CN1847200A - Pollution-less pesticide fertilizer for preventing and controlling blight and its production process - Google Patents
Pollution-less pesticide fertilizer for preventing and controlling blight and its production process Download PDFInfo
- Publication number
- CN1847200A CN1847200A CN 200610076105 CN200610076105A CN1847200A CN 1847200 A CN1847200 A CN 1847200A CN 200610076105 CN200610076105 CN 200610076105 CN 200610076105 A CN200610076105 A CN 200610076105A CN 1847200 A CN1847200 A CN 1847200A
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- Prior art keywords
- fertilizer
- content
- blight
- present
- matrine
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- Granted
Links
- 239000003337 fertilizer Substances 0.000 title claims abstract description 84
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 18
- 239000000575 pesticide Substances 0.000 title abstract description 7
- ZSBXGIUJOOQZMP-UHFFFAOYSA-N Isomatrine Natural products C1CCC2CN3C(=O)CCCC3C3C2N1CCC3 ZSBXGIUJOOQZMP-UHFFFAOYSA-N 0.000 claims abstract description 20
- ZSBXGIUJOOQZMP-JLNYLFASSA-N Matrine Chemical compound C1CC[C@H]2CN3C(=O)CCC[C@@H]3[C@@H]3[C@H]2N1CCC3 ZSBXGIUJOOQZMP-JLNYLFASSA-N 0.000 claims abstract description 20
- 229930014456 matrine Natural products 0.000 claims abstract description 20
- 239000004021 humic acid Substances 0.000 claims abstract description 18
- ABBQHOQBGMUPJH-UHFFFAOYSA-M Sodium salicylate Chemical compound [Na+].OC1=CC=CC=C1C([O-])=O ABBQHOQBGMUPJH-UHFFFAOYSA-M 0.000 claims abstract description 15
- 239000001397 quillaja saponaria molina bark Substances 0.000 claims abstract description 15
- 229930182490 saponin Natural products 0.000 claims abstract description 15
- 150000007949 saponins Chemical class 0.000 claims abstract description 15
- 229960004025 sodium salicylate Drugs 0.000 claims abstract description 15
- KGBXLFKZBHKPEV-UHFFFAOYSA-N boric acid Chemical compound OB(O)O KGBXLFKZBHKPEV-UHFFFAOYSA-N 0.000 claims abstract description 14
- 239000004327 boric acid Substances 0.000 claims abstract description 14
- 241001122767 Theaceae Species 0.000 claims abstract 3
- 239000003814 drug Substances 0.000 claims description 54
- 239000000203 mixture Substances 0.000 claims description 19
- OICGFSUWXCJLCO-UHFFFAOYSA-N 1-ethylsulfonylsulfanylethane Chemical compound CCSS(=O)(=O)CC OICGFSUWXCJLCO-UHFFFAOYSA-N 0.000 claims description 18
- USNIOMZPRQJXNU-UHFFFAOYSA-N [Cu].[Mg].[Zn].[Mn] Chemical compound [Cu].[Mg].[Zn].[Mn] USNIOMZPRQJXNU-UHFFFAOYSA-N 0.000 claims description 17
- 239000000470 constituent Substances 0.000 claims description 16
- 229910052761 rare earth metal Inorganic materials 0.000 claims description 16
- 150000002910 rare earth metals Chemical class 0.000 claims description 15
- BESJRHHIPGWPTC-UHFFFAOYSA-N azane;copper Chemical compound N.[Cu] BESJRHHIPGWPTC-UHFFFAOYSA-N 0.000 claims description 14
- 239000002994 raw material Substances 0.000 claims description 14
- 239000002253 acid Substances 0.000 claims description 12
- BFSVOASYOCHEOV-UHFFFAOYSA-N 2-diethylaminoethanol Chemical compound CCN(CC)CCO BFSVOASYOCHEOV-UHFFFAOYSA-N 0.000 claims description 11
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 claims description 11
- FUZZWVXGSFPDMH-UHFFFAOYSA-M hexanoate Chemical compound CCCCCC([O-])=O FUZZWVXGSFPDMH-UHFFFAOYSA-M 0.000 claims description 11
- 239000011591 potassium Substances 0.000 claims description 11
- 229910052700 potassium Inorganic materials 0.000 claims description 11
- 238000003756 stirring Methods 0.000 claims description 9
- ZOXJGFHDIHLPTG-UHFFFAOYSA-N Boron Chemical compound [B] ZOXJGFHDIHLPTG-UHFFFAOYSA-N 0.000 claims description 8
- 229910052796 boron Inorganic materials 0.000 claims description 8
- 238000000034 method Methods 0.000 claims description 8
- 150000001875 compounds Chemical class 0.000 claims description 6
- 239000000843 powder Substances 0.000 claims description 6
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- 210000003608 fece Anatomy 0.000 claims description 3
- 239000012467 final product Substances 0.000 claims description 3
- 239000010871 livestock manure Substances 0.000 claims description 3
- 229910001220 stainless steel Inorganic materials 0.000 claims description 3
- 239000010935 stainless steel Substances 0.000 claims description 3
