CN1428404A - Combustion agent composition for generating colour brilliance lamp, and its mking method - Google Patents
Combustion agent composition for generating colour brilliance lamp, and its mking method Download PDFInfo
- Publication number
- CN1428404A CN1428404A CN02103367A CN02103367A CN1428404A CN 1428404 A CN1428404 A CN 1428404A CN 02103367 A CN02103367 A CN 02103367A CN 02103367 A CN02103367 A CN 02103367A CN 1428404 A CN1428404 A CN 1428404A
- Authority
- CN
- China
- Prior art keywords
- weight meter
- incendiary material
- incendiary
- lamp
- material composition
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G OR C10K; LIQUIFIED PETROLEUM GAS; USE OF ADDITIVES TO FUELS OR FIRES; FIRE-LIGHTERS
- C10L1/00—Liquid carbonaceous fuels
- C10L1/003—Marking, e.g. coloration by addition of pigments
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G OR C10K; LIQUIFIED PETROLEUM GAS; USE OF ADDITIVES TO FUELS OR FIRES; FIRE-LIGHTERS
- C10L1/00—Liquid carbonaceous fuels
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G OR C10K; LIQUIFIED PETROLEUM GAS; USE OF ADDITIVES TO FUELS OR FIRES; FIRE-LIGHTERS
- C10L1/00—Liquid carbonaceous fuels
- C10L1/02—Liquid carbonaceous fuels essentially based on components consisting of carbon, hydrogen, and oxygen only
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G OR C10K; LIQUIFIED PETROLEUM GAS; USE OF ADDITIVES TO FUELS OR FIRES; FIRE-LIGHTERS
- C10L1/00—Liquid carbonaceous fuels
- C10L1/10—Liquid carbonaceous fuels containing additives
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G OR C10K; LIQUIFIED PETROLEUM GAS; USE OF ADDITIVES TO FUELS OR FIRES; FIRE-LIGHTERS
- C10L10/00—Use of additives to fuels or fires for particular purposes
- C10L10/02—Use of additives to fuels or fires for particular purposes for reducing smoke development
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G OR C10K; LIQUIFIED PETROLEUM GAS; USE OF ADDITIVES TO FUELS OR FIRES; FIRE-LIGHTERS
- C10L1/00—Liquid carbonaceous fuels
- C10L1/10—Liquid carbonaceous fuels containing additives
- C10L1/12—Inorganic compounds
- C10L1/1216—Inorganic compounds metal compounds, e.g. hydrides, carbides
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G OR C10K; LIQUIFIED PETROLEUM GAS; USE OF ADDITIVES TO FUELS OR FIRES; FIRE-LIGHTERS
- C10L1/00—Liquid carbonaceous fuels
- C10L1/10—Liquid carbonaceous fuels containing additives
- C10L1/12—Inorganic compounds
- C10L1/1225—Inorganic compounds halogen containing compounds
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G OR C10K; LIQUIFIED PETROLEUM GAS; USE OF ADDITIVES TO FUELS OR FIRES; FIRE-LIGHTERS
- C10L1/00—Liquid carbonaceous fuels
- C10L1/10—Liquid carbonaceous fuels containing additives
- C10L1/12—Inorganic compounds
- C10L1/1233—Inorganic compounds oxygen containing compounds, e.g. oxides, hydroxides, acids and salts thereof
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G OR C10K; LIQUIFIED PETROLEUM GAS; USE OF ADDITIVES TO FUELS OR FIRES; FIRE-LIGHTERS
- C10L1/00—Liquid carbonaceous fuels
- C10L1/10—Liquid carbonaceous fuels containing additives
- C10L1/12—Inorganic compounds
- C10L1/1291—Silicon and boron containing compounds
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G OR C10K; LIQUIFIED PETROLEUM GAS; USE OF ADDITIVES TO FUELS OR FIRES; FIRE-LIGHTERS
- C10L1/00—Liquid carbonaceous fuels
- C10L1/10—Liquid carbonaceous fuels containing additives
- C10L1/14—Organic compounds
- C10L1/16—Hydrocarbons
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G OR C10K; LIQUIFIED PETROLEUM GAS; USE OF ADDITIVES TO FUELS OR FIRES; FIRE-LIGHTERS
- C10L1/00—Liquid carbonaceous fuels
- C10L1/10—Liquid carbonaceous fuels containing additives
- C10L1/14—Organic compounds
- C10L1/18—Organic compounds containing oxygen
- C10L1/182—Organic compounds containing oxygen containing hydroxy groups; Salts thereof
- C10L1/1822—Organic compounds containing oxygen containing hydroxy groups; Salts thereof hydroxy group directly attached to (cyclo)aliphatic carbon atoms
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G OR C10K; LIQUIFIED PETROLEUM GAS; USE OF ADDITIVES TO FUELS OR FIRES; FIRE-LIGHTERS
- C10L1/00—Liquid carbonaceous fuels
- C10L1/10—Liquid carbonaceous fuels containing additives
- C10L1/14—Organic compounds
- C10L1/18—Organic compounds containing oxygen
- C10L1/185—Ethers; Acetals; Ketals; Aldehydes; Ketones
- C10L1/1857—Aldehydes; Ketones
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G OR C10K; LIQUIFIED PETROLEUM GAS; USE OF ADDITIVES TO FUELS OR FIRES; FIRE-LIGHTERS
- C10L1/00—Liquid carbonaceous fuels
- C10L1/10—Liquid carbonaceous fuels containing additives
- C10L1/14—Organic compounds
- C10L1/22—Organic compounds containing nitrogen
- C10L1/23—Organic compounds containing nitrogen containing at least one nitrogen-to-oxygen bond, e.g. nitro-compounds, nitrates, nitrites
- C10L1/231—Organic compounds containing nitrogen containing at least one nitrogen-to-oxygen bond, e.g. nitro-compounds, nitrates, nitrites nitro compounds; nitrates; nitrites
Landscapes
- Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Engineering & Computer Science (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Combustion & Propulsion (AREA)
- Liquid Carbonaceous Fuels (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
- Fats And Perfumes (AREA)
- Cosmetics (AREA)
Abstract
The present invention discloses a lamp fuel composition for producing colored flames comprising a coloring agent, a fuel, a fuel supporter, a capillary linker and a scent and obtainable by heating the ingredients while stirring and cooling, and a method of manufacturing the same. The composition for producing colored flame can provide stably and continuously flames of different colors such as red, green, orange, yellow, blue, violet, light purple, white rose and rainbow color according to the used coloring agents, upon burning. The composition is useful as decorative illumination.
Description
Technical field
The present invention relates to a kind of lamp incendiary material composition and manufacture method thereof that is used to produce colored radiance.More particularly, the present invention relates to a kind of be used for upholstery or various celebrating red-letter days, produce lamp incendiary material composition and the desirable manufacture method thereof of magnificent colored radiance.
