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CN1691288A - Substrate cleaning apparatus and method - Google Patents

Substrate cleaning apparatus and method Download PDF

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Publication number
CN1691288A
CN1691288A CNA2005100679314A CN200510067931A CN1691288A CN 1691288 A CN1691288 A CN 1691288A CN A2005100679314 A CNA2005100679314 A CN A2005100679314A CN 200510067931 A CN200510067931 A CN 200510067931A CN 1691288 A CN1691288 A CN 1691288A
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substrate
space
gas
chamber
wafer
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CN100388430C (en
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守屋刚
中山博之
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Tokyo Electron Ltd
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    • H10P72/0402
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01JELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
    • H01J37/00Discharge tubes with provision for introducing objects or material to be exposed to the discharge, e.g. for the purpose of examination or processing thereof
    • H01J37/32Gas-filled discharge tubes
    • H01J37/32009Arrangements for generation of plasma specially adapted for examination or treatment of objects, e.g. plasma sources
    • H01J37/32082Radio frequency generated discharge
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01JELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
    • H01J37/00Discharge tubes with provision for introducing objects or material to be exposed to the discharge, e.g. for the purpose of examination or processing thereof
    • H01J37/32Gas-filled discharge tubes
    • H01J37/32431Constructional details of the reactor
    • H01J37/3266Magnetic control means
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01JELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
    • H01J37/00Discharge tubes with provision for introducing objects or material to be exposed to the discharge, e.g. for the purpose of examination or processing thereof
    • H01J37/32Gas-filled discharge tubes
    • H01J37/32431Constructional details of the reactor
    • H01J37/32798Further details of plasma apparatus not provided for in groups H01J37/3244 - H01J37/32788; special provisions for cleaning or maintenance of the apparatus
    • H01J37/32816Pressure
    • H01J37/32834Exhausting
    • H10P70/20
    • H10P70/56

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  • Engineering & Computer Science (AREA)
  • Plasma & Fusion (AREA)
  • Chemical & Material Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Cleaning Or Drying Semiconductors (AREA)
  • Drying Of Semiconductors (AREA)
  • Plasma Technology (AREA)

Abstract

本发明提供一种不损伤基板,可以充分去除附着于基板的背面的异物的基板清洗装置。作为基板清洗装置的等离子体处理装置(1)备有:腔室(10);配置于该腔室(10)内并载置晶片(W)的基座(11);配置于该基座(11),施加高电压的电极板(20);给所述腔室(10)内排气的粗排放管线;在基座(11)和晶片(W)之间产生空间(S)的顶推销(30);把N2气体供给到空间(S)的传热气体供给孔(27),和向腔室10内导入处理气体等的浇淋头(33),在生成空间S时,极性不同的高电压交互地施加于电极板(20),N2气体向着晶片(W)的背面喷出到空间(S),并且腔室(10)内被排气,进而在腔室(10)内被减压时,N2气体向腔室(10)导入。

Figure 200510067931

The present invention provides a substrate cleaning device capable of sufficiently removing foreign matter adhering to the back surface of the substrate without damaging the substrate. A plasma processing apparatus (1) as a substrate cleaning apparatus includes: a chamber (10); a susceptor (11) disposed in the chamber (10) on which a wafer (W) is placed; disposed on the susceptor ( 11), Electrode plates (20) for applying high voltage; rough discharge lines for degassing the chamber (10); push pins for creating space (S) between susceptor (11) and wafer (W) (30); N2 gas is supplied to the heat transfer gas supply hole (27) of the space (S), and the pouring head (33) that introduces processing gas etc. in the chamber 10, when generating the space S, the polarity Different high voltages are alternately applied to the electrode plate (20), N gas is ejected to the space (S) toward the back side of the wafer (W), and the chamber (10) is exhausted, and then in the chamber (10) When the inside is depressurized, N2 gas is introduced into the chamber (10).

Figure 200510067931

Description

基板清洗装置和基板清洗方法Substrate cleaning device and substrate cleaning method

技术领域technical field

本发明涉及基板清洗装置和基板清洗方法,特别是涉及去除附着于施加了等离子体处理的基板的背面的异物的基板清洗装置和基板清洗方法。The present invention relates to a substrate cleaning device and a substrate cleaning method, and more particularly, to a substrate cleaning device and a substrate cleaning method for removing foreign matter adhering to the back surface of a substrate subjected to plasma treatment.

背景技术Background technique

通常,在半导体器件的制造过程中,对作为被处理体的半导体晶片(以下称为‘晶片’),施行蚀刻或溅射、CVD(化学气相成长)等用等离子体的处理(以下称为‘等离子体处理’)。Generally, in the manufacturing process of a semiconductor device, a semiconductor wafer (hereinafter referred to as "wafer") as an object to be processed is subjected to plasma processing (hereinafter referred to as "wafer") such as etching or sputtering, CVD (chemical vapor phase growth), etc. plasma treatment').

例如,用来施行蚀刻处理的等离子体处理装置80,如图8中所示,备有:收容晶片的圆筒形容器81,配置于该圆筒形容器81的内部,作为载置晶片的载置台的基座82,与载置晶片的面(以下称为‘载置面’)相对并配置成贯通基座82的顶推销83。基座82在载置面上配置有连接于直流电源84的电极的静电卡盘85,进而,在其内部,有连接于高频电源86的下部电极87(例如,参照专利文献1)。For example, as shown in FIG. 8, a plasma processing apparatus 80 for performing an etching process includes a cylindrical container 81 for accommodating wafers, which is arranged inside the cylindrical container 81 as a carrier for placing wafers. The base 82 of the stage is opposed to the surface on which the wafer is placed (hereinafter referred to as "placement surface"), and is arranged so that the ejector pins 83 of the base 82 penetrate therethrough. The susceptor 82 has an electrostatic chuck 85 connected to an electrode of a DC power source 84 disposed on the mounting surface, and further has a lower electrode 87 connected to a high frequency power source 86 therein (for example, refer to Patent Document 1).

在等离子体处理装置80中,静电卡盘85靠静电吸附力把晶片吸附于载置面后,把高频电力施加于下部电极87,在圆筒形容器81内的上面与基座82之间产生高频电场,使导入圆筒形容器81内的处理气体分离而产生等离子体。产生的等离子体靠围着晶片的周缘配置的聚集环(未图示)聚集于晶片的表面,蚀刻在晶片的表面上所形成的氧化膜。In the plasma processing device 80, after the electrostatic chuck 85 adsorbs the wafer on the mounting surface by the electrostatic adsorption force, high-frequency power is applied to the lower electrode 87, between the upper surface of the cylindrical container 81 and the base 82. A high-frequency electric field is generated to separate the processing gas introduced into the cylindrical container 81 to generate plasma. The generated plasma is condensed on the surface of the wafer by means of a condensing ring (not shown) arranged around the periphery of the wafer to etch the oxide film formed on the surface of the wafer.

此外,施行了蚀刻处理的晶片,靠顶推销83从载置面抬起,由进入圆筒形容器81的关节臂(Scalar arm)等搬送装置(未图示)从圆筒形容器81中搬出。In addition, the wafer subjected to the etching process is lifted from the mounting surface by the push pin 83, and is carried out from the cylindrical container 81 by a transfer device (not shown) such as a scalar arm entering the cylindrical container 81. .

在蚀刻处理中产生的等离子体当中,未聚集于晶片的表面者,碰撞于圆筒形容器81的内壁而产生颗粒。此外,在蚀刻处理中,产生反应生成物。虽然这些颗粒或反应生成物其大部分靠未图示的排气装置从圆筒形容器81中排出,但是残留于圆筒形容器81内的一部分颗粒或反应生成物堆积于载置面。此外,基座82起因于等离子体等而产生的颗粒也堆积于载置面。这些堆积于载置面的颗粒或反应生成物在晶片载置于载置面时,作为异物附着于晶片背面。作为这种附着于晶片背面的颗粒或反应生成物的去除方法,用清洗液等的湿清洗是公知的。Among the plasma generated in the etching process, those not collected on the surface of the wafer collide with the inner wall of the cylindrical container 81 to generate particles. In addition, during the etching process, reaction products are generated. Most of these particles or reaction products are exhausted from the cylindrical container 81 by an exhaust device (not shown), but a part of the particles or reaction products remaining in the cylindrical container 81 accumulates on the mounting surface. In addition, particles generated in the susceptor 82 due to plasma or the like are also deposited on the mounting surface. These particles or reaction products accumulated on the mounting surface adhere to the back surface of the wafer as foreign matter when the wafer is mounted on the mounting surface. Wet cleaning with a cleaning solution or the like is known as a method for removing such particles and reaction products adhering to the back surface of the wafer.

此外,作为不使用清洗液的方法,在靠顶推销抬起来的晶片与载置面之间产生等离子体,通过产生的等离子体的离子的溅射的作用,或自由基引起的化学反应的作用去除晶片背面的颗粒的去除方法也是公知的(例如,参照专利文献2)。In addition, as a method that does not use cleaning liquid, plasma is generated between the wafer lifted by the push pin and the mounting surface, and the action of ion sputtering by the generated plasma, or the action of chemical reaction caused by radicals A method for removing particles on the back surface of a wafer is also known (for example, refer to Patent Document 2).

【专利文献1】特开平5-226291号公报(图1)[Patent Document 1] Japanese Unexamined Patent Publication No. 5-226291 (Fig. 1)

【专利文献2】美国专利第4962049号公报(第二栏第67行至第三栏第17行)[Patent Document 2] U.S. Patent No. 4,962,049 (line 67 of the second column to line 17 of the third column)

但是,如果反复晶片清洗则清洗液被污染。因而,存在着因在晶片清洗中被污染的清洗液中所含有的颗粒等晶片表面被污染这样的问题。此外,蚀刻处理所施加的晶片被搬入下道工序的腔室时,未去除的颗粒有时污染该腔室内部。However, if wafer cleaning is repeated, the cleaning solution becomes contaminated. Therefore, there is a problem that the surface of the wafer is contaminated by particles or the like contained in the cleaning liquid contaminated during the cleaning of the wafer. In addition, when the wafer to which the etching process has been applied is carried into a subsequent chamber, unremoved particles may contaminate the interior of the chamber.

此外,在靠等离子体去除晶片背面的颗粒的场合,由产生的等离子体对晶片表面施行过度的等离子体处理而损伤晶片。例如,存在着对晶片表面施行过度的蚀刻处理而产生过度蚀刻这样的问题。In addition, when plasma is used to remove particles on the back surface of the wafer, the generated plasma performs excessive plasma treatment on the wafer surface and damages the wafer. For example, there is a problem in that excessive etching is performed on the surface of the wafer and excessive etching occurs.

发明内容Contents of the invention

本发明的目的在于提供一种不损伤基板,可以充分去除附着于基板的背面的异物的基板清洗装置和基板清洗方法。An object of the present invention is to provide a substrate cleaning device and a substrate cleaning method capable of sufficiently removing foreign matter adhering to the back surface of the substrate without damaging the substrate.

为了实现上述目的,技术方案1所述的基板清洗装置,其特征在于,备有:收容基板的收容室;配置于该收容室内,载置前述基板的载置台;配置于该载置台,施加电压时把前述基板吸附于前述载置台的电极;对前述收容室内进行排气的排气装置;使该载置台和前述基板离开而在前述载置台和前述基板之间产生空间的分开装置;以及把气体供给到前述空间的气体供给装置,在产生前述空间时,电压施加于前述电极,前述气体供给装置把气体供给到前述空间,前述排气装置对前述收容室进行排气。In order to achieve the above object, the substrate cleaning device according to technical solution 1 is characterized in that it is equipped with: a storage chamber for storing the substrate; a mounting table arranged in the storage chamber to mount the substrate; an electrode for adsorbing the substrate to the mounting table; an exhaust device for exhausting the chamber; a separation device for separating the mounting table from the substrate to create a space between the mounting table and the substrate; and The gas supply device for supplying gas to the space applies a voltage to the electrodes when the space is created, the gas supply device supplies gas to the space, and the exhaust device exhausts the storage chamber.

技术方案2所述的基板清洗装置,其特征在于,在技术方案1所述的基板清洗装置中,还备有在前述收容室内被减压且产生前述空间时,把气体导入前述收容室内的气体导入部。The substrate cleaning apparatus according to claim 2 is characterized in that, in the substrate cleaning apparatus according to claim 1, a gas that introduces the gas into the storage chamber when the pressure in the storage chamber is reduced and the space is created is further provided. import department.