- 238000002156 mixing Methods 0.000 claims description 2
- UPPXMONNNGGKMB-UHFFFAOYSA-N 3-O-(alpha-L-rhamnopyranosyl-(1->2)-beta-D-glucopyranosyl-(1->2)-beta-D-glucopyranosyl)spergulagenic acid Natural products OC1C(O)C(O)C(C)OC1OC1C(OC2C(OC(CO)C(O)C2O)OC2C(C3C(C4C(C5(CCC6(CCC(C)(CC6C5=CC4)C(O)=O)C(O)=O)C)(C)CC3)(C)CC2)(C)C)OC(CO)C(O)C1O UPPXMONNNGGKMB-UHFFFAOYSA-N 0.000 claims 1
- AOILXFWEUKCKQQ-UHFFFAOYSA-N Saponin 8 Natural products COC(=O)C1(C)CCC2(CCC3(C)C(=CCC4C5(C)CCC(OC6OC(CO)C(O)C(O)C6OC7OC(CO)C(O)C(O)C7O)C(C)(C)C5CCC34C)C2C1)C(=O)OC8OC(CO)C(O)C(O)C8O AOILXFWEUKCKQQ-UHFFFAOYSA-N 0.000 claims 1
- 230000012010 growth Effects 0.000 abstract description 6
- 229910052802 copper Inorganic materials 0.000 abstract description 2
- 230000000050 nutritive effect Effects 0.000 abstract description 2
- PUKLDDOGISCFCP-JSQCKWNTSA-N 21-Deoxycortisone Chemical compound C1CC2=CC(=O)CC[C@]2(C)[C@@H]2[C@@H]1[C@@H]1CC[C@@](C(=O)C)(O)[C@@]1(C)CC2=O PUKLDDOGISCFCP-JSQCKWNTSA-N 0.000 abstract 1
- QJZYHAIUNVAGQP-UHFFFAOYSA-N 3-nitrobicyclo[2.2.1]hept-5-ene-2,3-dicarboxylic acid Chemical compound C1C2C=CC1C(C(=O)O)C2(C(O)=O)[N+]([O-])=O QJZYHAIUNVAGQP-UHFFFAOYSA-N 0.000 abstract 1
- JDLKFOPOAOFWQN-VIFPVBQESA-N Allicin Natural products C=CCS[S@](=O)CC=C JDLKFOPOAOFWQN-VIFPVBQESA-N 0.000 abstract 1
- 208000035240 Disease Resistance Diseases 0.000 abstract 1
- FCYKAQOGGFGCMD-UHFFFAOYSA-N Fulvic acid Natural products O1C2=CC(O)=C(O)C(C(O)=O)=C2C(=O)C2=C1CC(C)(O)OC2 FCYKAQOGGFGCMD-UHFFFAOYSA-N 0.000 abstract 1
- JDLKFOPOAOFWQN-UHFFFAOYSA-N allicin Chemical compound C=CCSS(=O)CC=C JDLKFOPOAOFWQN-UHFFFAOYSA-N 0.000 abstract 1
- 235000010081 allicin Nutrition 0.000 abstract 1
- 150000001413 amino acids Chemical class 0.000 abstract 1
- 150000003863 ammonium salts Chemical class 0.000 abstract 1
- 238000013329 compounding Methods 0.000 abstract 1
- 229940095100 fulvic acid Drugs 0.000 abstract 1
- 239000002509 fulvic acid Substances 0.000 abstract 1
- 229910052749 magnesium Inorganic materials 0.000 abstract 1
- 229910052748 manganese Inorganic materials 0.000 abstract 1
- 229910052725 zinc Inorganic materials 0.000 abstract 1
- 201000010099 disease Diseases 0.000 description 28
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 28
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- 241000082085 Verticillium <Phyllachorales> Species 0.000 description 9
- 239000007921 spray Substances 0.000 description 9
- 238000012360 testing method Methods 0.000 description 9
- 244000061458 Solanum melongena Species 0.000 description 7
- 235000002597 Solanum melongena Nutrition 0.000 description 7
- 238000011835 investigation Methods 0.000 description 7
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- 239000003905 agrochemical Substances 0.000 description 6
- 239000007788 liquid Substances 0.000 description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 6
- 244000269722 Thea sinensis Species 0.000 description 5
- TWFZGCMQGLPBSX-UHFFFAOYSA-N carbendazim Chemical compound C1=CC=C2NC(NC(=O)OC)=NC2=C1 TWFZGCMQGLPBSX-UHFFFAOYSA-N 0.000 description 5
- 235000019198 oils Nutrition 0.000 description 5
- 235000013311 vegetables Nutrition 0.000 description 5
- 208000024891 symptom Diseases 0.000 description 4
- 240000008067 Cucumis sativus Species 0.000 description 3
- 235000010799 Cucumis sativus var sativus Nutrition 0.000 description 3
- 241000918585 Pythium aphanidermatum Species 0.000 description 3
- 241000607479 Yersinia pestis Species 0.000 description 3
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- UHPMCKVQTMMPCG-UHFFFAOYSA-N 5,8-dihydroxy-2-methoxy-6-methyl-7-(2-oxopropyl)naphthalene-1,4-dione Chemical compound CC1=C(CC(C)=O)C(O)=C2C(=O)C(OC)=CC(=O)C2=C1O UHPMCKVQTMMPCG-UHFFFAOYSA-N 0.000 description 2
- FRXSZNDVFUDTIR-UHFFFAOYSA-N 6-methoxy-1,2,3,4-tetrahydroquinoline Chemical compound N1CCCC2=CC(OC)=CC=C21 FRXSZNDVFUDTIR-UHFFFAOYSA-N 0.000 description 2
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- 241000193738 Bacillus anthracis Species 0.000 description 2
- 241000894006 Bacteria Species 0.000 description 2
- 241000219112 Cucumis Species 0.000 description 2
- 235000015510 Cucumis melo subsp melo Nutrition 0.000 description 2
- 241000223218 Fusarium Species 0.000 description 2
