CN1790074A - Method for manufacturing optical fiber array connector - Google Patents
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- CN1790074A CN1790074A CN 200510112241 CN200510112241A CN1790074A CN 1790074 A CN1790074 A CN 1790074A CN 200510112241 CN200510112241 CN 200510112241 CN 200510112241 A CN200510112241 A CN 200510112241A CN 1790074 A CN1790074 A CN 1790074A
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- 239000013307 optical fiber Substances 0.000 title claims abstract description 37
- 238000000034 method Methods 0.000 title claims abstract description 25
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 23
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims abstract description 8
- 239000000919 ceramic Substances 0.000 claims abstract description 5
- 239000011521 glass Substances 0.000 claims abstract description 3
- 239000005385 borate glass Substances 0.000 claims abstract 2
- 239000000853 adhesive Substances 0.000 claims description 9
- 230000001070 adhesive effect Effects 0.000 claims description 9
- 238000005520 cutting process Methods 0.000 claims description 3
- 238000006073 displacement reaction Methods 0.000 claims description 3
- 239000000835 fiber Substances 0.000 claims description 3
- 239000011343 solid material Substances 0.000 claims description 3
- 238000003780 insertion Methods 0.000 claims 1
- 230000037431 insertion Effects 0.000 claims 1
- 238000004891 communication Methods 0.000 abstract description 9
- 230000003287 optical effect Effects 0.000 abstract description 9
- 238000005245 sintering Methods 0.000 abstract description 4
- 239000000126 substance Substances 0.000 abstract description 3
- 239000000758 substrate Substances 0.000 abstract description 3
- 239000000463 material Substances 0.000 abstract 1
- KRHYYFGTRYWZRS-UHFFFAOYSA-N Fluorane Chemical compound F KRHYYFGTRYWZRS-UHFFFAOYSA-N 0.000 description 14
- MCMNRKCIXSYSNV-UHFFFAOYSA-N Zirconium dioxide Chemical compound O=[Zr]=O MCMNRKCIXSYSNV-UHFFFAOYSA-N 0.000 description 4
- 239000002241 glass-ceramic Substances 0.000 description 3
- 238000012545 processing Methods 0.000 description 3
- 238000002679 ablation Methods 0.000 description 2
- 239000005388 borosilicate glass Substances 0.000 description 2
- 239000013078 crystal Substances 0.000 description 2
- 239000002184 metal Substances 0.000 description 2
- 238000005498 polishing Methods 0.000 description 2
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 description 1
- 229910010293 ceramic material Inorganic materials 0.000 description 1
- RKTYLMNFRDHKIL-UHFFFAOYSA-N copper;5,10,15,20-tetraphenylporphyrin-22,24-diide Chemical compound [Cu+2].C1=CC(C(=C2C=CC([N-]2)=C(C=2C=CC=CC=2)C=2C=CC(N=2)=C(C=2C=CC=CC=2)C2=CC=C3[N-]2)C=2C=CC=CC=2)=NC1=C3C1=CC=CC=C1 RKTYLMNFRDHKIL-UHFFFAOYSA-N 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
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- 238000005530 etching Methods 0.000 description 1
- 238000003754 machining Methods 0.000 description 1
- 238000009740 moulding (composite fabrication) Methods 0.000 description 1
- 239000011148 porous material Substances 0.000 description 1
- 239000010703 silicon Substances 0.000 description 1
- 229910052710 silicon Inorganic materials 0.000 description 1
- 230000009466 transformation Effects 0.000 description 1
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Abstract
一种用于光通讯的光纤列阵连接器的制造方法,该方法的要点是结合飞秒激光照射、化学处理方法在石英玻璃,硼酸盐玻璃,微晶玻璃或透光性陶瓷等基板材料内制造出列阵贯通孔,然后将光纤插入贯通孔内并固定而制造成光纤列阵连接器。本方法避免了以往制造方法所需的预先制造模具,毛坯烧结等步骤,具有制造工艺简单,孔间距的精度高和生产成本低的特点。
A method for manufacturing an optical fiber array connector for optical communication, the key point of the method is to combine femtosecond laser irradiation and chemical treatment to manufacture array through holes in substrate materials such as quartz glass, borate glass, microcrystalline glass or translucent ceramics, and then insert the optical fiber into the through hole and fix it to manufacture the optical fiber array connector. This method avoids the steps of pre-manufacturing molds and blank sintering required by previous manufacturing methods, and has the characteristics of simple manufacturing process, high precision of hole spacing and low production cost.
