CN1508139A - Process for extracting rubusoside of fruit of Gorsvenor Momordica - Google Patents
Process for extracting rubusoside of fruit of Gorsvenor Momordica Download PDFInfo
- Publication number
- CN1508139A CN1508139A CNA021280657A CN02128065A CN1508139A CN 1508139 A CN1508139 A CN 1508139A CN A021280657 A CNA021280657 A CN A021280657A CN 02128065 A CN02128065 A CN 02128065A CN 1508139 A CN1508139 A CN 1508139A
- Authority
- CN
- China
- Prior art keywords
- momordica
- fruit
- grosvenor
- gorsvenor
- membrane separation
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 235000009815 Momordica Nutrition 0.000 title claims abstract description 60
- 241000218984 Momordica Species 0.000 title claims abstract description 60
- 235000013399 edible fruits Nutrition 0.000 title claims abstract description 26
- 238000000034 method Methods 0.000 title claims description 23
- YWPVROCHNBYFTP-UHFFFAOYSA-N Rubusoside Natural products C1CC2C3(C)CCCC(C)(C(=O)OC4C(C(O)C(O)C(CO)O4)O)C3CCC2(C2)CC(=C)C21OC1OC(CO)C(O)C(O)C1O YWPVROCHNBYFTP-UHFFFAOYSA-N 0.000 title claims description 16
- YWPVROCHNBYFTP-OSHKXICASA-N rubusoside Chemical compound O([C@]12C(=C)C[C@@]3(C1)CC[C@@H]1[C@@](C)(CCC[C@]1([C@@H]3CC2)C)C(=O)O[C@H]1[C@@H]([C@@H](O)[C@H](O)[C@@H](CO)O1)O)[C@@H]1O[C@H](CO)[C@@H](O)[C@H](O)[C@H]1O YWPVROCHNBYFTP-OSHKXICASA-N 0.000 title claims description 16
- 238000000926 separation method Methods 0.000 claims abstract description 24
- 239000000706 filtrate Substances 0.000 claims abstract description 23
- 239000012528 membrane Substances 0.000 claims abstract description 19
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 16
- 239000000047 product Substances 0.000 claims abstract description 16
- 239000011573 trace mineral Substances 0.000 claims abstract description 10
- 235000013619 trace mineral Nutrition 0.000 claims abstract description 10
- 239000012535 impurity Substances 0.000 claims abstract description 8
- 239000000835 fiber Substances 0.000 claims abstract description 7
- 150000004676 glycans Chemical class 0.000 claims abstract description 7
- 229920001282 polysaccharide Polymers 0.000 claims abstract description 7
- 239000005017 polysaccharide Substances 0.000 claims abstract description 7
- 102000004169 proteins and genes Human genes 0.000 claims abstract description 7
- 108090000623 proteins and genes Proteins 0.000 claims abstract description 7
- 238000001291 vacuum drying Methods 0.000 claims abstract description 6
- 239000003895 organic fertilizer Substances 0.000 claims abstract description 4
- 238000001914 filtration Methods 0.000 claims abstract description 3
- 238000002791 soaking Methods 0.000 claims abstract 3
- 239000002904 solvent Substances 0.000 claims description 13
- 230000000712 assembly Effects 0.000 claims description 11
- 238000000429 assembly Methods 0.000 claims description 11
- 238000001035 drying Methods 0.000 claims description 7
- 239000001814 pectin Substances 0.000 claims description 6
- 229920001277 pectin Polymers 0.000 claims description 6
- 235000010987 pectin Nutrition 0.000 claims description 6
- 235000011171 Thladiantha grosvenorii Nutrition 0.000 claims description 4
- 239000012634 fragment Substances 0.000 claims description 4
- 238000013467 fragmentation Methods 0.000 claims description 4
- 238000006062 fragmentation reaction Methods 0.000 claims description 4
- 239000002994 raw material Substances 0.000 claims description 4
- 238000004064 recycling Methods 0.000 claims description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 4
- 235000021022 fresh fruits Nutrition 0.000 claims description 3
- 238000001728 nano-filtration Methods 0.000 claims description 3
- 238000000108 ultra-filtration Methods 0.000 claims description 3
- 241001409321 Siraitia grosvenorii Species 0.000 claims 1
- 239000011877 solvent mixture Substances 0.000 claims 1
- 235000019441 ethanol Nutrition 0.000 abstract description 8
- 238000000605 extraction Methods 0.000 abstract description 7
- 229930182470 glycoside Natural products 0.000 abstract description 5
- 150000002338 glycosides Chemical class 0.000 abstract description 5
