CN201177606Y - Hand-held second generation X fluorescent spectrometer - Google Patents
Hand-held second generation X fluorescent spectrometer Download PDFInfo
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- CN201177606Y CN201177606Y CNU2007201962146U CN200720196214U CN201177606Y CN 201177606 Y CN201177606 Y CN 201177606Y CN U2007201962146 U CNU2007201962146 U CN U2007201962146U CN 200720196214 U CN200720196214 U CN 200720196214U CN 201177606 Y CN201177606 Y CN 201177606Y
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- spectrometer
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- fixed
- fluorescence spectrophotometer
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- 229910052751 metal Inorganic materials 0.000 claims abstract description 10
- 239000002184 metal Substances 0.000 claims abstract description 10
- 238000012545 processing Methods 0.000 claims abstract description 10
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 5
- 230000005855 radiation Effects 0.000 claims description 5
- 239000000741 silica gel Substances 0.000 claims description 5
- 229910002027 silica gel Inorganic materials 0.000 claims description 5
- 239000013307 optical fiber Substances 0.000 claims description 4
- 238000005259 measurement Methods 0.000 abstract description 8
- NJPPVKZQTLUDBO-UHFFFAOYSA-N novaluron Chemical compound C1=C(Cl)C(OC(F)(F)C(OC(F)(F)F)F)=CC=C1NC(=O)NC(=O)C1=C(F)C=CC=C1F NJPPVKZQTLUDBO-UHFFFAOYSA-N 0.000 abstract 2
- 230000005284 excitation Effects 0.000 abstract 1
- 238000012360 testing method Methods 0.000 description 17
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 8
- 238000000034 method Methods 0.000 description 7
- 230000003287 optical effect Effects 0.000 description 5
- 239000004033 plastic Substances 0.000 description 5
- 229920003023 plastic Polymers 0.000 description 5
- 229910052757 nitrogen Inorganic materials 0.000 description 4
- 238000013461 design Methods 0.000 description 3
- 238000000921 elemental analysis Methods 0.000 description 3
- 229910052745 lead Inorganic materials 0.000 description 3
- 239000007788 liquid Substances 0.000 description 3
- 239000000463 material Substances 0.000 description 3
- 230000002285 radioactive effect Effects 0.000 description 3
- 230000035945 sensitivity Effects 0.000 description 3
- 239000000758 substrate Substances 0.000 description 3
- 238000004458 analytical method Methods 0.000 description 2
- 229910052793 cadmium Inorganic materials 0.000 description 2
- 238000005057 refrigeration Methods 0.000 description 2
- 230000005477 standard model Effects 0.000 description 2
- 229910001051 Magnalium Inorganic materials 0.000 description 1
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 1
- ATJFFYVFTNAWJD-UHFFFAOYSA-N Tin Chemical compound [Sn] ATJFFYVFTNAWJD-UHFFFAOYSA-N 0.000 description 1
- 229910052770 Uranium Inorganic materials 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000010276 construction Methods 0.000 description 1
- 238000012937 correction Methods 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 239000011159 matrix material Substances 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 229910052700 potassium Inorganic materials 0.000 description 1
- 239000011591 potassium Substances 0.000 description 1
- 235000013619 trace mineral Nutrition 0.000 description 1
- 239000011573 trace mineral Substances 0.000 description 1
- JFALSRSLKYAFGM-UHFFFAOYSA-N uranium(0) Chemical compound [U] JFALSRSLKYAFGM-UHFFFAOYSA-N 0.000 description 1
- 238000012795 verification Methods 0.000 description 1
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- Analysing Materials By The Use Of Radiation (AREA)
Abstract
A handheld secondary X fluorescence spectrometer comprises a main body and a palm computer, wherein the main body is made into a shape of a portable gun and includes a left housing, a trigger, a right housing and pedestal; a detector and a light source emission system are fixed in the front part of the gun body in the right housing; a printed circuit board and a signal processing system are fixed in the middle part of the gun body in the right housing; the pedestal is fixed at the tail part of the gun body in the right housing; a battery is fixed in the position of the trigger in the right housing; a battery cover covers the battery; the light source system includes a high-voltage power supply and a X-ray tube; the X-ray tube adopts an integral package structure; and a metal radiator is arranged on the housing the integral package structure. The X fluorescence spectrometer has the advantages of no pollution, safe excitation source, stable measurement, less consumables, high resolution, accurate measurement, smart structure and good portability. The spectrometer more suits field operation and has greater advantages in measuring large objects.
