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CN1621821A - Structure and method for measuring thermal-expansion coefficient of polycrystalline silicon thin film - Google Patents

Structure and method for measuring thermal-expansion coefficient of polycrystalline silicon thin film Download PDF

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CN1621821A
CN1621821A CN 200410065842 CN200410065842A CN1621821A CN 1621821 A CN1621821 A CN 1621821A CN 200410065842 CN200410065842 CN 200410065842 CN 200410065842 A CN200410065842 A CN 200410065842A CN 1621821 A CN1621821 A CN 1621821A
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polysilicon
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curved
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CN100368795C (en
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黄庆安
张宇星
李伟华
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Southeast University
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Abstract

测量多晶硅薄膜热膨胀系数的测量结构及其测量方法是基于表面加工工艺的多晶硅薄膜热膨胀系数的在线检测结构,该结构由一个多晶硅双直梁结构以及两个多晶硅弯梁结构构成,在直梁的中间部分镀有铝膜,多晶硅弯梁结构由两个相同的弯梁组成,弯梁中间的顶端设有尖端,其尖端对着铝膜;测量方法为:制备测量梁结构;在室温时对直梁分别通入一微小电流I1和I0,测量其两端的电压V1和V0,得出电阻率ρ1和ρ0;选择两弯梁结构组中的任一个弯梁,总长为L2,对其通入电流I2,测量其两端的电压V2,测量出电阻率ρ2,对弯梁的两端分别通入缓慢增加的电流,观察连接弯梁与直梁锚区的欧姆表的读数是否有一个从无穷大到有限值的跳变;就可以得出热膨胀系数α。

Figure 200410065842

The measurement structure and measurement method for measuring the thermal expansion coefficient of polysilicon thin films are based on the online detection structure of the thermal expansion coefficient of polysilicon thin films based on surface processing technology. The structure is composed of a polysilicon double straight beam structure and two polysilicon curved beam structures. Partially coated with aluminum film, the polysilicon curved beam structure is composed of two identical curved beams, the top of the curved beam is provided with a tip, and its tip is facing the aluminum film; the measurement method is: prepare the measuring beam structure; measure the straight beam at room temperature Pass a small current I 1 and I 0 respectively, measure the voltages V 1 and V 0 at both ends, and obtain the resistivity ρ 1 and ρ 0 ; choose any one of the two curved beam structure groups, and the total length is L 2 , pass the current I 2 to it, measure the voltage V 2 at both ends, measure the resistivity ρ 2 , pass a slowly increasing current to the two ends of the curved beam respectively, and observe the ohmmeter connecting the anchorage area of the curved beam and the straight beam Whether there is a jump from infinity to finite value in the reading of the reading; the coefficient of thermal expansion α can be obtained.

Figure 200410065842

Description

Measure the measurement structure and the measuring method thereof of polysilicon membrane thermal expansivity
Technical field
The present invention is based on the online detection architecture of the polysilicon membrane thermal expansivity of surface processing technique, belongs to the technical field of MEMS (microelectromechanical systems) technological parameter test.
Technical background
The film thermal expansivity is a very important parameter for the design of MEMS device.On the one hand, the thermal expansion of membraneous material has considerable influence to device performance, and for example, the mismatch of film and substrate thermal expansivity can produce thermal stress, causes malformation or damage; On the other hand, thermal expansion is the power resources of low-grade fever actuator.Many documents have provided body material coefficient of thermal expansion coefficient, but the thermal expansivity of body material coefficient of thermal expansion coefficient and membraneous material and incomplete same, therefore can not the phase trans-substitution.And, even with a kind of membraneous material through different process, thermal expansivity also may be different.Therefore, it is significant that the MEMS structure of micromechanics film thermal expansivity can be accurately measured in proposition.
The test structure that several polysilicon membrane thermal expansivity based on the MEMS technology had been arranged before the present invention.Yet these test structures are more or less some following problems of existence always, make them can not realize online detection.For example, certain structures need detect in vacuum or annular seal space; Some needs comparatively complicated testing tool; Some relies on other too many material parameter; The movement locus of some test structure is curve rather than straight line, makes troubles to test; The measurand of certain structures is difficult to accurate measurement; A lot of testing schemes adopt traditional optical detection method, rather than measure with electrical quantities, therefore, are difficult to carry out other expansion utilization of the encapsulation of road, back and some.