- AEMOLEFTQBMNLQ-BKBMJHBISA-N alpha-D-galacturonic acid Chemical compound O[C@H]1O[C@H](C(O)=O)[C@H](O)[C@H](O)[C@H]1O AEMOLEFTQBMNLQ-BKBMJHBISA-N 0.000 abstract 1
- 238000001816 cooling Methods 0.000 abstract 1
- RFSUNEUAIZKAJO-ARQDHWQXSA-N Fructose Chemical compound OC[C@H]1O[C@](O)(CO)[C@@H](O)[C@@H]1O RFSUNEUAIZKAJO-ARQDHWQXSA-N 0.000 description 4
- 229930091371 Fructose Natural products 0.000 description 4
- 239000005715 Fructose Substances 0.000 description 4
- 239000004615 ingredient Substances 0.000 description 4
- 239000000243 solution Substances 0.000 description 4
- 239000000126 substance Substances 0.000 description 4
- 244000185386 Thladiantha grosvenorii Species 0.000 description 3
- 239000002956 ash Substances 0.000 description 3
- 238000007654 immersion Methods 0.000 description 3
- 239000000203 mixture Substances 0.000 description 3
- 238000003672 processing method Methods 0.000 description 3
- 239000002351 wastewater Substances 0.000 description 3
- 239000002253 acid Substances 0.000 description 2
- 230000001476 alcoholic effect Effects 0.000 description 2
- 239000007864 aqueous solution Substances 0.000 description 2
- 238000009264 composting Methods 0.000 description 2
- 239000012141 concentrate Substances 0.000 description 2
- 235000009508 confectionery Nutrition 0.000 description 2
- 229930182478 glucoside Natural products 0.000 description 2
- 150000008131 glucosides Chemical class 0.000 description 2
- 239000003960 organic solvent Substances 0.000 description 2
- 235000017048 Garcinia mangostana Nutrition 0.000 description 1
- 240000006053 Garcinia mangostana Species 0.000 description 1
- ILRCGYURZSFMEG-UHFFFAOYSA-N Salidroside Natural products OC1C(O)C(O)C(CO)OC1OCCC1=CC=C(O)C=C1 ILRCGYURZSFMEG-UHFFFAOYSA-N 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- 150000007516 brønsted-lowry acids Chemical class 0.000 description 1
- 150000007528 brønsted-lowry bases Chemical class 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 238000004042 decolorization Methods 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 150000002191 fatty alcohols Chemical class 0.000 description 1
- 229930003935 flavonoid Natural products 0.000 description 1
- 150000002215 flavonoids Chemical class 0.000 description 1
- 235000017173 flavonoids Nutrition 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 235000003599 food sweetener Nutrition 0.000 description 1
- 238000007429 general method Methods 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000011785 micronutrient Substances 0.000 description 1
- 235000013369 micronutrients Nutrition 0.000 description 1
- 230000001681 protective effect Effects 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 239000011347 resin Substances 0.000 description 1
- 229920005989 resin Polymers 0.000 description 1
- ILRCGYURZSFMEG-RQICVUQASA-N salidroside Chemical compound O[C@@H]1[C@@H](O)[C@H](O)[C@@H](CO)OC1OCCC1=CC=C(O)C=C1 ILRCGYURZSFMEG-RQICVUQASA-N 0.000 description 1
- 239000003765 sweetening agent Substances 0.000 description 1
- -1 yield is low Substances 0.000 description 1
Landscapes
- Separation Using Semi-Permeable Membranes (AREA)
- Medicines Containing Plant Substances (AREA)
- Polysaccharides And Polysaccharide Derivatives (AREA)
Abstract
The extraction process of grosvenor's momordica fruit glycoside includes the following steps: breaking grosvenor's monordica fruit, adding ethyl alcohol solution, soaking for 5-15 hr. at 30-60 deg.C, filtering to obtain filtrate, cooling to 20-35 deg.C, making the filtrate pass through pressure pump and under the working pressure of 0.01-0.2 MPa feeding said filtrate into three membrane separation components successively: first stage, trapping and separating out concentrated grosvenor's monordica fruit fibre, protein, pectine and impurity which can be used for making organic fertilizer; second storage, vacuum drying the obtained concentrated grosvenor's monordica fruit glycoside solution to obtain grosvenor's monorica fruit glycoside product; and third stage, obtain the concentrated grosvenor's momordica fruit polysaccharide and trace elements.