Background technology
In prior art, Korean application patent (for example No.2001-1240 and 2000-73621) discloses some and has been used for upholster or celebrating decoration, produces the finish of colored radiance as the oil lamp wick.But these finishes can only produce red and green radiance.And the metallic colloidal solution that in those are used, serves as tinting material be by electrolysis in ethanolic soln metal-salt with in the high pressure heating chamber of sealing, add hot preparation.Therefore these painted salt are not to be evenly dispersed in this colloidal solution.So these compositions are imperfect when burning, the brilliant instability and the brilliant colour of generation are impure, and be not bright.Equally, this finish almost can not be preserved for a long time, because the solvent stability that is included in the finish is poor.Therefore, the present invention has considered above-mentioned shortcoming, and the objective of the invention is with improving the dissemination of painted salt in colloidal solution, a kind of lamp incendiary material composition and production method thereof that can produce purified, magnificent colored radiance stably, continuously is provided.Another object of the present invention provides and a kind ofly can prolong the shelf time, and can produce the lamp incendiary material composition and the production method thereof of stable colored radiance with the method for the blending ratio of suitably controlling volatile solvent.
Summary of the invention
The invention provides a kind of lamp incendiary material composition, this lamp incendiary material composition is to produce in interior method by comprising the following steps: select a kind of tinting material; The stable painted colloidal solution of a kind of this tinting material of preparation is evenly dispersed in the colloidal solution painted salt; Add incendiary material in this colloidal solution, incendiary material balustrade and fragrance material under agitation heat this solution, and cooling.
According to the present invention, the tinting material that is used for lamp incendiary material composition requires to select according to the color of radiance.When this lamp illuminates, can be by the colored brilliant feature decorative effect decision tinting material that produces.
According to employed tinting material, being used to produce colored brilliant composition can provide different colours, for example red, and green is orange, yellow, blueness, pansy, lilac, white rugose rose look and irised radiance.Be used to make the method for compositions that produces various colored radiance, slightly different each other.
Propylene glycol is a kind of ethylene glycol.Can in its molecular structure form, form an ehter bond and a hydroxyl (OH) be arranged according to propylene glycol used in the present invention at the place, end of its structure.These characteristics allow this compound of propylene glycol can dissolve effectively or the toner that is scattered here and there, and best stability is provided.Yet it has some disadvantageous aspects, promptly owing to high viscosity, uses wick may hinder its sorption, and owing to its kindling temperature height, is not easy to light.In order to overcome these difficulties, according to the present invention, in propylene glycol, add ethers, ethylene glycol ethyl ether for example, ethylene glycol monomethyl ether and analogue thereof, and amine, for example dimethyl formamide, Trimethylamine 99 and analogue thereof with suitable ratio.Thereby improved this composition combustibility, tinting material also can easily dissolve or be dispersed in this solvent.And can add alcohols, for example ethanol and analogue thereof make the The above results optimizing.
According to the present invention, use lauryl alcohol also can promote to absorb by the kapillary of wick, although because the solvent that uses among the present invention it nonpolar chemical structure is arranged, as oil and paraffin, and can easily discharge the advantage of tinting material, but it is very poor by the absorptivity of wick.Lauryl alcohol can be dispersed in propylene glycol without difficulty, ethylene glycol monoethyl ether, and methyl ether is in ethanol and the analogue thereof.Lauryl alcohol lipid acid can play a part to supply with the lamp incendiary material continuously to wick.Camphor is through being commonly used for perfume material, but it also can be used as the incendiary material balustrade.Turps has pine tree fragrance.It can play the fragrance auxiliary agent, and is a kind of brilliant toughener.
This composition has lot of advantages, is harmless as its products of combustion, and does not produce pollutent, does not also have cigarette ash, health more when therefore doing general the use than traditional paraffin or kerosene.Lauryl alcohol and turps can be used for preventing the wick sclerosis, thereby wick is extended working time.And the ethylene glycol that uses in the incendiary material composition according to the present invention has very high kindling temperature, if because careless, the lamp prompting that said composition is housed has been used up, and fire is not easy expansion, and this is favourable.
The incendiary material that is used to prepare stable colloidal solution according to the present invention comprises that for example, ethers is as dme, the ethyl methyl ether, diethyl ether, dipropyl ether, diisopropyl ether, dibutyl ether, 1, the 2-glycol dimethyl ether, tetrahydrofuran (THF), 1,4 dioxanes, glycol dimethyl ether, vinyl isobutyl ether, β, β '-dichloro-diethyl ether, dibromomethylbenzene glycidyl ether and analogue thereof; And amine, poly ether imide for example, ethylene glycol butyl ether, ethyl cellosolve, methylamine, ethamine, propylamine, Isopropylamine, Frucoter, isobutylamine, sec-butylamine, TERTIARY BUTYL AMINE, hexahydroaniline, benzylamine, Trimethylamine 99, triethylamine, tripropyl amine, N, N-xylidene(s), diethylamino-ethylamine, alpha-naphthylamine, 3 methoxypropyl amine, alkoxy propyl amine, polyoxyethylene oleyl amine and analogue thereof.
Equally, the incendiary material (taking on the incendiary material balustrade simultaneously) that is used to guarantee to produce stable radiance can comprise, alcohols for example is as methyl alcohol, ethanol, propyl alcohol, Virahol, butanols, isopropylcarbinol, sec-butyl alcohol, the trimethyl carbinol, amylalcohol, hexanol, enanthol, octanol, nonyl alcohol, decyl alcohol, vinyl carbinol, cyclopentanol, hexalin, phenylcarbinol or the like; Glycols, as propylene glycol, ethylene glycol, dipropylene glycol, glycerine, glycol ether, triglycol, trimethylene glycol, hexylene glycol, butyleneglycol, 1,3 butyleneglycol, thiodiglycol, sulfo-glycol acid amide, polypropylene glycol, propanediol alginate; Methylene dichloride; N-BUTYL ACETATE; Acetone, acetonitrile; Ethyl acetate and analogue thereof.
But the selection of these incendiary materials and mixture ratio are practical applications, and after the present invention discloses, are made improvements by any way by experienced industry technology personnel, and this practical application and be included into scope of the present invention by experienced technician's improvement.
Embodiment
Describe the present invention in detail with embodiment below.
