CN201352204Y - Special sample table for measuring fiber orientation by using X-ray diffraction instrument - Google Patents
Special sample table for measuring fiber orientation by using X-ray diffraction instrument Download PDFInfo
- Publication number
- CN201352204Y CN201352204Y CNU2009201054107U CN200920105410U CN201352204Y CN 201352204 Y CN201352204 Y CN 201352204Y CN U2009201054107 U CNU2009201054107 U CN U2009201054107U CN 200920105410 U CN200920105410 U CN 200920105410U CN 201352204 Y CN201352204 Y CN 201352204Y
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- worm
- base
- fixed block
- sample
- orientation
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- 239000000835 fiber Substances 0.000 title claims abstract description 12
- 238000002441 X-ray diffraction Methods 0.000 title abstract 2
- 230000005540 biological transmission Effects 0.000 abstract description 7
- 239000000523 sample Substances 0.000 description 23
- 239000000463 material Substances 0.000 description 8
- 239000013078 crystal Substances 0.000 description 7
- 239000002657 fibrous material Substances 0.000 description 3
- 238000002050 diffraction method Methods 0.000 description 2
- 238000000034 method Methods 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 235000014676 Phragmites communis Nutrition 0.000 description 1
- 239000013068 control sample Substances 0.000 description 1
- 238000005096 rolling process Methods 0.000 description 1
- 238000009987 spinning Methods 0.000 description 1
- 238000005491 wire drawing Methods 0.000 description 1
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Abstract
The utility model discloses a special sample table for measuring fiber orientation by using an X-ray diffraction instrument, comprising a motor, a worm, a worm wheel, a base, a guide track, a sliding block, an adjusting screw and a fixed block, the motor is connected with the worm by transmission; the worm is connected with the worm wheel by meshing; the base and the worm wheel are corresponding by precise positioning of a shaft hole; the fixed block and the guide track are fixedly arranged on the base, the sliding block is arranged in the guide track in a sliding manner; and one end of the adjusting screw is connected with the sliding block, and the other end thereof is connected with the fixed block. The special sample table has the advantages of simple structure, transmission by using the worm wheel, low cost and durability. The adoption of the worm wheel-worm structure can drive a sample to rotate and place the sample at the center of the worm wheel, thereby meeting the transmission scanning way.
Description
Technical field
The utility model relates to a kind of X-ray diffractometer and measures the special-purpose sample stage of the fiber degree of orientation.
Background technology
Polycrystalline material is made up of many crystal grain, if the crystalline orientation of these crystal grain is fully random, then the macro property of this crystal is isotropic.Yet behind the deformation processes such as general polycrystalline material process is rolling, stretching, extruding, spinning, wire drawing, some regularity can appear in the crystalline orientation of each crystal grain, and material also just presents certain anisotropy.In polycrystalline material, certain regularity appears in the crystalline orientation of crystal grain, and perhaps the crystallography face is concentrated toward some certain surface of material profile, and perhaps crystallographic direction and crystallography face all have concentrating to a certain degree, then claim to have preferred orientation in this polycrystalline material.The crystallographic direction of fibrous material tends to be parallel to the silk direction of principal axis of material, becomes rotational symmetry to distribute, and generally represents the size of material preferred orientation degree with the degree of orientation.
The utility model content
The purpose of this utility model provides a kind of X-ray diffractometer and measures the special-purpose sample stage of the fiber degree of orientation, and is simple in structure, easy to use, the degree of accuracy height.
For achieving the above object, technical scheme provided by the utility model is: a kind of X-ray diffractometer is measured the special-purpose sample stage of the fiber degree of orientation, include motor, worm screw, worm gear, base, guide rail, slide block, set screw and fixed block, described motor is connected with worm drive; Described worm and wheel is connected with a joggle; Described base and worm gear are accurately located correspondence by axis hole; Described fixed block and guide rail are fixedly installed on the base, and described slide block is located in the guide rail slidably; Described set screw one end is connected with slide block, and an end is connected with fixed block.
Described slide block is provided with two, and all is located in the guide rail slidably.
Described motor is a stepper motor.
The advantage that the utlity model has: this product structure is simple, adopts worm-drive, and cost is low, and is durable in use.Adopt worm-and-wheel gear, drive the sample rotation, sample is positioned over the worm gear center, satisfies the transmission scan mode.
Description of drawings:
Below in conjunction with the drawings and specific embodiments the utility model is described in further detail.