Description
技术领域technical field
本发明涉及光通讯,特别是一种结合飞秒脉冲激光照射和化学处理方法的光通讯用的光纤列阵连接器的制造方法。The invention relates to optical communication, in particular to a method for manufacturing an optical fiber array connector for optical communication combined with femtosecond pulsed laser irradiation and chemical treatment.
背景技术Background technique
迄今为止,用于固定光纤、连接光纤与光通讯部件以及光纤间的连接器及光纤列阵连接器一般在微晶玻璃、硅基板、石英玻璃等表面机械加工成V形槽,或采用ZrO2陶瓷通过使用金属模具生产毛坯,然后烧结,最后机械加工形成小孔。V形槽的机械加工精度为±5μm,为保证V形槽的精度需要经过切削抛光进行形状修正。但工序繁琐,生产效率低。另外,用ZrO2陶瓷,孔之间距离的精度为±2μm,由于加工时的应力作用,烧结过程中晶体结构从正方晶系向单斜晶系转变,使得连接器产生膨胀,影响尺寸精度。这些方法制备的光纤连接器和光纤阵列连接器,虽然插入光纤后可用粘接剂进行加固,具有操作比较简单的一面,但有两个以上贯穿孔和列阵贯穿孔的孔间距离的精度受金属模具制造、成形、烧结、加工过程的种种因素的影响,要将精度控制在1μm以下是十分困难的。So far, the connectors and fiber array connectors used to fix optical fibers, connect optical fibers and optical communication components, and optical fibers are generally machined into V-shaped grooves on the surface of microcrystalline glass, silicon substrate, quartz glass, etc., or use ZrO2 Ceramics are produced by using a metal mold as a blank, then sintered and finally machined to form the pores. The machining accuracy of the V-shaped groove is ±5μm. To ensure the accuracy of the V-shaped groove, it needs to be corrected by cutting and polishing. But the procedure is loaded down with trivial details, and production efficiency is low. In addition, with ZrO2 ceramics, the accuracy of the distance between the holes is ±2μm. Due to the stress during processing, the crystal structure changes from tetragonal to monoclinic during sintering, which causes the connector to expand and affects the dimensional accuracy. The optical fiber connectors and optical fiber array connectors prepared by these methods can be reinforced with adhesives after the optical fibers are inserted, and have a relatively simple operation, but the accuracy of the distance between the holes with more than two through holes and the array of through holes is affected. Due to the influence of various factors in metal mold manufacturing, forming, sintering and processing, it is very difficult to control the precision below 1 μm.
发明内容Contents of the invention
本发明目的在于克服上述现有技术的缺陷,一种高精度光纤列阵连接器的制备方法,本发明方法应具有制造工艺简单,孔间距的精度高和生产成本低的特点。The purpose of the present invention is to overcome the defects of the above-mentioned prior art and provide a method for preparing a high-precision optical fiber array connector. The method of the present invention should have the characteristics of simple manufacturing process, high precision of hole spacing and low production cost.
本发明的技术解决方案如下:Technical solution of the present invention is as follows:
一种高精度光纤列阵连接器的制造方法,该方法包括下列步骤:A method for manufacturing a high-precision fiber optic array connector, the method comprising the following steps:
①将可透过飞秒激光的固体材料制成长六面体的板块;① Make a long hexahedron plate from a solid material that can pass through the femtosecond laser;
②所述的板块的插入光纤的一端面固定在一具有高精度位移的三维移动平台上,并使该板块的Z轴垂直于所述的三维移动平台;② An end face of the plate into which the optical fiber is inserted is fixed on a three-dimensional mobile platform with high-precision displacement, and the Z-axis of the plate is perpendicular to the three-dimensional mobile platform;
③将一飞秒激光束聚焦照射所述的板块的下表面,然后所述的飞秒激光束利用三维移动平台的沿Z轴运动由下向上地扫描烧蚀所述的板块,形成一条贯通线,再根据需要移动三维移动平台沿水平的X轴和Y轴运动,再进行飞秒激光扫描烧蚀,获得多条间隔均匀的列阵贯通线;③ Focus a femtosecond laser beam on the lower surface of the plate, and then use the three-dimensional mobile platform to scan and ablate the plate from bottom to top to form a through line , and then move the three-dimensional mobile platform along the horizontal X-axis and Y-axis according to the needs, and then perform femtosecond laser scanning and ablation to obtain multiple uniformly spaced array through lines;
④将具有贯通线的板块浸泡在氢氟酸中侵蚀,形成列阵贯通孔;④ Soak the plates with through-lines in hydrofluoric acid and corrode to form an array of through-holes;
⑤在贯通孔中插入光纤,用粘接剂固定,制成光纤列阵接连器。⑤Insert the optical fiber in the through hole and fix it with an adhesive to make an optical fiber array connector.