Description
Technical field
The utility model relates to a kind of trace element detector device, especially a kind of X fluorescent energy dispersive spectrometer of hand-held, and simultaneously in the fast detecting sample, the multiple element from potassium (K) to uranium (U).The on-the-spot on-line detector device of this instrument for developing at the RoHS instruction of European Union specially, five kinds of elements that relate in the main measure R oHS instruction, six kinds of materials.
Background technology
Mainly there is following shortcoming in the X fluorescence spectrophotometer of Tui Chuing in the market:
1. excitaton source.The still employing that has falls behind, and has been subjected to the isotope radioactive source that control is give stricted orders by country.The isotope radioactive source is that whole day does not have not, can radiate radiation ray no matter whether test all, and operator and environment are had radiation pollution.In view of the reason of secure context, the isotope radioactive source has been subjected to the control of give stricting orders of national departments concerned, and the user is had many restrictive conditions and verification process.And high-voltage power supply and X-ray pipe excitaton source that this money instrument adopts are a kind of foolproof excitaton sources.When instrument is in non-test mode, will have X ray and produce.When test,, avoided the escape of X ray to greatest extent also by structural design.So be a kind of testing tool of environmental sound.
2. detector refrigeration mode.Aspect detector, the detector that still adopts the liquid nitrogen refrigerating technical support that falls behind that has.Adopt the X fluorescence spectrophotometer of liquid nitrogen refrigerating, except bulky, its nitrogen need regularly go to replenish owing to the cause that can not stop to volatilize, for the operator, and very loaded down with trivial details and trouble.And because on the refrigeration principle, often can not guarantee that with the detector of liquid nitrogen refrigerating detector works under the state of constant temperature, all measurement results also can instability.
3. detector.Equally aspect detector, what have still adopts relatively backward proportional counter tube, and this detector is because on the analysis principle, resolution is poor, measure micro-aspect, effect is poor.
4. apparatus structure.Instrument in the market mainly is desk-top, even vertical.Volume ratio is huger, can only use in indoor even laboratory, bothers very much aspect transportation, and exists the danger that data will be proofreaied and correct again.Meeting some big, as outcase of refrigerator, during automobile case etc., the use aspect is inconvenience quite.
5. can not switch optical filter.In the ROHS test, the sample of corresponding metallic matrix and plastic substrate is difficult to obtain correct measurement result; When making full elemental analysis, wider elemental range there are not good sensitivity and accuracy.
Summary of the invention
In order to overcome the shortcoming of above-mentioned X fluorescence spectrophotometer, order of the present utility model provides a kind of hand-hold China second-generation X fluorescence spectrophotometer, and this spectrometer has the unexistent premium properties of general X fluorescence spectrophotometer by the improvement to original structure.