Embodiment 1: the lamp incendiary material preparation of compositions that is used to produce red radiance
Being used to produce red brilliant lamp incendiary material composition is to be made of material as shown in table 1 below.Table 1 component ratio (%, w/w) lithium salts or strontium salt 0.04-0.1 ethanol 5-10 propylene glycol 40-60 ethyl cellosolve 20-30 dimethyl formamide 10-30 camphor 0.3-1 turps 0.01-0.1 lauryl alcohol 0.2-2 add up to 100
Being used to produce red brilliant incendiary material composition is prepared by the following step.Be used for producing the tinting material preparation process of red radiance in preparation, ethanol and drop in the container together as the lithium salts or the strontium salt of painted salt, and make 30 minutes ultrasonication at 30 ℃, produce first solution thus.By this step processing, painted salt can be evenly dispersed in the ethanol.
Preparation is used for the stable colloid coloring solution of lamp incendiary material in next step.Dimethyl formamide and ethyl cellosolve are added in first solution, and the solution that is produced is just produced the stable colloidal solution that is used for red radiance by any one is handled in following two working methods.
1) the first solution input is stirred in the bath, add dimethyl formamide and ethyl cellosolve at 40-50 ℃.The solution that is produced stirs under 50-250 rotations per minute condition, produces the stable colloidal solution that is used for red radiance.
2) first solution is dropped in the electrolyzer, add dimethyl formamide and ethyl cellosolve at 40-50 ℃.The solution that is produced is made anode with strontium, with 12 volts of dc voltages and 10-15 ampere electric current, at 30 ℃, does electrolysis in 30 minutes.This solution in the baking oven for heating of a sealing, produces the stable colloidal solutions that is used for red radiance in high pressure in the time of about 250 ℃ then.
Finally from from 1) or 2) stable colloidal solutions that obtains the working method, in the time of 50-60 ℃, drop in the polymerization reactor, under stirring, per minute 50-250 revolution adds propylene glycol at leisure.After stirring 10 minutes, add camphor, lauryl alcohol and turps.Follow stirring, this solution reheats 20 minutes, and cool to room temperature.
The said composition that obtains is a kind of colourless transparent liquid like this, and when burning in air, under the effect of the painted colloidal solution that contains lithium salts or strontium salt, produces the radiance of azarin.
However, the quantity of painted salt that is used for the present composition is than littler (0.04-0.1% calculates by weight) that be used for cosmetic formulations, and its produces the radiance of azarin, and it can be used in decorative illumination whereby.
The tinting material that can be used for producing red radiance comprises lithium salts, lithium acetate for example, acetoacetic acid lithium, the methyl ethyl diketone lithium, Lithamide, lithium chloride, lithium fluoride, lithium nitrate, Lithium Sulphate and analogue thereof, perhaps strontium salt, strontium acetate methyl ethyl diketone strontium for example, Strontium carbonate powder, strontium chloride, strontium nitrate, strontium oxalate Strontium Sulphate and analogue thereof.
Embodiment 2: the lamp incendiary material composition burn agent preparation of compositions that is used to produce green radiance
Being used to produce green brilliant lamp incendiary material composition is to be made of material as shown in table 2 below.Table 2 component ratio (%, w/w) boric acid 3.5-4 ethanol 5-10 propylene glycol 40-60 ethyl cellosolve 20-30 butanols 10-30 camphor 0.3-1 turps 0.01-0.1 lauryl alcohol 0.2-2 adds up to 100
Being used to produce green brilliant incendiary material composition is prepared by the following step.Be used for producing the step of green brilliant tinting material in preparation, the boric acid input is contained in the alcoholic acid container, at room temperature or stir a little while 40-50 ℃ the time, it is dissolved fully.With this solution ultrasonication,, handled 30 minutes then, generate first solution at 30 ℃.By this step processing, boric acid can be evenly dispersed in the ethanol.
Be used for the step of the stable colloid coloring solution of lamp incendiary material in preparation, in the bath that the first solution input is being stirred, in the time of 40-50 ℃, add butanols and ethyl cellosolve.The solution that is produced stirs under per minute 50-250 revolution, produces the stable colloidal solution that is used for green radiance.
Finally,, in the time of 50-60 ℃, drop in the polymerization reactor, under per minute 50-250 revolution stirs, add propylene glycol at leisure stable colloidal solutions.After stirring 10 minutes, add camphor, lauryl alcohol and turps.Follow stirring, this solution reheats 20 minutes and cool to room temperature.
The said composition that obtains is a kind of colourless transparent liquid like this, and when burning in air, the painted colloidal solution that contains boric acid produces the radiance of bright green.Be a kind of nontoxic and harmless material as the boric acid of tinting material in the present invention, boric acid can be used for makeup, sanitas, toothpaste, sterilizing agent and analogue thereof.Therefore, said composition can be used in indoor and the out of door decoration.
Equally, when this incendiary material composition burn, boric acid also can burn under the wick temperature well.Therefore can prevent this wick sclerosis.
Except boric acid, also have some metal-salts of knowing also can produce green radiance.But because brilliant poor stability can not use those metal-salts.
Embodiment 3: the lamp incendiary material composition burn agent preparation of compositions that is used to produce orange radiance
The lamp incendiary material composition that is used to produce orange radiance is to be made of material as shown in table 3 below.Table 3 component ratio (%, w/w) borax 0.02-0.1 sodium salt 0.02-.1 ethanol 5-10 propylene glycol 40-60 ethyl cellosolve 20-30 butanols 5-10 camphor 0.5-1 turps 0.01-0.1 lauryl alcohol 0.3-0.5 adds up to 100
The incendiary material composition that is used to produce orange radiance is prepared by the following step.Be used for producing the step of orange brilliant tinting material in preparation, boric acid and sodium salt input are contained in the alcoholic acid container, at room temperature or 40-50 ℃ the time, the companion stirs, and it is dissolved fully.With this solution ultrasonication,, handled 30 minutes then, generate first solution at 30 ℃.By this step processing, borax and sodium salt can be evenly dispersed in the ethanol.
Be used for the step of the stable colloid coloring solution of lamp incendiary material in preparation, in the bath that the first solution input is being stirred, in the time of 40-50 ℃, add butanols and ethyl cellosolve.The solution that is produced stirs under per minute 50-250 revolution condition, produces the stable colloidal solution that is used for orange radiance.
Finally,, in the time of 50-60 ℃, drop in the polymerization reactor, under per minute 50-250 revolution whipped state, add propylene glycol at leisure stable colloidal solutions.After stirring 10 minutes, add camphor, lauryl alcohol and turps.Follow stirring, this solution reheats 20 minutes and cool to room temperature.
The said composition that obtains is a kind of colourless transparent liquid like this, and when burning in air, contain this borax and sodium salt do the painted colloidal solution of tinting material provide bright orange radiance.Be nontoxic and harmless material as the borax of tinting material and sodium salt in the present invention, they do not produce harmful products of combustion.
