CN2080863U - Energy-saving distillator - Google Patents
Energy-saving distillator Download PDFInfo
- Publication number
- CN2080863U CN2080863U CN 90218158 CN90218158U CN2080863U CN 2080863 U CN2080863 U CN 2080863U CN 90218158 CN90218158 CN 90218158 CN 90218158 U CN90218158 U CN 90218158U CN 2080863 U CN2080863 U CN 2080863U
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- energy
- saving
- distilling device
- saving distilling
- described energy
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- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
Abstract
The utility model belongs to a chemical process appliance for distilling and purifying liquid chemicals, which is characterized in that the utility model is an integral column-shaped energy-saving distillator comprising a heating evaporator (7), a filling purifier (9), a condensate preheater (13), a kettle bottom blow down cooler (18), a distributor valve (2) connected to a raw material inlet (1) and a product outlet (17), wherein, the condensate preheater (13) is designed to be a structure of an external jacket and an internal spiral coil pipe by using heat energy released during phase transfer. The energy-saving distillator has the advantages of convenient installation, easy operation, short process flow, low power consumption, stable production quality, etc.
Description
The utility model belongs to a kind of chemical process equipment that distills the purification liquid chemical.
The distilling apparatus of known technology is to have each parts of distillation still, distillation column, separator, aerial condenser and recipient to connect to be assembled at least.These devices are installed difficulty, and the floor space that has is big, and the height that has is about eight meters, and operation is difficult for grasping.In addition, the weak point of these devices is that still-process all uses air as cooling medium, and cooling effectiveness is low, and the heat energy that is discharged during phase transfer in cooling procedure is not utilized, thereby has increased the input of external heat, and power consumption is big, the production cost height.
The utility model purpose provides a kind of novel energy-conserving distilling apparatus of integral cylindrical.The energy-saving distilling device that the utility model provides, it is characterized in that including the heating fumigators of three spiral coils that penetrate heating wire, insert the charge pipe of a connection distributing valve in the packing layer that in the filler clarifier in this device stage casing, has a sieve plate to hold up, there is the but spiral coil of MEDIA FLOW warp of a cooling lower end that blow down cooler is positioned at the energy-saving distilling device, and this device epimere is that hot device is given in the cooling of external jacket and inside spin coil arrangement and the material inlet place connects a distributing valve and product outlet is combined as integral cylindrical distillation purifying plant.This device is easy for installation, and floor space is little, and technological process is short, and is easy and simple to handle.This device has overcome the shortcoming of known technology distilling apparatus, epimere at device has a condensation to give hot device, the cold liquid charging stock that enters distilling apparatus from the outside condensation of flowing through is given hot device and is carried out heat exchange from heating fumigators and through the liquid juice steam of filler purification utensil, make liquid vapors be condensed into liquid, flow out by product outlet, simultaneously liquid charging stock is heated near boiling point, and drenches in the heating fumigators by the sieve plate of charge pipe through the filler clarifier.The heat energy that this heat exchanging process has been discharged when having made full use of phase transfer has reduced the input of external heat, therefore, has reduced power consumption and production cost.Owing to enter the liquid charging stock of heating fumigators and be evaporated having a narrow range of temperature of liquid and overcome " bumping " and " sudden and violent shake " phenomenon.
It is a four-way changeover valve that this device connects a special four-way distributing valve in import department, carry out the adjusting of the liquid charging stock flow direction and flow by distributing valve, temperature with control low boilers exit, can regulate liquid level in the heating fumigators equally, and keep evaporating liquid to be in fluidized state all the time.Regulating and distributing valve makes production realize serialization with regard to the energy control operation.
Under will be described in more detail the utility model in conjunction with the accompanying drawings.
Fig. 1 is the vertical sectional view of energy-saving distilling device.