The technical scheme that the utility model adopted is: a kind of hand-hold China second-generation X fluorescence spectrophotometer, comprise fuselage and the palm PC that is attached thereto, wherein, in the described fuselage light-source system is installed, detector system, signal Processing and MCA system, light-source system (comprising high pressure and light pipe) is launched X ray, after X ray acts on the sample, each atom in the sample can be inspired feature X fluorescence, these X fluorescence are detected device and receive, and analyze to be converted into electric signal, and electric signal is through the processing of MCA module, be transferred to again in the palm PC (PDA), on the user interface of software, show; Wherein, described fuselage be shaped as the rifle shape that is easy to carry about with one, described fuselage comprises left shell, trigger, right shell and base, wherein, detector, light source radiation system are fixed in body of a gun front portion in the right shell, and printed circuit board (PCB), signal processing system then are fixed in body of a gun middle part in the right shell, base is fixed in body of a gun afterbody in the right shell simultaneously, and the trigger stationkeeping has battery in the described right shell, is covered with a battery cover on this battery; Described light-source system comprises high-voltage power supply and X-ray pipe, and described X-ray pipe adopts integrated encapsulating structure, adds metal heat sink on the shell of described integrated encapsulating structure.
Because instrument in the market mainly is desk-top, even vertical.Volume ratio is huger, can only use in indoor even laboratory, bothers very much aspect transportation, and exists the danger that data will be proofreaied and correct again.Meeting some big, as outcase of refrigerator, during automobile case etc., the use aspect is inconvenience quite.And rifle shape structure Design makes that the utility model volume very little (size), weight only are about 1.2kg, and is easy to carry and transport, and the advantage when operation in the open air and measurement big article is incomparable.
Described metal heat sink comprises left radiating block and right radiating block.The installing additional of the integrated encapsulating structure of X-ray pipe and metal heat sink greatly reduces the temperature of X-ray plumber when doing, and helps prolonging the serviceable life of X-ray pipe.
Described spectrometer is provided with switching device of optical fiber.This installs changeable 2 groups of optical filters, and in the ROHS test, therefore the sample of these 2 groups of optical filters corresponding metallic matrixes of difference and plastic substrate all has correct measurement result; When making full elemental analysis, wider elemental range there are good sensitivity and accuracy.
Be mounted with a palm PC (PDA) on the shell of described spectrometer, be connected for wireless blue tooth between described PDA and the described spectrometer.Therefore in test process, the hand-holdable PDA of operating personnel observes and controls, and can arbitrarily move in certain distance, makes test process more flexible, and is more humane.
The front end of described spectrometer is provided with microswitch.This microswitch has guaranteed just can start the X-ray pipe when instrument is close to sample, and the output X ray makes instrument more secure to people's security.
Described spectrometer is provided with and detects a mouthful buffered silica gel spare support.
Described spectrometer can use 110/220 volt of AC power, also can use the 9VDC adapter, makes the power supply of instrument battery charge and continuous coverage.Increased the convenience of using, be used in combination selectable unit-fixed testing jig, can make the utility model also be used for indoor follow-on test, realized a machine double-purpose as desk-top instrument.
The beneficial effects of the utility model are: this instrument is pollution-free, safe excitaton source; Measure and stablize, consumptive material is few; The resolution height is measured accurately; Small volume and less weight is more suitable for site work, and the advantage when the test big article is particularly outstanding.
Description of drawings
Below in conjunction with drawings and Examples the utility model is further specified.
Fig. 1 is an one-piece construction synoptic diagram of the present utility model.
Fig. 2 is the structural representation of right shell part of the utility model and PDA part.
Fig. 3 is the structural representation of trigger portion of the present utility model.
Fig. 4 is the structural representation of base portion of the present utility model.
Fig. 5 is mouthful structural representation of buffered silica gel spare holder part that detects of the present utility model.
1, palm PC; 2, left shell; 3, left radiating block; 4, printed circuit board (PCB); 5, detector; 6, detect a mouthful buffered silica gel spare support; 7, collimating apparatus; 8, high pressure light pipe; 9, right radiating block; 10, trigger; 11, battery cover; 12, battery, 13, right shell; 14, base; 31, switching device of optical fiber; 32, microswitch.
