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CN1588558B - A scanning probe microscope probe driving device - Google Patents

A scanning probe microscope probe driving device Download PDF

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Publication number
CN1588558B
CN1588558B CN2004100700039A CN200410070003A CN1588558B CN 1588558 B CN1588558 B CN 1588558B CN 2004100700039 A CN2004100700039 A CN 2004100700039A CN 200410070003 A CN200410070003 A CN 200410070003A CN 1588558 B CN1588558 B CN 1588558B
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piezoelectric ceramic
probe
ceramic tube
pairs
crystal
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CN1588558A (en
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白雪冬
梁学锦
陈东敏
王恩哥
薛其坤
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Institute of Physics of CAS
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Abstract

本发明公开了一种扫描探针显微镜的探针驱动装置,包括固定槽、夹紧套层、滑块、剪切晶体和压电陶瓷管,滑块通过固定在其外表面相对两侧的两对剪切晶体设置在夹紧套层内,与矩形套层夹紧并可沿其内壁滑动,夹紧套层通过固定在其外壁相对两侧的两对剪切晶体设置在固定槽内,与固定槽夹紧并可沿与所述滑块上剪切晶体驱动方向垂直的方向横向滑动,压电陶瓷管与滑块轴向固定,与滑块连接的压电陶瓷管负责探针纵向移动,与探针连接的压电陶瓷管负责三维方向上位置的细调。该装置可在非常有限的小空间内实现扫描探针显微镜的探针(或样品)位置在三维方向上大范围地高精度调节。

The invention discloses a probe driving device of a scanning probe microscope, which comprises a fixing groove, a clamping sleeve, a slider, a shear crystal and a piezoelectric ceramic tube. The pair of shearing crystals are arranged in the clamping sleeve, clamped with the rectangular sleeve and can slide along its inner wall, and the clamping sleeve is arranged in the fixing groove through two pairs of shearing crystals fixed on opposite sides of the outer wall. The fixing groove is clamped and can slide laterally along the direction perpendicular to the driving direction of the shear crystal on the slider. The piezoelectric ceramic tube is axially fixed to the slider, and the piezoelectric ceramic tube connected to the slider is responsible for the longitudinal movement of the probe. The piezoelectric ceramic tube connected with the probe is responsible for the fine adjustment of the position in three dimensions. The device can realize large-scale and high-precision adjustment of the position of the probe (or sample) of the scanning probe microscope in the three-dimensional direction in a very limited small space.

Description

一种扫描探针显微镜探针驱动装置 A scanning probe microscope probe driving device

技术领域technical field

本发明涉及一种驱动装置,尤其涉及一种安装在电子显微镜中的扫描探针显微镜探针驱动装置。The invention relates to a driving device, in particular to a scanning probe microscope probe driving device installed in an electron microscope.

背景技术Background technique

人们采用新近发明的扫描探针显微镜技术来测量材料微区的表面结构和表面物理、化学和力学等性质,扫描探针显微镜通常包括机械和电子学两部分,机械部分控制扫描探针显微镜探针的移动,电子学部分负责各种信号的加载和对探测到的数据信号进行处理。近几年,随着纳米技术的不断发展,人们投入大量的人力、物力对纳米结构和物性表征的新方法新技术进行研究,但由于纳米材料结构的微观化,如何操纵纳米材料并进行原位结构和物性的表征,成为摆在研究人员面前的一个难题。现有的可直接观察微观结构的设备是电子显微镜,将其与扫描探针显微镜联合使解决上述难题成为可能,而电子显微镜的样品传输和操作空间非常有限,在现有技术中,无法在如此之小的操作空间内在三维方向上大范围地精确驱动扫描探针显微镜的探针。People use the newly invented scanning probe microscope technology to measure the surface structure and surface physical, chemical and mechanical properties of material micro-regions. Scanning probe microscopes usually include two parts, mechanical and electronic, and the mechanical part controls the scanning probe microscope probe. The electronic part is responsible for loading various signals and processing the detected data signals. In recent years, with the continuous development of nanotechnology, people have invested a lot of manpower and material resources in the research of new methods and technologies for nanostructure and physical property characterization. However, due to the microscopic structure of nanomaterials, how to manipulate nanomaterials and perform in-situ The characterization of structure and physical properties has become a difficult problem for researchers. The existing equipment that can directly observe the microstructure is the electron microscope. Combining it with the scanning probe microscope makes it possible to solve the above problems. However, the sample transportation and operation space of the electron microscope are very limited. The tip of the scanning probe microscope can be precisely driven in a large range in three dimensions within a small operating space.

