CN1651560A - Bottle cleaner for cleaning recovered bottles - Google Patents
Bottle cleaner for cleaning recovered bottles Download PDFInfo
- Publication number
- CN1651560A CN1651560A CN 200410077723 CN200410077723A CN1651560A CN 1651560 A CN1651560 A CN 1651560A CN 200410077723 CN200410077723 CN 200410077723 CN 200410077723 A CN200410077723 A CN 200410077723A CN 1651560 A CN1651560 A CN 1651560A
- Authority
- CN
- China
- Prior art keywords
- bottle
- agent
- grams
- washing
- washing agent
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 238000004140 cleaning Methods 0.000 title claims description 7
- 238000005406 washing Methods 0.000 claims abstract description 27
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims abstract description 20
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 14
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 claims abstract description 13
- 239000004530 micro-emulsion Substances 0.000 claims abstract description 8
- 239000007787 solid Substances 0.000 claims abstract description 8
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 claims abstract description 5
- 239000002518 antifoaming agent Substances 0.000 claims abstract description 5
- 239000003960 organic solvent Substances 0.000 claims abstract description 5
- 229910000029 sodium carbonate Inorganic materials 0.000 claims abstract description 5
- 235000019830 sodium polyphosphate Nutrition 0.000 claims abstract description 5
- 102220601533 Transforming growth factor-beta-induced protein ig-h3_A92R_mutation Human genes 0.000 claims abstract description 4
- 239000003795 chemical substances by application Substances 0.000 claims description 29
- 229940051841 polyoxyethylene ether Drugs 0.000 claims description 8
- 229920000056 polyoxyethylene ether Polymers 0.000 claims description 8
- 239000004615 ingredient Substances 0.000 claims description 7
- 235000011121 sodium hydroxide Nutrition 0.000 claims description 7
- RNMDNPCBIKJCQP-UHFFFAOYSA-N 5-nonyl-7-oxabicyclo[4.1.0]hepta-1,3,5-trien-2-ol Chemical compound C(CCCCCCCC)C1=C2C(=C(C=C1)O)O2 RNMDNPCBIKJCQP-UHFFFAOYSA-N 0.000 claims description 4
- 150000002191 fatty alcohols Chemical class 0.000 claims description 4
- -1 polyoxyethylene nonylphenol Polymers 0.000 claims description 4
- 229920001296 polysiloxane Polymers 0.000 claims description 4
- 235000017550 sodium carbonate Nutrition 0.000 claims description 4
- 238000011084 recovery Methods 0.000 claims 2
- AEQDJSLRWYMAQI-UHFFFAOYSA-N 2,3,9,10-tetramethoxy-6,8,13,13a-tetrahydro-5H-isoquinolino[2,1-b]isoquinoline Chemical compound C1CN2CC(C(=C(OC)C=C3)OC)=C3CC2C2=C1C=C(OC)C(OC)=C2 AEQDJSLRWYMAQI-UHFFFAOYSA-N 0.000 abstract 1
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 abstract 1
- IGFHQQFPSIBGKE-UHFFFAOYSA-N Nonylphenol Natural products CCCCCCCCCC1=CC=C(O)C=C1 IGFHQQFPSIBGKE-UHFFFAOYSA-N 0.000 abstract 1
- 239000003599 detergent Substances 0.000 abstract 1
- 239000011521 glass Substances 0.000 abstract 1
- 229910052914 metal silicate Inorganic materials 0.000 abstract 1
- SNQQPOLDUKLAAF-UHFFFAOYSA-N nonylphenol Chemical compound CCCCCCCCCC1=CC=CC=C1O SNQQPOLDUKLAAF-UHFFFAOYSA-N 0.000 abstract 1
- 239000011734 sodium Substances 0.000 abstract 1
- 229910052708 sodium Inorganic materials 0.000 abstract 1
- 239000000176 sodium gluconate Substances 0.000 abstract 1
- 229940005574 sodium gluconate Drugs 0.000 abstract 1
- 235000012207 sodium gluconate Nutrition 0.000 abstract 1
- 230000007935 neutral effect Effects 0.000 description 8
- 235000013405 beer Nutrition 0.000 description 6
- 239000002585 base Substances 0.000 description 5
- 239000007788 liquid Substances 0.000 description 5
- 239000000203 mixture Substances 0.000 description 5
- 238000004519 manufacturing process Methods 0.000 description 3
- 235000013361 beverage Nutrition 0.000 description 2
- 238000007599 discharging Methods 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 239000003513 alkali Substances 0.000 description 1
- ANBBXQWFNXMHLD-UHFFFAOYSA-N aluminum;sodium;oxygen(2-) Chemical compound [O-2].[O-2].[Na+].[Al+3] ANBBXQWFNXMHLD-UHFFFAOYSA-N 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000004945 emulsification Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000012467 final product Substances 0.000 description 1
- 239000003292 glue Substances 0.000 description 1
- 231100000252 nontoxic Toxicity 0.000 description 1