技术方案3所述的基板清洗装置,其特征在于,在技术方案1或2所述的基板清洗装置中,电压不连续地施加于前述电极。The substrate cleaning device according to claim 3 is characterized in that, in the substrate cleaning device according to claim 1 or 2, a voltage is applied discontinuously to the electrodes.

技术方案4所述的基板清洗装置,其特征在于,在技术方案3所述的基板清洗装置中,极性不同的电压交互地施加于前述电极。The substrate cleaning device according to claim 4 is characterized in that, in the substrate cleaning device according to claim 3 , voltages with different polarities are alternately applied to the electrodes.

技术方案5所述的基板清洗装置,其特征在于,在技术方案4所述的基板清洗装置中,前述电压的绝对值为500V以上。The substrate cleaning device according to claim 5 is characterized in that, in the substrate cleaning device according to claim 4 , the absolute value of the voltage is 500 V or more.

技术方案6所述的基板清洗装置,其特征在于,在技术方案5所述的基板清洗装置中,前述电压的绝对值为2kV以上。The substrate cleaning device according to claim 6 is characterized in that, in the substrate cleaning device according to claim 5 , the absolute value of the voltage is 2 kV or more.

技术方案7所述的基板清洗装置,其特征在于,在技术方案1至6中的任何一项中所述的基板清洗装置中,前述排气装置在产生前述空间时,把前述收容室内的压力保持于133Pa以上。The substrate cleaning device according to technical solution 7 is characterized in that, in the substrate cleaning device described in any one of technical solutions 1 to 6, when the aforementioned exhaust device generates the aforementioned space, the pressure in the aforementioned storage chamber Keep it above 133Pa.

技术方案8所述的基板清洗装置,其特征在于,在技术方案7所述的基板清洗装置中,其特征在于,前述排气装置在产生前述空间时,把前述收容室内的压力保持于1.33×103~1.33×104Pa的范围内。The substrate cleaning device according to claim 8 is characterized in that, in the substrate cleaning device according to claim 7, the exhaust device maintains the pressure in the storage chamber at 1.33× when the space is created. In the range of 10 3 to 1.33×10 4 Pa.

为了实现上述目的,技术方案9所述的基板清洗装置,其特征在于,备有:收容基板的收容室;配置于该收容室内,载置前述基板的载置台;对前述收容室内进行排气的排气装置;使该载置台和前述基板离开而在前述载置台和前述基板之间产生空间,并且接触于前述基板而把电压施加于前述基板的分开装置;把气体供给到前述空间的气体供给装置;和将气体导入前述收容室内的气体导入装置,在产生前述空间时,电压施加于前述基板,前述气体供给装置把气体供给到前述空间,前述排气装置对前述收容室进行排气,进而,在前述收容室内被减压且产生前述空间时,前述气体导入部把气体导入前述收容室内。In order to achieve the above object, the substrate cleaning apparatus according to claim 9 is characterized in that it includes: a storage chamber for storing the substrate; a mounting table arranged in the storage chamber on which the substrate is placed; Exhaust device; separation device for separating the mounting table and the substrate to create a space between the mounting table and the substrate, and contacting the substrate to apply voltage to the substrate; gas supply for supplying gas to the space device; and a gas introduction device for introducing gas into the aforementioned storage chamber, when the aforementioned space is generated, a voltage is applied to the aforementioned substrate, the aforementioned gas supply device supplies gas to the aforementioned space, and the aforementioned exhaust device exhausts the aforementioned storage chamber, and When the pressure in the storage chamber is reduced and the space is created, the gas introduction part introduces gas into the storage chamber.

为了实现上述目的,技术方案10所述的基板清洗方法,是去除附着于基板的背面的异物的基板清洗方法,其特征在于,其中包括:把基板收容于收容室的收容步骤;把前述基板载置于配置于前述收容室的载置台的载置步骤;使前述载置台和前述基板离开以便在前述载置台和前述基板之间产生空间的离开步骤;在产生前述空间时,把电压施加于配置于前述载置台的电极的电压施加步骤;在产生前述空间时,把气体供给到前述空间的气体供给步骤;和在产生前述空间时,给前述收容室内排气的排气步骤。In order to achieve the above object, the substrate cleaning method described in technical solution 10 is a substrate cleaning method for removing foreign matter adhering to the back surface of the substrate, which is characterized in that it includes: a storage step of storing the substrate in a storage chamber; A placing step of placing the mounting table arranged in the aforementioned storage chamber; a separating step of separating the aforementioned mounting table and the aforementioned substrate so as to create a space between the aforementioned mounting table and the aforementioned substrate; when creating the aforementioned space, applying a voltage to the placement a step of applying a voltage to the electrodes of the mounting table; a gas supply step of supplying gas to the space when the space is created; and an exhaust step of exhausting the air in the housing when the space is created.

技术方案11所述的基板清洗方法,其特征在于,在技术方案10所述的基板清洗方法中,还包括在前述收容室内被减压且产生前述空间时,把气体导入前述收容室内的气体导入步骤。The method for cleaning a substrate according to claim 11 is characterized in that, in the method for cleaning a substrate according to claim 10 , further comprising a gas introduction method for introducing gas into the storage chamber when the pressure in the storage chamber is reduced and the space is created. step.

技术方案12所述的基板清洗方法,其特征在于,在技术方案10或11所述的基板清洗方法中,在前述电压施加步骤里,把电压不连续地施加于前述电极。The substrate cleaning method according to claim 12 is characterized in that, in the substrate cleaning method according to claim 10 or 11, in the voltage applying step, a voltage is applied discontinuously to the electrodes.

技术方案13所述的基板清洗方法,其特征在于,在技术方案12所述的基板清洗方法中,在前述电压施加步骤里,把极性不同的电压交互地施加于前述电极。The substrate cleaning method according to claim 13 is characterized in that, in the substrate cleaning method according to claim 12, in the voltage applying step, voltages with different polarities are alternately applied to the electrodes.

为了实现上述目的,技术方案14中所述的基板清洗方法,是去除附着于基板的背面的异物的基板清洗方法,其特征在于,其中包括:把基板收容于收容室的收容步骤;把前述基板载置于配置于前述收容室的载置台的载置步骤;使前述载置台和前述基板离开以便在前述载置台和前述基板之间产生空间的离开步骤;在产生前述空间时,把电压施加于前述基板的电压施加步骤;在产生前述空间时,把气体供给到前述空间的气体供给步骤;在产生前述空间时,给前述收容室内排气的排气步骤;以及在前述收容室内被减压且产生前述空间时,把气体导入前述收容室内的气体导入步骤。In order to achieve the above object, the substrate cleaning method described in technical solution 14 is a substrate cleaning method for removing foreign matter adhering to the back surface of the substrate, which is characterized in that it includes: a storage step of storing the substrate in a storage chamber; a step of placing on a stage arranged in the storage chamber; a step of separating the stage and the substrate so as to create a space between the stage and the substrate; when creating the space, applying a voltage to A step of applying a voltage to the substrate; a gas supply step of supplying gas to the space when the space is created; an exhaust step of exhausting the inside of the storage room when the space is created; and depressurizing and A gas introducing step of introducing gas into the aforementioned storage chamber when the aforementioned space is generated.

如果用技术方案1所述的基板清洗装置,则因为在载置台和基板之间产生空间时,电压施加于配置于载置台的电极,故在上述空间中产生静电场而静电的应力作用于基板的背面。借此,附着于基板的背面的异物脱离。此外,因为在产生上述空间时,气体供给到空间,收容室内被排气,故在空间中产生气流,脱离的异物靠该气流从空间中被排出,进而从收容室被排气。因而,基板清洗装置可以不损伤基板而充分去除附着于基板的背面的异物。If the substrate cleaning device described in claim 1 is used, when a space is created between the mounting table and the substrate, a voltage is applied to the electrodes arranged on the mounting table, so an electrostatic field is generated in the space and electrostatic stress acts on the substrate. The back. Thereby, the foreign matter adhering to the back surface of the substrate is detached. In addition, when the above-mentioned space is created, gas is supplied to the space and the storage chamber is exhausted, so an airflow is generated in the space, and the detached foreign objects are discharged from the space by the airflow, and then exhausted from the storage chamber. Therefore, the substrate cleaning apparatus can sufficiently remove foreign matter adhering to the back surface of the substrate without damaging the substrate.

如果用技术方案2所述的基板清洗装置,则由于在收容室内被减压时,气体被导入收容室内,所以在收容室内产生行进冲击波,附着于基板的背面的异物靠该冲击波向空间脱离。因而,可以不损伤基板而高效率地去除附着于基板的背面的异物。According to the substrate cleaning device according to claim 2, since the gas is introduced into the storage chamber when the storage chamber is depressurized, a traveling shock wave is generated in the storage chamber, and foreign matter adhering to the back surface of the substrate is separated into the space by the shock wave. Therefore, foreign matter adhering to the back surface of the substrate can be efficiently removed without damaging the substrate.

如果用技术方案3所述的基板清洗装置,则因为电压不连续地施加于电极,故向基板的电压的施加反复。借此,静电的应力反复作用于基板的背面。因而,可以更充分地去除附着于基板的背面的异物。According to the substrate cleaning device according to claim 3, since the voltage is applied discontinuously to the electrodes, the application of the voltage to the substrate is repeated. Thus, electrostatic stress repeatedly acts on the back surface of the substrate. Therefore, foreign matter adhering to the back surface of the substrate can be more sufficiently removed.

如果用技术方案4所述的基板清洗装置,则因为极性不同的电压交互地施加,故可以防止基板的带电。如果基板带电,则通过电压的施加作用于基板的背面的电气的应力减小。因而,通过防止基板的带电,可以防止附着于基板的背面的异物的去除效率的降低。According to the substrate cleaning device according to claim 4, since voltages with different polarities are alternately applied, electrification of the substrate can be prevented. When the substrate is charged, the electrical stress acting on the back surface of the substrate due to the application of the voltage is reduced. Therefore, by preventing the electrification of the substrate, it is possible to prevent a reduction in the removal efficiency of foreign matter adhering to the back surface of the substrate.

如果用技术方案5所述的基板清洗装置,则因为在产生空间时施加于电极的电压为500V以上,故可以加大作用于基板的背面的电气的应力,可以可靠地进行异物的脱离。According to the substrate cleaning device described in claim 5, since the voltage applied to the electrode is 500 V or more when the space is created, the electrical stress acting on the back surface of the substrate can be increased, and the foreign matter can be reliably detached.

如果用技术方案6所述的基板清洗装置,则因为上述电压为2kV以上,故可以更加加大上述静电的应力。If the substrate cleaning device described in claim 6 is used, since the above-mentioned voltage is 2 kV or more, the above-mentioned electrostatic stress can be further increased.

如果用技术方案7所述的基板清洗装置,则因为排气装置把收容室内的压力保持于133Pa以上,故在空间中可以产生气体粘性力大的粘性流。从基板的背面脱离的异物被卷入粘性流而与收容室内的气体一起从收容室中被排气。因而,可以可靠地去除附着于基板的背面的异物。If the substrate cleaning device described in claim 7 is used, since the exhaust device maintains the pressure in the storage chamber at 133 Pa or higher, a viscous flow with a large gas viscous force can be generated in the space. The foreign matter detached from the back surface of the substrate is drawn into the viscous flow and exhausted from the storage chamber together with the gas in the storage chamber. Thus, foreign matter adhering to the back surface of the substrate can be reliably removed.

如果用技术方案8所述的基板清洗装置,则因为排气装置把收容室内的压力保持于1.33×103~1.33×104Pa的范围内,故在空间中可以可靠地产生粘性流。According to the substrate cleaning device according to claim 8, since the exhaust device maintains the pressure in the storage chamber within the range of 1.33×10 3 to 1.33×10 4 Pa, viscous flow can be reliably generated in the space.

如果用技术方案9所述的基板清洗装置,则因为在载置台和基板之间产生空间时,分开装置把电压施加于基板,故在上述空间中产生静电场而静电的应力作用于基板的背面。借此,附着于基板的背面的异物脱离。进而,因为在产生空间且收容室内被减压时,气体导入部把气体导入收容室内,故在收容室内产生行进冲击波,附着于基板的背面的异物靠该冲击波向空间脱离。此外,因为在产生上述空间时,气体供给到空间,收容室内被排气,故在空间中产生气流,脱离的异物被该气流从空间中排出,进而从收容室中排气。因而,基板清洗装置,可以不损伤基板而充分去除附着于基板的背面的异物。If the substrate cleaning device described in technical scheme 9 is used, since the separation device applies a voltage to the substrate when a space is generated between the mounting table and the substrate, an electrostatic field is generated in the space and electrostatic stress acts on the back surface of the substrate. . Thereby, the foreign matter adhering to the back surface of the substrate is detached. Furthermore, when a space is created and the chamber is decompressed, the gas introduction unit introduces gas into the chamber, so a traveling shock wave is generated in the chamber, and foreign matter adhering to the back surface of the substrate escapes into the space by the shock wave. In addition, when the above-mentioned space is created, gas is supplied into the space and the storage chamber is exhausted, so an airflow is generated in the space, and the detached foreign matter is discharged from the space by the airflow, and then exhausted from the storage chamber. Therefore, the substrate cleaning apparatus can sufficiently remove foreign matter adhering to the back surface of the substrate without damaging the substrate.

