CN1332015C - Formula and technology of preparing distilled spirit by fermentation of sisal hemp stem - Google Patents
Formula and technology of preparing distilled spirit by fermentation of sisal hemp stem Download PDFInfo
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- CN1332015C CN1332015C CNB2005100686572A CN200510068657A CN1332015C CN 1332015 C CN1332015 C CN 1332015C CN B2005100686572 A CNB2005100686572 A CN B2005100686572A CN 200510068657 A CN200510068657 A CN 200510068657A CN 1332015 C CN1332015 C CN 1332015C
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- 244000198134 Agave sisalana Species 0.000 title claims abstract description 39
- 238000000855 fermentation Methods 0.000 title claims abstract description 15
- 230000004151 fermentation Effects 0.000 title claims abstract description 15
- 235000011624 Agave sisalana Nutrition 0.000 title description 2
- 240000004808 Saccharomyces cerevisiae Species 0.000 claims abstract description 12
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims abstract description 12
- 238000000034 method Methods 0.000 claims abstract description 12
- 235000011389 fruit/vegetable juice Nutrition 0.000 claims abstract description 9
- 235000000346 sugar Nutrition 0.000 claims abstract description 9
- 235000020357 syrup Nutrition 0.000 claims abstract description 5
- 239000006188 syrup Substances 0.000 claims abstract description 5
- 238000001816 cooling Methods 0.000 claims abstract description 4
- 239000004615 ingredient Substances 0.000 claims abstract description 4
- 239000006228 supernatant Substances 0.000 claims abstract description 4
- 235000021552 granulated sugar Nutrition 0.000 claims abstract description 3
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 7
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 4
- 239000002253 acid Substances 0.000 claims description 3
- 238000007689 inspection Methods 0.000 claims description 3
- 239000000047 product Substances 0.000 claims description 3
- 238000012360 testing method Methods 0.000 claims description 3
- 230000032683 aging Effects 0.000 claims description 2
- 238000010411 cooking Methods 0.000 claims description 2
- 238000010998 test method Methods 0.000 claims description 2
- 239000000203 mixture Substances 0.000 claims 1
- 238000004519 manufacturing process Methods 0.000 abstract description 5
- 230000008569 process Effects 0.000 abstract description 4
- 239000004927 clay Substances 0.000 abstract description 2
- 239000007788 liquid Substances 0.000 description 5
- 239000000835 fiber Substances 0.000 description 4
- 239000006227 byproduct Substances 0.000 description 3
- 238000004821 distillation Methods 0.000 description 3
- 238000011081 inoculation Methods 0.000 description 3
- 238000002156 mixing Methods 0.000 description 2
- 241000746976 Agavaceae Species 0.000 description 1
- 244000025254 Cannabis sativa Species 0.000 description 1
- 235000012766 Cannabis sativa ssp. sativa var. sativa Nutrition 0.000 description 1
- 235000012765 Cannabis sativa ssp. sativa var. spontanea Nutrition 0.000 description 1
- 244000193174 agave Species 0.000 description 1
- 230000001476 alcoholic effect Effects 0.000 description 1
- 235000009120 camo Nutrition 0.000 description 1
- 235000005607 chanvre indien Nutrition 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 230000007123 defense Effects 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 230000018109 developmental process Effects 0.000 description 1
- 239000012153 distilled water Substances 0.000 description 1
- 238000011156 evaluation Methods 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 238000011049 filling Methods 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 230000036541 health Effects 0.000 description 1
- 239000011487 hemp Substances 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 238000005065 mining Methods 0.000 description 1
- 230000008520 organization Effects 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 230000035755 proliferation Effects 0.000 description 1
- 239000008213 purified water Substances 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 235000020374 simple syrup Nutrition 0.000 description 1
- 238000010025 steaming Methods 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 238000009423 ventilation Methods 0.000 description 1
- 238000011514 vinification Methods 0.000 description 1
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Abstract
本发明公开了一种剑麻柄发酵制备蒸馏酒的工艺。工艺主要为:将剑麻柄,切块;蒸煮,冷却后切碎,榨汁;用砂糖糖浆调整成分总糖达15~20%,用柠檬酸调剑麻汁pH值为3.5~4.5,然后加入50毫克/升的SO2;再接种4~5%酿酒活性干酵母和1~2%生香活性干酵母;温度保持28~30℃,进行发酵;然后蒸馏;在酒中加入土陶片,密封,在阴凉处陈酿半年;用虹吸法吸取上清液,过滤;调配;检验、装瓶后即为剑麻酒成品。本发明利用剑麻柄等废弃物发酵制酒,达到综合利用剑麻柄等废弃物的目的。
The invention discloses a process for preparing distilled wine by fermenting sisal stalks. The main process is as follows: cut the sisal stalk into pieces; cook it, chop it after cooling, and squeeze the juice; adjust the total sugar of the ingredients to 15-20% with granulated sugar syrup, adjust the pH of the sisal juice to 3.5-4.5 with citric acid, and then Add 50 mg/L of SO 2 ; then inoculate 4-5% brewer's active dry yeast and 1-2% aroma-producing active dry yeast; keep the temperature at 28-30°C for fermentation; then distill; add clay tablets to the wine , sealed, and aged for half a year in a cool place; the supernatant was absorbed by siphon method, filtered; blended; inspected and bottled, it was the finished sisal wine. The invention utilizes wastes such as sisal stems to ferment wine to achieve the purpose of comprehensive utilization of wastes such as sisal stems.