Description
(1) technical field
The invention belongs to a kind of processing method of from Grosvenor Momordica, extracting sweet glucoside.
(2) technical background
Grosvenor Momordica is the well-known pharmaceutically-active fruit that has, and its contained Momordica-Glycosides can be used as medicine and also can be used as sweeting agent, and its contained fructose and trace element can be used as the additive of protective foods.It mainly is water or buck lixiviate that present people extract the method that effective ingredient is used in the Grosvenor Momordica, and the filtrate concentrate drying promptly gets product.Effective ingredient extraction yield in the Grosvenor Momordica is low like this, products obtained therefrom composition complexity.
The patent application of some research Grosvenor Momordica effective ingredient extracting method is now also arranged, as Chinese invention patent application 87101850 " extracting method of mangosteen sweetener ", Chinese invention patent application 02113548.7 " method of extraction separation multiple components from Grosvenor Momordica ".These methods all are to adopt different resin decolorization, removal impurity, and effective ingredients such as absorption Momordica-Glycosides wash out with organic solvent again, and concentrate drying gets product.Though also can isolate different compositions such as Momordica-Glycosides, grosvenor momordica flavonoid, momordica grosvenori polysaccharide, yield is low, product purity is not high, complex process, facility investment is big, the product cost height.And need in the production process to use a large amount of bronsted lowry acids and bases bronsted lowries, and organic solvent such as Fatty Alcohol(C12-C14 and C12-C18), a large amount of high concentrated organic wastewaters of generation need reinvestment to handle, otherwise with contaminate environment.
(3) summary of the invention
The purpose of this invention is to provide a kind of new processing method of from Grosvenor Momordica, extracting sweet glucoside, adopt membrane separation technique, extract Momordica-Glycosides, momordica grosvenori polysaccharide and trace element, Grosvenor Momordica fiber, protein, pectin and impurity respectively.This processing method product yield height, the purity height, equipment is simple, and cost is low, and does not produce the waste water of any contaminate environment.
Process for extracting rubusoside of fruit of Gorsvenor Momordica of the present invention comprises the steps:
1 Grosvenor Momordica is cleaned, fragmentation;
2 add alcohol solvent, under 30～60 ℃ of temperature, soak 5～15 hours.
3 filter the Grosvenor Momordica leach liquor, and temperature is reduced to 20～35 ℃; Pomace is discarded;
4 filtrates are sent into three kinds of membrane separation assemblies through pressure pump order under 0.01～0.2Mpa operating pressure;
5 by the first heavy film.Hold back and isolate spissated Grosvenor Momordica fiber, protein, pectin and impurity, send, be used to make organic fertilizer from first relief outlet;
6 residual filtrate are held back and are isolated spissated Momordica-Glycosides solution by the second heavy film, send from second relief outlet, through vacuum-drying, get the Momordica-Glycosides product;
7 residual filtrate are held back and are isolated spissated momordica grosvenori polysaccharide and trace element by triple films, send from the 3rd relief outlet, are dense thick Grosvenor Momordica massecuite;
8 discharge recycling use by the residual filtrate behind triple films from solvent outlet.
The advantage of process for extracting rubusoside of fruit of Gorsvenor Momordica of the present invention is: 1 separation, extraction and a concentrated step finish, and technology is simple, once can get multiple product, and can produce continuously; 2 yield height, the product purity height, the total salidroside content of gained Momordica-Glycosides reaches 85%, and Grosvenor Momordica massecuite total reducing sugar and micronutrient levels all are higher than the general method products obtained therefrom more than or equal to 20%; 3 need to use the second alcohol and water to be solvent, and recyclable recycling, conservation, and cost descends greatly; 4 solvent for use are pollution-free, also do not produce any waste water and dregs that influences environment; 5 equipment are simple, establish money low.