Summary of the invention
Technical matters: the object of the present invention is to provide a kind of measurement structure and measuring method thereof of measuring the polysilicon membrane thermal expansivity, this structure and measuring method can realize the purpose of the required technological parameter of monitoring device manufacturing process at test surfaces processing polysilicon membrane thermal expansivity under the physical environment.
Technical scheme: the measurement structure of measurement polysilicon membrane thermal expansivity of the present invention is on forming, and this measurement structure is made of the two straight beam structures of a polysilicon and two polysilicon camber beam structures; Wherein, in the two straight beam structures of polysilicon, the two ends of polysilicon straight beam are separately fixed in the anchor district on both sides, are coated with the aluminium film at the center section of straight beam, are coated with the aluminium film at the center section of straight beam; Polysilicon camber beam structure is made up of two identical camber beams, and the two ends of camber beam are separately fixed in the anchor district, and the two ends of camber beam are separately fixed in two anchor districts, and the top in the middle of camber beam is provided with the tip, and it is most advanced and sophisticated facing to the aluminium film; Top in the middle of camber beam is provided with the tip, and it is most advanced and sophisticated facing to the aluminium film; The anchor district is positioned on the plane of same layer-of-substrate silicon.
The distance of the top of two camber beams to the promptly most advanced and sophisticated top of the initial distance of straight beam to the aluminium film is 2 μ m~8 μ m, and it is unequal that the top of two camber beams separates the initial distance of two straight beams of other distance; The width of polysilicon beam is 2 μ m~8 μ m, and thickness all is 1.5 μ m~3 μ m; The overall width of two straight beams equals the width of every camber beam in the polysilicon camber beam structure in the dual poly straight beam structure.
The length of polysilicon straight beam is 300 μ m~600 μ m, and camber beam length is 300 μ m~600 μ m, and all camber beams and straight beam angle are 0.01~0.05rad; And the length of the length of polysilicon camber beam and polysilicon straight beam is inequality.
The method of measuring is:
Measure current value and shift value in the two camber beam structures respectively, just can obtain thermal expansivity by calculating again.
1. at first calculate the medial temperature increment of every camber beam by the calorifics relational expression:
ΔT = J 2 ρ 0 k p m 2 [ mL 2 - tanh ( mL 2 ) mL 2 ] - - - - - - - - - - - - - ( 1 )
m = η k p h - J 2 ρ 0 ξ k p - - - - - - - - - ( 2 )
Δ T is the medial temperature increment, and m is middle parameter, κ pBe the thermal conductivity of polysilicon, η is the equivalent heat transfer coefficient of bent beam lower surface and substrate, and J is the current density by bent beam, ρ 0The resistivity of polysilicon when being room temperature, ξ is the temperature coefficient of polysilicon resistance, L is the total length of bent beam.
2. then by displacement--medial temperature increment relation formula calculates thermal expansivity
δ = αΔT L 2 cos ( θ ) ( L 2 4 - w 2 ) L 2 4 tan 2 ( θ ) + w 2 - - - - - - - - - - - - ( 3 )
Wherein w is the width of camber beam, and θ is the angle of camber beam and level, and α is a thermal expansivity, and δ is the displacement on camber beam top.
The two straight beam structures of polysilicon and two polysilicon camber beam structures are used surface processing technique, and its preparation process is;
The preparation silicon substrate,
Deposit layer of silicon dioxide layer on silicon substrate,
Deposit one deck silicon nitride layer on silicon dioxide layer,
Deposit one deck Pyrex (PSG) sacrifice layer on the silicon nitride layer again,
Deposit polysilicon on PSG,
Make the polysilicon beam by lithography,
Deposit layer of aluminum on polysilicon layer,
Make aluminium lamination in the anchor district and the aluminium film on the straight beam by lithography,
Releasing sacrificial layer.