如果用技术方案10所述的基板清洗方法,则因为在载置台和基板之间产生空间时,电压施加于设置于载置台的电极,故在上述空间中产生静电场而静电的应力作用于基板的背面。借此,附着于基板的背面的异物脱离。此外,因为在产生上述空间时,气体供给到空间,收容室内被排气,故在空间中产生气流,脱离的异物靠该气流从空间被排出,进而从收容室中被排气。因而,可以不损伤基板而充分去除附着于基板的背面的异物。If the substrate cleaning method described in claim 10 is used, since a voltage is applied to electrodes provided on the mounting table when a space is generated between the mounting table and the substrate, an electrostatic field is generated in the space and electrostatic stress acts on the substrate. The back. Thereby, the foreign matter adhering to the back surface of the substrate is detached. In addition, when the above-mentioned space is created, gas is supplied into the space and the storage chamber is exhausted, so an airflow is generated in the space, and the detached foreign objects are discharged from the space by the airflow, and then exhausted from the storage chamber. Therefore, foreign matter adhering to the back surface of the substrate can be sufficiently removed without damaging the substrate.

如果用技术方案11所述的基板清洗方法,则由于在产生上述空间且收容室内被减压时,气体被导入收容室内,所以在收容室内产生行进冲击波,附着于基板的背面的异物靠该冲击波向空间脱离。因而,可以不损伤基板而高效率地去除附着于基板的背面的异物。If the substrate cleaning method described in claim 11 is used, since the gas is introduced into the storage chamber when the above-mentioned space is generated and the storage chamber is decompressed, a traveling shock wave is generated in the storage chamber, and the foreign matter adhering to the back surface of the substrate is moved by the shock wave. Get out of space. Therefore, foreign matter adhering to the back surface of the substrate can be efficiently removed without damaging the substrate.

如果用技术方案12所述的基板清洗方法,则因为电压不连续地施加于电极,故向基板的电压的施加反复。借此,静电的应力反复作用于基板的背面。因而,可以更充分地去除附着于基板的背面的异物。According to the substrate cleaning method described in claim 12, since the voltage is applied discontinuously to the electrodes, the application of the voltage to the substrate is repeated. Thus, electrostatic stress repeatedly acts on the back surface of the substrate. Therefore, foreign matter adhering to the back surface of the substrate can be more sufficiently removed.

如果用技术方案13所述的基板清洗方法,则因为极性不同的电压交互地施加,故可以防止基板的带电。如果基板带电,则通过电压的施加作用于基板的背面的电气的应力减小。因而,通过防止基板的带电,可以防止附着于基板的背面的异物的去除效率的降低。According to the substrate cleaning method described in claim 13, since voltages with different polarities are alternately applied, electrification of the substrate can be prevented. When the substrate is charged, the electrical stress acting on the back surface of the substrate due to the application of the voltage is reduced. Therefore, by preventing the electrification of the substrate, it is possible to prevent a reduction in the removal efficiency of foreign matter adhering to the back surface of the substrate.

如果用技术方案14所述的基板清洗方法,则因为在载置台和基板之间产生空间时,电压施加于基板,故在上述空间中产生静电场而静电的应力作用于基板的背面。借此,附着于基板的背面的异物脱离。进而,因为在产生空间且收容室内被减压时,气体导入收容室内,故在收容室内产生行进冲击波,附着于基板的背面的异物靠该冲击波向空间脱离。此外,因为在产生上述空间时,气体供给到空间,收容室内被排气,故在空间中产生气流,脱离的异物被该气流从空间中排出,进而从收容室中排气。因而,可以不损伤基板而充分去除附着于基板的背面的异物。According to the substrate cleaning method described in claim 14, since a voltage is applied to the substrate when a space is created between the stage and the substrate, an electrostatic field is generated in the space and electrostatic stress acts on the back surface of the substrate. Thereby, the foreign matter adhering to the back surface of the substrate is detached. Furthermore, when a space is created and the chamber is depressurized, gas is introduced into the chamber, so a traveling shock wave is generated in the chamber, and foreign matter adhering to the back surface of the substrate escapes into the space by the shock wave. In addition, when the above-mentioned space is created, gas is supplied into the space and the storage chamber is exhausted, so an airflow is generated in the space, and the detached foreign matter is discharged from the space by the airflow, and then exhausted from the storage chamber. Therefore, foreign matter adhering to the back surface of the substrate can be sufficiently removed without damaging the substrate.

附图说明Description of drawings

图1是表示作为根据本发明的第一实施方式的基板清洗装置的等离子体处理装置的概略构成的截面图。1 is a cross-sectional view showing a schematic configuration of a plasma processing apparatus as a substrate cleaning apparatus according to a first embodiment of the present invention.

图2是图1的等离子体处理装置中所实行的基板清洗处理的顺序图。FIG. 2 is a sequence diagram of a substrate cleaning process performed in the plasma processing apparatus of FIG. 1 .

图3是表示作为根据本发明的第二实施方式的基板清洗装置的等离子体处理装置中的顶推销的概略构成的图。3 is a diagram showing a schematic configuration of a push pin in a plasma processing apparatus as a substrate cleaning apparatus according to a second embodiment of the present invention.

图4是表示根据本发明的第三实施方式的基板清洗装置的概略构成的截面图。4 is a cross-sectional view showing a schematic configuration of a substrate cleaning apparatus according to a third embodiment of the present invention.

图5是表示图4的基板处理装置所配置的基板处理系统的概略构成的图。FIG. 5 is a diagram showing a schematic configuration of a substrate processing system disposed in the substrate processing apparatus of FIG. 4 .

图6是示意地表示本发明的实施例中的从晶片的背面的去除颗粒的情形的图,图6(a)是示意地表示在阀V1打开期间,向电极板20反复交互施加+2kV和-2kV的电压的场合的空间S的情形的图,图6(b)是示意地表示从图6(a)开始经过数秒后的空间S的情形的图,图6(c)是示意地表示从图6(b)开始经过数秒后的空间S的情形的图。Fig. 6 is a diagram schematically showing the situation of removing particles from the back side of the wafer in an embodiment of the present invention. Fig. 6(a) schematically shows that +2kV and Figure 6(b) is a diagram schematically showing the situation of the space S after a few seconds have elapsed from FIG. 6(a), and FIG. 6(c) is a diagram schematically showing A diagram of the state of the space S after a few seconds have elapsed from FIG. 6( b ).

图7是表示本发明的实施例中的颗粒的去除的观测结果的曲线。Fig. 7 is a graph showing observation results of particle removal in Examples of the present invention.

图8是表示历来的用来对晶片施行蚀刻处理的等离子体处理装置的概略构成的图。FIG. 8 is a diagram showing a schematic configuration of a conventional plasma processing apparatus for etching a wafer.

符号说明:1、56等离子体处理装置;10、43腔室;11基座;12、65排气路;13隔板;14APC(自动压力控制阀);15TMP(涡轮分子泵);16、46DP(干式泵);17、45排气管;18高频电源;19匹配器;20、35、47电极板;22、41、48直流电源;24聚集环;25冷却介质室;26配管;27传热气体供给孔;28传热气体供给线;29传热气体供给管;30、40顶推销;31、52搬入搬出口;32、53门阀;33浇淋头;34通气孔;36电极支撑体;37缓冲室;38处理气体导入管;39磁铁;42基板清洗装置;44工作台;49气体供给孔;50气体供给线;51销子;54气体导入管;55基板处理系统;57、62搬送臂;58负载锁定室;59处理站;60负载端口;61方位器;63负载单元;64气体供给管。Explanation of symbols: 1, 56 plasma processing device; 10, 43 chamber; 11 base; 12, 65 exhaust path; 13 partition; 14APC (automatic pressure control valve); 15TMP (turbomolecular pump); 16, 46DP (dry pump); 17, 45 exhaust pipe; 18 high-frequency power supply; 19 matcher; 20, 35, 47 electrode plate; 22, 41, 48 DC power supply; 24 gathering ring; 25 cooling medium chamber; 26 piping; 27 heat transfer gas supply hole; 28 heat transfer gas supply line; 29 heat transfer gas supply pipe; 30, 40 push pins; 37 buffer chamber; 38 processing gas introduction pipe; 39 magnet; 42 substrate cleaning device; 44 worktable; 49 gas supply hole; 50 gas supply line; 51 pin; 54 gas introduction pipe; 55 substrate processing system; 57 , 62 transfer arm; 58 load lock chamber; 59 processing station; 60 load port; 61 positioner; 63 load unit; 64 gas supply pipe.

具体实施方式Detailed ways

下面,参照附图就本发明的实施方式进行说明。Hereinafter, embodiments of the present invention will be described with reference to the drawings.

首先,就作为根据本发明的第一实施方式的基板清洗装置的等离子体处理装置进行详述。First, a plasma processing apparatus as a substrate cleaning apparatus according to a first embodiment of the present invention will be described in detail.

图1是表示作为根据本发明的第一实施方式的基板清洗装置的等离子体处理装置的概略构成的截面图。1 is a cross-sectional view showing a schematic configuration of a plasma processing apparatus as a substrate cleaning apparatus according to a first embodiment of the present invention.

在图1中,作为对晶片W施行蚀刻处理的蚀刻处理装置所构成的等离子体处理装置1有金属制,例如,铝或不锈钢制的圆筒形腔室(收容室)10,在该腔室10内,设有作为载置晶片W的工作台的圆柱形的基座(载置台)11。In FIG. 1, a plasma processing apparatus 1 constituted as an etching processing apparatus for performing etching processing on a wafer W has a metal, for example, a cylindrical chamber (accommodating chamber) 10 made of aluminum or stainless steel. Inside 10, a cylindrical susceptor (mounting table) 11 as a table on which the wafer W is placed is provided.

在腔室10的侧壁与基座11之间,形成作为把基座11上方的气体向腔室10之外排出的流路发挥功能的排气路12。在此排气路12的中途配置环状的挡板13,排气路12的相比于挡板13而在下游的空间连通于作为可变式蝶形阀的自动压力控制阀(automatic pressure controlvalve)(以下称为‘APC’)14。APC 14连接于作为抽真空用的排气泵的涡轮分子泵(以下称为‘TMP’)15,进而,经由TMP 15连接于作为排气泵的干式泵(以下称为‘DP’)16。虽然以下把由APC 14、TMP 15和DP 16所构成的排气流路称为‘主排放管线’,但是此主排放管线不仅由APC 14进行腔室10内的压力控制而且由TMP 15和DP16把腔室10内减压到几乎真空状态。Between the side wall of the chamber 10 and the susceptor 11 is formed an exhaust passage 12 that functions as a flow passage for exhausting gas above the susceptor 11 to the outside of the chamber 10 . A ring-shaped baffle 13 is arranged in the middle of the exhaust passage 12, and the space downstream of the exhaust passage 12 compared with the baffle 13 communicates with an automatic pressure control valve (automatic pressure control valve) which is a variable butterfly valve. ) (hereinafter referred to as 'APC')14. The APC 14 is connected to a turbomolecular pump (hereinafter referred to as 'TMP') 15 as an exhaust pump for vacuuming, and further connected to a dry pump (hereinafter referred to as 'DP') 16 as an exhaust pump via the TMP 15. Although the exhaust flow path composed of APC 14, TMP 15 and DP 16 is referred to as a 'main discharge line' below, this main discharge line is not only controlled by the APC 14 in the chamber 10 but also by the TMP 15 and DP16. The inside of the chamber 10 is decompressed to a nearly vacuum state.

此外,上述排气路12的相比于隔板13而处于下游的空间,连接于与主排放管线分开的排气流路(以下称为‘粗排放管线’)(排气装置)。使此粗排放管线与上述空间与DP 16连通。备有直径例如为25mm的排气管17、和设在排气管17的中途的阀V2。此阀V2可以隔断上述空间与DP 16。粗排放管线由DP 16排出腔室10内的空气。In addition, the space downstream of the partition plate 13 in the exhaust passage 12 is connected to an exhaust flow passage (hereinafter referred to as "rough exhaust line") (exhaust device) separate from the main exhaust line. Connect this coarse discharge line with the above space and DP 16. An exhaust pipe 17 having a diameter of, for example, 25 mm, and a valve V2 provided in the middle of the exhaust pipe 17 are provided. This valve V2 can isolate the above space from DP 16. The coarse exhaust line is used to exhaust the air in the chamber 10 from the DP 16.