- 230000003000 nontoxic effect Effects 0.000 description 1
- 238000012856 packing Methods 0.000 description 1
- 230000035699 permeability Effects 0.000 description 1
- ZRHANBBTXQZFSP-UHFFFAOYSA-M potassium;4-amino-3,5,6-trichloropyridine-2-carboxylate Chemical compound [K+].NC1=C(Cl)C(Cl)=NC(C([O-])=O)=C1Cl ZRHANBBTXQZFSP-UHFFFAOYSA-M 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 239000010865 sewage Substances 0.000 description 1
- 229910001388 sodium aluminate Inorganic materials 0.000 description 1
- 239000008234 soft water Substances 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
Landscapes
- Detergent Compositions (AREA)
Abstract
A bottle washing detergent for recovering glass bottles is composed of the solid component A prepared from sodium hydroxide, sodium carbonate, sodium metal-silicate, sodium gluconate and A92R, and the water-base microemulsion B prepared from emtrol polyoxyvinylether, nonylphenol polyoxyvinylether, emtrol polyoxyvinylether sulfate, organic solvent, sodium polyphosphate, organosilicon defoaming agent and water. Its advantages are high penetrability and high detergency.
Description
Technical field
The present invention relates to a kind of composition, relate to a kind of industrial clean-out system that is used to reclaim old bottle specifically.
Background technology
Beverage that China produces and beer are at present all based on bottled.Wherein major part is to utilize returnable bottle washing back to reuse.According to statistics, national beverage ultimate production in 2002 is 2,025 ten thousand tons.Because great majority are to utilize returnable bottle, so the washing of bottle is most important, otherwise will directly influence the quality of product.Beer, the bottle-washing agent of soda pop still do not have national standard at present.Beer, soda pop are in the canned production of automatization, and the cleaning quality that reclaims vial is the key link, if cleaning control is bad, the beer quality of brewageing are seriously influenced, and mouthfeel is bad to be the quality problems that highly vigilant of is answered in brewage.。
At present, domestic a lot of employing liquid caustic sodas are made washing composition, though can reach the washing requirement substantially, caustic soda has corrosive nature to the cleaning returnable bottle, and it is fuzzy opaque to wash the back body, discharging of waste liquid basicity height, deficiencies such as contaminate environment.In recent years, though the appearance of related compound bottle-washing agent is arranged, these bottle-washing agents can not make whole of label paper come off; And washing effect is poor, washes out still to leave millimeter paper glue trace on the bottle, washes out a bottle luminance difference, the time have the residual phenomenon of alkali lye to occur; The use temperature height, drawback such as the power consumption water loss is big.In order better to satisfy beer, the cleaning quality of soda pop returnable bottle needs the strong noresidue bottle-washing agent of a kind of high-effective cleansing power.
Summary of the invention
The objective of the invention is to overcome the drawback of existing bottle-washing agent, a kind of highly effective and safe that has of suitable automatization wash bottle processing condition is provided, multi-functional, low consumption also can reduce the solid-liquid two-pack bottle-washing agent of cost of sewage disposal.
Bottle-washing agent of the present invention adopts advanced scientific formula to make the solid-liquid two-pack bottle-washing agent that solid ingredient A and microemulsion water base agent B by identical weight form.
Solid ingredient A is counted by weight percentage, and is made up of caustic soda 60～90%, yellow soda ash 2.5～12.5%, Starso 1～10%, Sunmorl N 60S 0.5～10%, A92R 0.5～10%.
Microemulsion water base agent B is counted by weight percentage, and is made up of following component: fatty alcohol-polyoxyethylene ether 1～5%, polyoxyethylene nonylphenol ether 2～8%, fatty alcohol polyoxyethylene ether sulfate 1～5%, organic solvent 2～6%, sodium polyphosphate 4～12%, silicone antifoam agent 0.5～3%, surplus are water.
The preparation method of solid ingredient A and microemulsion water base agent B is simple, only need with each component by weight the content ratio mix and get final product.