This measuring method is specially:
Girder construction is measured in a, preparation, promptly prepares two straight beam structures and two polysilicon camber beam structures, and the geometry of these two camber beams is identical, but the top is from the initial distance difference of straight beam;
B, when room temperature, the straight beam in the straight beam structure is fed a Weak current I 0, measure the voltage V at its two ends 0, according to relational expression V 0 I 0 = ρ 0 L 1 wh Draw that length is L when room temperature 1The electricalresistivity of polysilicon straight beam 0, again to feeding another Weak current I in the straight beam 1, measure its both end voltage V 1, according to relational expression V 1 I = ρ 1 L 1 wh Measuring feeding electric current is I 1The time, length is L 1The electricalresistivity of polysilicon beam 1,
Any camber beam in c, the selection two camber beam structural group, length overall is L 2, it is fed electric current I 2, measure the voltage V at its two ends 2, and according to relational expression V 2 I = ρ 2 L 2 wh Measuring and feeding electric current is I 2The time, length is L 2The electricalresistivity of polysilicon camber beam 2,
D, according to the relational expression of resistivity-medial temperature increment:
ρ 1 ρ 0 - 1 ρ 2 ρ 0 - 1 = ΔT 1 ΔT 2 [ m L 1 2 - tan ( m L 1 2 ) mL 1 2 / mL 2 2 - tan ( mL 2 2 ) mL 2 2 ] Draw m, m is middle parameter;
E, mistake relational expression m = η k p h - J 2 ρ 0 ξ k p Draw η, ρ 0, ξ; η is the equivalence of polysilicon beam lower surface
F, the coefficient of heat transfer, ρ 0Be polysilicon beam resistivity at room temperature, ξ is a polysilicon beam temperature coefficient at room temperature, and h is the thickness of beam, κ pBe the thermal conductivity of polysilicon, J is the current density in the beam;
G, the two ends of camber beam are fed the electric current of slow increase respectively, whether the reading of observing the ohmmeter that connects camber beam and straight beam anchor district has a saltus step from the infinity to the finite value; As not having, illustrate that then two beams also do not come in contact, continue to increase current value; If any saltus step, illustrate that then contact has taken place two beams, note this moment size, according to relational expression by current value J = I wh Calculate current density, J 1, the displacement of camber beam is δ 1+ Δ δ, and wherein, δ 1 is the actual displacement of camber beam, and Δ δ is an error term;
H, camber beam is repeated above step f, write down another group current density, J again 2With displacement δ 2+ Δ δ, with above parameter substitution relational expression ΔT = J 2 ρ 0 k p m 2 [ mL 2 - tanh ( mL 2 ) mL 2 ] , And two formulas are subtracted each other, promptly
( δ 1 + Δδ ) - ( δ 2 + Δδ ) = α ( ΔT 1 - ΔT 2 ) L 2 cos ( θ ) ( L 2 4 - w 2 ) L 2 4 tan 2 ( θ ) + w 2
According to following formula, just can draw thermalexpansioncoefficient again.
Technique effect: advantage of the present invention is as follows
(1) this structure is used surface processing technique, and test structure is based on the combination of common straight beam and camber beam structure, so technology and structure are all comparatively simple;
(2) this structure does not relate to some special measurement means, so method of testing is simple;
(3) this structure has been considered the influence of fabrication error to measuring, so precision is higher;
(4) because other unknown material parameter that measurement is relied on is less, therefore the independence of measuring is better;
(5) owing to consider that various forms of heats run off in physical environment, so it need not measure under particular surroundingss such as vacuum or seal hatch, and lower to the requirement of measuring equipment;
(6) Ce Shi result can show with the electricity scale, therefore can realize online detection.
Description of drawings
Fig. 1 is the floor map of thermal expansivity test structure of the present invention.
Fig. 2 is the schematic perspective view of thermal expansivity test structure in the embodiment of the invention.
Have among the above figure: anchor district 11,12,13,14,15,16, straight beam 31,32, camber beam 21,22, tip 211,221, aluminium film 311,321; Aluminum lead layer 41, polysilicon layer 42, silicon nitride layer 43, silicon dioxide layer 44, layer-of-substrate silicon 45.