(4) description of drawings
Fig. 1 is the process flow sheet of process for extracting rubusoside of fruit of Gorsvenor Momordica of the present invention.
(5) embodiment
The concrete technical process of process for extracting rubusoside of fruit of Gorsvenor Momordica of the present invention as shown in Figure 1.
It is broken that 1 broken fresh Fructus Momordicae or dried fructus momordicae are cleaned the back, and the fragment out to out is 0.5～2 centimetre, do not squish kernel simultaneously.
2 immersion ethanol add water and are mixed with 30～80% ethanolic solns, in the Grosvenor Momordica after the adding fragmentation.When being raw material with fresh fruit, Grosvenor Momordica is 1 to 1～3 with the weight ratio of alcohol solvent, and when being raw material with dry fruit, Grosvenor Momordica is 1 to 10～15 with the weight ratio of alcohol solvent.Mixture soaked 5～15 hours under 40～60 ℃ of temperature.
3 filtering mixts filter with 150～250 mesh filter screens, the Grosvenor Momordica leach liquor, the leach liquor pH value is 3～8, liquid temperature drop to 20～35 ℃.
4 first step pressurization separation and Extraction Grosvenor Momordica leach liquor is sent into pressure pump, under 0.01～0.08Mpa operating pressure, send into the first heavy membrane separation assemblies, by the first heavy film, hold back and isolate spissated Grosvenor Momordica fiber, protein, pectin, impurity and ash, send from first relief outlet, be used to make organic fertilizer;
The 5 second stage remaining filtrate of pressurization separation and Extraction is sent into the second heavy membrane separation assemblies by second pressure pump under 0.05～0.1Mpa operating pressure.By the second heavy film, to hold back and isolate spissated Momordica-Glycosides solution, concentration is 25～30 degree Beaume, sends from second relief outlet, through vacuum-drying, drying temperature is for being less than or equal to 75 ℃.Get the Momordica-Glycosides product;
6 third stage pressurization separation and Extraction secondary separates the remaining filtrate in back by the 3rd pressure pump, sends into triple membrane separation assemblies under 0.1～0.2Mpa operating pressure.By triple films, to hold back and isolate spissated arhat fructose and trace element etc., concentration is 25～30 degree Beaume, sends from the 3rd relief outlet, is dense thick Grosvenor Momordica massecuite product.
7 by the discharge of the residual filtrate behind triple films recycling use.
Embodiment 1:
Get 1 kilogram in Grosvenor Momordica fresh fruit, be broken for 1～2 centimetre fragment, add 2 kilogram 40% the alcoholic acid aqueous solution, heat, keep 40～50 ℃ of temperature, soaked 10 hours to 50 ℃.Filter with 200 mesh filter screens, get the Grosvenor Momordica leach liquor, discarded pomace can be used for composting etc.The leach liquor pH value is 5.Leach liquor is cooled to 25～30 ℃, through first step pressure pump, under 0.01～0.03Mpa operating pressure,, hold back and isolate spissated Grosvenor Momordica fiber, protein, pectin, impurity and ash totally 80 grams, send from first relief outlet by the first heavy ultra-filtration membrane separation assembly; Residual filtrate weighs nanofiltration membrane separation assembly by second through second stage pressure pump under 0.04～0.06Mpa operating pressure, hold back and isolate spissated Momordica-Glycosides solution, concentration is 28 degree Beaume, send from second relief outlet, through vacuum-drying, drying temperature is 50～70 ℃, gets Momordica-Glycosides 20 grams, and chemical examination wherein contains general glycoside 85%.Second stage residual filtrate is passed through triple RO membrane separation assemblies through third stage pressure pump under 0.10～0.15Mpa operating pressure, hold back and isolate spissated arhat fructose and trace element etc., concentration is 30 degree Beaume, send from the 3rd relief outlet, be dense thick Grosvenor Momordica massecuite product 600 grams, chemical examination wherein contains polysaccharide and trace element 70%.The alcohol solvent that leaches directly reclaims and is used for the Grosvenor Momordica immersion.