发明内容Contents of the invention

针对现有技术存在的不足,本发明的目的在于提供一种可在小空间内实现扫描探针显微镜的探针(或样品)位置在三维方向上大范围高精度地调节的驱动装置。In view of the deficiencies in the prior art, the purpose of the present invention is to provide a driving device capable of adjusting the position of the probe (or sample) of a scanning probe microscope in a large range and with high precision in three-dimensional directions in a small space.

为实现上述目的,本发明扫描探针显微镜探针驱动装置包括固定槽、夹紧套层、滑块、剪切晶体和压电陶瓷管,滑块通过固定在其外表面相对两侧的两对剪切晶体设置在夹紧套层内,与矩形套层夹紧并可沿其内壁滑动,夹紧套层通过固定在其外壁相对两侧的两对剪切晶体设置在固定槽内,与固定槽夹紧并可沿与所述滑块上剪切晶体驱动方向垂直的方向横向滑动,压电陶瓷管与滑块轴向固定,与滑块连接的压电陶瓷管负责纵向移动,另一压电陶瓷管负责三维方向位置的细调。In order to achieve the above object, the scanning probe microscope probe driving device of the present invention includes a fixed groove, a clamping sleeve, a slider, a shear crystal and a piezoelectric ceramic tube. The shearing crystal is set in the clamping sleeve, clamped with the rectangular sleeve and can slide along its inner wall, and the clamping sleeve is arranged in the fixing groove through two pairs of shearing crystals fixed on the opposite sides of the outer wall, and fixed The groove is clamped and can slide laterally along the direction perpendicular to the driving direction of the shear crystal on the slider. The piezoelectric ceramic tube is fixed axially with the slider, and the piezoelectric ceramic tube connected with the slider is responsible for longitudinal movement. The other piezoelectric ceramic tube is The electroceramic tube is responsible for the fine adjustment of the three-dimensional direction position.

进一步地,所述固定槽的外表面呈圆弧形,其内表面呈与夹紧套层相配的阶梯状。Further, the outer surface of the fixing groove is arc-shaped, and the inner surface is stepped to match the clamping sleeve.

进一步地,所述夹紧套层为一矩形套筒。Further, the clamping sleeve is a rectangular sleeve.

进一步地,所述滑块呈长方体状。Further, the slider is in the shape of a cuboid.

进一步地,所述剪切晶体的位置靠近滑块、夹紧套层的两端,其厚度与安装间隙相配。Further, the position of the shear crystal is close to the two ends of the slider and the clamping sleeve, and its thickness matches the installation gap.

进一步地,所述压电陶瓷管为两个,两压电陶瓷管对接后安装在滑块的一端。Further, there are two piezoelectric ceramic tubes, and the two piezoelectric ceramic tubes are butted and installed at one end of the slider.

进一步地,所述压电陶瓷管为两个,也可分别安装在滑块的两端。Further, there are two piezoelectric ceramic tubes, which can also be respectively installed at both ends of the slider.

进一步地,所述负责三维方向位置细调的压电陶瓷管的顶端设置有探针安装座。Further, the top end of the piezoelectric ceramic tube responsible for the fine adjustment of the three-dimensional direction is provided with a probe mounting seat.

进一步地,所述压电陶瓷管、探针安装座、滑块之间采用绝缘材料连接,连接处用真空绝缘树脂胶进行固化。Further, the piezoelectric ceramic tube, the probe mount, and the slider are connected by insulating material, and the connection is cured with vacuum insulating resin glue.

进一步地,所述剪切晶体与矩形套层、固定槽之间设有绝缘层,该绝缘层可为薄的宝石片。Further, an insulating layer is provided between the shear crystal, the rectangular sleeve layer and the fixing groove, and the insulating layer may be a thin gemstone sheet.

本发明通过四对剪切晶体和与滑块固定的第一压电陶瓷管分别来控制探针在横向和纵向上的移动,再通过与探针粘接的第二压电陶瓷管完成三维方向上位置的细调,由于剪切晶体和压电陶瓷管的高精度驱动功能,使得本发明在三维方向的粗调范围在1mm以上,细调精度在0.1nm。In the present invention, four pairs of shear crystals and the first piezoelectric ceramic tube fixed to the slider are used to control the movement of the probe in the horizontal and vertical directions respectively, and then the three-dimensional direction is realized through the second piezoelectric ceramic tube bonded to the probe. For the fine adjustment of the upper position, due to the high-precision driving function of the shear crystal and the piezoelectric ceramic tube, the coarse adjustment range in the three-dimensional direction of the present invention is more than 1 mm, and the fine adjustment accuracy is 0.1 nm.