Embodiment
This measurement structure is made of the two straight beam structures of a polysilicon and two polysilicon camber beam structures; Wherein, in the two straight beam structures of polysilicon, the two ends of polysilicon straight beam 31,32 are separately fixed at the anchor district 13,16 on both sides) on, be coated with aluminium film 311 at the center section of straight beam 31, be coated with aluminium film 321 at the center section of straight beam 32; Polysilicon camber beam structure is made up of two identical camber beams 21,22, the two ends of camber beam 21 are separately fixed in the anchor district 11,12, the two ends of camber beam 22 are separately fixed in two anchor districts 14,15, and the top in the middle of camber beam 21 is provided with tip 211, and its tip 211 is facing to aluminium film 311; Top in the middle of camber beam 22 is provided with tip 221, and its tip 221 is facing to aluminium film 321; Anchor district 11,12,13,14,15,16 is positioned on the plane of same layer-of-substrate silicon.The top of two camber beams to the initial distance of straight beam promptly most advanced and sophisticated 211 top be 2 μ m~8 μ m to the distance of aluminium film 311, it is unequal that the top of two camber beams separates the initial distance of two straight beams of other distance; The width of polysilicon beam is 2 μ m~8 μ m, and thickness all is 1.5 μ m~3 μ m; The overall width of two straight beams 31,32 equals the width of every camber beam 21,22 in the polysilicon camber beam structure in the dual poly straight beam structure.The length of polysilicon straight beam 31,32 is 300 μ m~600 μ m, and camber beam 21,22 length are 300 μ m~600 μ m, and all camber beams and straight beam angle are 0.01~0.05rad; And the length of the length of polysilicon camber beam and polysilicon straight beam is inequality.
On forming, it is made of the two straight beam structures of polysilicon and two polysilicon camber beam structural group.On the relation of position, two camber beam structures are at the two ends of two straight beam structures, and the top of two camber beams is all towards two straight beam structures.On physical dimension, two camber beams are identical, and just their tops separately are inequality from the initial distance of two straight beams; The thickness of all polysilicon beams is all identical; The width of straight beam is 1/2 of a camber beam width; The length of all camber beams is all identical, and the length of all straight beams is also identical; The length of camber beam and the length of straight beam are inequality; All camber beams are all identical with the angle of level.The present invention is a kind of online detection architecture of the polysilicon membrane thermal expansivity based on surface processing technique, and as shown in Figure 2, its process structure layer is made up of layer-of-substrate silicon, silicon dioxide layer, silicon nitride layer, polysilicon layer, aluminum lead layer.The manufacturing process steps of camber beam and two straight beams is as follows:
The preparation silicon substrate,
Deposit layer of silicon dioxide layer,
Deposit one deck silicon nitride layer,
Deposit one deck PSG is as sacrifice layer,
The deposit polysilicon,
Make the polysilicon beam by lithography,
The deposit layer of aluminum,
Photoetching aluminium,
Releasing sacrificial layer.
Concrete testing procedure is as follows:
(1) extraction of parameter m in the middle of:
1. when room temperature, straight beam is fed a Weak current I 0(0.1mA~0.5mA guarantees that the temperature of camber beam does not almost change) measures the voltage V at its two ends 0, according to relational expression
V 0 I 0 = ρ 0 L 1 wh Can draw the electricalresistivity of the polysilicon when room temperature 0,
Wherein h is the thickness of two straight beams, and w is the overall width of two straight beams, L 1Be the length of two straight beams,
2. above two straight beams are fed another Weak current I again 1(this moment, resistivity was along with variation has taken place in the rising of beam temperature) measures its both end voltage V 1, and according to relational expression V 1 I = ρ 1 L 1 wh Just can measure feeding electric current is I 1The time, length is L 1The electricalresistivity of polysilicon beam 1,
3. (length overall is L to select any camber beam in the two camber beam structural group 2), it is fed electric current I 2, measure the voltage V at its two ends 2, and according to relational expression V 2 I = ρ 2 L 2 wh Just can measure and feed electric current is I 2The time, length is L 2The electricalresistivity of dual poly beam 2,
4. according to the relational expression of resistivity-medial temperature increment:
ρ 1 ρ 0 - 1 ρ 2 ρ 0 - 1 = ΔT 1 ΔT 2 = [ m L 1 2 - tan ( mL 1 2 ) mL 1 2 / mL 2 2 - tan ( mL 2 2 ) mL 2 2 ]
Just can obtain m, pass through relational expression: m = η k p h - J 2 ρ 0 ξ k p Just can draw η, ρ 0, ξ; η is the equivalent heat transfer coefficient of polysilicon beam lower surface, ρ 0, ξ be respectively polysilicon beam resistivity at room temperature with and temperature coefficient.