The energy-saving distilling device comprises as shown in Figure 1: 1, material inlet, 2, distributing valve, 3, the external jacket layer, 4, internal layer spiral coil, 5, interior chuck layer, 6, charge pipe, 7, heating fumigators, 8, heating element heater, 9, the filler clarifier, 10, sieve plate, 11, packing layer, 12, central tube, 13, condensation gives hot device, 14, low boilers outlet, 15, thermometer boss, 16, outer spiral coil, 17, product outlet, 18, blow down cooler, 19, sewage draining exit, 20, cooling medium inlet, 21, cooling medium outlet.
The course of work of energy-conservation distilling apparatus is described as example to produce reagent of sulfuric acid.
The distributing valve (2) of regulating import (1) connection makes with charge pipe (6) and communicates, the industrial sulphuric acid raw material flows into heating fumigators (7) from import (1) through charge pipe (6), when the sulfuric acid liquid level rises to certain altitude in the heating fumigators (7), cut off and distribute (2) to stop to feed in raw material, and the power supply of the heating element heater (8) in the connection heating fumigators (7), sulfuric acid is heated to boiling in the heating fumigators (7), and the filler clarifier (9) of passing through on the sulfuric acid vapor enters condensation and gives hot device (13). Should regulate and distribute at the same time valve (2) makes raw material sulphuric acid enter the bottom of outer clip jacket layer (3), the entrance that is increased to the spiral coil (4) that is arranged in inner clip jacket layer (5) when the raw material sulphuric acid liquid level spirals and descends, given heat near boiling point by the finished product condensate liquid (reagent of sulfuric acid) in the inner clip jacket layer (5), by charge pipe (6) to filler clarifier (9) with carry out interior backflow washing from the sulfuric acid vapor of heating fumigators (7), acid solution flows in the heating fumigators (7) through the sieve plate (10) of filler clarifier (9). The sulfuric acid vapor that has purified arrives condensation along central tube (12) and gives in the inner clip jacket layer (5) of hot device (13), carries out heat exchange with the cold raw material acid of the spiral coil that is arranged in this chuck layer (4) and is condensed. The reagent of sulfuric acid that condensation is got off reaches overflow height and flows into the finished product cooling spiral coil pipe (16) that is arranged in outer clip jacket layer (3) and further discharged by product outlet (17) after the cooling by the raw material acid of outer clip jacket layer (3) when liquid level raises in inner clip jacket layer (5). The incoagulable gas that is not condensed and low-boiling-point substance are discharged by low boilers outlet (14) and are collected. Point for measuring temperature (15) can be measured the temperature of outlet (14). Utilize distributing valve (2) to regulate that the flow direction of raw material acid and flow are controlled makes the temperature mouthful (14) located and the sulfuric acid liquid level in the heating fumigators (7), and make sulfuric acid remain fluidized state. After blow down cooler (18) cooling of acid sludge by bottom of device, discharge from bottom effluent outlet (19).
The heat energy that discharges owing to taking full advantage of phase transfer makes and produces one ton of reagent of sulfuric acid power consumption is 400～500 kilowatts. The time/ton. And one ton of reagent of sulfuric acid power consumption of employing known technology device production is 1000 kilowatts. The time/ton.
Embodiment:
Integral cylindrical energy-saving distilling device provided by the utility model is to make with quartz glass or hard glass, and its manufacture method is known glass processing technology.
Claims (7)
1, the energy-saving distilling device that is used for liquid chemical, hot device (13), still bottom blowdown cooler (18) are given in the condensation of it is characterized in that heating fumigators is arranged (7), filler clarifier (9), external jacket and inside spin coil arrangement, material inlet (1) locates to connect a distributing valve (2) and product outlet (17) is combined as integral cylindrical energy-saving distilling device.
2, according to the described energy-saving distilling device of claim 1, it is characterized in that three spiral coils are arranged in the heating fumigators (7), every helix tube has a heating wire to pass.