Embodiment
As Fig. 1, Fig. 2, Fig. 3, Fig. 4 and shown in Figure 5, a kind of hand-hold China second-generation X fluorescence spectrophotometer, comprise fuselage and the palm PC (1) that is attached thereto, wherein, in the described fuselage light-source system is installed, detector system, signal Processing and MCA system, light-source system (comprising high pressure and light pipe) is launched X ray, after X ray acted on the sample, each atom in the sample can be inspired feature X fluorescence, and these X fluorescence are detected device (5) and receive, analysis is converted into electric signal, electric signal is transferred in the palm PC (1) through the processing of MCA module again, shows on the user interface of software; Wherein, described fuselage be shaped as the rifle shape that is easy to carry about with one, described fuselage comprises left shell (2), trigger (10), right shell (13) and base (14), wherein, the collimating apparatus (7) of detector (5), light source radiation system and high pressure light pipe (8) are fixed in the interior body of a gun of right shell (13) front portion, printed circuit board (PCB) (4), signal processing system then are fixed in the interior body of a gun of right shell (13) middle part, base (14) is fixed in body of a gun afterbody in the right shell simultaneously, and, trigger (10) stationkeeping has battery (12) in the described right shell, is covered with a battery cover (11) on this battery; Described light-source system comprises high-voltage power supply and X-ray pipe, and described X-ray pipe adopts integrated encapsulating structure, adds metal heat sink on the shell of described integrated encapsulating structure, and described metal heat sink comprises left radiating block (3) and right radiating block (9).
On the one hand, instrument in the market mainly is desk-top, even vertical.Volume ratio is huger, can only use in indoor even laboratory, bothers very much aspect transportation, and exists the danger that data will be proofreaied and correct again.Meeting some big, as outcase of refrigerator, during automobile case etc., the use aspect is inconvenience quite.And rifle shape structure Design makes that the utility model volume very little (size), weight only are about 1.2kg, and is easy to carry and transport, and the advantage when operation in the open air and measurement big article is incomparable.
In addition, the installing additional of integrated encapsulating structure and metal heat sink greatly reduces the temperature of X-ray plumber when doing, and helps prolonging the serviceable life of X-ray pipe.
Described spectrometer is provided with switching device of optical fiber (31).This installs changeable 2 groups of optical filters, and in the ROHS test, therefore the sample of these 2 groups of optical filters corresponding metallic matrixes of difference and plastic substrate all has correct measurement result; When making full elemental analysis, wider elemental range there are good sensitivity and accuracy.
Be mounted with a palm PC (PDA) on the shell of described spectrometer, be connected for wireless blue tooth between described PDA and the described spectrometer.Therefore in test process, the hand-holdable PDA of operating personnel observes and controls, and can arbitrarily move in certain distance, makes test process more flexible, and is more humane.
The front end of described spectrometer is provided with microswitch (32).This microswitch has guaranteed just can start the X-ray pipe when instrument is close to sample, and the output X ray makes instrument more secure to people's security.
Described spectrometer is provided with and detects a mouthful buffered silica gel spare support (6).
Described spectrometer can use 110/220 volt of AC power, also can use the 9VDC adapter, makes the power supply of instrument battery charge and continuous coverage.Increased the convenience of using, be used in combination selectable unit-fixed testing jig, can make the utility model also be used for indoor follow-on test, realized a machine double-purpose as desk-top instrument.
The principle of work of software of the present utility model mainly comprises following five steps:
One, instrumental correction
Adjust the instrument enlargement factor, eliminate the influence that the peak floats, guarantee that testing sample is consistent with the mark sample condition.
Two, working curve
Composition per sample is different with base material, working curve is divided into five big classes: promptly survey the Cr in the plastics; Survey the Cr in the magnalium, Cd, Pb, Hg, Br surveys the Cd in the plastics, Pb, Hg, Br surveys the Cr in the metal, Cd, Pb, Hg, Br surveys in the scolding tin Pb etc.Each big class can be added many curves arbitrarily according to actual needs.