(2) measurement of thermalexpansioncoefficient:
1. the two ends of camber beam A are fed the electric current that slowly increases, the top that the thermal effect that electric current produces can make beam generation thermal expansion and promote beam travels forward.
Whether the reading of 2. observing the ohmmeter that connects camber beam and straight beam anchor district has a saltus step from the infinity to the finite value; As not having, illustrate that then two beams also do not come in contact, continue to increase current value; If any saltus step, illustrate that then contact has taken place two beams, note this moment size, according to relational expression by current value J = I wh Calculate current density, J 1, the displacement of camber beam is δ 1+ Δ δ, and wherein, δ 1 is the actual displacement of camber beam, and Δ δ is an error term.
3. to camber beam group B repeating step 1,2.Note J 2, δ 2+ Δ δ.
4. with above parameter substitution relational expression Δ&Tgr; = J 2 ρ 0 k p m 2 [ mL 2 - tanh ( mL 2 ) mL 2 ] And two formulas are subtracted each other, ( δ 1 + Δδ ) - ( δ 2 + δΔ ) = α ( ΔT 1 - ΔT 2 ) L 2 cos ( θ ) ( L 2 4 - w 2 ) L 2 4 tan 2 ( θ ) + w 2 , Wherein w is the width of camber beam, and θ is the angle of camber beam and level, and α is a thermal expansivity, and δ is the displacement on camber beam top.
According to following formula, just can draw thermalexpansioncoefficient.
Object lesson:
Two camber beam tops are respectively 3.5 μ m, 4 μ m from the initial top of straight beam distance among Fig. 1,2.The width of polysilicon straight beam all is 2 μ m, and the width of polysilicon camber beam is 4um; The thickness of all beams all is 2 μ m; The length overall of straight beam is 450 μ m, the length overall 500 μ m of camber beam; The angle of all camber beams and level is 0.05rad.
At first surface working dual poly straight beam and arbitrary polysilicon camber beam are fed the electric current of identical size.The voltage of measuring its two ends respectively just can calculate polysilicon resistivity, the temperature coefficient of resistivity and the equivalent heat transfer coefficient of beam and substrate at room temperature, utilizes these data just can ask for the polysilicon beam at a certain medial temperature increment that applies correspondence under the electric current according to the thermal modeling of beam again.
Then two camber beams are fed electric current identical, that increase progressively gradually (unsuitable excessive, as to guarantee that the maximum temperature point of beam is no more than 800K), the reading of observing the ohmmeter that connects camber beam and straight beam anchor district has or not saltus step.If no, then continue to increase electric current; If have, then explanation two beams this moment come in contact, and note this current value of camber beam constantly.The thermal modeling of utilizing the front to narrate just can calculate the medial temperature increment of the camber beam of this electric current correspondence, just can obtain the thermal expansivity of polysilicon again by model of structural mechanics.In concrete processing procedure, the camber beam structure has been adopted the method for error compensation, with cancellation because the influence that unrelieved stress, fabrication error etc. produce test.The thermal expansivity that can draw surface finished polysilicon thin film through measurements and calculations is approximately 2.58510-6, and the error of measurement is greatly about about 5.6%.