Embodiment 2:
Get 1 kilogram in Grosvenor Momordica dry fruit, be broken for 0.5～1.5 centimetre fragment, add 10 kilogram 50% the alcoholic acid aqueous solution, heat, keep 40～60 ℃ of temperature, soaked 15 hours to 60 ℃.Filter with 250 mesh filter screens, get the Grosvenor Momordica leach liquor, discarded pomace can be used for composting etc.The leach liquor pH value is 6.Leach liquor is cooled to 25～30 ℃, through first step pressure pump, under 0.02～0.05Mpa operating pressure,, hold back and isolate spissated Grosvenor Momordica fiber, protein, pectin, impurity and ash totally 30 grams, send from first relief outlet by the first heavy ultra-filtration membrane separation assembly; Residual filtrate weighs nanofiltration membrane separation assembly by second through second stage pressure pump under 0.05～0.08Mpa operating pressure, hold back and isolate spissated Momordica-Glycosides solution, concentration is 26 degree Beaume, send from second relief outlet, through vacuum-drying, 70 ℃ of drying temperatures get Momordica-Glycosides 80 grams, and chemical examination wherein contains general glycoside 85%.Second stage residual filtrate is passed through triple RO membrane separation assemblies through third stage pressure pump under 0.15～0.20Mpa operating pressure, hold back and isolate spissated arhat fructose and trace element etc., concentration is 30 degree Beaume, send from the 3rd relief outlet, be dense thick Grosvenor Momordica massecuite product 700 grams, chemical examination wherein contains polysaccharide and trace element 71%.The alcohol solvent that leaches directly reclaims and is used for the Grosvenor Momordica immersion.
Claims (10)
1 one kinds of process for extracting rubusoside of fruit of Gorsvenor Momordica is characterized by and comprise the steps:
1. Grosvenor Momordica is cleaned, fragmentation;
2. add alcohol solvent, under 30～60 ℃ of temperature, soaked 5～15 hours.
3. filter the Grosvenor Momordica leach liquor, and temperature is reduced to 20～35 ℃;
4. filtrate is sent into three kinds of membrane separation assemblies through pressure pump order under 0.01～0.2Mpa operating pressure;
5. by the first heavy film.Hold back and isolate spissated Grosvenor Momordica fiber, protein, pectin and impurity, send, be used to make organic fertilizer from first relief outlet;
6. residual filtrate is held back and is isolated spissated Momordica-Glycosides solution by the second heavy film, sends from second relief outlet, through vacuum-drying, gets the Momordica-Glycosides product;
7. residual filtrate is held back and is isolated spissated momordica grosvenori polysaccharide and trace element by triple films, sends from the 3rd relief outlet, is dense thick Grosvenor Momordica massecuite;
8. discharge directly recycling use from solvent outlet by the residual filtrate behind triple films.
2 process for extracting rubusoside of fruit of Gorsvenor Momordica as claimed in claim 1 is characterized by:
Used alcohol solvent is that ethanol adds 30～80% ethanolic solns that water is mixed with.
3 process for extracting rubusoside of fruit of Gorsvenor Momordica as claimed in claim 1 or 2 is characterized by:
When being raw material with fresh fruit, Grosvenor Momordica is 1 to 1～3 with the weight ratio of alcohol solvent, and when being raw material with dry fruit, Grosvenor Momordica is 1 to 10～15 with the weight ratio of alcohol solvent.
4 process for extracting rubusoside of fruit of Gorsvenor Momordica as claimed in claim 1 or 2 is characterized by:
The Grosvenor Momordica leach liquor weighs membrane separation assemblies by first through first step pressure pump under 0.01～0.0gMpa operating pressure;
First step residual filtrate weighs membrane separation assemblies by second through second stage pressure pump under 0.05～0.10Mpa operating pressure;
Second stage residual filtrate is passed through triple membrane separation assemblies through third stage pressure pump under 0.10～0.20Mpa operating pressure.
5 process for extracting rubusoside of fruit of Gorsvenor Momordica as claimed in claim 1 or 2 is characterized by:
The Grosvenor Momordica leach liquor weighs ultra-filtration membrane separation assembly by first through first step pressure pump under 0.01～0.03Mpa operating pressure;
First step residual filtrate weighs nanofiltration membrane separation assembly by second through second stage pressure pump under 0.04～0.06Mpa operating pressure;
Second stage residual filtrate is passed through triple RO membrane separation assemblies through third stage pressure pump under 0.10～0.15Mpa operating pressure.