在基座11上,等离子体生成用的高频电源18经由匹配器19电气上连接着。此高频电源18把规定的高频,例如,13.56MHz的高频电力施加于基座11。借此,基座11作为下部电极发挥功能。A high-frequency power source 18 for plasma generation is electrically connected to the susceptor 11 via a matching unit 19 . This high frequency power supply 18 applies a predetermined high frequency, for example, high frequency power of 13.56 MHz to the base 11 . Thereby, the susceptor 11 functions as a lower electrode.

在基座11的内部上方,配置着用静电吸附力吸附晶片W的由导电膜组成的圆盘状的电极板20。直流电源22电气上连接于电极板20。On the inside of the susceptor 11, a disc-shaped electrode plate 20 made of a conductive film is arranged to attract the wafer W by electrostatic attraction. The DC power supply 22 is electrically connected to the electrode plate 20 .

晶片W靠因从直流电源22施加于电极板20的直流电压而产生的库仑力或约翰逊-拉别克(Johnsen-Rahbek)力吸附保持于基座11的上面。此外,由硅(Si)等制成的圆环状的聚集环24把在基座11的上方产生的等离子体向晶片W聚集。The wafer W is attracted and held on the susceptor 11 by Coulomb force or Johnson-Rahbek force generated by the DC voltage applied from the DC power source 22 to the electrode plate 20 . In addition, an annular focusing ring 24 made of silicon (Si) or the like focuses plasma generated above susceptor 11 on wafer W. As shown in FIG.

此外,在基座11的内部,例如,设有在圆周方向上延长的环状的冷却介质室25。在此冷却介质室25中,从冷却单元(未图示)经由配管26循环供给规定温度的冷却介质,例如,冷却水,基座11上的晶片W的处理温度靠该冷却介质的温度来控制。In addition, inside the susceptor 11, for example, an annular coolant chamber 25 extending in the circumferential direction is provided. In this cooling medium chamber 25, a cooling medium of a predetermined temperature, such as cooling water, is circulated from a cooling unit (not shown) through a pipe 26, and the processing temperature of the wafer W on the susceptor 11 is controlled by the temperature of the cooling medium. .

在基座11的上面吸附晶片W的部分上,开孔了多个传热气体供给孔(气体供给装置)27。这些传热气体供给孔27经由配置于基座11内部的传热气体供给线28,连通于有阀V3的传热气体供给管29,把来自连接于传热气体供给管29的传热气体供给部(未图示)的传热气体,例如,He气供给到基座11的上面与晶片W的背面之间的间隙。借此,晶片W与基座11的热传递性提高。再者,阀V3可以隔断传热气体供给孔27与传热气体供给部。A plurality of heat transfer gas supply holes (gas supply means) 27 are opened in the upper surface of the susceptor 11 where the wafer W is adsorbed. These heat transfer gas supply holes 27 communicate with a heat transfer gas supply pipe 29 having a valve V3 via a heat transfer gas supply line 28 arranged inside the susceptor 11, and supply heat transfer gas from the heat transfer gas supply pipe 29 connected to the base 11. A heat transfer gas (not shown), for example, He gas, is supplied to the gap between the upper surface of the susceptor 11 and the rear surface of the wafer W. This improves the heat transfer between the wafer W and the susceptor 11 . Furthermore, the valve V3 can block the heat transfer gas supply hole 27 and the heat transfer gas supply part.

此外,在基座11的上面吸附晶片W的部分上,配置着作为从基座11的上面突出自如的提升销的多个顶推销(分开装置)30。这些顶推销30,通过电动机(未图示)的旋转运动靠滚珠丝杠等变换成直线运动,在图中上下方向上移动。在晶片W被吸附保持于基座11的上面时,顶推销30被收容于基座11,在从腔室10搬出施行蚀刻处理等等离子体处理结束的晶片W时,顶推销30从基座11的上面突出而使晶片W从基座11离开向上抬起。此时,在基座11的上面与晶片W的背面之间形成空间S。In addition, a plurality of ejector pins (separating means) 30 as lift pins protruding freely from the upper surface of the susceptor 11 are arranged on the portion where the wafer W is adsorbed on the upper surface of the susceptor 11 . These push pins 30 are converted into linear motion by a ball screw or the like by a motor (not shown) in rotation, and move vertically in the figure. When the wafer W is adsorbed and held on the upper surface of the susceptor 11, the push pins 30 are accommodated in the susceptor 11. The upper surface of the wafer W lifts away from the susceptor 11 and lifts up. At this time, a space S is formed between the upper surface of the susceptor 11 and the rear surface of the wafer W. As shown in FIG.

在腔室10的侧壁上,安装着开闭晶片W的搬入搬出口31的门阀32。此外,在腔室10的室顶部上,配置着处于接地电位的作为上部电极的浇淋头33。借此,来自高频电源18的高频电压施加于基座11与浇淋头33之间。On the side wall of the chamber 10, a gate valve 32 for opening and closing the loading and unloading port 31 of the wafer W is attached. In addition, on the ceiling of the chamber 10, a shower head 33 serving as an upper electrode at a ground potential is disposed. Thereby, the high-frequency voltage from the high-frequency power supply 18 is applied between the susceptor 11 and the shower head 33 .

室顶部的浇淋头33,包括具有多个通气孔34的下面的电极板35,和能够装拆地支撑该电极板35的电极支撑体36。此外,在该电极支撑体36的内部设有缓冲室37,来自处理气体供给部(未图示)的处理气体导入管38连接于此缓冲室37。在此处理气体导入管38的中途配置着阀V1。此阀V1可以隔断缓冲室37与处理气体供给部。此外,在腔室10的周围,配置着环状或同心状地延长的磁铁39。The shower head 33 at the top of the chamber includes a lower electrode plate 35 having a plurality of vent holes 34, and an electrode support 36 detachably supporting the electrode plate 35. In addition, a buffer chamber 37 is provided inside the electrode support 36 , and a processing gas introduction pipe 38 from a processing gas supply unit (not shown) is connected to the buffer chamber 37 . A valve V1 is disposed in the middle of the processing gas introduction pipe 38 . This valve V1 can isolate the buffer chamber 37 from the processing gas supply unit. In addition, around the chamber 10, a ring-shaped or concentrically extended magnet 39 is disposed.

在此等离子体处理装置1的腔室10内,由磁铁39形成朝一定方向的水平磁场,并且靠施加于基座11与浇淋头33之间的高频电压形成竖直方向的RF电场,借此,在腔室10内经由处理气体进行磁控管放电,在基座11的表面附近处由处理气体生成高密度的等离子体。In the chamber 10 of the plasma processing device 1, the magnet 39 forms a horizontal magnetic field in a certain direction, and a high-frequency voltage applied between the susceptor 11 and the pouring head 33 forms a vertical RF electric field, Accordingly, magnetron discharge is performed through the process gas in the chamber 10 , and high-density plasma is generated from the process gas in the vicinity of the surface of the susceptor 11 .

在此等离子体处理装置1中,在蚀刻处理之际,首先使门阀32成打开状态把加工对象的晶片W搬入腔室10内,载置于基座11之上。然后,从浇淋头33以规定的流量和流量比把处理气体(例如,规定的流量比率的由C4F8气体、O2气体和Ar气体组成的混合气体)导入腔室10内,靠APC 14等使腔室10内的压力成规定值。进而,从高频电源18把高频电力供给到基座11,从直流电源22把直流电压施加于电极板20,把晶片W吸附于基座11上。然后,从浇淋头33所喷出的处理气体如上所述等离子体化。在此等离子体中所生成的自由基或离子靠聚集环24聚集于晶片W的表面,蚀刻晶片W的表面。In this plasma processing apparatus 1 , at the time of etching, first, the gate valve 32 is opened, and the wafer W to be processed is carried into the chamber 10 and placed on the susceptor 11 . Then, the processing gas (for example, a mixed gas composed of C 4 F 8 gas, O 2 gas and Ar gas at a prescribed flow ratio) is introduced into the chamber 10 from the pouring head 33 at a prescribed flow rate and a flow ratio, and the The APC 14 and the like make the pressure in the chamber 10 a predetermined value. Further, high-frequency power is supplied to susceptor 11 from high-frequency power supply 18 , and DC voltage is applied to electrode plate 20 from DC power supply 22 to attract wafer W on susceptor 11 . Then, the processing gas ejected from the shower head 33 is plasma-formed as described above. Radicals or ions generated in the plasma are collected on the surface of the wafer W by the focusing ring 24 to etch the surface of the wafer W.

在上述等离子体处理装置1中,所生成的等离子体当中,未聚集于晶片W的表面者撞击腔室10的内壁等而产生颗粒。产生的颗粒当中,未被主排放管线或粗排放管线所排出的颗粒堆积于基座11的上面。此堆积于上面的颗粒,在晶片W载置于基座11的上面时,作为异物附着于晶片W的背面。适应于此,在等离子体处理装置1中,在对晶片W施行蚀刻处理后,靠顶推销30使晶片W从基座11的上面离开而产生空间S时,高电压施加于电极板20,N2气体等从传热气体供给孔27供给到空间S,腔室10内靠粗排放管线排气。进而,在腔室10内靠粗排放管线减压期间,从浇淋头33向腔室10内导入处理气体。借此,附着于晶片W的背面的颗粒被排出。下面,就在等离子体处理装置1中所实行的,排除附着于晶片W的背面的颗粒的基板清洗方法进行说明。In the plasma processing apparatus 1 described above, among the generated plasma, those not collected on the surface of the wafer W collide with the inner wall of the chamber 10 or the like to generate particles. Among the generated particles, those not discharged by the main discharge line or the rough discharge line are accumulated on the upper surface of the susceptor 11 . The particles deposited on the upper surface adhere to the back surface of the wafer W as foreign matter when the wafer W is placed on the upper surface of the susceptor 11 . Accordingly, in the plasma processing apparatus 1, when the wafer W is etched by the push pin 30 to separate the wafer W from the upper surface of the susceptor 11 to create a space S, a high voltage is applied to the electrode plates 20, N 2 Gas and the like are supplied to the space S from the heat transfer gas supply hole 27, and the inside of the chamber 10 is exhausted through the rough discharge line. Furthermore, the process gas is introduced into the chamber 10 from the shower head 33 while the chamber 10 is depressurized by the rough discharge line. Thereby, particles adhering to the back surface of the wafer W are discharged. Next, a substrate cleaning method for removing particles adhering to the back surface of the wafer W performed in the plasma processing apparatus 1 will be described.

图2是在图1的等离子体处理装置中所实行的基板清洗处理的顺序图。此基板清洗处理在对晶片W施行蚀刻处理后实行。FIG. 2 is a sequence diagram of a substrate cleaning process performed in the plasma processing apparatus of FIG. 1 . This substrate cleaning process is performed after etching the wafer W.

在图2中,本处理所实行的前提条件是晶片W被施行蚀刻处理且载置于基座11的上面的状态,电压未施加于电极板20(HV 0),APC14打开(APC OPEN)且TMP 15动作。也就是说,是腔室10内靠主排放管线减压(抽真空),阀V1~V3全都关闭(V1 CLOSE,V2 CLOSE,V3 CLOSE)的状态。In FIG. 2, the preconditions for this process are that the wafer W is etched and placed on the susceptor 11, the voltage is not applied to the electrode plate 20 (HV 0), the APC 14 is opened (APC OPEN), and TMP 15 action. That is to say, it is a state in which the chamber 10 is decompressed (vacuumized) by the main discharge line, and the valves V1-V3 are all closed (V1 CLOSE, V2 CLOSE, V3 CLOSE).

首先,收容于基座11的(PIN DOWN)顶推销30使晶片W从基座11离开而向上抬起(PIN UP)。此时,虽然顶推销30把晶片W从基座11抬起的高度未特别限制,但是优选是10~20mm。借此,在基座11的上面与晶片W的背面之间形成空间S。First, the (PIN DOWN) push pin 30 housed in the susceptor 11 lifts up (PIN UP) the wafer W away from the susceptor 11. At this time, the height at which the push pins 30 lift the wafer W from the susceptor 11 is not particularly limited, but is preferably 10 to 20 mm. Thereby, a space S is formed between the upper surface of the susceptor 11 and the back surface of the wafer W. As shown in FIG.