Beneficial effect of the present invention: the solid-liquid two-pack bottle-washing agent that the present invention adopts advanced scientific formula to make is nontoxic, environment friendly and pollution-free; Special advanced person fills a prescription and can dissolve bottle mark tackiness agent in the rapid permeability Beer Bottle millimeter paper, and whole of millimeter paper is come off; Source of pollution at returnable bottle can rapid emulsification disperse greasy dirt and various dirt; The special wash bottle factor of adding makes whole washing process more thorough, the bottle transparency height that washes out, noresidue in the bottle, white vase rate height; Specific soft water performance can effectively stop the fouling of bottle-washing agent; Efficient high function prescription can make wash temperature reduce by 10～15 degree than existing bottle-washing agent, and bottle-washing agent prolongs 2～5 days wash(ing)cycle, and the consumption reduction gain is more obvious.
Embodiment
Embodiment 1
Caustic soda 76 grams, yellow soda ash 11 grams, Starso 7 grams, Sunmorl N 60S 4 grams, A92R 2 grams are mixed and made into solid ingredient A;
Fatty alcohol-polyoxyethylene ether 2 grams, polyoxyethylene nonylphenol ether 7 grams, fatty alcohol polyoxyethylene ether sulfate 1 gram, organic solvent 5 grams, sodium polyphosphate 11 grams, silicone antifoam agent 2 grams, water 72 grams mix and make microemulsion water base agent B.
Embodiment 2
Caustic soda 85 grams, yellow soda ash 5 grams, Starso 3 grams, Sunmorl N 60S 2 grams, A92R5 gram are mixed and made into solid ingredient A;
Fatty alcohol-polyoxyethylene ether 3 grams, polyoxyethylene nonylphenol ether 5 grams, fatty alcohol polyoxyethylene ether sulfate 2 grams, organic solvent 4 grams, sodium polyphosphate 8 grams, silicone antifoam agent 1 gram, water 77 grams mix and make microemulsion water base agent B;
In rinse bath, add quantitative clear water, add 1.5% A by weight, 1.5% B; When being heated to 75～80 ℃, advances rinse bath solution the bottle washing; In washing process,, when dropping to 50～60 scopes, the ms value adds 0.3%A and 0.3%B by weight along with the increase of wash bottle quantity and the prolongation of time.When measuring sodium aluminate content discharging washing raffinate greater than 3% time, prepare new bottle-washing agent again.
In May, 2004, wash bottle was used on automatic production wash bottle line of 3.6/ hour of Beijing beer brewery groups company packing shop, had obtained ideal effect.Concrete outcome is as follows:
| ????4 | ??5.16 | Heavy dirt bottle | ????29.79 | Light | Neutral | ???99.66 | There is not influence |
| ????5 | ??5.17 | Heavy dirt bottle | ????27.87 | Light | Neutral | ???98.37 | There is not influence |
| ????6 | ??5.18 | Heavy dirt bottle | ????27.86 | Light | Neutral | ???98.02 | There is not influence |
| ????7 | ??5.19 | Heavy dirt bottle | ????26.73 | Light | Neutral | ???98.01 | There is not influence |
| ????8 | ??5.20 | Heavy dirt bottle | ????26.92 | Light | Neutral | ???99.20 | There is not influence |
| ????9 | ??5.22 | Heavy dirt bottle | ????22.48 | Light | Neutral | ???99.10 | There is not influence |
| ????10 | ??5.23 | Heavy dirt bottle | ????25.62 | Light | Neutral | ???99.88 | There is not influence |
| ????11 | ??5.24 | Heavy dirt bottle | ????19.33 | Light | Neutral | ???99.81 | There is not influence |
| Add up to | ????288.84 | ???99.81 |
Claims (3)
1, a kind of bottle-washing agent that reclaims vial cleaning usefulness is characterized in that being made of the solid ingredient A and the microemulsion water base agent B of identical weight.
2, recovery vial as claimed in claim 1 cleans the bottle-washing agent of usefulness, it is characterized in that described solid ingredient A counts by weight percentage, form by caustic soda 60～90%, yellow soda ash 2.5～12.5%, Starso 1～10%, Sunmorl N 60S 0.5～10%, A92R 0.5～10%.