6 process for extracting rubusoside of fruit of Gorsvenor Momordica as claimed in claim 1 or 2 is characterized by:
The fragment out to out is 0.5～2 centimetre after the Grosvenor Momordica fragmentation, does not squish kernel simultaneously.
7 process for extracting rubusoside of fruit of Gorsvenor Momordica as claimed in claim 1 or 2 is characterized by:
Soaking filtration back gained Grosvenor Momordica leach liquor pH value is 3～8.
8 process for extracting rubusoside of fruit of Gorsvenor Momordica as claimed in claim 1 or 2 is characterized by:
Spissated Momordica-Glycosides solution drying temperature is less than or equal to 75 ℃.
9 process for extracting rubusoside of fruit of Gorsvenor Momordica as claimed in claim 1 or 2 is characterized by:
Spissated Momordica-Glycosides solution drying temperature is 50～70 ℃.
10 process for extracting rubusoside of fruit of Gorsvenor Momordica as claimed in claim 1 or 2 is characterized by:
Soaking back Grosvenor Momordica and solvent mixture filters with 150～250 mesh filter screens.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 02128065 CN1266160C (en) | 2002-12-17 | 2002-12-17 | Process for extracting rubusoside of fruit of Gorsvenor Momordica |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 02128065 CN1266160C (en) | 2002-12-17 | 2002-12-17 | Process for extracting rubusoside of fruit of Gorsvenor Momordica |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN1508139A true CN1508139A (en) | 2004-06-30 |
| CN1266160C CN1266160C (en) | 2006-07-26 |
Family
ID=34231211
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 02128065 Expired - Fee Related CN1266160C (en) | 2002-12-17 | 2002-12-17 | Process for extracting rubusoside of fruit of Gorsvenor Momordica |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN1266160C (en) |
Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1324043C (en) * | 2005-05-26 | 2007-07-04 | 广西中医学院 | Prepn and use of high-purity momordica glycoside V |
| CN101289517B (en) * | 2008-05-30 | 2010-11-03 | 广西师范大学 | Process for abstracting momordica grosvenori polysaccharide |
| CN101249056B (en) * | 2008-01-11 | 2011-06-29 | 美晨集团股份有限公司 | Anti-inflammation gargle water and method of preparing the same |
| CN103100306A (en) * | 2012-12-25 | 2013-05-15 | 厦门市天泉鑫膜科技股份有限公司 | Extraction device of para hydroxybenzene glycine conversion liquid through film method and direct process of extraction device |
| CN101522058B (en) * | 2006-09-07 | 2014-01-29 | 维多利亚生物有限公司 | Sweetening compositions and methods of making them |
| CN103846008A (en) * | 2012-12-04 | 2014-06-11 | 厦门市天泉鑫膜科技股份有限公司 | Device for continuously concentrating and separating substance by membrane and separation method |
| CN106832050A (en) * | 2017-02-20 | 2017-06-13 | 湖南华诚生物资源股份有限公司 | The method that pectin is separated from Momordica grosvenori production waste residue |
| US11576412B2 (en) | 2016-10-24 | 2023-02-14 | Guilin Gfs Monk Fruit Corporation | Extracts from fruits of the Cucurbitaceae family, and methods of preparing thereof |
| CN118873985A (en) * | 2024-09-27 | 2024-11-01 | 云南绿华食品有限公司 | A device for extracting mogroside from mogroside powder with multi-stage absorption function |
-
2002
- 2002-12-17 CN CN 02128065 patent/CN1266160C/en not_active Expired - Fee Related
Cited By (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1324043C (en) * | 2005-05-26 | 2007-07-04 | 广西中医学院 | Prepn and use of high-purity momordica glycoside V |
| US11464247B2 (en) | 2006-09-07 | 2022-10-11 | Guilin Gfs Monk Fruit Corp. | Sweetening compositions and processes for preparing them |
| CN101522058B (en) * | 2006-09-07 | 2014-01-29 | 维多利亚生物有限公司 | Sweetening compositions and methods of making them |
| CN101249056B (en) * | 2008-01-11 | 2011-06-29 | 美晨集团股份有限公司 | Anti-inflammation gargle water and method of preparing the same |
| CN101289517B (en) * | 2008-05-30 | 2010-11-03 | 广西师范大学 | Process for abstracting momordica grosvenori polysaccharide |