Equally, when this incendiary material composition burn, borax and sodium salt also can burn under the wick temperature well.Therefore can advantageously prevent this wick sclerosis.
The tinting material that can be used for producing orange radiance can be from borax and sodium salt, for example from sodium-chlor, and sodium acetate, the sodium amide sodium cyanide is picked out in SODIUMNITRATE and the analogue thereof.
Embodiment 4: the lamp incendiary material composition burn agent preparation of compositions that is used to produce yellow radiance
Being used to produce yellow brilliant lamp incendiary material composition is to be made of material as shown in table 4 below.Table 4 component ratio (%, w/w) barium salt 0.02-0.1 calcium salt 0.02-0.1 ethanol 5-10 propylene glycol 40-60 ethyl cellosolve 20-40 butanols 10-20 camphor 0.5-1 turps 0.01-0.1 lauryl alcohol 0.3-0.5 adds up to 100
Being used to produce yellow brilliant incendiary material composition is prepared by the following step.Be used for producing the step of yellow brilliant tinting material in preparation, will contain in the alcoholic acid container, at room temperature or stir a little while 40-50 ℃ the time, it is dissolved fully as barium salt and a kind of calcium salt input of painted salt.With this solution ultrasonication,, handled 30 minutes then, generate first solution at 30 ℃.By this step processing, painted fused salt can be evenly dispersed in the ethanol.
Be used for the step of the stable colloid coloring solution of lamp incendiary material in preparation, in the bath that the first solution input is being stirred, in the time of 40-50 ℃, add butanols and ethyl cellosolve.The solution that is produced stirs under 50-250 rotations per minute condition, produces the stable colloidal solution that is used for yellow radiance.
Stable colloidal solutions drops in the polymerization reactor in the time of 50-60 ℃ the most at last, adds propylene glycol at leisure under 50-250 rotations per minute whipped state.After stirring 10 minutes, add camphor, lauryl alcohol and turps.Follow stirring, this solution reheats 20 minutes and cool to room temperature.
The said composition that obtains is a kind of colourless transparent liquid like this, and when burning in air, the painted colloidal solution that contains this barium salt and calcium salt provides soft yellow radiance.
The tinting material that can be used for producing yellow radiance can comprise barium salt, barium acetate for example, bariumchloride, barium fluoride, nitrate of baryta, barium oxalate, barium sulfate and analogue thereof, and calcium salt, for example lime acetate hydrate, Calcium Fluoride (Fluorspan), nitrocalcite, caoxalate, calcium sulfate and analogue thereof.
Embodiment 5: the lamp incendiary material composition burn agent preparation of compositions that is used to produce blue radiance
Being used to produce blue brilliant lamp incendiary material composition is made up of material as shown in table 5 below.Table 5 component ratio (%, w/w) mantoquita 0.04-0.1 butanols 5-10 ethanol 5-10 propylene glycol 40-55 ethyl cellosolve 25-35 dimethyl formamide 5-10 camphor 0.3-1.0 turps 0.01-0.1 lauryl alcohol 0.1-0.5 adds up to 100
Being used to produce blue brilliant incendiary material composition is prepared by the following step.Be used for producing blue brilliant tinting material preparation process, dropping into container, be subjected to ultrasonication,, handling 30 minutes, generating first solution at 30 ℃ with ethanol with as the mantoquita of painted salt.By this step processing, mantoquita can be evenly dispersed in the ethanol.
Preparation is used for the stable colloid coloring solution of lamp incendiary material in next step.Dimethyl formamide and ethyl cellosolve are added in first solution, and the solution that is produced is just produced the stable colloidal solution that is used for blue radiance by any one is handled in following two working methods.
1) during the first solution input stirs and bathes, adds dimethyl formamide and ethyl cellosolve at 40-50 ℃.The solution that is produced stirs under 50-250 rotations per minute condition, produces the stable colloidal solution that is used for red radiance.
2) first solution drops in the electrolyzer, adds dimethyl formamide and the molten fine profit of ethyl at 40-50 ℃.This resulting solution is made anode with metallic copper, with 12 volts of dc voltages and 10-15 ampere electric current, at 30 ℃, does electrolysis in 30 minutes.This solution in the baking oven for heating of a sealing, produces the stable colloidal solutions that is used for blue radiance in high pressure in the time of about 250 ℃ then.
Finally from from 1) or 2) stable colloidal solutions that obtains the working method, in the time of 50-60 ℃, drop in the polymerization reactor, under per minute 50-250 revolution whipped state, add propylene glycol at leisure.After stirring 10 minutes, add camphor, lauryl alcohol and turps.Follow stirring, this solution reheats 20 minutes, and cool to room temperature.
The said composition that obtains is a kind of colourless transparent liquid like this, and when burning in air, the painted colloidal solution that contains boric acid provides the radiance of sapphirine.
The tinting material that can be used for producing blue radiance can be from mantoquita, neutralized verdigris for example, and acetylacetone copper, cupric chloride, cupric cyanide, copper hydroxide, copper sulfate, the trifluoroacetyl venus crystals is picked out in cupric nitrate and the analogue thereof.
Embodiment 6: preparation produces the lamp incendiary material composition of pansy radiance
Producing pansy radiance lamp incendiary material composition is made of material as shown in table 6 below. table 6 component ratio (%, w/w) sylvite 0.1-0.5 cerium salt 0.5-1.0 butanols 10-15 ethanol 5-10 propane diols 40-55 ethyl cellosolve 20-0 dimethyl formamide 5-10 camphor 0.3-1.0 turpentine oil 0.01-0.1 laruyl alcohol 0.1-0.5 add up to 100
The lamp incendiary material composition of generation pansy radiance is prepared by following steps.Be used for producing the step of violaceous brilliant tinting material in preparation, boric acid and a kind of cerium salt input are contained in the alcoholic acid container, at room temperature or stir down 40-50 ℃ the time, it is dissolved fully.With this solution ultrasonication,, handled 30 minutes then, generate first solution at 30 ℃.By this step processing, painted fused salt can be evenly dispersed in the ethanol.
Be used for the step of the stable colloid coloring solution of lamp incendiary material in preparation, in the bath that the first solution input is being stirred, in the time of 40-50 ℃, add butanols, dimethyl formamide and ethyl cellosolve.The solution that is produced stirs under 50-250 rotations per minute condition, produces to be used for the stable colloidal solution of pansy radiance.
Stable colloidal solutions drops in the time of 50-60 ℃ in the polymerization reactor the most at last, adds propylene glycol at leisure under per minute 50-250 revolution stirs.Camphor adds camphor, lauryl alcohol and turps after stirring 10 minutes.Follow stirring, this solution reheats 20 minutes, and cool to room temperature.