接着,APC14关闭(APC CLOSE),并且排气管17的阀V2和传热气体供给管29的阀V3打开(V2 OPEN,V3 OPEN),传热气体供给孔27向抬起的晶片W的背面把N2气体喷出到空间S,粗排放管线把喷出到空间S的N2气体与腔室10内残存的气体一起向腔室10之外排出。借此,在空间S中产生从晶片W的背面向基座11的外周部流动的,气体粘性力大的粘性流。此时,因为如果腔室10内为规定的压力以上,则粘性流容易产生,故粗排放管线排出腔室10内的N2气体等,以便腔室10内的压力不低于规定的压力,例如,133Pa(1torr),优选是,腔室10内的压力维持于规定的压力范围,例如,1.33×103~1.33×104Pa(10~100torr)的范围。借此,可以在空间S中可靠地产生粘性流。粘性流卷入后述的从晶片W的背面脱离的颗粒并与腔室10内的气体一起从腔室10排出。Next, the APC 14 is closed (APC CLOSE), and the valve V2 of the exhaust pipe 17 and the valve V3 of the heat transfer gas supply pipe 29 are opened (V2 OPEN, V3 OPEN), and the heat transfer gas supply hole 27 is opened toward the rear surface of the lifted wafer W. The N 2 gas is ejected into the space S, and the N 2 gas ejected into the space S is discharged out of the chamber 10 together with the gas remaining in the chamber 10 through the rough discharge pipeline. Thereby, a viscous flow having a large gas viscous force is generated in the space S, flowing from the rear surface of the wafer W toward the outer peripheral portion of the susceptor 11 . At this time, since the viscous flow is likely to occur if the inside of the chamber 10 is above a predetermined pressure, the rough discharge line discharges N2 gas and the like in the chamber 10 so that the pressure inside the chamber 10 does not fall below the predetermined pressure, For example, 133 Pa (1 torr), it is preferable to maintain the pressure in the chamber 10 within a predetermined pressure range, for example, the range of 1.33×10 3 to 1.33×10 4 Pa (10 to 100 torr). Thereby, viscous flow can be reliably generated in the space S. The viscous flow entrains particles detached from the rear surface of the wafer W described later, and is discharged from the chamber 10 together with the gas in the chamber 10 .

接着,直流电源22把极性不同的高电压,例如,+500V和-500V的电压交互地施加于电极板20(HV+500,HV-500)。此时,起因于对电极板20的高电压的施加,在腔室10内,特别是,在空间S中产生静电场,静电的应力,例如,麦克斯韦(Maxwell)应力作用于晶片W的背面。借此,附着于晶片W的背面的颗粒的附着力减弱,该颗粒脱离。该脱离的颗粒被上述粘性流从空间S中排出到腔室10之外。上述静电的应力在对电极板20的高电压的施加时和停止时,有效地作用于晶片W的背面。这里,在等离子体处理装置1中,因为对电极板20的高电压的施加反复进行,故有效的静电的应力反复地作用于晶片W的背面。因而,可以更充分地去除附着于晶片W的背面的颗粒。Next, the DC power supply 22 alternately applies high voltages of different polarities, for example, voltages of +500V and -500V, to the electrode plate 20 (HV+500, HV-500). At this time, due to the application of the high voltage to the electrode plate 20, an electrostatic field is generated in the chamber 10, especially in the space S, and electrostatic stress, for example, Maxwell stress acts on the back surface of the wafer W. Thereby, the adhesive force of the particles adhering to the back surface of the wafer W is weakened, and the particles are detached. The detached particles are expelled from the space S to the outside of the chamber 10 by the above-mentioned viscous flow. The electrostatic stress described above effectively acts on the back surface of the wafer W when the high voltage is applied to the electrode plate 20 and when it is stopped. Here, in the plasma processing apparatus 1 , since the application of high voltage to the electrode plate 20 is repeated, effective electrostatic stress repeatedly acts on the back surface of the wafer W. Thus, particles adhering to the back surface of wafer W can be removed more sufficiently.

交互地对电极板20所施加的电压的绝对值优选大一些,例如,500V以上,优选是,2kV以上。借此,可以加大作用于晶片W的背面的静电的应力,可以可靠地进行颗粒的脱离。The absolute value of the voltage alternately applied to the electrode plates 20 is preferably larger, for example, 500V or more, preferably 2kV or more. Thereby, the electrostatic stress acting on the back surface of the wafer W can be increased, and the particles can be detached reliably.

此外,如果反复进行对电极板20的同一极性的高电压的施加,则电极板20带电(充电),结果,作用于晶片W的背面的静电的应力减小,有时附着于晶片W的背面的颗粒的去除效率降低。在等离子体处理装置1中,因为对电极板20交互地施加极性不同的高电压,故电极板20不会带电,可以防止附着于晶片W的背面的颗粒的去除效率的降低。In addition, when the high voltage of the same polarity is repeatedly applied to the electrode plate 20, the electrode plate 20 is charged (charged), and as a result, the stress of the static electricity acting on the back surface of the wafer W is reduced, and the electrode plate 20 may adhere to the back surface of the wafer W. The particle removal efficiency is reduced. In the plasma processing apparatus 1 , since high voltages of different polarities are alternately applied to the electrode plate 20 , the electrode plate 20 is not charged, and a reduction in removal efficiency of particles adhering to the back surface of the wafer W can be prevented.

再者,如上所述,上述静电的应力的有效的作用关系到对电极板20的高电压的施加的次数,与对电极板20的高电压的施加时间关系不大。因而,对电极板20的高电压的施加时间也可以为例如1秒以下。Furthermore, as described above, the effective action of the electrostatic stress is related to the frequency of application of the high voltage to the electrode plate 20 , and has little relationship to the application time of the high voltage to the electrode plate 20 . Therefore, the application time of the high voltage to the electrode plate 20 may be, for example, 1 second or less.

在上述对电极板20的极性不同的高电压的交互的施加期间,处理气体导入管38的阀V1打开(V1 OPEN),从浇淋头33代替处理气体向腔室10内导入非活性气体,例如,N2气体。此时,因为腔室10内靠粗排放管线减压,故在浇淋头33的正下方产生急剧的压力上升,借此,所导入的N2气体生成行进冲击波,所生成的行进冲击波达到抬起的晶片W。结果,冲击力加到晶片W上,附着于晶片W的背面的颗粒脱离。此时也是,脱离的颗粒被上述粘性流从空间S向腔室10之外排出。During the alternating application of high voltages with different polarities to the electrode plate 20, the valve V1 of the process gas introduction pipe 38 is opened (V1 OPEN), and an inert gas is introduced into the chamber 10 from the shower head 33 instead of the process gas. , for example, N2 gas. At this time, since the inside of the chamber 10 is depressurized by the rough discharge line, a sharp pressure rise is generated directly under the shower head 33, whereby the introduced N 2 gas generates a traveling shock wave, and the generated traveling shock wave reaches the height of the lift. The raised wafer W. As a result, impact force is applied to the wafer W, and the particles attached to the back surface of the wafer W are detached. Also at this time, the detached particles are discharged from the space S to the outside of the chamber 10 by the above-mentioned viscous flow.

再者,在等离子体处理装置1中,为了有效地进行N2气体导入时的腔室10内的浇淋头33正下方的压力上升,在处理气体导入管38中优选是在阀V1下游配置节流孔结构,例如,流量控制装置(质量流量控制器)或减速阀。In addition, in the plasma processing apparatus 1, in order to effectively increase the pressure immediately below the shower head 33 in the chamber 10 when N gas is introduced, the processing gas introduction pipe 38 is preferably disposed downstream of the valve V1. Orifice structures such as flow control devices (mass flow controllers) or deceleration valves.

然后,在处理气体导入管38的阀V1打开的状态(V1 OPEN),对电极板20的极性不同的高电压的交互的施加进行了规定次数,例如,4次后,处理气体导入管38的阀V1关闭(V1 CLOSE),APC 14打开(APC OPEN),并且排气管17的阀V2和传热气体供给管29的阀V3关闭(V2 CLOSE,V3 CLOSE),本处理结束。Then, in the state where the valve V1 of the processing gas introduction pipe 38 is open (V1 OPEN), high voltages with different polarities to the electrode plate 20 are alternately applied a predetermined number of times, for example, after 4 times, the processing gas introduction pipe 38 is closed. The valve V1 of the exhaust pipe 17 is closed (V1 CLOSE), the APC 14 is opened (APC OPEN), and the valve V2 of the exhaust pipe 17 and the valve V3 of the heat transfer gas supply pipe 29 are closed (V2 CLOSE, V3 CLOSE), and this process ends.

虽然上述施行了基板清洗处理的晶片W经由搬入搬出口31从腔室10中搬出,向搬送腔室,例如,负载锁定室搬入,但是由于充分去除了附着于晶片W的背面的颗粒,所以负载锁定室内不会被颗粒所污染。Although the above-mentioned wafer W subjected to the substrate cleaning process is carried out of the chamber 10 through the loading and unloading port 31, and is carried into a transfer chamber, for example, a load lock chamber, since the particles adhering to the back surface of the wafer W are sufficiently removed, the load The locked chamber will not be contaminated by particles.

如果用上述基板清洗方法,则因为在基座11和晶片W之间产生空间S时,极性不同的高电压交互地施加于电极板20,故在上述空间S中产生静电场而静电的应力作用于晶片W的背面,进而,在产生上述空间S且腔室10内靠粗排放管线减压时,因为N2气体被导入腔室10,故在腔室10内产生行进冲击波,所生成的行进冲击波使冲击力加在晶片W上。借此,附着于晶片W的背面的颗粒向空间S脱离。因而,因为在颗粒的脱离中不需要等离子体的离子引起的溅射,或自由基引起的化学反应,故不损伤晶片W。If the above-mentioned substrate cleaning method is used, since a space S is generated between the susceptor 11 and the wafer W, high voltages with different polarities are alternately applied to the electrode plate 20, so an electrostatic field is generated in the above-mentioned space S and electrostatic stress Acting on the back surface of the wafer W, and further, when the above-mentioned space S is generated and the chamber 10 is depressurized by the rough discharge line, because N gas is introduced into the chamber 10, a traveling shock wave is generated in the chamber 10, and the generated The traveling shock wave imparts an impact force on the wafer W. Thereby, the particles adhering to the back surface of the wafer W escape to the space S. As shown in FIG. Therefore, since sputtering by plasma ions or chemical reaction by radicals is not required for detachment of particles, wafer W is not damaged.

此外,因为在产生上述空间S时,N2气体从传热气体供给孔27喷出到空间S,喷出到该空间S的N2气体靠粗排放管线向腔室10之外排出,故在空间S中产生N2气体的粘性流。脱离的颗粒被卷入上述粘性流而从空间S中向腔室10之外排出。In addition, when the above-mentioned space S is generated, the N2 gas is ejected from the heat transfer gas supply hole 27 into the space S, and the N2 gas ejected into the space S is discharged to the outside of the chamber 10 through the rough discharge line. A viscous flow of N2 gas is generated in the space S. The detached particles are drawn into the above-mentioned viscous flow and discharged from the space S to the outside of the chamber 10 .

因而,可以不损伤晶片W而充分地去除附着于晶片W的背面的颗粒。Therefore, the particles adhering to the back surface of the wafer W can be sufficiently removed without damaging the wafer W.

在上述等离子体处理装置1中,虽然由粗排放管线排出腔室10内的N2气体等以便腔室10内的压力不低于规定的压力,但是也可以不靠粗排放管线,而通过减小APC 14的开度靠主排放管线,排出腔室10内的N2气体等以便腔室10内的压力不低于规定的压力,即使借助于此也可以在空间S中产生粘性流。In the above-mentioned plasma processing apparatus 1, although the N2 gas and the like in the chamber 10 are exhausted from the rough discharge line so that the pressure in the chamber 10 does not fall below a predetermined pressure, it is also possible to reduce the pressure by reducing the rough discharge line instead of the rough discharge line. The opening of the small APC 14 depends on the main discharge line to discharge the N2 gas in the chamber 10, etc. so that the pressure in the chamber 10 is not lower than the specified pressure, even by means of which a viscous flow can be generated in the space S.

此外,本发明不仅适用于作为蚀刻处理装置而构成的等离子体处理装置,也可运用于其他等离子体处理装置,例如,作为CVD装置或灰化装置而构成的等离子体处理装置。In addition, the present invention is applicable not only to a plasma processing apparatus configured as an etching processing apparatus, but also to other plasma processing apparatuses, for example, a plasma processing apparatus configured as a CVD apparatus or an ashing apparatus.