3, recovery vial as claimed in claim 1 cleans the bottle-washing agent of usefulness, it is characterized in that described microemulsion water base agent B counts by weight percentage, be made up of following component: fatty alcohol-polyoxyethylene ether 1～5%, polyoxyethylene nonylphenol ether 2～8%, fatty alcohol polyoxyethylene ether sulfate 1～5%, organic solvent 2～6%, sodium polyphosphate 4～12%, silicone antifoam agent 0.5～3%, surplus are water.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB2004100777238A CN1300290C (en) | 2004-12-29 | 2004-12-29 | Bottle cleaner for cleaning recovered bottles |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB2004100777238A CN1300290C (en) | 2004-12-29 | 2004-12-29 | Bottle cleaner for cleaning recovered bottles |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN1651560A true CN1651560A (en) | 2005-08-10 |
| CN1300290C CN1300290C (en) | 2007-02-14 |
Family
ID=34869099
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CNB2004100777238A Expired - Fee Related CN1300290C (en) | 2004-12-29 | 2004-12-29 | Bottle cleaner for cleaning recovered bottles |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN1300290C (en) |
Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101439341B (en) * | 2007-11-19 | 2011-06-15 | 北京北方微电子基地设备工艺研究中心有限责任公司 | Method for cleaning components of semi-conductor processing equipment |
| RU2422499C1 (en) * | 2010-02-19 | 2011-06-27 | Общество с ограниченной ответственностью "Технологии Третьего Тысячелетия" | Detergent |
| CN104479920A (en) * | 2014-12-04 | 2015-04-01 | 内蒙古河西航天科技发展有限公司 | Alkaline cleaner for yoghourt equipment |
| CN104479900A (en) * | 2015-01-14 | 2015-04-01 | 上海承瑶环保科技有限公司 | PEI bottle chip reusing treatment washing agent |
| CN105002023A (en) * | 2015-07-29 | 2015-10-28 | 三峡大学 | Preparation of solid bottle-washing additive |
| CN105176715A (en) * | 2015-09-10 | 2015-12-23 | 黑龙江大学 | Beer bottle cleaning agent and preparation method thereof |
| CN108559653A (en) * | 2018-05-18 | 2018-09-21 | 北京安洁康生物科技有限公司 | A kind of liquid removes mould wash bottle additive and its methods for making and using same |
| CN108715763A (en) * | 2018-06-20 | 2018-10-30 | 湖南辰砾新材料有限公司 | A kind of recycled beer glass bottle enamel |
| CN111621368A (en) * | 2019-02-28 | 2020-09-04 | 湖北茂华化工科技有限公司 | Efficient environment-friendly glass bottle cleaning agent and preparation method thereof |
Family Cites Families (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1066875A (en) * | 1992-06-09 | 1992-12-09 | 太原洗涤剂厂 | A kind of powder bottle washing agent and preparation method thereof |
| CA2251708C (en) * | 1996-04-09 | 2002-11-12 | Unilever Plc | Anti-etch bottle washing solution |
| RU2128214C1 (en) * | 1997-07-02 | 1999-03-27 | Акционерное общество закрытого типа "ФК" | Washing agent for cleaning glassware |
| CN1198469A (en) * | 1998-05-20 | 1998-11-11 | 重庆药用包装容器厂 | High-effect detergent for cleaning beverage bottle |
| CN1115401C (en) * | 2000-02-04 | 2003-07-23 | 上海华士实业总公司 | Detergent |
-
2004
- 2004-12-29 CN CNB2004100777238A patent/CN1300290C/en not_active Expired - Fee Related
Cited By (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101439341B (en) * | 2007-11-19 | 2011-06-15 | 北京北方微电子基地设备工艺研究中心有限责任公司 | Method for cleaning components of semi-conductor processing equipment |
| RU2422499C1 (en) * | 2010-02-19 | 2011-06-27 | Общество с ограниченной ответственностью "Технологии Третьего Тысячелетия" | Detergent |
| CN104479920A (en) * | 2014-12-04 | 2015-04-01 | 内蒙古河西航天科技发展有限公司 | Alkaline cleaner for yoghourt equipment |
| CN104479900A (en) * | 2015-01-14 | 2015-04-01 | 上海承瑶环保科技有限公司 | PEI bottle chip reusing treatment washing agent |
| CN105002023A (en) * | 2015-07-29 | 2015-10-28 | 三峡大学 | Preparation of solid bottle-washing additive |
| CN105002023B (en) * | 2015-07-29 | 2017-08-01 | 三峡大学 | A kind of preparation of solid wash bottle additive |
| CN105176715A (en) * | 2015-09-10 | 2015-12-23 | 黑龙江大学 | Beer bottle cleaning agent and preparation method thereof |
| CN105176715B (en) * | 2015-09-10 | 2018-01-23 | 黑龙江大学 | A kind of Detergent power |