- 241000238631 Hexapoda Species 0.000 description 2
- 206010028980 Neoplasm Diseases 0.000 description 2
- FJJCIZWZNKZHII-UHFFFAOYSA-N [4,6-bis(cyanoamino)-1,3,5-triazin-2-yl]cyanamide Chemical compound N#CNC1=NC(NC#N)=NC(NC#N)=N1 FJJCIZWZNKZHII-UHFFFAOYSA-N 0.000 description 2
- 230000000844 anti-bacterial effect Effects 0.000 description 2
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- 238000011161 development Methods 0.000 description 2
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- ZYECOAILUNWEAL-NUDFZHEQSA-N (4z)-4-[[2-methoxy-5-(phenylcarbamoyl)phenyl]hydrazinylidene]-n-(3-nitrophenyl)-3-oxonaphthalene-2-carboxamide Chemical compound COC1=CC=C(C(=O)NC=2C=CC=CC=2)C=C1N\N=C(C1=CC=CC=C1C=1)/C(=O)C=1C(=O)NC1=CC=CC([N+]([O-])=O)=C1 ZYECOAILUNWEAL-NUDFZHEQSA-N 0.000 description 1
- 240000002234 Allium sativum Species 0.000 description 1
- 235000016068 Berberis vulgaris Nutrition 0.000 description 1
- 241000335053 Beta vulgaris Species 0.000 description 1
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 1
- 241000221785 Erysiphales Species 0.000 description 1
- IWDQPCIQCXRBQP-UHFFFAOYSA-M Fenaminosulf Chemical compound [Na+].CN(C)C1=CC=C(N=NS([O-])(=O)=O)C=C1 IWDQPCIQCXRBQP-UHFFFAOYSA-M 0.000 description 1
- 244000068988 Glycine max Species 0.000 description 1
- 235000010469 Glycine max Nutrition 0.000 description 1
- 235000007688 Lycopersicon esculentum Nutrition 0.000 description 1
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- 240000003768 Solanum lycopersicum Species 0.000 description 1
- 244000061456 Solanum tuberosum Species 0.000 description 1
- 235000002595 Solanum tuberosum Nutrition 0.000 description 1
- BWPGKXYWPBQBPV-MWQJAWBESA-N Theasaponin Chemical compound O([C@H]1[C@H](O)[C@H](O[C@H]([C@@H]1O[C@H]1[C@@H]([C@@H](O)[C@@H](O)CO1)O[C@H]1[C@@H]([C@@H](O)[C@H](O)CO1)O)O[C@H]1CC[C@]2(C)[C@H]3CC=C4[C@@]([C@@]3(CC[C@H]2[C@@]1(CO)C)C)(C)C[C@@H](O)[C@@]1(CO)[C@@H](OC(C)=O)[C@@H](C(C[C@H]14)(C)C)OC(=O)C(\C)=C/C)C(O)=O)[C@@H]1O[C@H](CO)[C@H](O)[C@H](O)[C@H]1O BWPGKXYWPBQBPV-MWQJAWBESA-N 0.000 description 1
- BWPGKXYWPBQBPV-ZOADXXHESA-N Theasaponin Natural products O=C(O[C@@H]1[C@@H](OC(=O)C)[C@]2(CO)[C@@H](O)C[C@@]3(C)[C@@]4(C)[C@@H]([C@]5(C)[C@H]([C@@](CO)(C)[C@@H](O[C@@H]6[C@@H](O[C@@H]7[C@H](O[C@@H]8[C@@H](O)[C@H](O)[C@H](O)CO8)[C@H](O)[C@@H](O)CO7)[C@@H](O[C@H]7[C@H](O)[C@@H](O)[C@@H](O)[C@H](CO)O7)[C@H](O)[C@@H](C(=O)O)O6)CC5)CC4)CC=C3[C@@H]2CC1(C)C)/C(=C/C)/C BWPGKXYWPBQBPV-ZOADXXHESA-N 0.000 description 1
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- XOCUXOWLYLLJLV-UHFFFAOYSA-N [O].[S] Chemical group [O].[S] XOCUXOWLYLLJLV-UHFFFAOYSA-N 0.000 description 1
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- 238000004458 analytical method Methods 0.000 description 1
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- RRTCFFFUTAGOSG-UHFFFAOYSA-N benzene;phenol Chemical class C1=CC=CC=C1.OC1=CC=CC=C1 RRTCFFFUTAGOSG-UHFFFAOYSA-N 0.000 description 1
- CUBCNYWQJHBXIY-UHFFFAOYSA-N benzoic acid;2-hydroxybenzoic acid Chemical compound OC(=O)C1=CC=CC=C1.OC(=O)C1=CC=CC=C1O CUBCNYWQJHBXIY-UHFFFAOYSA-N 0.000 description 1
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- CRQQGFGUEAVUIL-UHFFFAOYSA-N chlorothalonil Chemical compound ClC1=C(Cl)C(C#N)=C(Cl)C(C#N)=C1Cl CRQQGFGUEAVUIL-UHFFFAOYSA-N 0.000 description 1
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Landscapes
- Fertilizers (AREA)
Abstract
The present invention is pollution-less pesticide fertilizer for preventing and controlling blight and its production process. The pesticide fertilizer is produced through treating allicin B with humic acid containing fulvic acid for synergizing and detoxicating; re-compounding with matrine, complex Cu, Zn, Mn, Mg and ammonium salt of amino acid, tea saponin, boric acid, sodium salicylate, RE and other matters; and adding synergist. The product of the present invention can provide crop with nutritive matter, promote crop growth, raise disease resistance of crop and raise crop yield.
Description
Technical field
The present invention relates to the nuisance-free medicinal fertilizer of diseases such as a kind of effective control farm crop are withered, verticillium, root rot and the production method of compound fertilizer and medicine fertilizer thereof.