所述的三维移动平台的移动精度为小于1μm。The movement precision of the three-dimensional mobile platform is less than 1 μm.
所述的长六面体的板块是由石英玻璃、硼硅酸盐玻璃、微晶玻璃或透明陶瓷经切割、表面抛光后制成的。The long hexahedral plate is made of quartz glass, borosilicate glass, glass-ceramics or transparent ceramics after cutting and surface polishing.
所述的飞秒激光束的平均功率5mW~500mW,脉冲频率为10Hz~200KHz,波长为750nm~800nm。所述的飞秒激光束的扫描速度为:5μm/s~5mm/s。The average power of the femtosecond laser beam is 5mW-500mW, the pulse frequency is 10Hz-200KHz, and the wavelength is 750nm-800nm. The scanning speed of the femtosecond laser beam is: 5 μm/s˜5 mm/s.
本发明的技术效果:Technical effect of the present invention:
本发明结合飞秒激光照射和化学处理,可以短时间高精度地在石英玻璃、硼硅酸盐玻璃、微晶玻璃和透明陶瓷材料上形成能插入光纤的表面呈喇叭口形的列阵小孔;Combining femtosecond laser irradiation and chemical treatment, the present invention can form trumpet-shaped array holes on the surface of quartz glass, borosilicate glass, glass ceramics and transparent ceramic materials in a short time and with high precision;
该方法在制造过程中不需要预先制模具,精度由三维移动平台来控制,很容易就可以将控制在1μm以下。This method does not require pre-made molds in the manufacturing process, and the precision is controlled by a three-dimensional mobile platform, which can be easily controlled below 1 μm.
另外该方法在制造过程中不需要烧结,避免了因变形、晶型转变等引入的精度误差。In addition, the method does not require sintering during the manufacturing process, which avoids precision errors caused by deformation and crystal transformation.
因此本发明方法具有工艺简单,孔间距的精度高和生产成本低的特点。Therefore, the method of the invention has the characteristics of simple process, high precision of hole spacing and low production cost.
附图说明Description of drawings
图1为飞秒激光扫描后的列阵贯通线Figure 1 shows the through-line of the array after femtosecond laser scanning
图2为氢氟酸腐蚀后形成的列阵贯通孔Figure 2 is an array of through holes formed after hydrofluoric acid etching
图中:1-基板,2-贯通列阵线,3-贯通列阵孔,4-喇叭口In the figure: 1-substrate, 2-through array line, 3-through array hole, 4-horn mouth
具体实施方式Detailed ways
下面结合附图和实施例对本发明作进一步说明,但不应以此限制本发明的保护范围。The present invention will be further described below in conjunction with the accompanying drawings and embodiments, but the protection scope of the present invention should not be limited thereby.