| CN108559653A (en) * | 2018-05-18 | 2018-09-21 | 北京安洁康生物科技有限公司 | A kind of liquid removes mould wash bottle additive and its methods for making and using same |
| CN108715763A (en) * | 2018-06-20 | 2018-10-30 | 湖南辰砾新材料有限公司 | A kind of recycled beer glass bottle enamel |
| CN111621368A (en) * | 2019-02-28 | 2020-09-04 | 湖北茂华化工科技有限公司 | Efficient environment-friendly glass bottle cleaning agent and preparation method thereof |
Also Published As
| Publication number | Publication date |
|---|---|
| CN1300290C (en) | 2007-02-14 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN1300290C (en) | Bottle cleaner for cleaning recovered bottles | |
| CN105176715B (en) | A kind of Detergent power | |
| CN109576077A (en) | Cleaning agent for optical glass | |
| CN107057878A (en) | A kind of environment-friendly type cleaning agent for optical glass and preparation method thereof | |
| CN103374726A (en) | Efficient multipurpose metal cleaning agent | |
| CN101735897A (en) | Separation film washing agent and using method thereof | |
| CN101250465B (en) | Electro-conductive glass substrate cleaning agent and preparation method thereof | |
| CN104312807A (en) | Acid washing bottle additive and application | |
| CN112251298A (en) | Super-concentrated laundry detergent and preparation method of diluent thereof | |
| CN110373275A (en) | It is a kind of without phosphorus except mould wash bottle additive | |
| CN1078243C (en) | Non-phosphate high-effect liquid laundry detergent | |
| CN1403559A (en) | Water-saving washing powder | |
| CN101314750A (en) | Silicon slice detergent and preparation thereof | |
| CN102453625A (en) | Detergent for food glass container | |
| CN104789391B (en) | A kind of biological degradable type cleaning agent and preparation method containing citrus seed oil | |
| CN108300599A (en) | A kind of environment protection multifunctional vial cleaning agent and its preparation method | |
| CN1115401C (en) | Detergent | |
| CN1133339A (en) | High-effective low foam washing liquid | |
| CN100485022C (en) | Automobile case cleaning agent | |
| CN1191238A (en) | Non-phosphate liquid laundry detergent | |
| CN101671608B (en) | Scale remover for sulfur scale in sulfur melting kettle | |
| CN103343347A (en) | Production method of oil removal agent for stainless steel | |
| CN1114680A (en) | Liquid detergent for washing bottle | |
| CN1191893A (en) | Multifunctional bottle cleaning agent | |
| CN1354244A (en) | Liquid detergent capable of resisting cross talk |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| C41 | Transfer of patent application or patent right or utility model | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20170203 Address after: 511455 Guangzhou Province, Nansha District, Dagang Town, high sand village street, No. 23 Patentee after: GUANGZHOU TAISHENG BIOTECHNOLOGY Co.,Ltd. Address before: Three good Panyu District Industrial Zone, Guangzhou Shawan Town, 511487 cities in Guangdong Province Patentee before: GUANGZHOU TAICHENG BIOCHEMICAL TECHNOLOGY CO.,LTD. Effective date of registration: 20170203 Address after: 511455 Guangzhou Province, Nansha District, Dagang Town, high sand village street, No. 23 Patentee after: GUANGZHOU TAISHENG BIOTECHNOLOGY Co.,Ltd. Address before: Guangzhou Province, Nansha District City, the town of Tai Po village, 23 village street, No. Patentee before: GUANGZHOU TAICHENG BIOCHEMICAL TECHNOLOGY CO.,LTD. |
|
| CP01 | Change in the name or title of a patent holder |
Address after: 511455 No. 23 Xincun Street, Gaosha Village, Dagang Town, Nansha District, Guangzhou City, Guangdong Province Patentee after: Guangzhou Taisheng Biotechnology Co.,Ltd. Address before: 511455 No. 23 Xincun Street, Gaosha Village, Dagang Town, Nansha District, Guangzhou City, Guangdong Province Patentee before: GUANGZHOU TAISHENG BIOTECHNOLOGY Co.,Ltd. |
|
| CP01 | Change in the name or title of a patent holder | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20070214 Termination date: 20211229 |
|
| CF01 | Termination of patent right due to non-payment of annual fee |