Background technology
In recent years, the disease of the blight of farm crop, verticillium, root rot is very serious, and these disease initial stage performances are not obvious, very easily ignored by people, when being in a bad way by the time the control late, these diseases by the peasant be referred to as the meaning " cancer of crops disease " cause very big loss to agriculture production.China is large agricultural country, agriculture production need be used a large amount of fertilizer and pesticides, the fertilizer and pesticide kind of Shi Yonging is aging for a long time, and agronomy is loaded down with trivial details, and disease is failed to accomplish to rely mainly on prevention, cause agriculture production cost height, benefit low, in order to increase output, force agriculture production to use the fertilizer and pesticide amount and rise year by year, consequent environment, water resources and the farm crop that have been serious pollution itself, this has not only destroyed the eubiosis, also serious harm people's health and safety.The resistance of farm crop harmful organism germ and insect is serious problems in the crop pest management, it brings very big obstacle for the control of various crop disease and pest, therefore, become the emphasis of many in recent years countries research for the resistance problem that solves the farm crop harmful organism.
Summary of the invention
The purpose of this invention is to provide a kind of efficient, safety, the multifunctional novel high-tech medicine fertilizer that can effectively prevent and treat diseases such as farm crop are withered, verticillium, root rot, this medicine fertilizer is a kind of green, ecology, environmental protection, safety, high-quality and efficient agricultural of can be used for, and adapts to the agricultural modernization development and is difficult for making the germ insect to produce the Multifunction high-tech Agricultural products of resistance.
Another object of the present invention provides a kind of compound fertilizer that contains the nuisance-free medicinal fertilizer of preventing and treating blight.
A further object of the present invention provides a kind of method of producing the nuisance-free medicinal fertilizer of control blight.
For achieving the above object, the present invention takes following technical scheme:
A kind of nuisance-free medicinal fertilizer of preventing and treating blight, this medicine fertilizer is to be made by following weight percentages:
Matrine (content of matrine 〉=90%) 1～2%
Kilnitamin copper zinc-manganese magnesium (effective constituent 〉=90%) 4～8%
Garlicin (ethylicin 〉=80%) 20～32%
Humic acids (comprising xanthohumic acid, HA+BFA 〉=60%) 23～33%
The ammonia copper (effective constituent 40%) 22～32% that mix more
Boric acid (boron content 16～18%) 0.5～1.5%
Sodium salicylate (content 〉=50%) 1～3%
Tea saponin (content 〉=80%) 6～10%
Rare earth (oxide content 〉=38%) 0.3～0.5%
Diethylamino ethanol caproate or potassium para-nitrophenate 0.05～0.15%
In medicine fertilizer of the present invention, the matrine that is adopted can extract matrine after pulverizing from kuh-seng, Herba Sophorae alopecuroidis; Also can be used as biological pesticide-matrine and directly buy from the market, as, the matrine that Inner Mongol Linhe City matrine head factory is produced, wherein content of matrine 〉=90%.
In medicine fertilizer of the present invention, the kilnitamin copper zinc-manganese magnesium that is adopted claims that also the villa garden is happy, farmer bacterium star.Can use the kilnitamin copper zinc-manganese magnesium of effective constituent 〉=90% of chemical plant, Dongguang, Harbin City production.
In medicine fertilizer of the present invention, the garlicin that is adopted contains 〉=80% ethylicin, pure ethylicin is colourless or little yellow oily liquid, the garlic stink is arranged, the bactericidal mechanism of ethylicin is to contain in two sulphur oxygen groups in its molecular structure and the thalline molecule-substance reaction of SH base, thereby suppresses the thalline eubolism, and ethylicin has hormesis to plant-growth, seed sprouting through treated with same is fast, the growth of seedling stalwartness.The garlicin that can use Henan the earth farmingization company limited to produce, wherein ethylicin 〉=80%.
In medicine fertilizer of the present invention, the humic acids that is adopted comprises xanthohumic acid, its content requirement HA+BFA 〉=60%.Humic acids is the natural organic substance of element of the first species's complexity, and it is present in soil, coal, lake, river and the ocean.Xanthohumic acid is a kind of humic acids, belongs to slightly acidic, and its functional group is not have the bonded free state, and therefore compatible agricultural chemicals scope is wide, and the complex body stability of formation is high, the better effects if of sustained-release synergistic.Xanthohumic acid has higher hydrophilic radical content, can bring into play good distribution, emulsifying effect, and the activity that improves agricultural chemicals is also had certain influence.The composite use of agricultural chemicals and xanthohumic acid can reduce pesticide dosage 1/3～1/2, prolongs drug effect 3～7 days.The humic acids that can use the logical Microbial Technics Ltd in Shanghai to produce, comprising xanthohumic acid, its content HA+BFA 〉=60%.
In medicine fertilizer of the present invention, the how mixed ammonia copper that is adopted is derosal and the composite mixture of kilnitamin copper, and product is 40% wettable powder, 15% suspension agent, trade(brand)name have withered must restrain, the disease of withering health, Gua Wang, golden gill are gone out prestige.The effective constituent that can use the Beijing YanHuaYongLe pesticide Co., Ltd to produce is 40% how mixed ammonia copper.
In medicine fertilizer of the present invention, the boric acid that is adopted is the product of boron content 16～18%.
In medicine fertilizer of the present invention, the sodium salicylate that is adopted is salicylic sodium salt, and Whitfield's ointment is the crude benzene phenols plant-growth regulator that a kind of plant materials contains.Can use the sodium salicylate of content 〉=50% of the logical Microbial Technics Ltd in Shanghai production.
In medicine fertilizer of the present invention, the tea saponin that is adopted claims theasaponin or tea saponin again, can extract from the product of its seed after oil expression.Tea saponin is a kind of non-ionic type natural surface active agent, the main emulsifying property of using it on agricultural chemicals, the surface tension of reduction preparation.Can use the tea saponin of content 〉=80% of Ningbo associating Bioisystech Co., Ltd production.