3,, it is characterized in that filler clarifier (9) is to have a charge pipe that connects distributing valve (2) to insert in the filler in the packing layer (11) that holds up of a plane sieve plate (10) according to the described energy-saving distilling device of claim 1.
4, according to the described energy-saving distilling device of claim 1, it is the double-decker that has external jacket (3) and interior chuck (5) to form that hot device (13) is given in the condensation that it is characterized in that external jacket and inside spin coil arrangement, has in external jacket (3) in a spiral coil (16) and the interior chuck (5) spiral coil (4) is arranged.
5,, it is characterized in that there is a spiral coil lower end that still bottom blowdown cooler (18) is positioned at the energy-saving distilling device according to the described energy-saving distilling device of claim 1.
6,, it is characterized in that the distributing valve (2) that material inlet (1) is located is a four-way changeover valve according to the described energy-saving distilling device of claim 1.
7,, it is characterized in that an integral cylindrical energy-saving distilling device is quartz glass or hard glass manufacturing according to the described energy-saving distilling device of claim 1.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 90218158 CN2080863U (en) | 1990-08-13 | 1990-08-13 | Energy-saving distillator |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 90218158 CN2080863U (en) | 1990-08-13 | 1990-08-13 | Energy-saving distillator |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN2080863U true CN2080863U (en) | 1991-07-17 |
Family
ID=4897030
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 90218158 Withdrawn CN2080863U (en) | 1990-08-13 | 1990-08-13 | Energy-saving distillator |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN2080863U (en) |
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102565118A (en) * | 2012-01-18 | 2012-07-11 | 辽宁同辉科技发展有限公司 | Distillation temperature tracker and distillation temperature tracking method thereof |
| CN103243010A (en) * | 2013-06-06 | 2013-08-14 | 遵义西南机械设备有限责任公司 | Distiller condenser for brewing white spirits |
| CN103721435A (en) * | 2013-12-16 | 2014-04-16 | 吴江华诚复合材料科技有限公司 | Distillation equipment |
| CN103992930A (en) * | 2014-05-03 | 2014-08-20 | 张家口奥斯特不锈钢工程有限公司 | Novel efficient energy-saving wine distillation equipment |
| CN109621473A (en) * | 2018-12-27 | 2019-04-16 | 昆山城东化工有限公司 | A kind of scraper-type distillation still |
| CN110461432A (en) * | 2017-03-08 | 2019-11-15 | J·庞斯·塞姆利斯 | liquid distillation unit |
-
1990
- 1990-08-13 CN CN 90218158 patent/CN2080863U/en not_active Withdrawn
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102565118A (en) * | 2012-01-18 | 2012-07-11 | 辽宁同辉科技发展有限公司 | Distillation temperature tracker and distillation temperature tracking method thereof |
| CN103243010A (en) * | 2013-06-06 | 2013-08-14 | 遵义西南机械设备有限责任公司 | Distiller condenser for brewing white spirits |
| CN103721435A (en) * | 2013-12-16 | 2014-04-16 | 吴江华诚复合材料科技有限公司 | Distillation equipment |
| CN103992930A (en) * | 2014-05-03 | 2014-08-20 | 张家口奥斯特不锈钢工程有限公司 | Novel efficient energy-saving wine distillation equipment |
| CN110461432A (en) * | 2017-03-08 | 2019-11-15 | J·庞斯·塞姆利斯 | liquid distillation unit |
| CN110461432B (en) * | 2017-03-08 | 2022-06-07 | J·庞斯·塞姆利斯 | liquid distillation unit |
| CN109621473A (en) * | 2018-12-27 | 2019-04-16 | 昆山城东化工有限公司 | A kind of scraper-type distillation still |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| C15 | Extension of patent right duration from 15 to 20 years for appl. with date before 31.12.1992 and still valid on 11.12.2001 (patent law change 1993) | ||
| RN01 | Renewal of patent term | ||
| C19 | Lapse of patent right due to non-payment of the annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |