CN1613771A - Method for separating red mud from alumina stripping slurry - Google Patents
Method for separating red mud from alumina stripping slurry Download PDFInfo
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- CN1613771A CN1613771A CN 200410091475 CN200410091475A CN1613771A CN 1613771 A CN1613771 A CN 1613771A CN 200410091475 CN200410091475 CN 200410091475 CN 200410091475 A CN200410091475 A CN 200410091475A CN 1613771 A CN1613771 A CN 1613771A
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- red mud
- alumina
- liquid
- separating
- cyclone
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- 238000000034 method Methods 0.000 title claims abstract description 30
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 title claims abstract description 28
- 239000002002 slurry Substances 0.000 title claims abstract description 22
- 238000004090 dissolution Methods 0.000 claims abstract description 14
- 239000007787 solid Substances 0.000 claims abstract description 14
- 238000005406 washing Methods 0.000 claims abstract description 9
- 238000000926 separation method Methods 0.000 claims abstract description 8
- 239000007788 liquid Substances 0.000 claims abstract description 5
- 239000007791 liquid phase Substances 0.000 claims abstract description 4
- 239000000463 material Substances 0.000 claims abstract description 4
- 210000000582 semen Anatomy 0.000 claims abstract description 4
- 239000007790 solid phase Substances 0.000 claims abstract description 4
- 238000001914 filtration Methods 0.000 claims description 2
- KKCBUQHMOMHUOY-UHFFFAOYSA-N sodium oxide Chemical compound [O-2].[Na+].[Na+] KKCBUQHMOMHUOY-UHFFFAOYSA-N 0.000 abstract description 13
- 229910001948 sodium oxide Inorganic materials 0.000 abstract description 13
- 238000005245 sintering Methods 0.000 abstract description 11
- 238000004519 manufacturing process Methods 0.000 abstract description 4
- 229910001570 bauxite Inorganic materials 0.000 abstract description 2
- 239000002994 raw material Substances 0.000 abstract description 2
- TWNQGVIAIRXVLR-UHFFFAOYSA-N oxo(oxoalumanyloxy)alumane Chemical compound O=[Al]O[Al]=O TWNQGVIAIRXVLR-UHFFFAOYSA-N 0.000 description 13
- 239000005432 seston Substances 0.000 description 11
- 230000029087 digestion Effects 0.000 description 7
- 239000012530 fluid Substances 0.000 description 6
- 230000000694 effects Effects 0.000 description 3
- 238000003672 processing method Methods 0.000 description 3
- 206010039509 Scab Diseases 0.000 description 2
- 239000004744 fabric Substances 0.000 description 2
- 229910001710 laterite Inorganic materials 0.000 description 2
- 239000011504 laterite Substances 0.000 description 2
- 238000007086 side reaction Methods 0.000 description 2
- 238000004131 Bayer process Methods 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 230000018109 developmental process Effects 0.000 description 1
- 230000002349 favourable effect Effects 0.000 description 1
- 238000009776 industrial production Methods 0.000 description 1
- 230000008929 regeneration Effects 0.000 description 1
- 238000011069 regeneration method Methods 0.000 description 1
- 238000010517 secondary reaction Methods 0.000 description 1
- 238000004062 sedimentation Methods 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
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- Filtration Of Liquid (AREA)
- Compounds Of Alkaline-Earth Elements, Aluminum Or Rare-Earth Metals (AREA)
Abstract
一种氧化铝溶出料浆分离赤泥的方法，涉及一种采用铝土矿为原料生产氧化铝的工艺方法，特别是其中的烧结法高浓度熟料溶出料浆中赤泥的分离方法。其特征在于其分离过程是首先采用旋流器在3－10秒钟内分离出溶出料中70％－90％的赤泥，且赤泥的液固比为1.0－2.5，将分离出的赤泥进入常规的洗涤系统；同时将经旋流器分离赤泥后的溢出液用叶滤机钟过滤1－2分钟，液相送入精液槽，固相进入赤泥洗涤系统。烧结法氧化铝生产采用此赤泥快速分离的方法，可使氧化铝和氧化钠净溶出率提高2％，分别达到93％和94％。
A method for separating red mud from alumina dissolution slurry relates to a process for producing alumina using bauxite as a raw material, in particular a method for separating red mud from sintering high-concentration clinker dissolution slurry. It is characterized in that the separation process is to first use a cyclone to separate 70%-90% of the red mud in the dissolution material within 3-10 seconds, and the liquid-solid ratio of the red mud is 1.0-2.5, and the separated red mud The mud enters the conventional washing system; at the same time, the overflow liquid after the red mud is separated by the cyclone is filtered with a leaf filter for 1-2 minutes, the liquid phase is sent to the semen tank, and the solid phase enters the red mud washing system. Sintering alumina production adopts the method of rapid separation of red mud, which can increase the net dissolution rate of alumina and sodium oxide by 2%, reaching 93% and 94% respectively.
Description
Technical field
A kind of method of separating red mud from alumina stripping slurry, relating to a kind of bauxite that adopts is the processing method of raw material production aluminum oxide, particularly red mud separation method in the sintering process high concentration chamotte stripping slurry wherein.
Background technology
In alumina sintering method production process, after carrying out the grog stripping, red mud need be isolated system.In time isolate red mud, have to utilize and improve the usefulness of producing, and the more important thing is that aluminum oxide and the sodium oxide avoided in red mud and the solution carry out secondary reaction, cause that aluminum oxide and sodium oxide loss produce.At present, along with the development of alumina producing technology, the progressively industrialization of intensified sintering technology, intensified sintering grog stripping slurry concentration height has improved the usefulness of alumina producing greatly.But by the concentration height of the dissolution fluid of intensified sintering, the secondary side reaction of red mud and solution is more violent.Aluminum oxide and sodium oxide loss strengthen.At present, what adopt on the industrial production is settlement separate, and disengaging time is for usually needing more than 1 hour.Because red mud from sintering process scabs easily, have difficulties at aspects such as operation and spoil disposals, adopt sedimentation strainer, pressure filter, vacuum filter and plate-and-frame filter press, or adopt swirler and horizontal screw centrifuge combined equipment, all can't steady operation.Because aluminum oxide and sodium oxide loss are bigger, make the grog aluminum oxide of intensified sintering and sodium oxide net digestion efficiency reduce by 1.2% and 1.5% respectively, if further stripping concentration improves, loss will further increase.
Summary of the invention
The objective of the invention is deficiency at above-mentioned prior art existence, energy sharp separation red mud is provided, effectively reduce aluminum oxide and sodium oxide loss that the secondary side reaction causes, avoid because of red mud contain alkali and a kind of flow process of the equipment operation problem that brings of scabbing is reasonable, equipment simply, easy handling, red mud good separating effect and the stable high separating red mud from alumina stripping slurry processing method of digesting efficiency of alumina.
Method of the present invention is achieved through the following technical solutions.
A kind of method of separating red mud from alumina stripping slurry, it is characterized in that its sepn process is at first to adopt swirler to isolate the red mud of 70%-90% in the stripping material in second at 3-10, and the liquid-solid ratio of red mud is 1.0-2.5, and isolated red mud is entered conventional washing system; To filter 1-2 minute with the leaf filter clock through the spillage behind the swirler separating red mud simultaneously, liquid phase is sent into the seminal fluid groove, and solid phase enters the laterite washing system.
A kind of method of separating red mud from alumina stripping slurry is characterized in that its sepn process is to adopt swirler separation and spillage to use leaf filter clock filter time summation less than 2 minutes.
A kind of method of separating red mud from alumina stripping slurry is characterized in that the spillage behind the swirler separating red mud is to adopt the efficient leaf filter of full-automatic vertical to carry out filtering.
The feature of method of the present invention is that flow process is reasonable, equipment is simple, easy handling, red mud good separating effect and stable, digesting efficiency of alumina height.Method of the present invention makes disengaging time shorten to 2 minutes, and the thick liquid seston content of output is saved wash water and reached 30% less than 2g/L, and aluminum oxide and the raising of sodium oxide net digestion efficiency reach 2%, reach respectively more than 93% and 94%.
Method of the present invention adopts the efficient leaf filter of full-automatic vertical, owing to, need not to open machine barrel with the solution recoil regenerated filter fabric of header tank, and favorable regeneration effect not only, and can keep in the machine barrel temperature consistent with temperature of charge, filter cloth is difficult for knot firmly.
Method of the present invention is applicable to the alumina producer of sintering process, integrated process and bayer process, is particularly useful for alumina by sintering factory, effectively reduces alumina production cost and improves output, has good popularization and application prospect.
Description of drawings
The technical process of accompanying drawing processing method of the present invention.
Concrete embodiment
A kind of method of separating red mud from alumina stripping slurry, its sepn process are at first to adopt swirler to isolate the red mud of 70%-90% in the stripping material in second at 3-10, and the liquid-solid ratio of red mud is 1.0-2.5, and isolated red mud is entered conventional washing system; To filter 1-2 minute with the leaf filter clock through the spillage behind the swirler separating red mud simultaneously, liquid phase is sent into the seminal fluid groove, and solid phase enters the laterite washing system.Grog stripping slurry 3 is pumped into swirler 1, and stripping slurry 3 is by swirler 1 separating most red mud 4, and its overflow 5 enters the efficient leaf filter 2 further separating red muds of full-automatic vertical, and the solution of the efficient leaf filter output of full-automatic vertical is thick liquid 6.The mud cake 7 that swirler underflow 4 and leaf filter draw off directly enters washing system 8.
Example 1
Grog stripping slurry liquid-solid ratio is 13.5, dissolution fluid alumina concentration 125g/L, the swirler disengaging time is 4.2 seconds kinds, underflow liquid-solid ratio 1.4, the overflow seston is 15g/L, and the spillage behind the swirler separating red mud filtered 1 minute with the leaf filter clock, and the seston content of leaf filter output solution is 0.8g/L, total points is 1.8 minutes from the time, calculates aluminum oxide and sodium oxide net digestion efficiency and is respectively 93.2% and 94.8%.