Three, intensity is calculated
Here adopt the method for peak back of the body ratio, peak area calculates with Gauss curve fitting.That is:
R: the left margin at peak
L: the right margin at peak
H: the height at peak.
X: Feng Dao location
X
0: the center trace location at peak
δ: the parameter relevant with the width at peak
Four, calculate content
Content by formula C=a*I+b calculates.
Coefficient a, b provides with least square method.
C
iBe the concentration of standard model i.
I
iBe the intensity of standard model i.
Five, report the result
Can be saved in needed file to the result who measures, and come out by printer prints.
Claims (7)
1. hand-hold China second-generation X fluorescence spectrophotometer, comprise fuselage and the palm PC that is attached thereto, wherein, light-source system, detector system are installed in the described fuselage, signal Processing and MCA system, wherein, light-source system comprises high pressure and light pipe, launches X ray, after X ray acts on the sample, each atom in the sample can be inspired feature X fluorescence, these X fluorescence are detected device and receive, and analyze to be converted into electric signal, and electric signal is through the processing of MCA module, be transferred to again in the palm PC, on the user interface of software, show; Wherein, described fuselage be shaped as the rifle shape that is easy to carry about with one, described fuselage comprises left shell, trigger, right shell and base, wherein, detector, light source radiation system are fixed in body of a gun front portion in the right shell, and printed circuit board (PCB), signal processing system then are fixed in body of a gun middle part in the right shell, base is fixed in body of a gun afterbody in the right shell simultaneously, and the trigger stationkeeping has battery in the described right shell, is covered with a battery cover on this battery; It is characterized in that: described light-source system comprises high-voltage power supply and X-ray pipe, and described X-ray pipe adopts integrated encapsulating structure, adds metal heat sink on the shell of described integrated encapsulating structure.
2, according to the described hand-hold China second-generation X of claim 1 fluorescence spectrophotometer, it is characterized in that: described metal heat sink comprises left radiating block (3) and right radiating block (9)
3. according to claim 1 or 2 described hand-hold China second-generation X fluorescence spectrophotometer, it is characterized in that: described spectrometer is provided with switching device of optical fiber.
4. according to the described hand-hold China second-generation X of claim 3 fluorescence spectrophotometer, it is characterized in that: be mounted with a palm PC on the shell of described spectrometer, be connected for wireless blue tooth between described palm PC and the described spectrometer.
5. according to the described hand-hold China second-generation X of claim 4 fluorescence spectrophotometer, it is characterized in that: the front end of described spectrometer is provided with microswitch.
6. according to the described hand-hold China second-generation X of claim 5 fluorescence spectrophotometer, it is characterized in that: described spectrometer is provided with and detects a mouthful buffered silica gel spare support.
7. according to the described hand-hold China second-generation X of claim 6 fluorescence spectrophotometer, it is characterized in that: described spectrometer can use 110/220 volt of AC power, also can use the 9VDC adapter, makes the power supply of instrument battery charge and continuous coverage.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNU2007201962146U CN201177606Y (en) | 2007-12-21 | 2007-12-21 | Hand-held second generation X fluorescent spectrometer |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNU2007201962146U CN201177606Y (en) | 2007-12-21 | 2007-12-21 | Hand-held second generation X fluorescent spectrometer |