接下来,就作为根据本发明的第二实施方式的基板清洗装置的等离子体处理装置进行详述。Next, a plasma processing apparatus as a substrate cleaning apparatus according to a second embodiment of the present invention will be described in detail.

由于作为根据本发明的第二实施方式的等离子体处理装置,其构成、作用与上述第一实施方式基本上是同一的,所以就重复的构成、作用省略说明,以下进行就不同的构成、作用的说明。Since the plasma processing apparatus according to the second embodiment of the present invention has basically the same configuration and functions as those of the above-mentioned first embodiment, the description of the redundant configuration and functions will be omitted, and the different configurations and functions will be described below. instruction of.

虽然在作为根据第二实施方式的基板清洗装置的等离子体处理装置中,与第一实施方式同样,在晶片W靠后述的顶推销40从基座11的上面离开而产生空间S时,产生静电场而静电的应力作用于晶片W的背面,但是在静电场不起因于对电极板20的高电压的施加,而起因于由顶推销40对晶片W的高电压的施加这一点上与第一实施方式不同。Although in the plasma processing apparatus as the substrate cleaning apparatus according to the second embodiment, similar to the first embodiment, when the wafer W is separated from the upper surface of the susceptor 11 by the push pin 40 described later and the space S is generated, the The electrostatic field and electrostatic stress act on the back surface of the wafer W, but the electrostatic field is not caused by the application of a high voltage to the electrode plate 20, but is caused by the application of a high voltage to the wafer W by the push pin 40. One embodiment is different.

图3是表示作为根据第二实施方式的基板清洗装置的等离子体处理装置中的顶推销的概略构成的图。3 is a diagram showing a schematic configuration of a push pin in a plasma processing apparatus as a substrate cleaning apparatus according to a second embodiment.

在图3中,顶推销40是由导电体组成的棒状体,接触于晶片W的背面的一端形成为半球状,另一端电气上连接于直流电源41。此外,虽然顶推销40的表面,为了防止从该表面的放电,优选是由介电体等所覆盖,但是半球状的一端的表面,为了对晶片W施加高电压,导体露出。顶推销40,通过电动机(未图示)的旋转运动靠滚珠丝杠等变换成直线运动,在图中上下方向上移动。In FIG. 3 , the push pin 40 is a rod-shaped body made of a conductor, one end contacting the back surface of the wafer W is formed in a hemispherical shape, and the other end is electrically connected to a DC power supply 41 . In addition, the surface of the push pin 40 is preferably covered with a dielectric or the like in order to prevent discharge from the surface, but the surface at one end of the hemispherical shape exposes a conductor to apply a high voltage to the wafer W. The push pin 40 is converted into a linear motion by a ball screw or the like from a rotational motion of a motor (not shown), and moves vertically in the figure.

此外,多个顶推销40在基座11的上面处配置于吸附晶片W的部分。而且,顶推销40从基座11的上面突出而使晶片W离开基座11向上抬起。此时,与第一实施方式同样,在基座11的上面与晶片W之间形成空间S。In addition, a plurality of ejector pins 40 are arranged on the upper surface of the susceptor 11 at a portion where the wafer W is adsorbed. Further, the ejector pins 40 protrude from the upper surface of the susceptor 11 to lift the wafer W away from the susceptor 11 upward. At this time, a space S is formed between the upper surface of the susceptor 11 and the wafer W as in the first embodiment.

在作为根据第二实施方式的基板清洗装置的等离子体处理装置中,对晶片W施行蚀刻处理后,在晶片W靠顶推销40离开基座11的上面而产生空间S时,高电压经由顶推销40从直流电源41施加于晶片W,N2气体从传热气体供给孔27供给到空间S,腔室10内靠粗排放管线排气。进而,在腔室10内靠粗排放管线减压期间,从浇淋头33向腔室10内导入处理气体。In the plasma processing apparatus as the substrate cleaning apparatus according to the second embodiment, after the etching process is performed on the wafer W, when the wafer W is separated from the upper surface of the susceptor 11 by the push pins 40 to create a space S, a high voltage is applied via the push pins. 40 is applied to the wafer W from the DC power supply 41, N 2 gas is supplied to the space S from the heat transfer gas supply hole 27, and the inside of the chamber 10 is exhausted through the rough discharge line. Furthermore, the process gas is introduced into the chamber 10 from the shower head 33 while the chamber 10 is depressurized by the rough discharge line.

此外,在作为根据第二实施方式的基板清洗装置的等离子体处理装置中所实行的基板清洗方法,虽然在代替极性不同的高电压交互地施加于电极板20,经由顶推销40,极性不同的高电压交互地施加于晶片W这一点上与第一实施方式不同,但是在空间S中产生静电场,静电的应力作用于晶片W的背面,附着于晶片W的背面的颗粒的附着力减弱,该颗粒脱离的情况,与第一实施方式是同一的。Further, in the substrate cleaning method carried out in the plasma processing apparatus as the substrate cleaning apparatus according to the second embodiment, although high voltages of different polarities are alternately applied to the electrode plate 20 via the push pin 40, the polarity Different from the first embodiment in that different high voltages are alternately applied to the wafer W, an electrostatic field is generated in the space S, the electrostatic stress acts on the back surface of the wafer W, and the adhesion of the particles attached to the back surface of the wafer W Weakening, the detachment of the particles is the same as that of the first embodiment.

此外,经顶推销40施加于晶片W的高电压例如500V以上,优选2kV以上,高电压的施加时间可以为1秒以下,这与实施方式1相同。In addition, the high voltage applied to the wafer W via the push pins 40 is, for example, 500 V or more, preferably 2 kV or more, and the application time of the high voltage may be 1 second or less, which is the same as in the first embodiment.

如果用上述基板清洗方法,则因为在基座11和晶片W之间产生空间S时,经由顶推销40,极性不同的高电压交互地施加于晶片W,故在上述空间S中产生静电场而静电的应力作用于晶片W的背面,进而,在产生上述空间S且腔室10内靠粗排放管线减压时,因为N2气体被导入腔室10,故在腔室10内产生行进冲击波,所生成的行进冲击波使冲击力加在晶片W上。借此,附着于晶片W的背面的颗粒向空间S脱离。因而,因为在颗粒的脱离中不需要等离子体的离子引起的溅射,或自由基引起的化学反应,故不损伤晶片W。If the above-mentioned substrate cleaning method is used, when a space S is generated between the susceptor 11 and the wafer W, high voltages with different polarities are alternately applied to the wafer W via the push pin 40, so an electrostatic field is generated in the space S. And electrostatic stress acts on the back surface of the wafer W, and then, when the above-mentioned space S is generated and the chamber 10 is depressurized by the rough discharge line, because N gas is introduced into the chamber 10, a traveling shock wave is generated in the chamber 10 , the generated traveling shock wave exerts an impact force on the wafer W. Thereby, the particles adhering to the back surface of the wafer W escape to the space S. As shown in FIG. Therefore, since sputtering by plasma ions or chemical reaction by radicals is not required for detachment of particles, wafer W is not damaged.

此外,因为在产生上述空间S时,N2气体从传热气体供给孔27喷出到空间S,喷出到该空间S的N2气体靠粗排放管线向腔室10之外排出,故在空间S中产生N2气体的粘性流。脱离的颗粒被卷入上述粘性流而从空间S中向腔室10之外排出。In addition, when the above-mentioned space S is generated, the N2 gas is ejected from the heat transfer gas supply hole 27 into the space S, and the N2 gas ejected into the space S is discharged to the outside of the chamber 10 through the rough discharge line. A viscous flow of N2 gas is generated in the space S. The detached particles are drawn into the above-mentioned viscous flow and discharged from the space S to the outside of the chamber 10 .

因而,可以不损伤晶片W而充分地去除附着于晶片W的背面的颗粒。Therefore, the particles adhering to the back surface of the wafer W can be sufficiently removed without damaging the wafer W.

接下来,就作为根据本发明的第三实施方式的基板清洗装置进行详述。Next, a substrate cleaning apparatus according to a third embodiment of the present invention will be described in detail.

根据第三实施方式的基板处理装置,在不对晶片W施行等离子体处理,仅进行晶片W的背面的清洗这一点上,与上述第一和第二实施方式不同。The substrate processing apparatus according to the third embodiment differs from the above-described first and second embodiments in that only the back surface of the wafer W is cleaned without performing plasma processing on the wafer W.

图4是表示根据本发明的第三实施方式的基板清洗装置的概略构成的截面图。4 is a cross-sectional view showing a schematic configuration of a substrate cleaning apparatus according to a third embodiment of the present invention.

在图4中,基板清洗装置42具有金属制例如铝或不锈钢制的箱状的腔室43,在该腔室43内,配置着载置晶片W的圆柱状的工作台44。In FIG. 4 , a substrate cleaning device 42 has a box-shaped chamber 43 made of metal such as aluminum or stainless steel, and a cylindrical table 44 on which a wafer W is placed is disposed in the chamber 43 .

在腔室43的侧壁与工作台44之间,形成作为把工作台44上方的气体向腔室43之外排出的流路发挥功能的排气路65。此排气路65连接于粗排放管线。此粗排放管线使排气路65与作为排气泵的DP 46连通,备有直径例如为25mm的排气管45和设置于排气管45的中途的阀V5。此阀V5可以隔断排气路65与DP 46。粗排放管线靠DP 46排出腔室43内的气体。Between the side wall of the chamber 43 and the table 44 is formed an exhaust passage 65 functioning as a flow passage for discharging the gas above the table 44 to the outside of the chamber 43 . This exhaust path 65 is connected to the rough exhaust line. This rough discharge line communicates the exhaust passage 65 with the DP 46 as an exhaust pump, and is equipped with an exhaust pipe 45 having a diameter of, for example, 25 mm and a valve V5 disposed in the middle of the exhaust pipe 45. This valve V5 can isolate the exhaust passage 65 and the DP 46. The rough discharge line exhausts the gas in the chamber 43 by DP 46.

在工作台44的内部上方,配置着由用来以静电吸附力吸附晶片W的导电膜组成的圆盘状的电极板47,直流电源48电气上连接于电极板47。晶片W靠因从直流电源48施加于电极板47的直流电压产生的库仑力吸附保持于工作台44的上面。A disk-shaped electrode plate 47 composed of a conductive film for attracting wafer W by electrostatic attraction is disposed above the table 44 , and a DC power supply 48 is electrically connected to the electrode plate 47 . The wafer W is attracted and held on the upper surface of the table 44 by the Coulomb force generated by the DC voltage applied from the DC power supply 48 to the electrode plate 47 .

在工作台44的上面吸附晶片W的部分上,开孔着多个气体供给孔49。这些气体供给孔49经由配置于工作台44内部的气体供给线50连通于具有阀V6的气体供给管64,把来自连接于气体供给管64的第一气体供给部(未图示)的气体,例如N2气体供给到工作台44的上面与晶片W的背面的间隙。再者,阀V6可以隔断气体供给孔49与第一气体供给部。A plurality of gas supply holes 49 are formed on the upper surface of the stage 44 where the wafer W is adsorbed. These gas supply holes 49 communicate with a gas supply pipe 64 having a valve V6 via a gas supply line 50 arranged inside the workbench 44, and the gas from a first gas supply part (not shown) connected to the gas supply pipe 64, For example, N 2 gas is supplied to the gap between the upper surface of the stage 44 and the back surface of the wafer W. Furthermore, the valve V6 can isolate the gas supply hole 49 from the first gas supply part.

此外,在工作台44的上面吸附晶片W的部分上,配置着从工作台44的上面突出的多个销子51。销子51抬起搬入腔室43内的晶片W使之从工作台44离开。此时,在工作台44的上面与晶片W的背面之间形成空间S。这些销子51与顶推销30同样也可以在图中上下方向上移动。In addition, a plurality of pins 51 protruding from the upper surface of the table 44 are arranged on the portion where the wafer W is adsorbed on the upper surface of the table 44 . The pins 51 lift the wafer W carried into the chamber 43 to leave the stage 44 . At this time, a space S is formed between the upper surface of the stage 44 and the back surface of the wafer W. As shown in FIG. These pins 51 can also move up and down in the figure like the push pin 30 .