In medicine fertilizer of the present invention, the rare earth that is adopted is agricultural rare-earth, can use the rare earth of oxide content 〉=38% of Chinese agricultural rare-earth center production.
In medicine fertilizer of the present invention, diethylamino ethanol caproate that is adopted or potassium para-nitrophenate can use applied chemistry system of Henan agricultural university, diethylamino ethanol caproate and potassium para-nitrophenate that Zheng Shi chemical industry company limited produces as synergistic agent.
The most preferred prescription of the nuisance-free medicinal fertilizer of control blight of the present invention is that this medicine fertilizer is to be made by following weight percentages:
Matrine (content of matrine 〉=90%) 1.5%
Kilnitamin copper zinc-manganese magnesium (effective constituent 〉=90%) 6%
Garlicin (ethylicin 〉=80%) 26%
Humic acids (comprising xanthohumic acid, HA+BFA 〉=60%) 28%
The ammonia copper (effective constituent 40%) 27% that mix more
Boric acid (boron content 16～18%) 1%
Sodium salicylate (content 〉=50%) 2%
Tea saponin (content 〉=80%) 8%
Rare earth (oxide content 〉=38%) 0.4%
Diethylamino ethanol caproate or potassium para-nitrophenate 0.1%
A kind of method of producing the nuisance-free medicinal fertilizer of control blight, this method comprises the steps:
(1), gets the raw materials ready by above-mentioned raw materials by weight percent.
(2), with the kilnitamin copper zinc-manganese magnesium dry pulvis that is that dusts, stand-by.
(3), humic acids is joined in the enamel reaction still, start stirrer, add garlicin, stir 20min, add the tea saponin powder, continue to stir 10min, add synergistic agent, matrine, kilnitamin copper zinc-manganese magnesium pulvis, rare earth, boric acid, sodium salicylate more successively, mix the agent of ammonia copper powder more, continue to stir 30min.
(4), mixture is sent in the stainless steel double worm mixer with transfer roller, mix 3-6min, get final product discharging, put into sealed vessel, send into automatic packing machine, carry out packing with transfer roller, the packaging products in boxes warehouse-in is stored in shady and cool dry notice wind environment, promptly makes the concentrated type pulvis.
Make the compound fertilizer that contains the nuisance-free medicinal fertilizer of preventing and treating blight, also comprise the steps:
(5), with above-mentioned concentrated type pulvis, allocate into by 3%～10% amount in the raw material of mixed organic manure or organic-inorganic compound fertilizer, after all raw material thorough mixing are even, production method is carried out granulation, oven dry, cooling, screening, packing routinely, promptly makes the ecological environment-friendly type medicine fertilizer that can prevent and treat diseases such as withered, verticillium, root rot.
The crop scope that product of the present invention is suitable for:
Cotton, vegetables, fruit tree, wheat class, paddy rice, beet, rape, peanut, potato class, soybean, forestry etc.
The main effect of product of the present invention:
Use the nuisance-free medicinal fertilizer of control blight of the present invention and can supply with the crop alimentary material, promote the healthy and strong growth of crop, improve the crop disease-resistant ability, sterilization simultaneously and adjusting and treatment are because of lacking the physiological disease that nutritive element causes.Can effectively prevent and treat the disease such as blight, root rot of cotton, vegetables, crop such as melon, diseases such as the bacterial wilt of plant, damping-off, samping off, leaf blight, leaf spot, gray mold, anthrax, Powdery Mildew are also had certain effect.
Advantage of the present invention is:
1, the nuisance-free medicinal fertilizer of control blight of the present invention is that material or the product of selecting to have multinomial activeconstituents is raw material, with the plurality of active ingredients scientific compatibility, makes its mutual synergy, the expanded functionality scope.
Product of the present invention can be widely used in cash crop such as cotton, vegetables, melon, fruit tree, grain and oil, existing good fertilizer efficiency has the effect of diseases such as control blight, root rot, bacterial wilt, damping-off, samping off again, has solved the difficult problem of preventing and treating of " withered, verticillium, root rot " that be regarded as the farm crop cancer.
2, product drug effect instant effect of the present invention, effective, toxicity is low, and Environmental compatibility is good, and use cost is low.
1. use product of the present invention and take effect after 3 days, the may command disease was stretched in 7～10 days, generally sprayed and can remove disease 2-3 time, and average preventive effect can reach more than 90%.
2. product of the present invention is made carrier with ethylicin with humic acids, makes ethylicin synergy more than 30%, has reduced the toxicity and the corrodibility of ethylicin, again with other components compatibility of the present invention, and mutually synergy more than 50%, and product easily degrades, and noresidue is preserved the ecological environment.
3. product of the present invention can provide crop nutrition content, regulates plant growth, improves crop disease prevention, resistance against diseases, promotes crop to improve output, improves quality, reduces the agriculture chemical amount of putting forward more than 30%, thereby has reduced agriculture production cost.
3, product of the present invention has had strong inhibitory effects to the pathogenic bacteria of various crop, is the multiple spot effect to germ, and germ is difficult for producing resistance.
4, product of the present invention can mix use with fertilizer, organic-inorganic compound fertilizer, also can allocate in fertilizer or the organic-inorganic raw material of mix-compound fertilizer by 3%～10% amount, produces the no-pollution multifunctional new-type fertilizer with agricultural chemicals effect.
The using method of product of the present invention is:
1, seed soaking:
1. prevent that cotton is withered, the verticillium evil: medicine is fertile in 400 times of water dilutions, at 50～60 ℃ of medical fertilizer liquids immersion cottonseed 30min down.