The said composition that obtains is a kind of colourless transparent liquid like this, and when burning in air, the painted colloidal solution that contains this saltpetre and calcium salt provides soft yellow radiance.
Can produce pansy radiance tinting material according to the present invention be cerium salt and sylvite.The cerium salt example that can use comprises the cerous acetate hydrate, methyl ethyl diketone cerium hydrate, Cerium II Chloride, cerous nitrate, Sedemesis, cerous sulfate and analogue thereof and the sylvite example that can use, comprise potassium acetate, methyl ethyl diketone potassium hemihydrate, Repone K, Potcrate, potassium cyanide, potassium ethylate, the Tripotassium iron hexacyanide, Potassium monofluoride, potassium oxalate mono-hydrate, vitriolate of tartar, sodium-potassium tartrate tetrahydrate, saltpetre and analogue thereof.
Embodiment 7: preparation produces the lamp incendiary material composition of lilac radiance
Producing lilac coloured light brightness lamp incendiary material composition is made of material as shown in table 7 below.Table 7 component ratio (%, w/w) cesium salt 0.5-1.0 butanols 10-15 ethanol 5-10 propylene glycol 40-55 ethyl cellosolve 20-30 dimethyl formamide 5-10 camphor 0.3-1.0 turps 0.01-0.1 lauryl alcohol 0.-10.5 adds up to 100
The lamp incendiary material composition of generation lilac radiance is prepared by following steps.Be used for producing the step of lilac radiance tinting material in preparation, the cesium salt input is contained in the alcoholic acid container, at room temperature or stir down 40-50 ℃ the time, it is dissolved fully.With this solution ultrasonication,, handled 30 minutes then, generate first solution at 30 ℃.By this step processing, painted salt can be evenly dispersed in the ethanol.
Be used for the step of the stable colloid coloring solution of lamp incendiary material in preparation, in the bath that the first solution input is being stirred, in the time of 40-50 ℃, add butanols, dimethyl formamide and ethyl cellosolve.The solution that is produced stirs under per minute 50-250 revolution condition, produces to be used for the stable colloidal solution of lilac radiance.
Stable colloidal solutions drops in the time of 50-60 ℃ in the polymerization reactor the most at last, adds propylene glycol at leisure under per minute 50-250 revolution stirs.Camphor adds camphor, lauryl alcohol and turps after stirring 10 minutes.Follow stirring, this solution reheats 20 minutes, and cool to room temperature.
The said composition that obtains is a kind of colourless transparent liquid like this, and when burning in air, the painted colloidal solution that contains this cesium salt produces the radiance of lilac.
The brilliant tinting material that can produce lilac according to the present invention is a cesium salt.The example of cesium salt comprises cesium acetate, methyl ethyl diketone caesium, cesium chloride, cesium fluoride, cesium sulfate, cesium nitrate, cesium oxalate and analogue thereof.
Embodiment 8: preparation produces the lamp incendiary material composition of white roseate radiance
The lamp incendiary material composition that produces white rugose rose coloured light brightness is made of material as shown in table 8 below.Table 8 component ratio (%, w/w) Nitromethane 99Min. 50-60 ethanol 5-10 dimethyl formamide 30-40 camphor 0.5-1.0 turps 0.01-0.1 lauryl alcohol 0.3-0.5 adds up to 100
Produce the white rugose rose look radiance lamp incendiary material composition by the following steps preparation in the step that is used for producing the stable colloid coloring solution of white rugose rose coloured light brightness, Nitromethane 99Min. is dropped into polymerization reactor, add dimethyl formamide and ethanol at 40-50 ℃.The solution of this generation heated 10 minutes under the 50-250 rotations per minute stirs.With camphor, lauryl alcohol and turps add this solution, and under agitation reheat is 20 minutes, and cool to room temperature.
Snowblink is considered as the radiance of white rugose rose look according to the present invention, usually at its edge with slight red tone.
Embodiment 9: preparation produces the lamp incendiary material composition of the colored radiance of iris
Producing the colored brilliant lamp incendiary material composition of iris is made of material as shown in table 9 below. table 9 component ratio (%, w/w) lithium salts or strontium salt 0.04-0.1 boric acid 3-4 mantoquita 0.01-0.05 ethanol 5-10 propane diols 40-60 ethyl cellosolve 20-30 dimethyl formamide 10-30 camphor 0.3-1.0 turpentine oil 0.01-0.1 laruyl alcohol 0.2-2 add up to 100
The lamp incendiary material composition of generation iris radiance is prepared by following steps.In the step of selecting to be used for producing iris radiance tinting material, select lithium salts, perhaps strontium and mantoquita.Selected painted salt is contained in the alcoholic acid container with boric acid input, at room temperature or 40-50 ℃, stir down dissolving fully.With this solution ultrasonication,, handled 30 minutes then, generate first solution at 30 ℃.By this step processing, painted salt can be evenly dispersed in the ethanol.
Be used for the step of the stable colloid coloring solution of lamp incendiary material in preparation, in the bath that the first solution input is being stirred, in the time of 40-50 ℃, add dimethyl formamide and ethyl cellosolve.The solution that is produced stirs under per minute 50-250 revolution, produces to be used for the stable colloidal solution of the colored radiance of iris.
Stable colloidal solutions drops in the time of 50-60 ℃ in the polymerization reactor the most at last, adds propylene glycol at leisure under the 50-250 rotations per minute stirs.After stirring 10 minutes, camphorate lauryl alcohol and turps.Follow stirring, this solution reheats 20 minutes, and cool to room temperature.
Obtain composition thus and be green liquid clearly, when in air, burning, emit excellent iris glory brightness by the painted colloidal solution that contains lithium (perhaps strontium) salt mantoquita and boric acid.Iris glory brightness is by the redness of lower part, the yellow at middle part, and blueness, the green tint on purple etc. and top is formed.
Can be used for producing iris glory brightness tinting material comprises the lithium salts that is used to produce red radiance and strontium salt and is used to produce blue brilliant mantoquita and boric acid.
As mentioned above, the present invention is used to produce colored brilliant lamp incendiary material composition and does not use any metal-salt that is pernicious to people, and is to use the colloidal solution of extreme small amount of coloring preparation.Therefore, its products of combustion is harmless.Equally, it does not produce pollutent, polluted air or generation smell and smog.And because colored salt is to be dispersed in the colloidal solution, the colored radiance of formation is not only stable, and seems thorough clearly, pure.Therefore, lamp incendiary material composition of the present invention is applicable to red-letter day or upholstery.Equally, lamp incendiary material composition can stably use, and because wick is non-sclerous, can use continuously for a long time.In addition, because preparation of compositions and kindling temperature are to do optimally-controlledly, so said composition has high kindling temperature, if because careless, the lamp prompting that composition is contained in the inside has been used up, and fire is not allowed the expansion of changing places yet.Therefore, said composition has the fp effect.
