三通阀,该三通阀具一入口、一第一出口和一第二出口,其中,该三通阀的入口通过与之相应连接的输料管道与该进料系统的出口相连接,该三通阀的第一出口与该固体质量流量计标定装置的第二管道入口相连接,该三通阀的第二出口通过一连接管与该反应装置相连接,该输料管道上还连接一载气输入装置。10. The dry feeding and reaction system according to claim 9, characterized in that the conversion device is a three-way valve, and the three-way valve has an inlet, a first outlet and a second outlet, wherein , the inlet of the three-way valve is connected to the outlet of the feed system through the correspondingly connected feeding pipeline, the first outlet of the three-way valve is connected to the second pipeline inlet of the solid mass flowmeter calibration device, The second outlet of the three-way valve is connected to the reaction device through a connecting pipe, and a carrier gas input device is also connected to the feeding pipeline. 11、如权利要求10所述的干法进料和反应的系统,其特征在于,该进料系统包括依次顺序相连的一常压储仓、一间歇下料装置和一发料罐。11. The dry feeding and reaction system according to claim 10, characterized in that the feeding system comprises an atmospheric storage bin, an intermittent feeding device and a feeding tank connected in sequence. 12、如权利要求11所述的干法进料和反应的系统,其特征在于,该间歇下料装置为一锁斗系统或一高压旋转给料器。12. The dry feeding and reaction system according to claim 11, characterized in that the intermittent feeding device is a lock hopper system or a high-pressure rotary feeder. 13、如权利要求11或12所述的干法进料和反应的系统,其特征在于,该常压储仓、该间歇下料装置和该发料罐上均装有一载气输入装置。13. The dry feeding and reaction system according to claim 11 or 12, characterized in that, the atmospheric storage bin, the intermittent feeding device and the feeding tank are equipped with a carrier gas input device.
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CN102070023A (en) * 2010-12-03 2011-05-25 重庆国际复合材料有限公司 Decompression discharge pipe and raw material mixing system adopting the same
CN102128666A (en) * 2011-02-11 2011-07-20 合肥工业大学 Method for calibrating Coriolis mass flowmeter
CN102466104A (en) * 2010-11-08 2012-05-23 通用电气公司 Pipeline and conveying method
CN110864773A (en) * 2019-12-03 2020-03-06 镇江市计量检定测试中心 Method and system for on-line inspection of accuracy of solid flowmeter
CN111044125A (en) * 2019-12-31 2020-04-21 华东理工大学 Method and storage medium for automatic calibration of flow point
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CN102466104A (en) * 2010-11-08 2012-05-23 通用电气公司 Pipeline and conveying method
CN102466104B (en) * 2010-11-08 2015-08-26 通用电气公司 Pipeline and delivery method
US9387997B2 (en) 2010-11-08 2016-07-12 General Electric Company Pipelines and conveying methods
CN102070023A (en) * 2010-12-03 2011-05-25 重庆国际复合材料有限公司 Decompression discharge pipe and raw material mixing system adopting the same
CN102128666A (en) * 2011-02-11 2011-07-20 合肥工业大学 Method for calibrating Coriolis mass flowmeter
CN102128666B (en) * 2011-02-11 2012-08-08 合肥工业大学 Method for calibrating Coriolis mass flowmeter
CN110864773A (en) * 2019-12-03 2020-03-06 镇江市计量检定测试中心 Method and system for on-line inspection of accuracy of solid flowmeter
CN111044125A (en) * 2019-12-31 2020-04-21 华东理工大学 Method and storage medium for automatic calibration of flow point
CN116399397A (en) * 2023-04-06 2023-07-07 中核四0四有限公司 A material liquid calibration system

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