2. prevent disease in cotton seedling stage:, pull the vernalization sowing out with 1: 2000～3000 times medical fertilizer liquid seed soaking 16～24h.
3. prevent diseases such as other crops are withered, Huang withers: soak seed according to a conventional method with 2000～4000 times of liquid.
2, the their early stage of diseases such as withered, verticillium, damping-off, bacterial wilt, root rot takes place when cotton, vegetables, peanut and other crops, with 600～1500 times of the fertile dilute with waters of invention medicine, spraying and irritate root, every 6-10 days once, 2-3 time continuously, can eliminate disease, make crop recover healthy and strong growth.
When 3, making pre-disease prevention and use, can mix uses with organic-inorganic compound fertilizer or fertilizer, every mu restrains with invention medicine fertilizer 100～200 and fertilizer mixes and does base manure (base fertilizer) usefulness, not only can increase fertilizer efficiency but also can effectively prevent and suppress crop pest.
Embodiment
Produce the nuisance-free medicinal fertilizer of control blight, get the raw materials ready by following raw materials by weight percent earlier:
Matrine 1.5%
Kilnitamin copper zinc-manganese magnesium (effective constituent 〉=90%) 6%
Garlicin (ethylicin 〉=80%) 26%
Humic acids (comprising xanthohumic acid, HA+BFA 〉=60%) 28%
The ammonia copper (effective constituent 40%) 27% that mix more
Boric acid (boron content 16～18%) 1%
Sodium salicylate (content 〉=50%) 2%
Tea saponin (content 〉=80%) 8%
Rare earth (oxide content 〉=38%) 0.4%
Diethylamino ethanol caproate or potassium para-nitrophenate 0.1%
It is dry for pulvis, stand-by kilnitamin copper zinc-manganese magnesium to be dusted again.
Then humic acids is joined in the enamel reaction still, start stirrer, add garlicin, stir 20min, add the tea saponin powder, continue to stir 10min, add synergistic agent, matrine, kilnitamin copper zinc-manganese magnesium pulvis, rare earth, boric acid, sodium salicylate more successively, mix the agent of ammonia copper powder more, continue to stir 30min.
At last mixture is sent in the stainless steel double worm mixer with transfer roller, mixed 3-6min, get final product discharging, make the concentrated type pulvis.
Get the raw materials ready by following several different raw materials by weight percent, and produce the nuisance-free medicinal fertilizer of control blight according to the method described above, can reach effect of the present invention equally through experiment.
Prescription 1:
Matrine 1.8%
Kilnitamin copper zinc-manganese magnesium (effective constituent 〉=90%) 4.7%
Garlicin (ethylicin 〉=80%) 21%
Humic acids (comprising xanthohumic acid, HA+BFA 〉=60%) 31%
The ammonia copper (effective constituent 40%) 31% that mix more
Boric acid (boron content 16～18%) 1%
Sodium salicylate (content 〉=50%) 2%
Tea saponin (content 〉=80%) 7%
Rare earth (oxide content 〉=38%) 0.45%
Diethylamino ethanol caproate or potassium para-nitrophenate 0.05%
Prescription 2:
Matrine 1%
Kilnitamin copper zinc-manganese magnesium (effective constituent 〉=90%) 7.5%
Garlicin (ethylicin 〉=80%) 32%
Humic acids (comprising xanthohumic acid, HA+BFA 〉=60%) 24.5%
The ammonia copper (effective constituent 40%) 22% that mix more
Boric acid (boron content 16～18%) 0.7%
Sodium salicylate (content 〉=50%) 2.3%
Tea saponin (content 〉=80%) 9.5%
Rare earth (oxide content 〉=38%) 0.4%
Diethylamino ethanol caproate or potassium para-nitrophenate 0.1%
Prescription 3:
Matrine 2%
Kilnitamin copper zinc-manganese magnesium (effective constituent 〉=90%) 5.5%
Garlicin (ethylicin 〉=80%) 27.5%
Humic acids (comprising xanthohumic acid, HA+BFA 〉=60%) 33%
The ammonia copper (effective constituent 40%) 23% that mix more
Boric acid (boron content 16～18%) 1.5%
Sodium salicylate (content 〉=50%) 1%
Tea saponin (content 〉=80%) 6%
Rare earth (oxide content 〉=38%) 0.35%
Diethylamino ethanol caproate or potassium para-nitrophenate 0.15%
Embodiment 1
Medicine fertilizer of the present invention cotton experiment field piece to long-term morbidity under different concns carries out and other agricultural chemicals crop simultaneous test, and test drug is divided into 6 groups, and every group of experimental concentration is respectively:
1,80% ethylicin missible oil is 3000 times;
2, fertile 500 times of oil slick of this medicine;
3, this medicine is fertile 1000 times;
4, this medicine is fertile 2000 times;
5,50% carbendazol wettable powder is 1000 times;
6, clear water.
Handle for every group and divide I, II, III, IV4 repetition, random alignment, the cultivation condition of all sub-districts is all consistent in the test, and the sub-district area is 70M
2
Spraying time and number of times:
Spraying time for the first time: be two leaves spray medicines when launching seedling stage.
Spraying time for the second time: the preceding spraying of buddingging.
Investigation method:
1, in cotton flowering and boll-setting period investigation: each handles the disease index that 100 strains are investigated in each sub-district.
2, disease index grade scale:
0 grade: healthy tree
1 utmost point: the diseased plant blade has the leaf color of performance below 25% to deepen, shrinkage, and it is yellow netted that vein is, and the blade that has is classical symptoms such as yellow or red-violet colour.
2 grades: the diseased plant blade has 25-50% performance symptom, and plant type is obviously downgraded.
3 grades: the diseased plant blade has 50-90% performance symptom, and plant type is obviously downgraded.