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| Publication Number | Publication Date |
|---|---|
| CN201177606Y true CN201177606Y (en) | 2009-01-07 |
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| CNU2007201962146U Expired - Fee Related CN201177606Y (en) | 2007-12-21 | 2007-12-21 | Hand-held second generation X fluorescent spectrometer |
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Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102854209A (en) * | 2011-07-01 | 2013-01-02 | 奥林巴斯Ndt公司 | X-ray analysis apparatus and x-ray analysis method |
| CN102967613A (en) * | 2012-12-05 | 2013-03-13 | 钢研纳克检测技术有限公司 | Rapid identifier of rare earth |
| CN104272095A (en) * | 2012-02-29 | 2015-01-07 | X射线光学系统公司 | Portable x-ray analyzer having vibration, thermal and/or moisture isolation from exterior environment |
| CN104535526A (en) * | 2014-12-17 | 2015-04-22 | 中国科学院长春光学精密机械与物理研究所 | Linear gradual filter type handheld intelligent spectrometer based on microcomputer Edison |
| CN104807842A (en) * | 2014-01-24 | 2015-07-29 | 奥林巴斯科技美国公司 | Test stand for XRF instrument enabling multi-way operation |
| CN106198472A (en) * | 2016-07-11 | 2016-12-07 | 天津出入境检验检疫局工业产品安全技术中心 | A kind of Split hand held fluorescence spectrophotometer |
| CN108254389A (en) * | 2016-12-29 | 2018-07-06 | 中核建中核燃料元件有限公司 | A portable mercury content detection instrument |
| CN110702740A (en) * | 2018-07-10 | 2020-01-17 | 郴州市佳迅电子仪器科技有限公司 | Engine oil quality detection instrument |
-
2007
- 2007-12-21 CN CNU2007201962146U patent/CN201177606Y/en not_active Expired - Fee Related
Cited By (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102854209A (en) * | 2011-07-01 | 2013-01-02 | 奥林巴斯Ndt公司 | X-ray analysis apparatus and x-ray analysis method |
| CN104272095A (en) * | 2012-02-29 | 2015-01-07 | X射线光学系统公司 | Portable x-ray analyzer having vibration, thermal and/or moisture isolation from exterior environment |
| CN104272095B (en) * | 2012-02-29 | 2017-05-17 | X射线光学系统公司 | Portable x-ray analyzer having vibration, thermal and/or moisture isolation from exterior environment |
| CN102967613A (en) * | 2012-12-05 | 2013-03-13 | 钢研纳克检测技术有限公司 | Rapid identifier of rare earth |
| CN104807842A (en) * | 2014-01-24 | 2015-07-29 | 奥林巴斯科技美国公司 | Test stand for XRF instrument enabling multi-way operation |
| US9683952B2 (en) | 2014-01-24 | 2017-06-20 | Olympus Scientific Solutions Americas Inc. | Test stand for XRF instrument enabling multi-way operation |
| CN104807842B (en) * | 2014-01-24 | 2017-11-28 | 奥林巴斯科技美国公司 | Testing stand for the XRF instrument of energy multi-mode operation |
| CN104535526A (en) * | 2014-12-17 | 2015-04-22 | 中国科学院长春光学精密机械与物理研究所 | Linear gradual filter type handheld intelligent spectrometer based on microcomputer Edison |
| CN106198472A (en) * | 2016-07-11 | 2016-12-07 | 天津出入境检验检疫局工业产品安全技术中心 | A kind of Split hand held fluorescence spectrophotometer |
| CN108254389A (en) * | 2016-12-29 | 2018-07-06 | 中核建中核燃料元件有限公司 | A portable mercury content detection instrument |
| CN110702740A (en) * | 2018-07-10 | 2020-01-17 | 郴州市佳迅电子仪器科技有限公司 | Engine oil quality detection instrument |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| C56 | Change in the name or address of the patentee |
Owner name: JIANGSU TIANRUI INSTRUMENT CO., LTD. Free format text: FORMER NAME: JIANGSU TIANRUI INFORMATION TECHNOLOGY CO., LTD. |
|
| CP03 | Change of name, title or address |
Address after: Room 215347, Tsinghua hi tech park, 1666 South Gate Road, Jiangsu, Kunshan, China Patentee after: Jiangsu Skyray Instrument Co., Ltd. Address before: Qinghua science park, No. 1666, Reed Road, Jiangsu, Kunshan Province, China: 215347 Patentee before: Jiangsu Skyray Information Technology Co., Ltd. |
|
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20090107 Termination date: 20151221 |
|
| EXPY | Termination of patent right or utility model |