请参阅图1和图2,本发明光纤列阵连接器的制造方法,包括下列步骤:Please refer to Fig. 1 and Fig. 2, the manufacturing method of optical fiber array connector of the present invention, comprises the following steps:
①将可透过飞秒激光的固体材料制成长六面体板块,如图1所示;① Make a long hexahedron plate from a solid material that can pass through the femtosecond laser, as shown in Figure 1;
②所述的板块的插入光纤的一端面固定在一具有高精度位移的三维移动平台上,并使这板块Z轴垂直于所述的三维移动平台;② An end face of the plate inserted into the optical fiber is fixed on a three-dimensional mobile platform with high-precision displacement, and the Z-axis of the plate is perpendicular to the three-dimensional mobile platform;
③将一飞秒激光束聚焦照射所述的板块的下表面,然后所述的飞秒激光束利用所述的三维移动平台的沿Z轴运动由下向上地扫描烧蚀所述的板块,形成一条贯通线,再根据需要移动三维移动平台沿水平的X轴和Y轴运动,再进行飞秒激光扫描烧蚀,获得具有间隔均匀的列阵贯通线,如图1中的2所示;③ focus a femtosecond laser beam on the lower surface of the plate, and then use the movement of the three-dimensional mobile platform along the Z axis to scan and ablate the plate from bottom to top to form A through-line, and then move the three-dimensional mobile platform along the horizontal X-axis and Y-axis according to the needs, and then perform femtosecond laser scanning and ablation to obtain an array of through-lines with uniform intervals, as shown in 2 in Figure 1;
④将具有贯通线的板块浸泡在氢氟酸中侵蚀,形成列阵贯通孔,如图2中的3所示;④ Soak the plates with through-lines in hydrofluoric acid and corrode to form an array of through-holes, as shown in 3 in Figure 2;
⑤在贯通孔中插入光纤,用粘接剂固定,制成光纤列阵接连器。⑤Insert the optical fiber in the through hole and fix it with an adhesive to make an optical fiber array connector.
所制得的孔径精度和孔间距离精度高的小孔列阵,并且表面具有一定的喇叭口形状(图2中4)。在飞秒激光的照射过程中,我们使用了高精度的三维移动平台(精度为100nm),从而可以实现将孔的尺寸和孔间距离的精度控制在1μm内。在孔中插入光纤,用粘接剂固定,形成光通讯用的连接器。此方法可实现加工精度高且价格便宜的光纤连接器及光纤列阵连接器。The obtained small hole array has high precision of hole diameter and distance between holes, and the surface has a certain bell mouth shape (4 in Fig. 2). During the irradiation of the femtosecond laser, we used a high-precision three-dimensional mobile platform (with an accuracy of 100nm), so that the accuracy of the size of the holes and the distance between the holes can be controlled within 1 μm. The optical fiber is inserted into the hole and fixed with an adhesive to form a connector for optical communication. The method can realize the optical fiber connector and the optical fiber array connector with high processing precision and low price.
本方法通过控制飞秒激光的各项参数(平均功率、脉冲频率、波长等)、激光的扫描速度(指三维平台的移动速度)以及使用不同倍率的聚焦镜头,来获得不同形状和尺寸的小孔,通过多次扫描的方法获得小孔阵列。In this method, various parameters of the femtosecond laser (average power, pulse frequency, wavelength, etc.), the scanning speed of the laser (referring to the moving speed of the three-dimensional platform) and the use of focusing lenses with different magnifications are used to obtain small laser beams of different shapes and sizes. Holes, through the method of multiple scans to obtain a small hole array.
下面是具体实施例:The following are specific examples:
实施例1:Example 1:
将5mW、脉冲频率为10Hz、波长为800nm的飞秒激光用100倍的透镜聚焦到5mm厚的抛光过的石英玻璃底部,然后由下向上以5μm/s的速度扫描,形成间隔为250μm的2×2根线。然后浸泡到4wt%的氢氟酸溶液中,并施加超声波,形成了表面具有喇叭口结构的直径为125μm的贯穿孔列阵。并且贯穿孔间的距离的精度为250±1μm。在孔中插入光纤,用粘接剂固定,形成光通讯用的光纤列阵连接器。Focus a 5mW femtosecond laser with a pulse frequency of 10Hz and a wavelength of 800nm on the bottom of a 5mm thick polished quartz glass with a 100x lens, and then scan from bottom to top at a speed of 5μm/s to form 2 laser beams with an interval of 250μm. × 2 wires. Then soak in 4wt% hydrofluoric acid solution, and apply ultrasonic waves, forming a through-hole array with a diameter of 125 μm and a trumpet structure on the surface. And the accuracy of the distance between the through holes is 250±1 μm. Insert the optical fiber into the hole and fix it with an adhesive to form an optical fiber array connector for optical communication.