Claims (5)

1.一种测量多晶硅薄膜热膨胀系数的测量结构,其特征在于在结构的组成上,该测量结构由一个多晶硅双直梁结构以及两个多晶硅弯梁结构构成;其中,在多晶硅双直梁结构中,多晶硅直梁(31、32)的两端分别固定在两边的锚区(13、16)上,在直梁(31)的中间部分镀有铝膜(311),在直梁(32)的中间部分镀有铝膜(321);多晶硅弯梁结构由两个相同的弯梁(21、22)组成,弯梁(21)的两端分别固定在锚区(11、12)上,弯梁(22)的两端分别固定在两个锚区(14、15)上,在弯梁(21)中间的顶端设有尖端(211),其尖端(211)对着铝膜(311);在弯梁(22)中间的顶端设有尖端(221),其尖端(221)对着铝膜(321);锚区(11、12、13、14、15、16)位于同一块硅衬底层的平面上。1. A measurement structure for measuring the coefficient of thermal expansion of a polysilicon film is characterized in that in the composition of the structure, the measurement structure is composed of a polysilicon double straight beam structure and two polysilicon curved beam structures; wherein, in the polysilicon double straight beam structure , the two ends of the polysilicon straight beam (31, 32) are respectively fixed on the anchor areas (13, 16) on both sides, and the middle part of the straight beam (31) is coated with an aluminum film (311), and on the straight beam (32) The middle part is coated with an aluminum film (321); the polysilicon curved beam structure is composed of two identical curved beams (21, 22), and the two ends of the curved beam (21) are respectively fixed on the anchorage areas (11, 12), and the curved beam The two ends of (22) are respectively fixed on two anchor areas (14,15), and the top in the middle of the curved beam (21) is provided with a tip (211), and its tip (211) faces the aluminum film (311); The top in the middle of the curved beam (22) is provided with a tip (221), and its tip (221) faces the aluminum film (321); the anchor regions (11, 12, 13, 14, 15, 16) are located on the same silicon substrate layer on flat surface. 2、根据权利要求1所述的测量多晶硅薄膜热膨胀系数的测量结构,其特征在于两弯梁的顶端到直梁的初始距离即尖端(211)的顶端到铝膜(311)的距离为2μm~8μm,两个弯梁的顶端离分别距两根直梁的初始距离不相等;多晶硅梁的宽度为2μm~8μm,厚度都为1.5μm~3μm;双多晶硅直梁结构中两根直梁(31、32)的总宽度等于多晶硅弯梁结构中每根弯梁(21、22)的宽度。2. The measurement structure for measuring the coefficient of thermal expansion of polysilicon thin films according to claim 1, characterized in that the initial distance from the tops of the two curved beams to the straight beams, that is, the distance from the top of the tip (211) to the aluminum film (311) is 2 μm~ 8 μm, the initial distances between the tops of the two curved beams and the two straight beams are not equal; the width of the polysilicon beams is 2 μm to 8 μm, and the thickness is 1.5 μm to 3 μm; in the double polysilicon straight beam structure, the two straight beams (31 The total width of , 32) is equal to the width of each curved beam (21, 22) in the polysilicon curved beam structure. 3、根据权利要求1所述的测量多晶硅薄膜热膨胀系数的测量结构,其特征在于多晶硅直梁(31、32)的长为300μm~600μm,弯梁(21、22)长为300μm~600μm,所有弯梁与直梁夹角为0.01~0.05rad;且多晶硅弯梁的长度与多晶硅直梁的长度不相同。3. The measurement structure for measuring the thermal expansion coefficient of polysilicon thin films according to claim 1, characterized in that the length of the polysilicon straight beams (31, 32) is 300 μm to 600 μm, and the length of the curved beams (21, 22) is 300 μm to 600 μm. The angle between the curved beam and the straight beam is 0.01-0.05 rad; and the length of the polysilicon curved beam is different from that of the polysilicon straight beam. 4.