Example 2
Grog stripping slurry liquid-solid ratio is 10.3, dissolution fluid alumina concentration 143g/L, the swirler disengaging time is 4.8 seconds kinds, underflow liquid-solid ratio 1.3, the overflow seston is 20g/L, and the spillage behind the swirler separating red mud filtered 2 minutes with the leaf filter clock, and the seston content of leaf filter output solution is 1.4g/L, total points is 1.8 minutes from the time, calculates aluminum oxide and sodium oxide net digestion efficiency and is respectively 93.0% and 94.3%.
Example 3
Grog stripping slurry liquid-solid ratio is 12, dissolution fluid alumina concentration 105g/L, the swirler disengaging time is 3.8 seconds kinds, underflow liquid-solid ratio 1.5, the overflow seston is 8g/L, and the spillage behind the swirler separating red mud filtered 1.5 minutes with the leaf filter clock, and the seston content of leaf filter output solution is 0.7g/L, total points is 1.6 minutes from the time, calculates aluminum oxide and sodium oxide net digestion efficiency and is respectively 93.8% and 95.2%.
Example 4
Grog stripping slurry liquid-solid ratio is 12, dissolution fluid alumina concentration 105g/L, the swirler disengaging time is 3 seconds kinds, underflow liquid-solid ratio 2.5, the overflow seston is 8g/L, and the spillage behind the swirler separating red mud filtered 1.8 minutes with the leaf filter clock, and the seston content of leaf filter output solution is 0.7g/L, total points is 1.6 minutes from the time, calculates aluminum oxide and sodium oxide net digestion efficiency and is respectively 93.8% and 95.2%.
Example 5
Grog stripping slurry liquid-solid ratio is 12, dissolution fluid alumina concentration 105g/L, the swirler disengaging time is 10 seconds kinds, underflow liquid-solid ratio 1.0, the overflow seston is 8g/L, and the spillage behind the swirler separating red mud filtered 2 minutes with the leaf filter clock, and the seston content of leaf filter output solution is 0.7g/L, total points is 1.6 minutes from the time, calculates aluminum oxide and sodium oxide net digestion efficiency and is respectively 93.8% and 95.2%.
Claims (3)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB2004100914752A CN1308241C (en) | 2004-11-25 | 2004-11-25 | Method for separating red mud from alumina stripping slurry |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB2004100914752A CN1308241C (en) | 2004-11-25 | 2004-11-25 | Method for separating red mud from alumina stripping slurry |
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| Publication Number | Publication Date |
|---|---|
| CN1613771A true CN1613771A (en) | 2005-05-11 |
| CN1308241C CN1308241C (en) | 2007-04-04 |
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| Application Number | Title | Priority Date | Filing Date |
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| CNB2004100914752A Expired - Lifetime CN1308241C (en) | 2004-11-25 | 2004-11-25 | Method for separating red mud from alumina stripping slurry |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1331555C (en) * | 2005-12-09 | 2007-08-15 | 贵阳铝镁设计研究院 | Red mud-filtering workshop arrangement method in alumina production line |
| CN100343172C (en) * | 2005-07-07 | 2007-10-17 | 贵阳铝镁设计研究院 | Tech. for filtering and transporting of red mud |
| CN100371248C (en) * | 2006-07-16 | 2008-02-27 | 山东铝业股份有限公司 | Red mud separating method for alumina producing Bayer process |
| CN100396383C (en) * | 2005-09-22 | 2008-06-25 | 贵阳铝镁设计研究院 | Coarse-fine red mud grading method |
Family Cites Families (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS5549115A (en) * | 1978-10-05 | 1980-04-09 | Nippon Light Metal Co Ltd | Pressure type leaf filter |
| AT401654B (en) * | 1994-10-14 | 1996-11-25 | Andritz Patentverwaltung | METHOD FOR DRAINING AND WASHING RED SLUDGE |
| CN1219702C (en) * | 2001-11-10 | 2005-09-21 | 中国长城铝业公司 | Red clay separating method for producing alumina by sintering process |
| CN1256279C (en) * | 2002-03-26 | 2006-05-17 | 中国铝业股份有限公司 | Red clay separation process for alumina sintering production |
-
2004
- 2004-11-25 CN CNB2004100914752A patent/CN1308241C/en not_active Expired - Lifetime
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN100343172C (en) * | 2005-07-07 | 2007-10-17 | 贵阳铝镁设计研究院 | Tech. for filtering and transporting of red mud |
| CN100396383C (en) * | 2005-09-22 | 2008-06-25 | 贵阳铝镁设计研究院 | Coarse-fine red mud grading method |
| CN1331555C (en) * | 2005-12-09 | 2007-08-15 | 贵阳铝镁设计研究院 | Red mud-filtering workshop arrangement method in alumina production line |
| CN100371248C (en) * | 2006-07-16 | 2008-02-27 | 山东铝业股份有限公司 | Red mud separating method for alumina producing Bayer process |
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| Publication number | Publication date |
|---|---|
| CN1308241C (en) | 2007-04-04 |
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Granted publication date: 20070404 |
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