Fig. 1 is a structural representation of the present utility model.
Wherein: 1 ... fixed block 2 ... set screw 3 ... slide block
4 ... guide rail 5 ... base 6 ... worm gear
7 ... worm screw 8 ... stepper motor
Embodiment:
A kind of X-ray diffractometer is as shown in Figure 1 measured the special-purpose sample stage of the fiber degree of orientation, includes stepper motor 8, worm screw 7, worm gear 6, base 5, guide rail 4, two slide blocks 3, set screw 2 and fixed blocks 1, and described stepper motor 8 is in transmission connection with worm screw 7; Described worm screw 7 is connected with a joggle with worm gear 6; Described base 5 and worm gear 6 are accurately located correspondence by axis hole; Described fixed block 1 and guide rail 4 are fixedly installed on the base 5, and described slide block 3 is located in the guide rail 4 slidably; Described set screw 2 one ends are connected with slide block 3, and an end is connected with fixed block 1.
Fiber sample is fixed on above two slide blocks 3 by screw and press strip, and rotation set screw 2 is stretching fiber sample.Set screw 2 one ends are connected with slide block 3, and an end is connected with fixed block 1, rotation set screw 2, and slide block 3 promptly moves in orbit.Press strip and above the slide block design have miniature sawtooth to make keeping parallelism between the sample.Convenient in order to change sample, fixed block 1, guide rail 4 are installed on the base 5, and base 5 can whole take off above sample stage, by one group of reed, is connected with worm gear 6, accurately locatees by axis hole between base 5 and the worm gear 6.
Stepper motor 8 is passed to worm screw 7 to rotation by one group of gear drive, worm screw 7 drives worm gear 6 and rotates, worm gear 6 drives sample and rotates, thereby make sample and diffraction plane become different angles, promptly transference silk axle becomes the crystal of different angles to respectively attend diffraction, and the transmission of high precision worm and gear can guarantee the accurate location of sample and little stepping angle and good location repeatability.
Set scanning angle, the control sample stage is rotated by predetermined manner, accepts the scanning strength signal that detector is beamed back simultaneously, draws the test collection of illustrative plates, and scanning calculates the degree of orientation of sample when finishing.
Instrument is by measuring the diffracted intensity of different angles, and software can calculate the degree of orientation of sample, and degree of orientation computing formula is: as the degree of orientation=diffraction peak high wide/180 °
The degree of orientation of measuring fibrous material is at first stretching sample, because fibrous material all is soft generally speaking, we design two can clamp the device that sample can move again simultaneously in opposite directions; Secondly, sample is wanted and can be shifted one's position, and makes with the silk axle to become the crystal of different angles to respectively attend diffraction, and we design a cover worm-and-wheel gear, drive the sample rotation, and sample is positioned over the worm gear center, satisfies the transmission scan mode.Drive sample and rotate the mode that also can select Harmonic Gears, consider that cost also has durable degree, so select worm-drive.
The above, it only is preferred embodiment of the present utility model, be not that the utility model is done any pro forma restriction, though the utility model discloses as above with preferred embodiment, yet be not in order to limit the utility model, any those skilled in the art, in not breaking away from the technical solutions of the utility model scope, when the technology contents that can utilize above-mentioned announcement is made a little change or is modified to the equivalent embodiment of equivalent variations, in every case be the content that does not break away from technical solutions of the utility model, according to technical spirit of the present utility model to any simple modification that above embodiment did, equivalent variations and modification all still belong in the scope of technical solutions of the utility model.
Claims (3)
1, a kind of X-ray diffractometer is measured the special-purpose sample stage of the fiber degree of orientation, and it is characterized in that: include motor, worm screw, worm gear, base, guide rail, slide block, set screw and fixed block, described motor is connected with worm drive; Described worm and wheel is connected with a joggle; Described base and worm gear are accurately located correspondence by axis hole; Described fixed block and guide rail are fixedly installed on the base, and described slide block is located in the guide rail slidably; Described set screw one end is connected with slide block, and an end is connected with fixed block.
2, X-ray diffractometer according to claim 1 is measured the special-purpose sample stage of the fiber degree of orientation, and it is characterized in that: described slide block is provided with two, and all is located in the guide rail slidably.