附图说明Description of drawings

图1为在滑块上固定剪切晶体的结构示意图;Fig. 1 is the structure diagram of fixed shear crystal on the slider;

图2为滑块与夹紧套层相固定的结构示意图;Fig. 2 is a schematic structural diagram of the slider and the clamping sleeve being fixed;

图3为夹紧套层安装在固定槽内的结构示意图;Fig. 3 is a schematic diagram of the structure of the clamping sleeve installed in the fixing groove;

图4为夹紧套层安装在固定槽内的立体示意图;Fig. 4 is a three-dimensional schematic view of the clamping sleeve installed in the fixing groove;

图5为压电陶瓷管的连接示意图;Figure 5 is a schematic diagram of the connection of the piezoelectric ceramic tube;

图6为本发明的整体结构示意图;Figure 6 is a schematic diagram of the overall structure of the present invention;

图7为压电陶瓷管分别设置在滑块两端的结构示意图;FIG. 7 is a structural schematic diagram of piezoelectric ceramic tubes respectively arranged at both ends of the slider;

图8为剪切晶体上的电极设置示意图;Fig. 8 is the schematic diagram of the electrode arrangement on the cut crystal;

图9为安装有金属管的压电陶瓷管的电极设置示意图;Fig. 9 is a schematic diagram of the electrode arrangement of the piezoelectric ceramic tube with the metal tube installed;

图10为安装在滑块上的压电陶瓷管的电极设置示意图。Fig. 10 is a schematic diagram of the electrode arrangement of the piezoelectric ceramic tube installed on the slider.

具体实施方式:Detailed ways:

如图1所示,滑块1呈长方体状,其外表面相对两侧固定有两对剪切晶体2。As shown in FIG. 1 , the slider 1 is in the shape of a cuboid, and two pairs of shear crystals 2 are fixed on opposite sides of its outer surface.

如图2所示,选用材质硬、质量轻的材料来制作滑块1,滑块1通过剪切晶体2固定在夹紧套层3内,与夹紧套层3夹紧并可沿其内壁滑动,夹紧套层3为一矩形套筒,在夹紧套层3的内壁与剪切晶体2之间设置有薄的宝石片,既起到很好的绝缘作用,又光滑耐磨,剪切晶体的面积大于与之粘结的宝石片的面积,以便留出空间来粘贴导线,当然,滑块也可制成具有其他截面形状的长条形,如截面为平行四边形,只要粘结剪切晶体的两个对边互相平行、能实现探针的横向移动即可,但是在有限的安装空间内,移动的距离和效率都将减小;夹紧套层3外壁相对两侧固定有两对剪切晶体4,固定剪切晶体4的外壁与滑块1上固定剪切晶体的外表面相垂直。As shown in Figure 2, the slider 1 is made of hard and light materials. The slider 1 is fixed in the clamping sleeve layer 3 by shearing the crystal 2, clamped with the clamping sleeve layer 3 and can be moved along its inner wall. Sliding, the clamping sleeve layer 3 is a rectangular sleeve, and a thin gem piece is arranged between the inner wall of the clamping sleeve layer 3 and the shearing crystal 2, which not only plays a good insulating role, but also is smooth and wear-resistant, and the shearing The area of the cut crystal is larger than the area of the gemstone that is bonded to it, so as to leave a space to paste the wire. Of course, the slider can also be made into a long strip with other cross-sectional shapes, such as a parallelogram in cross-section, as long as the bonding shears The two opposite sides of the cut crystal are parallel to each other, and the lateral movement of the probe can be realized, but in the limited installation space, the moving distance and efficiency will be reduced; two opposite sides of the outer wall of the clamping layer 3 are fixed For the shear crystal 4 , the outer wall of the fixed shear crystal 4 is perpendicular to the outer surface of the fixed shear crystal on the slider 1 .