在腔室43的侧壁上,安装着开闭晶片W的搬入搬出口52的门阀53。此外,在腔室43的室顶部上连接着从第二气体供给部(未图示)向腔室43内导入气体例如N2气体的气体导入管54。在此气体导入管54的中途配置着阀V4。此阀V4可以隔断腔室43内与第二气体供给部。A gate valve 53 for opening and closing the loading and unloading port 52 of the wafer W is attached to the side wall of the chamber 43 . In addition, a gas introduction pipe 54 for introducing gas such as N 2 gas into the chamber 43 from a second gas supply unit (not shown) is connected to the ceiling of the chamber 43 . A valve V4 is disposed in the middle of the gas introduction pipe 54 . This valve V4 can isolate the inside of the chamber 43 from the second gas supply unit.

此基板清洗装置42,例如,配置于并行型的基板处理系统,去除附着于由该基板处理系统备有的后述的等离子体处理装置56施行了等离子体处理的晶片W的背面的颗粒。This substrate cleaning apparatus 42 is arranged, for example, in a parallel type substrate processing system, and removes particles adhering to the back surface of the wafer W subjected to plasma processing by a plasma processing apparatus 56 described later provided in the substrate processing system.

图5是表示图4的基板处理装置所配置的基板处理系统的概略构成的图。FIG. 5 is a diagram showing a schematic configuration of a substrate processing system disposed in the substrate processing apparatus of FIG. 4 .

在图5中,基板处理系统55备有:由蚀刻处理晶片W的等离子体处理装置56和配置了把晶片W交接于该等离子体处理装置56的环型单张拾取式的搬送臂57的负载锁定室58所构成的处理站59,收容储存一批晶片W的载置箱的负载端口60,预对正晶片W的方位器61,上述基板清洗装置42,以及作为矩形的公共搬送路,配置了关节型双臂式的搬送臂62的负载单元63。虽然处理站59、负载端口60、方位器61和基板清洗装置42能够装拆地连接于负载单元63,但是基板清洗装置42配置于与负载单元63的长边方向相关的一端,经由负载单元63与方位器61相对。In FIG. 5 , a substrate processing system 55 is provided with a plasma processing apparatus 56 for etching a wafer W and a load equipped with a ring-shaped single pick-up transfer arm 57 for transferring the wafer W to the plasma processing apparatus 56. A processing station 59 constituted by a lock chamber 58, a load port 60 for accommodating a loading box storing a batch of wafers W, an orientation device 61 for pre-aligning wafers W, the above-mentioned substrate cleaning device 42, and a rectangular common transfer path are arranged. The load unit 63 of the articulated double-arm type conveying arm 62 is provided. Although the processing station 59, the load port 60, the orientation device 61, and the substrate cleaning device 42 are detachably connected to the load unit 63, the substrate cleaning device 42 is disposed at one end related to the longitudinal direction of the load unit 63, and passes through the load unit 63. Opposite to the azimuth 61.

在此基板处理系统55中,在等离子体处理装置56中施行了等离子体处理的晶片W,靠负载锁定室58内的搬送臂57和负载单元63内的搬送臂62搬入基板清洗装置42。基板清洗装置42实行后述的基板清洗方法而去除附着于晶片W的背面的颗粒。In this substrate processing system 55 , the wafer W subjected to plasma processing in the plasma processing apparatus 56 is carried into the substrate cleaning apparatus 42 by the transfer arm 57 in the load lock chamber 58 and the transfer arm 62 in the load unit 63 . The substrate cleaning device 42 performs a substrate cleaning method described later to remove particles adhering to the back surface of the wafer W.

下面,就在基板清洗装置42中所实行的基板清洗方法进行说明。Next, a substrate cleaning method performed in the substrate cleaning device 42 will be described.

此基板清洗方法所实行的前提条件是晶片W被施行蚀刻处理且载置于工作台44的上面的状态,电压未施加于电极板47,阀V4~V6全都关闭的状态。The prerequisites for this substrate cleaning method are that the wafer W is etched and placed on the table 44 , no voltage is applied to the electrode plate 47 , and all valves V4 to V6 are closed.

首先,向腔室43搬入的晶片W载置于从工作台44的上面突出的销子51上。此时,销子51把晶片W从工作台44抬起的高度,与第一实施方式同样,为10~20mm就可以了。借此,在工作台44的上面与晶片W的背面之间形成空间S。First, the wafer W loaded into the chamber 43 is placed on the pins 51 protruding from the upper surface of the table 44 . At this time, the height at which the pins 51 lift the wafer W from the table 44 may be 10 to 20 mm as in the first embodiment. Thereby, a space S is formed between the upper surface of the stage 44 and the back surface of the wafer W. As shown in FIG.

接着,门阀53关闭,并且排气管45的阀V5和气体供给管64的阀V6打开,气体供给孔49向抬起的晶片W的背面把N2气体喷出到空间S,粗排放管线把喷出到空间S的N2气体向腔室43之外排出。借此,在空间S中产生从晶片W的背面向工作台44的外周部流动的N2气体的粘性流。此时,与第一实施方式同样,按照腔室43内的压力不低于规定的压力的方式粗排放管线排出腔室43内的N2气体。粘性流卷入后述的从晶片W的背面脱离的颗粒并从腔室43排出。Then, the gate valve 53 is closed, and the valve V5 of the exhaust pipe 45 and the valve V6 of the gas supply pipe 64 are opened, and the gas supply hole 49 ejects N gas to the space S toward the back surface of the lifted wafer W, and the rough discharge line The N 2 gas injected into the space S is exhausted to the outside of the chamber 43 . Thereby, in the space S, a viscous flow of N 2 gas flowing from the back surface of the wafer W toward the outer peripheral portion of the stage 44 is generated. At this time, as in the first embodiment, the N 2 gas in the chamber 43 is exhausted from the rough discharge line so that the pressure in the chamber 43 does not fall below a predetermined pressure. The viscous flow entrains particles detached from the back surface of the wafer W described later and is discharged from the chamber 43 .

接着,直流电源48把极性不同的高电压交互地施加于电极板47。此时,在空间S中产生静电场,静电的应力作用于晶片W的背面,附着于晶片W的背面的颗粒的附着力减弱,该颗粒脱离,与第一实施方式是同样的。然后,脱离的颗粒被上述粘性流从空间S中排出到腔室43之外。Next, the DC power supply 48 alternately applies high voltages with different polarities to the electrode plates 47 . At this time, an electrostatic field is generated in the space S, and electrostatic stress acts on the back surface of the wafer W, so that the adhesion of the particles adhering to the back surface of the wafer W is weakened, and the particles detach, as in the first embodiment. Then, the detached particles are discharged from the space S to the outside of the chamber 43 by the above-mentioned viscous flow.

进而,对电极板47所施加的高电压,例如,500V以上,优选是,2kV以上。以及高电压的施加时间,例如也可以是1秒以下的情况与第一实施方式是同样的。Furthermore, the high voltage applied to the electrode plate 47 is, for example, 500V or higher, preferably 2kV or higher. And the case where the application time of the high voltage may be, for example, 1 second or less is the same as that of the first embodiment.

在上述对晶片W的极性不同的高电压的交互的施加期间,气体导入管54的阀V4打开,N2气体从气体导入管54导入腔室43内。此时,因为腔室43内靠粗排放管线减压,故在腔室43的室顶部的正下方产生急剧的压力上升,所导入的N2气体生成行进冲击波,冲击力因所生成的行进冲击波而加到晶片W上,附着于晶片W的背面的颗粒脱离,与第一实施方式是同样的。此时也是,脱离的颗粒被上述粘性流从空间S向腔室43之外排出。再者,在基板清洗装置42中,与第一实施方式同样,在气体导入管54中优选是在阀V4下游配置节流孔结构。During the above-described alternating application of high voltages of different polarities to the wafer W, the valve V4 of the gas introduction pipe 54 is opened, and N 2 gas is introduced into the chamber 43 from the gas introduction pipe 54 . At this time, because the inside of the chamber 43 is decompressed by the rough discharge line, a sharp pressure rise occurs immediately below the top of the chamber 43, and the introduced N gas generates a traveling shock wave, and the impact force is caused by the generated traveling shock wave. On the other hand, when it is applied to the wafer W, the particles adhering to the back surface of the wafer W are detached, which is the same as that of the first embodiment. Also at this time, the detached particles are discharged from the space S to the outside of the chamber 43 by the above-mentioned viscous flow. In addition, in the substrate cleaning apparatus 42 , as in the first embodiment, it is preferable to arrange an orifice structure in the gas introduction pipe 54 downstream of the valve V4 .

然后,在气体导入管54的阀V4打开的状态,对晶片W的极性不同的高电压的交互的施加进行了规定次数后,气体导入管54的阀V4、排气管45的阀V5和气体供给管64的阀V6关闭,本处理结束。虽然上述施行了基板清洗处理的晶片W经由搬入搬出口52从腔室43中搬出,向负载单元63或负载端口60搬入,但是由于充分去除了附着于晶片W的背面的颗粒,所以负载单元63或负载端口60内不会被颗粒所污染。Then, after the valve V4 of the gas introduction pipe 54 is opened, high voltages with different polarities are alternately applied to the wafer W a predetermined number of times, the valve V4 of the gas introduction pipe 54, the valve V5 of the exhaust pipe 45, and The valve V6 of the gas supply pipe 64 is closed, and this process ends. Although the above-mentioned wafer W subjected to the substrate cleaning process is carried out of the chamber 43 through the loading and unloading port 52, and loaded into the load unit 63 or the load port 60, since the particles adhering to the back surface of the wafer W are sufficiently removed, the load unit 63 Or the inside of the load port 60 will not be polluted by particles.

如果用上述基板清洗方法,则因为在工作台44和晶片W之间产生空间S时,极性不同的高电压交互地施加于晶片W,故在上述空间S中产生静电场而静电的应力作用于晶片W的背面,进而,在产生上述空间S且腔室43内靠粗排放管线减压时,因为N2气体被导入腔室43,故在腔室43内产生行进冲击波,所生成的行进冲击波使冲击力加在晶片W上。借此,附着于晶片W的背面的颗粒向空间S脱离。因而,因为在颗粒的脱离中不需要等离子体,故不损伤晶片W。If the above-mentioned substrate cleaning method is used, since a space S is generated between the workbench 44 and the wafer W, high voltages with different polarities are alternately applied to the wafer W, so an electrostatic field is generated in the above-mentioned space S and the stress of the static electricity acts. On the back side of the wafer W, further, when the above-mentioned space S is generated and the inside of the chamber 43 is depressurized by the rough discharge line, because N gas is introduced into the chamber 43, a traveling shock wave is generated in the chamber 43, and the generated traveling shock wave The shock wave applies an impact force to the wafer W. As shown in FIG. Thereby, the particles adhering to the back surface of the wafer W escape to the space S. As shown in FIG. Therefore, since plasma is not required for detachment of particles, wafer W is not damaged.

此外,因为在产生上述空间S时,N2气体从气体供给孔49喷出到空间S,喷出到该空间S的N2气体靠粗排放管线向腔室43之外排出,故在空间S中产生N2气体的粘性流。脱离的颗粒被卷入上述粘性流而从空间S中向腔室43之外排出。In addition, since the N gas is ejected from the gas supply hole 49 into the space S when the above-mentioned space S is generated, and the N gas ejected into the space S is discharged to the outside of the chamber 43 through the rough discharge line, the space S A viscous flow of N2 gas is produced in the The detached particles are drawn into the above-mentioned viscous flow and discharged from the space S to the outside of the chamber 43 .

因而,可以不损伤晶片W而充分地去除附着于晶片W的背面的颗粒。Therefore, the particles adhering to the back surface of the wafer W can be sufficiently removed without damaging the wafer W.

在上述基板清洗装置42中,虽然基板清洗装置42备有独自的DP46,但是也可以基板清洗装置42和等离子体处理装置56共有DP,借此,可以简化基板处理系统55的构成。In the substrate cleaning device 42 described above, although the substrate cleaning device 42 has its own DP 46 , the substrate cleaning device 42 and the plasma processing device 56 may share a DP, thereby simplifying the configuration of the substrate processing system 55 .

虽然在上述实施方式中,就等离子体处理装置作为基板清洗装置发挥功能的场合,或设置专用的基板清洗装置的场合进行了说明,但是构成基板处理系统的其他装置,也可以作为根据本发明的基板清洗装置发挥功能。Although in the above-mentioned embodiment, the occasion where the plasma processing apparatus functions as a substrate cleaning apparatus or the occasion where a dedicated substrate cleaning apparatus is provided has been described, other apparatuses constituting the substrate processing system may also be used as the substrate cleaning apparatus according to the present invention. The substrate cleaning device functions.