4 grades: the diseased plant blade almost all shows symptom, even dried-up coming off, and acute wilting death appears in the withered or whole strain of stem branch.
3, drug effect is calculated:
4, poisoning investigation and grade scale:
After spraying 1,3,7 day and investigate the influence of medicament harvesting time, the poisoning grade scale to cotton:
-: no poisoning.
+: slight poisoning.
++: obviously poisoning, can restore, can not cause the cotton underproduction.
The poisoning of +++: height influences the cotton normal growth, causes to a certain degree output and mass loss.
++ ++: serious poisoning, plant growth is obstructed, and output and mass loss are serious.
The time efficacy survey data of different chemical control cotton wilts see Table 1.
Table 1:
| Chemicals treatment | Preventive effect between repetition (%) | Average preventive effect (%) | The poisoning situation | |||
| I | II | III | IV | |||
| 4000 times of 1000 times of ethylicins of the fertile 1000 times of fertile 5000 times of derosal of medicine of the present invention of the fertile 2000 times of medicines of the present invention of medicine of the present invention | 70.6 89.7 93.0 40.9 60.0 | 69.0 86.0 91.0 43.0 54.0 | 73.0 86.8 92.4 42.1 53.0 | 71.1 81.4 95.0 39.0 59.0 | 70.0 86.0 92.0 42.0 56.5 | - - + - - |
This test shows that by table 1 result the preventive effect of the anti-cotton wilt of the fertile 5000 times of field sprays of medicine of the present invention is the highest, reaches 92%, but blade is had slight poisoning, and this concentration not too is fit to do the cotton field spraying; Use 1000 and 2000 times preventive effect to be respectively 86% and 70.0%, and do not have poisoning.The preventive effect of 80% ethylicin missible oil, 50% carbendazol wettable powder is respectively 56.5%, 42.0%, all is starkly lower than the preventive effect of invention medicine fertilizer.
Statistical study: the preventive effect of 5 chemicals treatment is carried out variance analysis and newly answer the range assay seeing Table 2.
Table 2: the preventive effect significance test of difference table of different chemical control cotton wilts
| Chemicals treatment | Average preventive effect arcsine transformation value | Significance test of difference | |
| 0.05 | 0.01 | ||
| The fertile 2000 times of 82% ethylicin EC4000 50% derosal WP1000 of fertile 1000 times of these medicines of fertile 500 times of these medicines of this medicine | 74.3 69.0 57.0 49.0 41.0 | a a a ab b | A A A A AB |
Table 2 shows that the preventive effect difference of fertile 1000 times and the 2000 times liquid of medicine of the present invention is not remarkable, but reaches 0.05 level with two single agent and the preventive effect difference that contrasts many bacterium number.
Embodiment 2
Medicine fertilizer of the present invention is tested the prevention effect of booth eggplant blight and the influence of eggplant output:
Medicine fertilizer of the present invention is to the prevention effect of booth eggplant blight:
With the fertile 1000 times of diluents spraying of medicine of the present invention, the spray clear water is contrast
| Handle | Investigation strain number (strain) | Morbidity strain number (strain) | Sickness rate (%) |
| Medicine fertilizer of the present invention | 76 | 40 | 52.6 |
| Contrast | 74 | 64 | 86.5 |
Three eggplant ground are experimental field arranged, and blight weighs about 50%, and what have is dead, and after spraying goods of the present invention 2 times (per 7 days 1 time), the state of an illness stops development, and the anosis feelings of new blade that grow new root, bear can be yielded positive results again.
Medicine fertilizer of the present invention is to the influence of booth eggplant output
| Handle | Plant height (cm) | Stem thick (cm) | The number of blade (sheet) | Average yield per mu | Comparison is shone | ||||
| 0 day | 14 days | 0 day | 14 days | 0 day | 14 days | Kg/ mu | Mu volume increase (kg) | ％ | |
| Medicine fertilizer of the present invention | 24.2 | 45 | 0.5 | 0.9 | 9 | 15 | 1320 | 220 | 20 |
| Contrast | 25 | 40 | 0.5 | 0.6 | 9 | 13 | 1100 | 0 | 0 |
Test-results shows, uses medicine fertilizer of the present invention and can be greatly improved to booth eggplant output.
Embodiment 3
Medicine fertilizer of the present invention is at the effect of fruit tree:
800 times of sprayings of this product dilute with water, the spray clear water is contrast
Interpretation of result: test-results shows, annual field sprays 3 times, the fruit tree that sprays medicine fertilizer can obviously promote fruit growth, average fruit comparison is according to weightening finish 16.8g, stained area increases by 17.25%, one-level fruit rate improves 10.5%, and soluble solid increases by 0.53%, can find out also that simultaneously fruit tree crown diameter and dried girth obviously increase.
In the field range estimation, the fruit tree leaves look dark green of using medicine fertilizer of the present invention, and feel is thicker, and fruit ring spot, anthrax contrast are light, and is remarkable to preventing and treating the disease effect, and have tangible increase output to improve the effect of quality.
Embodiment 4
The effect of the fertile control of medicine of the present invention eggplant verticillium wilt
The place: oasis, Fengtai experimental field
Oasis, Fengtai test-results experimental field
| Handle 486m 2 | Investigation strain number (strain) | The verticillium their early stage | Stimulation ratio (%) | ||
| Diseased plant rate (%) | Disease refers to | Prevention effect (%) | |||
| The nuisance-free medicinal fertilizer of control blight | 100 | 2.13 | 2.13 | 87 | 26.83 |
| Thiophanate_methyl (by the operation instruction dispenser) | 100 | 8.07 | 8.07 | 51 | 15.21 |
| CK | 100 | 21.2 | 16.4 | ||
By different concns and three revision tests, spray with the medical fertilizer liquid of the present invention of 700 times of weaker concns, irritate root simultaneously, every strain 300ml, average preventive effect is greater than 80%.