一种用于权利要求1所述的测量多晶硅薄膜热膨胀系数的测量结构的测量方法,其特征在于该测量方法为:4. a measuring method for measuring the measuring structure of polysilicon thin film thermal expansion coefficient as claimed in claim 1, is characterized in that this measuring method is: a、制备测量梁结构,即制备一个双直梁结构和两个多晶硅弯梁结构,这两个弯梁的几何结构完全相同,但顶端离直梁的初始距离不同;a. Prepare the measuring beam structure, that is, prepare a double straight beam structure and two polysilicon curved beam structures. The geometric structures of the two curved beams are exactly the same, but the initial distances from the top to the straight beam are different; b、在室温时对直梁结构中的直梁(31、32)通入一微小电流I0,测量其两端的电压V0,根据关系式 V 0 I 0 = ρ 0 L 1 wh 得出在室温时长度为L1的多晶硅直梁的电阻率ρ0,再对直梁(31、32)中通入另一微小电流I1,测量其两端电压V1,根据关系式 V 1 I = ρ 1 L 1 wh 测量出在通入电流为I1时,长度为L1的多晶硅梁的电阻率ρ1b. At room temperature, pass a small current I 0 to the straight beams (31, 32) in the straight beam structure, and measure the voltage V 0 at both ends, according to the relationship V 0 I 0 = ρ 0 L 1 wh Obtain the resistivity ρ 0 of the polysilicon straight beam whose length is L 1 at room temperature, then pass another tiny current I 1 into the straight beam (31, 32), and measure the voltage V 1 at its two ends, according to the relationship V 1 I = ρ 1 L 1 wh Measure the resistivity ρ 1 of the polysilicon beam whose length is L 1 when the input current is I 1 , c、选择两弯梁结构组中的任一个弯梁,总长为L2,对其通入电流I2,测量其两端的电压V2,并根据关系式 V 2 I = ρ 2 L 2 wh 测量出通入电流为I2时,长度为L2的多晶硅弯梁的电阻率ρ2c. Select any curved beam in the two curved beam structure groups, the total length is L 2 , pass current I 2 to it, measure the voltage V 2 at both ends, and according to the relation V 2 I = ρ 2 L 2 wh Measure the resistivity ρ 2 of the polysilicon curved beam with length L 2 when the input current is I 2 , d、根据电阻率—平均温度增量的关系式:d. According to the relationship between resistivity and average temperature increment: ρ 1 ρ 0 - 1 ρ 2 ρ 0 - 1 = Δ T 1 Δ T 2 = [ mL 1 2 - tan ( mL 1 2 ) mL 1 2 / mL 2 2 - tan ( mL 2 2 ) mL 2 2 ] 得出m,m是中间参量。 ρ 1 ρ 0 - 1 ρ 2 ρ 0 - 1 = Δ T 1 Δ T 2 = [ mL 1 2 - the tan ( mL 1 2 ) mL 1 2 / mL 2 2 - the tan ( mL 2 2 ) mL 2 2 ] Get m, m is an intermediate parameter. e、通过关系式 m = η k p h - J 2 ρ 0 ξ k p 得出η、ρ0、ξ;η是多晶硅梁下表面的等效换热系数,ρ0是多晶硅梁在室温下的电阻率,ξ是多晶硅梁在室温下的温度系数,h是梁的厚度,kp是多晶硅的热导率,J是梁中的电流密度;e, through the relationship m = η k p h - J 2 ρ 0 ξ k p η, ρ 0 , ξ are obtained; η is the equivalent heat transfer coefficient of the lower surface of the polysilicon beam, ρ 0 is the resistivity of the polysilicon beam at room temperature, ξ is the temperature coefficient of the polysilicon beam at room temperature, and h is the thickness of the beam , k p is the thermal conductivity of polysilicon, J is the current density in the beam; f、对弯梁(21)的两端分别通入缓慢增加的电流,观察连接弯梁与直梁锚区的欧姆表的读数是否有一个从无穷大到有限值的跳变;如无,则说明两个梁还未发生接触,继续增大电流值;如有跳变,则说明两个梁已经发生了接触,记录下此刻通过电流值的大小,根据关系式 J = I wh 计算出电流密度J1,弯梁的移动距离是δ1+Δδ,其中,δ1是弯梁的实际移动距离,Δδ是误差项;f. To the two ends of the curved beam (21), feed slowly increasing currents respectively, and observe whether the reading of the ohmmeter connecting the curved beam and the anchorage area of the straight beam has a jump from infinity to a finite value; if there is no, it means The two beams have not been in contact yet, continue to increase the current value; if there is a jump, it means