例如,在负载锁定室作为根据本发明的基板处理装置发挥功能的场合,该负载锁定室备有:搬送臂、给负载锁定室排气的排气装置,以及把气体导入负载锁定室内的气体导入装置,搬送臂优选是包括从晶片载置面突出的销子、在晶片W和晶片载置面之间产生静电场的电极、以及向背面喷出气体的气体喷射装置。在此负载锁定室内,在晶片W被销子从晶片载置面抬起而产生空间S时,高电压施加于电极,气体向晶片W的背面喷射,负载锁定室内靠排气装置排气。进而,在负载锁定室内被排气装置减压期间,从气体导入装置向负载锁定室内导入气体。For example, in the case where a load lock chamber functions as a substrate processing apparatus according to the present invention, the load lock chamber is equipped with a transfer arm, an exhaust device for exhausting the load lock chamber, and a gas introduction device for introducing gas into the load lock chamber. The device, the transfer arm preferably includes a pin protruding from the wafer placement surface, an electrode for generating an electrostatic field between the wafer W and the wafer placement surface, and a gas injection device for ejecting gas toward the back surface. In the load lock chamber, when the wafer W is lifted from the wafer mounting surface by pins to create a space S, a high voltage is applied to the electrodes, and the gas is sprayed to the back of the wafer W, and the load lock chamber is exhausted by an exhaust device. Furthermore, while the load lock chamber is decompressed by the exhaust device, gas is introduced into the load lock chamber from the gas introduction device.

实施例Example

接下来,具体地说明本发明的实施例。Next, examples of the present invention will be specifically described.

以下的实施例,在上述等离子体处理装置1中实行。The following examples are carried out in the plasma processing apparatus 1 described above.

首先,准备颗粒大量地附着于背面的晶片W,把该晶片W载置于腔室10内的从基座11突出的顶推销30之上。First, a wafer W on which a large amount of particles adheres to the back surface is prepared, and the wafer W is placed on the ejector pins 30 protruding from the susceptor 11 in the chamber 10 .

然后,靠主排放管线使腔室10内减压后,关闭APC 14,并且打开排气管17的阀V2和传热气体供给管29的阀V3,一边给腔室10内稳定地排气,一边从传热气体供给孔27把N2气体向晶片W的背面喷出。借此,一边使腔室10内保持于6.65×103Pa(50torr)以上,一边在空间S中产生粘性流。Then, after the chamber 10 is depressurized by the main discharge line, the APC 14 is closed, and the valve V2 of the exhaust pipe 17 and the valve V3 of the heat transfer gas supply pipe 29 are opened to stably exhaust the chamber 10. While the N 2 gas is sprayed from the heat transfer gas supply hole 27 toward the back surface of the wafer W. Thereby, a viscous flow is generated in the space S while keeping the inside of the chamber 10 at 6.65×10 3 Pa (50 torr) or higher.

接着,打开阀V1以流量7.0×104 SCCM把N2气体导入腔室10内。在阀V1打开期间,把对电极板20的+2kV和-2kV的电压的交互施加反复6次,然后,关闭阀V1。进而,再次,打开阀V1以流量7.0×104 SCCM把N2气体导入腔室10内,在阀V1打开期间,把对电极板20的+2kV和-2kV的电压的交互施加反复5次,然后,关闭阀V1。此时,把激光照射于空间S,通过由CCD摄像机摄像而观测起因于颗粒的杂散光。所摄像的杂散光的情形示于图6。Next, the valve V1 was opened to introduce N 2 gas into the chamber 10 at a flow rate of 7.0×10 4 SCCM. While the valve V1 was open, the alternating application of voltages of +2 kV and -2 kV to the electrode plate 20 was repeated six times, and then the valve V1 was closed. Furthermore, the valve V1 was opened again to introduce N2 gas into the chamber 10 at a flow rate of 7.0×10 4 SCCM, and the alternating application of +2kV and -2kV voltages to the electrode plate 20 was repeated 5 times while the valve V1 was open. Then, valve V1 is closed. At this time, the space S is irradiated with laser light, and the stray light caused by the particles is observed by imaging with a CCD camera. The state of the captured stray light is shown in FIG. 6 .

图6(a)是示意地表示在阀V1打开期间,把对电极板20的+2kV和-2kV的电压的交互施加反复的场合的空间S的情形的图。这里,颗粒靠因所导入的N2气体而产生的行进冲击波和因电压的交互施加而产生的静电的应力从晶片W的背面大量地脱离,观测到脱离的颗粒成为一群L的情形。FIG. 6( a ) is a diagram schematically showing the state of the space S when alternating voltages of +2 kV and -2 kV are repeatedly applied to the electrode plate 20 while the valve V1 is open. Here, a large number of particles are detached from the back surface of the wafer W by the traveling shock wave generated by the introduced N gas and the electrostatic stress generated by the alternating application of voltage, and it is observed that the detached particles form a group L.

图6(b)是示意地表示从图6(a)开始经过几秒后的空间S的情形的图。这里,在空间S中观测到颗粒的一群L因从晶片W的背面向基座11的外周部流动的粘性流而从空间S排出的情形。FIG. 6( b ) is a diagram schematically showing the state of the space S after several seconds have elapsed from FIG. 6( a ). Here, in the space S, it is observed that a group L of particles is discharged from the space S by the viscous flow flowing from the back surface of the wafer W toward the outer peripheral portion of the susceptor 11 .

图6(c)是示意地表示从图6(b)开始经过几秒后的空间S的情形的图。这里,观测到颗粒的一群L从空间S完全排除的情形。FIG. 6( c ) is a diagram schematically showing the state of the space S after several seconds have elapsed from FIG. 6( b ). Here, a situation in which a population L of particles is completely excluded from the space S is observed.

汇总这些观测结果的曲线示于图7。A graph summarizing these observations is shown in FIG. 7 .

在图7中,横轴是时间,纵轴表示颗粒的个数、电压值和压力值。此外,VE表示施加于电极板20的电压,VW表示因VE而在晶片W引起的电压。P表示腔室10内的压力。进而,图中所绘制的各点表示在各观测时间所观测到的颗粒的个数。再者,P的值成为恒定的部分是腔室10内的压力超出可测量范围的部分。In FIG. 7, the horizontal axis represents time, and the vertical axis represents the number of particles, voltage value and pressure value. In addition, VE represents the voltage applied to the electrode plate 20, and V W represents the voltage induced on the wafer W due to VE. P denotes the pressure inside the chamber 10 . Furthermore, each point plotted in the graph represents the number of particles observed at each observation time. In addition, the portion where the value of P becomes constant is the portion where the pressure in the chamber 10 exceeds the measurable range.

由图7可以看出,在阀V1刚刚打开而N2气体大量地导入腔室10内后,颗粒因产生的行进冲击波而大量地从晶片W的背面脱离,进而,颗粒通过反复对电极板20的电压的交互施加而进一步脱离。借此可以看出,通过N2气体向腔室10内的大量导入和上述电压的交互施加的反复可以使附着于晶片W的背面的颗粒充分地脱离。进而可以看出,因为在第二次的N2气体向腔室10内的大量导入和上述电压的交互施加的反复中脱离的颗粒减少,所以通过进行一次N2气体向腔室10内的大量导入和上述电压的交互施加的反复,可以有效地使颗粒脱离。It can be seen from FIG. 7 that after the valve V1 is opened and a large amount of N2 gas is introduced into the chamber 10, the particles are largely detached from the back surface of the wafer W due to the generated traveling shock waves, and then the particles pass through the electrode plate 20 repeatedly. Further detachment by alternating application of voltage. It can be seen from this that the particles adhering to the back surface of the wafer W can be sufficiently detached by repeating the introduction of a large amount of N 2 gas into the chamber 10 and the above-mentioned alternating application of the voltage. Furthermore, it can be seen that the number of detached particles decreases in the repetition of the second large amount of N2 gas introduction into the chamber 10 and the above-mentioned alternating application of the voltage, so by performing a large amount of N2 gas into the chamber 10 once, The repetition of the introduction and the alternating application of the above-mentioned voltage can effectively detach the particles.

此外,虽然由同时设在粗排放管线的中途的,利用激光散射法的颗粒监视器观测到经由粗排放管线从腔室10内所排出的颗粒,但是可以得到与图7同样的观测结果。借此可以看出粘性流从腔室10内有效地排出脱离的颗粒。In addition, although the particles discharged from the chamber 10 through the rough discharge line were observed by the particle monitor using the laser light scattering method provided in the middle of the rough discharge line, the same observation results as in FIG. 7 were obtained. From this it can be seen that the viscous flow efficiently expels dislodged particles from within the chamber 10 .

Claims (14)

1. a base plate cleaning device is characterized in that, has
Accommodate the reception room of substrate;
Be disposed in this reception room the mounting table of the described substrate of mounting;
Be disposed at this mounting table, make described substrate be adsorbed in the electrode of described mounting table when applying voltage;
To carrying out the exhaust apparatus of exhaust in the described reception room;
This mounting table and described substrate are left and between described mounting table and described substrate, produce the separating device in space; With
Gas is supplied to the gas supply device in described space,
When producing described space, voltage puts on described electrode, and described gas supply device supplies to described space to gas, and described exhaust apparatus carries out exhaust to described reception room.
2. base plate cleaning device as claimed in claim 1 is characterized in that,
Also have and in described reception room, be depressurized and when producing described space, gas is imported gas introduction part in the described reception room.
3. base plate cleaning device as claimed in claim 1 or 2 is characterized in that,
Voltage puts on described electrode discontinuously.
4. base plate cleaning device as claimed in claim 3 is characterized in that,
The voltage that polarity is different alternatively puts on described electrode.
5. base plate cleaning device as claimed in claim 4 is characterized in that,
The absolute value of described voltage is more than the 500V.
6. base plate cleaning device as claimed in claim 5 is characterized in that,
The absolute value of described voltage is more than the 2kV.
7. as each described base plate cleaning device in the claim 1 to 6, it is characterized in that,
Described exhaust apparatus remains in the pressure in the described reception room when producing described space
8. base plate cleaning device as claimed in claim 7 is characterized in that,
Described exhaust apparatus remains in 1.33 * 10 to the pressure in the described reception room when producing described space 3~1.33 * 10 4In the scope of Pa.
9. a base plate cleaning device is characterized in that, has
Accommodate the reception room of substrate;
Be disposed in this reception room the mounting table of the described substrate of mounting;
To carrying out the exhaust apparatus of exhaust in the described reception room;
This mounting table and described substrate are left and between described mounting table and described substrate, produce the space, and voltage is put on the separating device of described substrate with described substrate contacts;
Gas is supplied to the gas supply device in described space; With
In described reception room, import the gas introduction part of gas,
When producing described space, voltage puts on described substrate, described gas supply device supplies to described space to gas, described exhaust apparatus carries out exhaust to described reception room, and then, in described reception room, be depressurized and when producing described space, described gas introduction part imports gas in the described reception room.
10. a substrate-cleaning method is removed the foreign matter at the back side that is attached to substrate, it is characterized in that this method comprises
Substrate is contained in the step of accommodating of reception room;
The mounting step of described substrate-placing in the mounting table that is disposed at described reception room;
Described mounting table and described substrate are left so that between described mounting table and described substrate, produce the step of leaving in space;
When producing described space, the voltage that voltage is put on the electrode that is disposed at described mounting table applies step;
When producing described space, gas is supplied to the gas supplying step in described space; With
When producing described space, to carrying out the steps of exhausting of exhaust in the described reception room.
11. substrate-cleaning method as claimed in claim 10 is characterized in that,
Also be included in when being depressurized and producing described space in the described reception room, the gas that gas is imported in the described reception room imports step.
12. as claim 10 or 11 described substrate-cleaning methods, it is characterized in that,
Apply in the step at described voltage, voltage is put on described electrode discontinuously.
13. substrate-cleaning method as claimed in claim 12 is characterized in that,
Apply in the step at described voltage, the voltages different polarity alternatively put on described electrode.
14. a substrate-cleaning method is removed the foreign matter at the back side that is attached to substrate, it is characterized in that this method comprises:
Substrate is contained in the step of accommodating of reception room;
The mounting step of described substrate-placing in the mounting table that is disposed at described reception room;
Described mounting table and described substrate are left so that between described mounting table and described substrate, produce the step of leaving in space;
When producing described space, the voltage that voltage is put on described substrate applies step;
When producing described space, gas is supplied to the gas supplying step in described space;
When producing described space, to carrying out the steps of exhausting of exhaust in the described reception room; With
In described reception room, be depressurized and when producing described space, the gas that gas is imported in the described reception room imports step.
CNB2005100679314A 2004-04-28 2005-04-28 Substrate cleaning device and substrate cleaning method Expired - Fee Related CN100388430C (en)

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