| CN103846008A (en) * | 2012-12-04 | 2014-06-11 | 厦门市天泉鑫膜科技股份有限公司 | Device for continuously concentrating and separating substance by membrane and separation method |
| CN103100306A (en) * | 2012-12-25 | 2013-05-15 | 厦门市天泉鑫膜科技股份有限公司 | Extraction device of para hydroxybenzene glycine conversion liquid through film method and direct process of extraction device |
| CN103100306B (en) * | 2012-12-25 | 2015-04-08 | 厦门市天泉鑫膜科技股份有限公司 | Extraction device of para hydroxybenzene glycine conversion liquid through film method and direct process of extraction device |
| US11576412B2 (en) | 2016-10-24 | 2023-02-14 | Guilin Gfs Monk Fruit Corporation | Extracts from fruits of the Cucurbitaceae family, and methods of preparing thereof |
| CN106832050A (en) * | 2017-02-20 | 2017-06-13 | 湖南华诚生物资源股份有限公司 | The method that pectin is separated from Momordica grosvenori production waste residue |
| CN106832050B (en) * | 2017-02-20 | 2019-08-09 | 湖南华诚生物资源股份有限公司 | Method for separating pectin from mangosteen production waste residue |
| CN118873985A (en) * | 2024-09-27 | 2024-11-01 | 云南绿华食品有限公司 | A device for extracting mogroside from mogroside powder with multi-stage absorption function |
| CN118873985B (en) * | 2024-09-27 | 2024-12-13 | 云南绿华食品有限公司 | Siraitia grosvenorii powder sweet glycoside extraction device with multistage absorption function |
Also Published As
| Publication number | Publication date |
|---|---|
| CN1266160C (en) | 2006-07-26 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN101961371B (en) | Method for extracting and separating ginsenoside, flavone and polysaccharide from sweet gynostemma pentaphylla | |
| CN1228968A (en) | Production method for extracting flavonoid compound extract or powder from bamboo leaf | |
| CN116023422B (en) | Method for extracting ginsenoside from ginseng residue and utilizing residue after extraction | |
| CN100336822C (en) | Method for extracting chimonin | |
| CN1266160C (en) | Process for extracting rubusoside of fruit of Gorsvenor Momordica | |
| CN110892987A (en) | Preparation method of wolfberry syrup | |
| CN1854149A (en) | Extraction of Momordica grosvenori beet aglucone V | |
| CN111588043B (en) | Preparation method of dietary fiber based on Siraitia grosvenorii waste | |
| CN104403022A (en) | Preparation method of laminarin | |
| CN103349850B (en) | A kind of method for extracting active ingredient in wax-apple | |
| CN1248992C (en) | Preparation of oligomer and monomer from tannin by catalytic hydrogen degradation | |
| CN109627350A (en) | A kind of extracting method of mulberry leaf active material | |
| CN113429401A (en) | Mangiferin extraction and separation method | |
| CN103520256A (en) | Preparation method of high-purity gynostemma pentaphylla total saponin for veterinary drug | |
| CN112457431A (en) | Production method of dry and wet raw material blended pectin | |
| CN1224022A (en) | New process for extracting tea saponin | |
| CN104402952B (en) | A kind of method that mandarin oil and aurantiamarin are extracted in orange peel | |
| CN109467580B (en) | Extraction process of naringin | |
| CN115645452A (en) | Grading extraction preparation method of phyllanthus emblica polyphenol | |
| CN103159612B (en) | Industrialization production technology for extracting ginkgolic acid from Ginkgo testa | |
| CN102719485A (en) | Transformation method of ethanol by utilizing starch in momordica grosvenori swingle roots | |
| CN114031589A (en) | A kind of method for extracting proanthocyanidins from Aronia nigra | |
| CN113662976A (en) | Extraction method of purslane extract and obtained product | |
| CN113082124A (en) | Method for simultaneously preparing vitex rotundifolia seed oil and flavone extract | |
| CN112724190A (en) | Method for extracting ecdysone from herba Eragrostis Nigrae |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| C17 | Cessation of patent right | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20060726 Termination date: 20100118 |