Claims (13)
1. one kind produces colored brilliant lamp incendiary material composition, mainly comprise the incendiary material tinting material, incendiary material, incendiary material balustrade and fragrance material, it is characterized in that: be used to produce lithium or the strontium salt that red brilliant lamp incendiary material composition comprises 0.04-0.1% weight meter, the propylene glycol of 40-60% weight meter, the ethyl cellosolve of 20-30% weight meter, the dimethyl formamide of 10-30% weight meter, 0.3-1 the camphor of weight meter, the turps of 0.01-0.1% weight meter, the ethanol of the lauryl alcohol of 0.2-2% weight meter and 5-10% weight meter.
2 one kinds of lamp incendiary material compositions that produce colored radiance, mainly comprise the incendiary material tinting material, incendiary material, incendiary material balustrade and fragrance material, it is characterized in that: kind is used to produce the boric acid that green brilliant lamp incendiary material composition comprises 3.5-4% weight meter, the propylene glycol of 40-60% weight meter, the ethyl cellosolve of 20-30% weight meter, the butanols of 10-30% weight meter, the ethanol of 5-10% weight meter, the camphor of 0.3-1% weight meter, the lauryl alcohol of the turps of 0.01-0.1% weight meter and 0.2-2% weight meter.
3. one kind produces colored brilliant lamp incendiary material composition, mainly comprise the incendiary material tinting material, incendiary material, incendiary material balustrade and fragrance material, it is characterized in that: the lamp incendiary material composition that is used to produce orange radiance comprises the borax of 0.02-0.1% weight meter, the sodium salt of 0.02-0.1% weight meter, the ethanol of 5-10% weight meter, the propylene glycol of 40-60% weight meter, 20-30% weight meter ethyl cellosolve, the butanols of 5-10% weight meter, the camphor of 0.5-1% weight meter, the lauryl alcohol of the turps of 0.01-0.1% weight meter and 0.3-0.5% weight meter.
4. one kind produces colored brilliant lamp incendiary material composition, mainly comprise the incendiary material tinting material, incendiary material, incendiary material balustrade and fragrance material, it is characterized in that: be used to produce the barium salt that yellow brilliant lamp incendiary material composition comprises 0.02-0.1% weight meter, the calcium salt of 0.02-0.1% weight meter, the ethanol of 5-10% weight meter, the propylene glycol of 40-60% weight meter, the ethyl cellosolve of 20-40% weight meter, the butanols of 10-20% weight meter, the camphor of 0.5-1% weight meter, the lauryl alcohol of the turps of 0.01-0.1% weight meter and 0.3-0.5% weight meter.
5. one kind produces colored brilliant lamp incendiary material composition, mainly comprise the incendiary material tinting material, incendiary material, incendiary material balustrade and fragrance material, it is characterized in that: be used to produce the mantoquita that blue brilliant lamp incendiary material composition comprises 0.04-0.1% weight meter, the ethanol of 5-10% weight meter, the propylene glycol of 40-55% weight meter, the ethyl cellosolve of 25-35% weight meter, the butanols of 5-10% weight meter, the dimethyl formamide of 5-10% weight meter, the camphor of 0.3-1.0% weight meter, the lauryl alcohol of the turps of 0.01-0.1% weight meter and 0.1-0.5% weight meter.
6. one kind produces colored brilliant lamp incendiary material composition, mainly comprise the incendiary material tinting material, incendiary material, incendiary material balustrade and fragrance material, it is characterized in that: the lamp incendiary material composition that is used to produce pansy radiance comprises the sylvite of 0.1-0.5% weight meter, the cerium salt of 0.5-1.0% weight meter, the ethanol of 5-10% weight meter, the propylene glycol of 40-55% weight meter, the butanols of 10-15% weight meter, the ethyl cellosolve of 20-30% weight meter, the dimethyl formamide of 5-10% weight meter, the camphor of 0.3-1.0% weight meter, the lauryl alcohol of the turps of 0.01-0.1% weight meter and 0.1-0.5% weight meter.
7. one kind produces colored brilliant lamp incendiary material composition, mainly comprise the incendiary material tinting material, incendiary material, incendiary material balustrade and fragrance material, it is characterized in that: the lamp incendiary material composition that is used to produce lilac radiance comprises the cesium salt of 0.5-1.0% weight meter, the ethanol of 5-10% weight meter, the propylene glycol of 40-55% weight meter, the butanols of 10-15% weight meter, the ethyl cellosolve of 20-30% weight meter, the dimethyl formamide of 5-10% weight meter, the camphor of 0.3-1.0% weight meter, the lauryl alcohol of the turps of 0.01-0.1% weight meter and 0.1-0.5% weight meter.
8. one kind produces colored brilliant lamp incendiary material composition, mainly comprise the incendiary material tinting material, incendiary material, incendiary material balustrade and fragrance material, it is characterized in that: the lamp incendiary material composition that is used to produce white rugose rose coloured light brightness comprises the Nitromethane 99Min. of 50-60% weight meter, the ethanol of 5-10% weight meter, the dimethyl formamide of 30-40% weight meter, the turps of the camphor 0.01-0.1% weight meter of 0.5-1.0% weight meter and the lauryl alcohol of 0.3-0.5% weight meter.
9. one kind produces colored brilliant lamp incendiary material composition, mainly comprise the incendiary material tinting material, incendiary material, incendiary material balustrade and fragrance material, it is characterized in that: be used to produce lithium or the strontium salt that the colored brilliant lamp incendiary material composition of rainbow comprises 0.04-0.1% weight meter, the boric acid of 3-4% weight meter, the mantoquita of 0.01-0.05% weight meter, the ethanol of 5-10% weight meter, the propylene glycol of 40-60% weight meter, the ethyl cellosolve of 20-30% weight meter, the camphor of the dimethyl formamide 0.3-1.0% weight meter of 10-30% weight meter, the lauryl alcohol of the turps of 0.01-0.1% weight meter and 0.2-2% weight meter.
10. lamp incendiary material composition manufacturing method that produces colored radiance, this method comprises the following steps: that (a) drops into reactor to ethanol and tinting material, at room temperature or 40-50 ℃, under agitation with its dissolving, the using ultrasound ripple generates first solution; (b) or (i) first solution is put into the stirring bath, and under agitation add incendiary material, generate stable colloidal solution; Perhaps (ii) first solution is put into electrolyzer, add incendiary material, and electrolytic metal salt generates stable colloidal solutions; And (c) in the stable colloidal solution that in (b) step, produces, add incendiary material balustrade and fragrance material, under agitation heat subsequently, then cool to room temperature.