that the two beams have been in contact, record the current value passing through at this moment, according to the relationship J = I wh Calculate the current density J 1 , the moving distance of the curved beam is δ1+Δδ, where δ1 is the actual moving distance of the curved beam, and Δδ is the error term; g、对弯梁(22)重复以上步骤f,再记录另一组电流密度J2和移动距离δ2+Δδ,将以上参数代入关系式 ΔT = J 2 ρ 0 k p m 2 [ mL 2 - tanh ( mL 2 ) mL 2 ] , 并将两式相减,即g. Repeat the above step f for the curved beam (22), then record another set of current density J 2 and moving distance δ2+Δδ, and substitute the above parameters into the relational formula ΔT = J 2 ρ 0 k p m 2 [ mL 2 - tanh ( mL 2 ) mL 2 ] , and subtract the two equations, that is, (( δδ 11 ++ ΔδΔδ )) -- (( δδ 22 ++ ΔδΔδ )) == αα (( ΔTΔT 11 -- ΔTΔT 22 )) LL 22 coscos (( θθ )) (( LL 22 44 -- ww 22 )) LL 22 44 tanthe tan 22 (( θθ )) ++ ww 22 再根据上式,就可以得出热膨胀系数α。According to the above formula, the coefficient of thermal expansion α can be obtained. 5、根据权利要求4所述的测量多晶硅薄膜热膨胀系数的测量结构的测量方法,其特征在于测量梁结构的制备方法为:5. The method for measuring the measuring structure for measuring the coefficient of thermal expansion of polysilicon thin films according to claim 4, characterized in that the preparation method of the measuring beam structure is as follows: a、制备硅衬底,a. Prepare the silicon substrate, b、在硅衬底上淀积一层二氧化硅层,b. Deposit a layer of silicon dioxide on the silicon substrate, c、在二氧化硅层上淀积一层氮化硅层,c. Depositing a silicon nitride layer on the silicon dioxide layer, d、再氮化硅层上淀积一层硼硅玻璃牺牲层,d. Deposit a sacrificial layer of borosilicate glass on the silicon nitride layer, e、在硼硅玻璃牺牲层上面淀积多晶硅,e. Depositing polysilicon on the sacrificial layer of borosilicate glass, f、光刻出多晶硅梁,f. Photoetching polysilicon beams, g、在多晶硅层上淀积一层铝g. Deposit a layer of aluminum on the polysilicon layer h、光刻出锚区上的铝层以及直梁上的铝膜,h, photoetching the aluminum layer on the anchor area and the aluminum film on the straight beam, i、释放牺牲层。i. Release the sacrificial layer.
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CN102564650A (en) * 2011-12-20 2012-07-11 华中科技大学 Micro electro mechanical system (MEMS) sensor for measuring stress of phase-change memory and preparation process for MEMS sensor
CN102608149A (en) * 2012-01-10 2012-07-25 东南大学 Polycrystalline silicon CTE (Coefficient of Thermal Expansion) online test structure
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CN102564650A (en) * 2011-12-20 2012-07-11 华中科技大学 Micro electro mechanical system (MEMS) sensor for measuring stress of phase-change memory and preparation process for MEMS sensor
CN102608149A (en) * 2012-01-10 2012-07-25 东南大学 Polycrystalline silicon CTE (Coefficient of Thermal Expansion) online test structure
CN102608149B (en) * 2012-01-10 2014-06-11 东南大学 Polycrystalline silicon CTE (Coefficient of Thermal Expansion) online test structure
CN104359938A (en) * 2014-11-25 2015-02-18 中国建筑材料科学研究总院 Method for testing thermal expansion coefficient of coating
TWI676025B (en) * 2018-08-10 2019-11-01 國立中山大學 System and method for measuring a thermal expansion coefficient
CN112326721A (en) * 2020-10-30 2021-02-05 河海大学 Method for extracting thermal expansion coefficient of multilayer film

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