如图3、图4所示,固定槽5的外表面呈圆弧形,其内表面呈与夹紧套层3相配的阶梯状,装有滑块1的夹紧套层3通过其外壁相对两侧的两对剪切晶体4设置在固定槽5内,固定槽5的内壁上开有与剪切晶体4相配的安装槽6,夹紧套层3与固定槽5夹紧并可沿与滑块1上剪切晶体驱动方向垂直的方向横向滑动。As shown in Figure 3 and Figure 4, the outer surface of the fixing groove 5 is arc-shaped, and its inner surface is in the shape of a ladder matching the clamping sleeve 3, and the clamping sleeve 3 with the slider 1 is opposite to each other through its outer wall. Two pairs of shear crystals 4 on both sides are arranged in the fixed groove 5, and the inner wall of the fixed groove 5 is provided with an installation groove 6 matched with the shear crystal 4, and the clamping sleeve layer 3 is clamped with the fixed groove 5 and can be aligned with Slider 1 slides laterally in a direction perpendicular to the driving direction of the shear crystal.

如图5所示,压电陶瓷管6和压电陶瓷管7之间用绝缘材料做成的连接头连接,连接头中间粗,两侧细,细端插入压电陶瓷管,探针的安装座为金属管9,压电陶瓷管7和细金属管9之间用绝缘堵头8连接,绝缘堵头8中心钻有一个细孔,用于插入细金属管9。As shown in Figure 5, the piezoelectric ceramic tube 6 and the piezoelectric ceramic tube 7 are connected by a connector made of insulating material. The connector is thick in the middle and thin on both sides, and the thin end is inserted into the piezoelectric ceramic tube. The seat is a metal tube 9, and the piezoelectric ceramic tube 7 and the thin metal tube 9 are connected with an insulating plug 8, and the center of the insulating plug 8 is drilled with a thin hole for inserting the thin metal tube 9.

如图6所示,压电陶瓷管6和滑块1之间也是用绝缘材料连接,所用的绝缘连接材料选用硬质且少放气的材料,绝缘材料做成一端细,插入压电陶瓷管,另一端粗,与滑块1粘接,所有粘接和可能松动的地方都用真空绝缘树脂胶固化牢固。压电陶瓷管的设置也可采用如图7所示的方式,压电陶瓷管6粘接在滑块的一端,压电陶瓷管7粘接在滑块的另一端。As shown in Figure 6, the piezoelectric ceramic tube 6 and the slider 1 are also connected by an insulating material. The used insulating connecting material is made of a material that is hard and less outgassed. , the other end is thick, and it is glued to the slider 1, and all the glued and possibly loose places are solidified with vacuum insulating resin glue. The setting of the piezoelectric ceramic tube can also adopt the method as shown in FIG. 7 , the piezoelectric ceramic tube 6 is bonded to one end of the slider, and the piezoelectric ceramic tube 7 is bonded to the other end of the slider.

如图8所示每组剪切晶体有两个电极,负责驱动电压的加载;如图9所示,与安装探针的金属管9相固定的压电陶瓷管7有5个电极,分别负责横向(4个电极)和纵向(1个电极)移动的驱动电压的加载;如图10所示,与滑块连接的压电陶瓷管2有两个电极,加载驱动电压使陶瓷管伸缩,通过伸缩速度的不同,引起探针纵向移动。As shown in Figure 8, each group of shear crystals has two electrodes, which are responsible for the loading of the driving voltage; The loading of driving voltage for lateral (4 electrodes) and vertical (1 electrode) movement; as shown in Figure 10, the piezoelectric ceramic tube 2 connected to the slider has two electrodes, and the driving voltage is applied to make the ceramic tube expand and contract. The difference in telescopic speed causes the probe to move longitudinally.

剪切晶体与连接在一起的滑块是否绝缘均可,如果绝缘(滑块采用绝缘材料制成),则需要的引线增多,需要将剪切晶体与滑块接触一侧的电极引线并在一起接地,如果不绝缘(滑块由金属材料制成),只需将滑块接地即可,滑块和矩形套层上每两对剪切晶体的导线串连在一起,以便同时加电压,使它们剪切移动方向和幅度一致,完成某一横向方向的移动。Whether the shear crystal and the slider connected together can be insulated or not, if it is insulated (the slider is made of insulating material), more leads are needed, and the electrode leads on the contact side of the shear crystal and the slider need to be combined together Grounding, if it is not insulated (the slider is made of metal material), you only need to ground the slider, and the wires of every two pairs of shear crystals on the slider and the rectangular sleeve are connected in series so that voltage can be applied at the same time, so that They shear and move in the same direction and amplitude, and complete a movement in a certain lateral direction.