11. a kind of lamp incendiary material composition manufacturing method that produces colored radiance according to claim 10, it is characterized in that: it is select independently in the group be made up of ethers of incendiary material in (i) and (ii) to can be used for step (b), dme for example, the ethyl methyl ether, diethyl ether, dipropyl ether, diisopropyl ether, dibutyl ether, glycol dimethyl ether, tetrahydrofuran (THF), 1, the 4-dioxane, anisole, vinyl isobutyl ether, β, β ' dichloro-diethyl ether, dibromocresyl glycidyl ether or the like; And amine, poly ether imide for example, ethylene glycol butyl ether, ethyl cellosolve, methylamine, ethamine, propylamine, Isopropylamine, butylamine, isobutylamine, sec-butylamine, TERTIARY BUTYL AMINE, hexahydroaniline, benzylamine, Trimethylamine 99, triethylamine, tripropyl amine, N, N-xylidene(s), diethylamino-ethylamine, alpha-naphthylamine, 3 methoxypropyl amine, alkoxy propyl amine, polyoxyethylene oleyl amine.
12. a kind of lamp incendiary material composition manufacturing method that produces colored radiance according to claim 10 is characterized in that: can be used in the group that the incendiary material in the step (c) is made up of alcohols select, methylene dichloride for example, N-BUTYL ACETATE, acetone, acetonitrile, ethyl acetate, methyl alcohol, ethanol, propyl alcohol, Virahol, butanols, isopropylcarbinol, sec-butyl alcohol, the trimethyl carbinol, amylalcohol, hexanol, enanthol, octanol, nonyl alcohol decyl alcohol, vinyl carbinol, cyclopentanol, hexalin, phenylcarbinol or the like; And glycols, propylene glycol for example, ethylene glycol, dipropylene glycol, glycerine, glycol ether, triglycol, dipropylene glycol, hexylene glycol, butyleneglycol, 1,3 butylene glycol, thiodiglycol, mercaptoethanol ammonium, azanol ethylene glycol (cefatrizine glycol), polypropylene glycol, propanediol alginate.
13. a kind of lamp incendiary material composition manufacturing method that produces colored radiance according to claim 10 is characterized in that: pick out a kind of material in the group that the fragrance material in the composition is made up of camphor and turps.
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| KR200185176 | 2001-12-26 | ||
| KR10-2001-0085176A KR100440724B1 (en) | 2001-12-26 | 2001-12-26 | Composition of lamp fuel for colored flames and manufacturing method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN1428404A true CN1428404A (en) | 2003-07-09 |
| CN1183234C CN1183234C (en) | 2005-01-05 |
Family
ID=19717614
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CNB021033676A Expired - Fee Related CN1183234C (en) | 2001-12-26 | 2002-01-28 | Combustion agent composition for generating colour brilliance lamp, and its mking method |
Country Status (5)
| Country | Link |
|---|---|
| EP (1) | EP1323812A3 (en) |
| JP (1) | JP3764391B2 (en) |
| KR (1) | KR100440724B1 (en) |
| CN (1) | CN1183234C (en) |
| AU (1) | AU770156B2 (en) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101434877A (en) * | 2008-12-12 | 2009-05-20 | 青岛安芙兰芳香制品有限公司 | Artistic color flame lamp and fuel thereof |
| CN101258226B (en) * | 2005-07-07 | 2013-09-11 | 因诺斯佩克德国有限责任公司 | Fuel composition and fuel additive composition |
| US8870981B2 (en) | 2007-01-11 | 2014-10-28 | Innospec Limited | Additive fuel composition, and method of use thereof |
| CN113121312A (en) * | 2020-01-13 | 2021-07-16 | 潘小秋 | Rice potassium ethoxide oxidant and preparation method thereof |
Families Citing this family (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2004018593A1 (en) * | 2002-08-22 | 2004-03-04 | Hwalim Technological Co., Ltd | A fuel composition and a device for colored flames |
| JP4515137B2 (en) * | 2004-04-20 | 2010-07-28 | 株式会社東海 | Liquid fuel for combustion equipment |
| US20090042153A1 (en) * | 2007-07-09 | 2009-02-12 | Harry Ronen | Liquid fuel composition for a lamp with a colored flame |
| CN102388118A (en) * | 2009-02-11 | 2012-03-21 | 阿格瓦知识产权公司 | Fuel composition comprising alkyl ester |
| CN102311814A (en) * | 2011-08-10 | 2012-01-11 | 薛安清 | Emulsified methanol fuel and preparation method thereof |
| EP2865734B1 (en) | 2013-10-25 | 2019-02-20 | Sara Carine Wilma Torfs | Use of safe fuel in wicked open geometry devices |
| JP7250304B2 (en) * | 2018-09-26 | 2023-04-03 | 国立大学法人室蘭工業大学 | Propellant for gas generator for turbine drive and method for producing the same |
Family Cites Families (16)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB190615279A (en) * | 1906-07-05 | 1907-07-05 | James St Clair Legge | Improvements in, or connected with, Fuel for Internal Combustion Engines. |
| GB404046A (en) * | 1932-07-16 | 1934-01-11 | Ig Farbenindustrie Ag | Process for ameliorating the smell of the exhaust gases of internal-combustion engines |
| US4624633A (en) * | 1985-01-09 | 1986-11-25 | Mtc-Choice, Inc. | High percentage glycol fuel and burner |
| JPS6259219A (en) * | 1985-09-10 | 1987-03-14 | Ikeda Mohandou:Kk | Antitussive, expectorant, analgesic and sedative agent for external use |
| JP2553181B2 (en) * | 1989-01-10 | 1996-11-13 | 有限会社 群馬火工製造所 | Method for producing colored flame solid fuel |
| FR2690689A3 (en) * | 1991-03-07 | 1993-11-05 | Balland Benoit | Flame colouring system for burner using spirit on other fuel - uses block of solid fuel, e.g. in shape of ring, containing salts or borate(s) to produce colours |
| FR2695400A1 (en) * | 1992-02-03 | 1994-03-11 | D Eramo Norbert | Hydrocarbon-based fuels producing coloured flame - obtd. from compsns. contg. hydrocarbon, ion colourants and co-solvent |
| FR2694014A1 (en) * | 1992-06-19 | 1994-01-28 | Balland Benoit | Fuel for spirit lamps - gives coloured flame with insect repellent properties if required |
| FR2727688B1 (en) * | 1995-12-04 | 1997-05-09 | Jacquelin Guy | LIQUID FUEL PRODUCTS, BURNING WITH FLAMES OF VARIOUS COLORS. SIMPLIFIED DECORATIVE LIGHTING DEVICES USING SUCH PRODUCTS |
| NL1003391C2 (en) * | 1996-06-21 | 1997-12-23 | Gerard Stulen | Liquid fuel for oil lamps that burns with a coloured flame |