Embodiment 5
Medicine fertilizer of the present invention is to the prevention effect and the effect of increasing production of early blight of tomato
The place: oasis, Fengtai experimental field
The nuisance-free medicinal fertilizer of control blight suppresses the effect research table to early blight of tomato
| Handle 420m 2 | Investigation strain number (strain) | Morbidity strain number (strain) | Sickness rate (%) | Relative control effect (%) | Stimulation ratio (%) |
| The nuisance-free medicinal fertilizer of control blight | 100 | 0 | 0 | 100 | 36.73 |
| M-tetrachlorophthalodinitrile | 100 | 1 | 1 | 80 | 18.63 |
| CK | 100 | 5 | 5 |
Medicine fertilizer of the present invention with 700 times of weaker concns carries out foliage-spray to tomato, irritates root 1 time, every strain 400ml, and its antibacterial prevention effect increases production 36.73% up to 98%.
Embodiment 6
Medicine fertilizer of the present invention is to the prevention effect and the effect of increasing production of cucumber fusarium axysporum
The place: oasis, Fengtai experimental field
Cucumber fusarium axysporum is prevented and treated test-results, test area 666m
2, three are repeated mean number, and 300ml is irritated in every strain.
| Handle 666m 2 | Investigation strain number () | 7 days diseased plant numbers (strain) behind the medicine | Sickness rate (%) | Blight inhibiting rate (%) | Irritate several regeneration situations of 5 days diseased plants behind the root once more | Stimulation ratio (%) |
| The nuisance-free medicinal fertilizer of control blight is irritated root 300ml/ strain for 1: 800 times | 200 | 1 | 0.5 | ＞80 | New root increases obviously | 58.33 |
| Fenaminosulf | 200 | 34 | 17 | 30.6 | New root is few | 15.42 |
| CK | 200 | 49 | 24.5 | No new root |
Just spray at cucumber premorbid or morbidity with the medicine fertilizer of the present invention of 800 times of weaker concns, irritate root simultaneously, every strain 300-600 milliliter, 3-5 days 1 time, general 2-3 time is that the may command disease is stretched, average preventive effect finds that greater than 80% product of the present invention has preventive and therapeutic effect to the multiple diseases of farm crop in test is on probation.
The nuisance-free medicinal fertilizer of control blight of the present invention is according to the check of safe edible agricultural-food vegetable products quality standard, and all projects are all qualified.
Claims (4)
1, a kind of nuisance-free medicinal fertilizer of preventing and treating blight is characterized in that: this medicine fertilizer is to be made by following weight percentages:
Matrine 1～2%
Kilnitamin copper zinc-manganese magnesium 4～8%
Garlicin 20～32%
Humic acids 23～33%
The ammonia copper 22～32% that mix more
Boric acid 0.5～1.5%
Sodium salicylate 1～3%
Tea saponin 6～10%
Rare earth 0.3～0.5%
Diethylamino ethanol caproate or potassium para-nitrophenate 0.05～0.15%
Wherein, content of matrine 〉=90% in the above-mentioned prescription; Effective constituent 〉=90% of kilnitamin copper zinc-manganese magnesium; Ethylicin content 〉=80% in the garlicin; Humic acids comprises xanthohumic acid, and HA+BFA 〉=60%; The effective constituents of mixing ammonia copper are 40% more; Boron content is 16～18% in the boric acid; The content of sodium salicylate 〉=50%; The content of tea saponin 〉=80%; Oxide content in the rare earth 〉=38%.
2, the nuisance-free medicinal fertilizer of control blight according to claim 1 is characterized in that: this medicine fertilizer is to be made by following weight percentages:
Matrine 1.5%
Kilnitamin copper zinc-manganese magnesium 6%
Garlicin 26%
Humic acids 28%
The ammonia copper 27% that mix more
Boric acid 1%
Sodium salicylate 2%
Tea saponin 8%
Rare earth 0.4%
Diethylamino ethanol caproate or potassium para-nitrophenate 0.1%
3, the method for the nuisance-free medicinal fertilizer of the described control blight of a kind of production claim 1, it is characterized in that: this method comprises the steps:
(1), gets the raw materials ready by above-mentioned raw materials by weight percent;
(2), with the kilnitamin copper zinc-manganese magnesium dry pulvis that is that dusts, stand-by;
(3), humic acids is joined in the enamel reaction still, start stirrer, add garlicin, stir 20min, add the tea saponin powder, continue to stir 10min, add diethylamino ethanol caproate or potassium para-nitrophenate, matrine, kilnitamin copper zinc-manganese magnesium pulvis, rare earth, boric acid, sodium salicylate more successively, mix the agent of ammonia copper powder more, continue to stir 30min;
(4), mixture is sent in the stainless steel double worm mixer with transfer roller, mix 3-6min, get final product discharging, make the concentrated type pulvis.
4, a kind of compound fertilizer is characterized in that: this compound fertilizer is made for a mixed organic manure raw material or an organic inorganic composite mixed fertilizer raw material, and contains the nuisance-free medicinal fertilizer of the described control blight of claim 1 of 3～10 weight %.
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| CNB2006100761050A CN1331396C (en) | 2006-04-26 | 2006-04-26 | Pollution-less pesticide fertilizer for preventing and controlling blight and its production process |
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| CNB2006100761050A CN1331396C (en) | 2006-04-26 | 2006-04-26 | Pollution-less pesticide fertilizer for preventing and controlling blight and its production process |
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| CN1331396C CN1331396C (en) | 2007-08-15 |
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