实施例2:Example 2:
将100mW、脉冲频率为1KHz、波长为750nm的飞秒激光用50倍的透镜聚焦到5mm厚的抛光过的石英玻璃底部,然后由下向上以1000μm/s的速度扫描,形成间隔为250μm的6×6根线。然后浸泡到4wt%的氢氟酸溶液中,并施加超声波,形成了表面具有喇叭口结构的直径为125μm的贯穿孔列阵。并且贯穿孔间的距离的精度为250±1μm。在孔中插入光纤,用粘接剂固定,形成光通讯用的光纤列阵连接器。Focus the 100mW femtosecond laser with pulse frequency of 1KHz and wavelength of 750nm on the bottom of the 5mm thick polished quartz glass with a 50 times lens, and then scan from bottom to top at a speed of 1000μm/s to form 6 laser beams with an interval of 250μm. ×6 wires. Then soak in 4wt% hydrofluoric acid solution, and apply ultrasonic waves, forming a through-hole array with a diameter of 125 μm and a trumpet structure on the surface. And the accuracy of the distance between the through holes is 250±1 μm. Insert the optical fiber into the hole and fix it with an adhesive to form an optical fiber array connector for optical communication.
实施例3:Example 3:
将500mW、脉冲频率为200KHz、波长为850nm的飞秒激光用2倍的透镜聚焦到5mm厚的抛光过的石英玻璃底部,然后由下向上以5000μm/s的速度扫描,形成间隔为250μm的10×10根线。然后浸泡到4wt%的氢氟酸溶液中,并施加超声波,形成了表面具有喇叭口结构的直径为125μm的贯穿孔列阵。并且贯穿孔间的距离的精度为250±1μm。在孔中插入光纤,用粘接剂固定,形成光通讯用的光纤列阵连接器。Focus the 500mW femtosecond laser with pulse frequency of 200KHz and wavelength of 850nm on the bottom of a 5mm thick polished quartz glass with a 2x lens, and then scan from bottom to top at a speed of 5000μm/s to form 10 laser beams with an interval of 250μm. ×10 wires. Then soak in 4wt% hydrofluoric acid solution, and apply ultrasonic waves, forming a through-hole array with a diameter of 125 μm and a trumpet structure on the surface. And the accuracy of the distance between the through holes is 250±1 μm. Insert the optical fiber into the hole and fix it with an adhesive to form an optical fiber array connector for optical communication.
实施例4:Example 4:
将100mW的脉冲频率为50Hz、波长为775nm的飞秒激光用20倍的透镜聚焦到5mm厚的抛光过的微晶玻璃底部,然后由下向上以50μm/s的速度扫描,形成间隔为500μm的8×8根线。然后浸泡到5wt%的氢氟酸溶液中并施加超声波,形成了表面具有喇叭口结构的直径为126μm的贯穿孔阵列。并且贯穿孔间的距离的精度为500±1μm。在孔中插入光纤,用粘接剂固定,形成光通讯用的光纤列阵连接器。Focus the 100mW femtosecond laser with a pulse frequency of 50Hz and a wavelength of 775nm on the bottom of a 5mm thick polished glass-ceramic with a 20x lens, and then scan from bottom to top at a speed of 50μm/s to form a 500μm interval. 8×8 wires. Then it is soaked in 5wt% hydrofluoric acid solution and ultrasonic waves are applied to form an array of through holes with a diameter of 126 μm and a trumpet structure on the surface. And the accuracy of the distance between the through holes is 500±1 μm. Insert the optical fiber into the hole and fix it with an adhesive to form an optical fiber array connector for optical communication.
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN110779682A (en) * | 2019-09-25 | 2020-02-11 | 江苏法尔胜光通信科技有限公司 | Ytterbium-doped active optical fiber all-fiber laser test system suitable for high power and test method thereof |
| US11104605B2 (en) | 2019-11-26 | 2021-08-31 | Corning Research & Development Corporation | Process for making multi-fiber, physical contact fiber ferrule assemblies |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110779682A (en) * | 2019-09-25 | 2020-02-11 | 江苏法尔胜光通信科技有限公司 | Ytterbium-doped active optical fiber all-fiber laser test system suitable for high power and test method thereof |
| US11104605B2 (en) | 2019-11-26 | 2021-08-31 | Corning Research & Development Corporation | Process for making multi-fiber, physical contact fiber ferrule assemblies |
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