| KR100301147B1 (en) * | 1999-05-12 | 2001-09-13 | 임진만 | Composition of lamp fuel for green colored flame |
| KR100295012B1 (en) * | 1999-06-02 | 2001-07-03 | 임진만 | Composition of lamp fuel for red colored flame and method thereof |
| KR100329332B1 (en) * | 1999-06-07 | 2002-03-23 | 임진만 | Colored flame candle and method thereof |
| DE19961547A1 (en) * | 1999-12-20 | 2001-06-21 | Wedenig Albin | Coloration of flames comprises introducing copper metal or copper alloy into combustion zone of open flame |
| US6488726B1 (en) * | 2001-02-20 | 2002-12-03 | Jinman Lim | Lamp fuel composition for colored flames and manufacturing method thereof |
| KR100443413B1 (en) * | 2001-07-30 | 2004-08-09 | 김민지 | A producting method of alcohol lamp |
-
2001
- 2001-12-26 KR KR10-2001-0085176A patent/KR100440724B1/en not_active Expired - Fee Related
-
2002
- 2002-01-17 AU AU11966/02A patent/AU770156B2/en not_active Ceased
- 2002-01-18 EP EP02290129A patent/EP1323812A3/en not_active Withdrawn
- 2002-01-23 JP JP2002014728A patent/JP3764391B2/en not_active Expired - Fee Related
- 2002-01-28 CN CNB021033676A patent/CN1183234C/en not_active Expired - Fee Related
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101258226B (en) * | 2005-07-07 | 2013-09-11 | 因诺斯佩克德国有限责任公司 | Fuel composition and fuel additive composition |
| US8870981B2 (en) | 2007-01-11 | 2014-10-28 | Innospec Limited | Additive fuel composition, and method of use thereof |
| CN101636476B (en) * | 2007-01-11 | 2015-08-12 | 因诺斯佩克有限公司 | Composition, method and purposes |
| CN101434877A (en) * | 2008-12-12 | 2009-05-20 | 青岛安芙兰芳香制品有限公司 | Artistic color flame lamp and fuel thereof |
| CN113121312A (en) * | 2020-01-13 | 2021-07-16 | 潘小秋 | Rice potassium ethoxide oxidant and preparation method thereof |
Also Published As
| Publication number | Publication date |
|---|---|
| CN1183234C (en) | 2005-01-05 |
| KR100440724B1 (en) | 2004-07-21 |
| JP3764391B2 (en) | 2006-04-05 |
| AU770156B2 (en) | 2004-02-12 |
| EP1323812A3 (en) | 2006-01-04 |
| AU1196602A (en) | 2003-07-03 |
| JP2003193073A (en) | 2003-07-09 |
| KR20030054768A (en) | 2003-07-02 |
| EP1323812A2 (en) | 2003-07-02 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN1428404A (en) | Combustion agent composition for generating colour brilliance lamp, and its mking method | |
| CN1236013C (en) | Long-afterglow fluorescent material | |
| CN109652214B (en) | Smokeless aromatherapy candle and manufacturing process thereof | |
| CN1550469A (en) | clear glass with blue rim tint | |
| CN1055348A (en) | Glass composition | |
| CN1912083A (en) | Candle body material composition for colour flame candle and its application | |
| US4204895A (en) | Green flare compositions | |
| CN1306013C (en) | A fuel composition and a device for colored flames | |
| CN1258489C (en) | Low temp. sealing lead-containingless tin phosphate series glass and composite material using the same | |
| CN104341925B (en) | A kind of luminescence generated by light coating and preparation method thereof | |
| CN1154621C (en) | Luminous glaze | |
| US6488726B1 (en) | Lamp fuel composition for colored flames and manufacturing method thereof | |
| CN101045861A (en) | Whole color fluorescent material and preparation method thereof | |
| CN113801658A (en) | Preparation method of boron phosphate/manganese pyrophosphate composite fluorescent powder with pink fluorescence | |
| KR20160113471A (en) | Phosphor, Method of fabricating the same, and Light Emitting Device of using the same | |
| JPH01245093A (en) | Fuel generating colored flame | |
| KR100598144B1 (en) | Phosphorescent pigment composition with long afterglow time | |
| CN1043339A (en) | Color flame candles | |
| JPS63258987A (en) | Illumination liquid fuel generating colored flame | |
| CN1074024C (en) | High brightness luminous paint and its producing method | |
| CN1445350A (en) | Soybean oil container candle | |
| KR100295012B1 (en) | Composition of lamp fuel for red colored flame and method thereof | |
| DE19961547A1 (en) | Coloration of flames comprises introducing copper metal or copper alloy into combustion zone of open flame | |
| US660114A (en) | Process of manufacturing incandescent bodies. | |
| DE19961548A1 (en) | Coloration of flames comprises incorporating color-producing substances into sustained-release matrix and positioning product in combustion zone of flame |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| ASS | Succession or assignment of patent right |
Owner name: COOPERSANTA CO., LTD. Free format text: FORMER OWNER: REN ZHENWAN Effective date: 20050422 |
|
| C41 | Transfer of patent application or patent right or utility model | ||
| TA01 | Transfer of patent application right |
Effective date of registration: 20050422 Address after: The South Korean city of Seoul Jiulongpo party Yidong loose 185 GA Applicant after: Santa Cruz Corporation Address before: Seoul City, Korea Applicant before: Ren Zhenwan |
|
| CI01 | Correction of invention patent gazette |
Correction item: Patentee Correct: Saint Cloud Limited False: Ren Zhenwan Number: 1 Page: 585 Volume: 21 |
|
| CI03 | Correction of invention patent |
Correction item: Patentee Correct: Saint Cloud Limited False: Ren Zhenwan Number: 1 Page: The title page Volume: 21 |
|
| COR | Change of bibliographic data |
Free format text: CORRECT: PATENTEE; FROM: REN ZHENWAN TO: SANTA CRUZ CO., LTD |
|
| ERR | Gazette correction |
Free format text: CORRECT: PATENTEE; FROM: REN ZHENWAN TO: SANTA CRUZ CO., LTD |
|
| ASS | Succession or assignment of patent right |
Owner name: HUOLINTECH CO., LTD. Free format text: FORMER OWNER: SANTA CRUZ CO., LTD. Effective date: 20090515 |
|
| C41 | Transfer of patent application or patent right or utility model | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20090515 Address after: Seoul special city Patentee after: KK Lin TECH Address before: The South Korean city of Seoul Jiulongpo party Yidong loose 185 GA Patentee before: Santa Cruz Corporation |
|
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20050105 Termination date: 20150128 |
|
| EXPY | Termination of patent right or utility model |