Claims (7)

1. driving device for scan probe microscopic probe, it is characterized in that, comprise pickup groove, clamp jacket layer, slide block, shear crystal for two pairs first, shear crystal for two pairs second, first piezoelectric ceramic tube and second piezoelectric ceramic tube, described slide block is arranged in the described clamping jacket layer by the described two pairs first shearing crystal that are fixed on its relative both sides of outside surface, clamp also and can slide with described clamping jacket layer along its inwall, described clamping jacket layer is arranged in the described pickup groove by the described two pairs second shearing crystal that are fixed on its relative both sides of outer wall, clamp also and can laterally slide with described pickup groove along the direction vertical with the described two pairs first shearing crystal-driven directions on the described slide block, be installed in an end of described slide block after described first piezoelectric ceramic tube and the butt joint of second piezoelectric ceramic tube, described first piezoelectric ceramic tube and described slide block axial restraint, the top of described second piezoelectric ceramic tube is provided with the probe mount pad that is used to install probe, shear crystal and described two pairs second by described two pairs first and shear crystal control probes moving in the horizontal, by described first piezoelectric ceramic tube control probe moving in the vertical, finish the fine tuning of position on the three-dimensional by described second piezoelectric ceramic tube again, shear crystal for every group two electrodes are arranged, be responsible for the loading of driving voltage, described first piezoelectric ceramic tube has two electrodes, load driver voltage makes this ceramic pipe flexible, difference by stretching speed, cause that probe vertically moves, described second piezoelectric ceramic tube has 5 electrodes, and wherein 4 electrodes are responsible for loading the driving voltage that laterally moves, 1 electrode is responsible for loading the driving voltage that vertically moves.
2. driving device for scan probe microscopic probe, it is characterized in that, comprise pickup groove, clamp jacket layer, slide block, shear crystal for two pairs first, shear crystal for two pairs second, first piezoelectric ceramic tube and second piezoelectric ceramic tube, described slide block is arranged in the described clamping jacket layer by the described two pairs first shearing crystal that are fixed on its relative both sides of outside surface, clamp also and can slide with described clamping jacket layer along its inwall, described clamping jacket layer is arranged in the described pickup groove by the described two pairs second shearing crystal that are fixed on its relative both sides of outer wall, clamp also and can laterally slide with described pickup groove along the direction vertical with the described two pairs first shearing crystal-driven directions on the described slide block, described first piezoelectric ceramic tube and second piezoelectric ceramic tube are installed in the two ends of described slide block respectively, with described slide block axial restraint, the top of described second piezoelectric ceramic tube is provided with the probe mount pad that is used to install probe, shear crystal and two pairs second by described two pairs first and shear crystal control probe moving in the horizontal, by described first piezoelectric ceramic tube control probe moving in the vertical, finish the fine tuning of position on the three-dimensional by described second piezoelectric ceramic tube again, shear crystal for every group two electrodes are arranged, be responsible for the loading of driving voltage, described first piezoelectric ceramic tube has two electrodes, load driver voltage makes this ceramic pipe flexible, difference by stretching speed, cause that probe vertically moves, described second piezoelectric ceramic tube has 5 electrodes, and wherein 4 electrodes are responsible for loading the driving voltage that laterally moves, 1 electrode is responsible for loading the driving voltage that vertically moves.
3, driving device for scan probe microscopic probe as claimed in claim 1 or 2 is characterized in that, the outside surface of described pickup groove is circular arc, its inside surface be with described clamping jacket layer match stepped.
4. driving device for scan probe microscopic probe as claimed in claim 1 or 2 is characterized in that described clamping jacket layer is a rectangular sleeve.
5. driving device for scan probe microscopic probe as claimed in claim 1 or 2 is characterized in that described slide block is rectangular-shaped.
6. driving device for scan probe microscopic probe as claimed in claim 1 or 2, it is characterized in that, the position of described two pairs first shearing crystal is the two ends of close described slide block respectively, the position of described two pairs second shearing crystal is the two ends of close described clamping jacket layer respectively, and described two pairs first thickness and the assemblage gaps of shearing crystal and two pairs second shearing crystal match.
7. driving device for scan probe microscopic probe as claimed in claim 1 or 2 is characterized in that, adopts insulating material to be connected between described first piezoelectric ceramic tube and the described slide block, and the junction is cured with the vacuum insulation resin glue.
8. driving device for scan probe microscopic probe as claimed in claim 1 or 2 is characterized in that, is provided with insulation course between described two pairs first shearing crystal and the described clamping jacket layer, and this insulation course is thin jewel sheet.
CN2004100700039A 2004-07-30 2004-07-30 A scanning probe microscope probe driving device Expired - Fee Related CN1588558B (en)

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