3, X-ray diffractometer according to claim 1 is measured the special-purpose sample stage of the fiber degree of orientation, and it is characterized in that: described motor is a stepper motor.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNU2009201054107U CN201352204Y (en) | 2009-01-22 | 2009-01-22 | Special sample table for measuring fiber orientation by using X-ray diffraction instrument |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNU2009201054107U CN201352204Y (en) | 2009-01-22 | 2009-01-22 | Special sample table for measuring fiber orientation by using X-ray diffraction instrument |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN201352204Y true CN201352204Y (en) | 2009-11-25 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CNU2009201054107U Expired - Lifetime CN201352204Y (en) | 2009-01-22 | 2009-01-22 | Special sample table for measuring fiber orientation by using X-ray diffraction instrument |
Country Status (1)
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| CN (1) | CN201352204Y (en) |
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102435626A (en) * | 2011-09-13 | 2012-05-02 | 丹东通达科技有限公司 | Table type X-ray diffractometer |
| CN102661963A (en) * | 2012-06-01 | 2012-09-12 | 吉林大学 | Special X-ray diffraction and scattering analysis device for fiber material |
| CN103487298A (en) * | 2013-06-19 | 2014-01-01 | 联新（开平）高性能纤维有限公司 | Sample holder used for fibers tested by X-ray diffraction |
| CN109490343A (en) * | 2018-12-04 | 2019-03-19 | 西北工业大学 | A kind of serial crystallography sample transport device and method |
| WO2019069956A1 (en) * | 2017-10-03 | 2019-04-11 | 国立大学法人名古屋大学 | Method for measuring degree of orientation of fibers, device for measuring degree of orientation of fibers, and program for controlling device for measuring degree of orientation of fibers |
| CN116481457A (en) * | 2023-04-20 | 2023-07-25 | 陕西师范大学 | A carbon fiber material X-ray diffraction transmission sample quality detection system and method |
-
2009
- 2009-01-22 CN CNU2009201054107U patent/CN201352204Y/en not_active Expired - Lifetime
Cited By (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102435626A (en) * | 2011-09-13 | 2012-05-02 | 丹东通达科技有限公司 | Table type X-ray diffractometer |
| CN102661963A (en) * | 2012-06-01 | 2012-09-12 | 吉林大学 | Special X-ray diffraction and scattering analysis device for fiber material |
| CN102661963B (en) * | 2012-06-01 | 2014-02-12 | 吉林大学 | X-ray diffraction and scattering analysis device for fiber materials |
| CN103487298A (en) * | 2013-06-19 | 2014-01-01 | 联新（开平）高性能纤维有限公司 | Sample holder used for fibers tested by X-ray diffraction |
| CN103487298B (en) * | 2013-06-19 | 2016-12-28 | 联新（开平）高性能纤维有限公司 | A kind of X-ray diffraction test fiber specimen holder |
| WO2019069956A1 (en) * | 2017-10-03 | 2019-04-11 | 国立大学法人名古屋大学 | Method for measuring degree of orientation of fibers, device for measuring degree of orientation of fibers, and program for controlling device for measuring degree of orientation of fibers |
| JP2019066389A (en) * | 2017-10-03 | 2019-04-25 | 国立大学法人名古屋大学 | Method for measuring fiber orientation degree, fiber orientation degree measuring device, and control program of fiber orientation degree measuring device |
| KR20210071871A (en) * | 2017-10-03 | 2021-06-16 | 고쿠리츠 다이가쿠 호우징 도우카이 고쿠리츠 다이가쿠 기코우 | A method for measuring fiber orientation, a fiber orientation measuring device, and a control program for a fiber orientation measuring device |
| US11360035B2 (en) | 2017-10-03 | 2022-06-14 | National University Corporation Tokai National Higher Education And Research System | Method for measuring fiber orientation degree, fiber orientation degree measurement apparatus, and control computer program for fiber orientation degree measurement apparatus |
| KR102556672B1 (en) | 2017-10-03 | 2023-07-18 | 고쿠리츠 다이가쿠 호우징 도우카이 고쿠리츠 다이가쿠 기코우 | Fiber orientation measurement method, fiber orientation measurement device, and control program for the fiber orientation measurement device |
| CN109490343A (en) * | 2018-12-04 | 2019-03-19 | 西北工业大学 | A kind of serial crystallography sample transport device and method |
| CN116481457A (en) * | 2023-04-20 | 2023-07-25 | 陕西师范大学 | A carbon fiber material X-ray diffraction transmission sample quality detection system and method |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CX01 | Expiry of patent term |
Granted publication date: 20091125 |
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| CX01 | Expiry of patent term |