Description
技术领域technical field
本发明涉及一种制酒工艺,特别是利用剑麻柄发酵制备蒸馏酒的工艺。The invention relates to a wine making process, in particular to a process for preparing distilled wine by fermenting sisal stalks.
背景技术Background technique
剑麻是一种龙舌兰科龙舌兰属的叶纤维作物,原产于墨西哥的龙加丹半岛,学名为:Agave Sisalana Perrine。英文名:Sisal。别名:西纱尔麻。主产国家有墨西哥、巴西、坦桑尼亚等国,在中国主要生长于雷州半岛及广西部分地区。Sisal is a leaf fiber crop of the Agave genus in the Agave family. It is native to the Longatan Peninsula in Mexico, and its scientific name is Agave Sisalana Perrine. English name: Sisal. Alias: Sisar hemp. The main producing countries are Mexico, Brazil, Tanzania and other countries. In China, it mainly grows in Leizhou Peninsula and parts of Guangxi.
剑麻产品为国防、工矿、渔航、农商、医疗卫生等事业不可缺少的物资,从工业到农业,从专业用品到日用品,从大工程到普通家庭,剑麻用品已是无处不在。据联合国粮农组织报告,全世界每年对剑麻纤维的需求量约为80~100万吨,而且需求量仍将以每年10~15%的速度增长,剑麻产业成为名副其实的朝阳产业。Sisal products are indispensable materials for national defense, industrial and mining, fishing, aviation, agriculture, commerce, medical and health care, etc. From industry to agriculture, from professional supplies to daily necessities, from large projects to ordinary households, sisal products are everywhere. According to the report of the Food and Agriculture Organization of the United Nations, the annual demand for sisal fiber in the world is about 800,000 to 1 million tons, and the demand will still increase at an annual rate of 10 to 15%. The sisal industry has become a veritable sunrise industry.
在剑麻纤维的生产过程中留下了大量副产品剑麻柄,均废弃不用,开发利用这些副产品,对充分利用剑麻这一天然资源,具有积极的意义,而利用剑麻柄发酵制备蒸馏酒的配方及工艺还未见报道。In the production process of sisal fiber, a large number of by-products sisal stalks are left, all of which are discarded. The development and utilization of these by-products has positive significance for making full use of sisal as a natural resource. The use of sisal stalks to ferment distilled wine The formula and process of it have not been reported yet.
发明内容Contents of the invention
本发明的目的是提供一种利用剑麻纤维的生产过程中留下的副产品剑麻柄发酵制备蒸馏酒的工艺。The purpose of the present invention is to provide a process for preparing distilled wine by fermenting the by-product sisal stalk left in the production process of sisal fiber.
制备工艺步骤如下:The preparation process steps are as follows:
采用剑麻柄,切块;加水高压蒸煮3小时,冷却后切碎,榨汁;用砂糖糖浆调整成分总糖达15~20%,用柠檬酸调剑麻汁pH值为3.5~4.5,然后加入50毫克/升的SO2;再接种4~5%的酿酒活性干酵母和1~2%生香活性干酵母;温度保持28~30℃,进行发酵8~10天;然后蒸馏,出酒温度一般控制在30℃以下,中馏酒接酒混合酒度达50°;在酒中加入土陶片,密封,在阴凉处陈酿半年;用虹吸法吸取上清液,过滤;采用正交试验法,选择影响口感的酒度、总糖、总酸主要成分为试验因素,对剑麻酒进行调配;检验、装瓶后即为剑麻酒成品。Use sisal stalks, cut into pieces; add water and high-pressure cook for 3 hours, chop and squeeze the juice after cooling; adjust the total sugar of the ingredients to 15-20% with granulated sugar syrup, adjust the pH value of the sisal juice to 3.5-4.5 with citric acid, and then Add 50 mg/L of SO 2 ; then inoculate 4-5% brewer's active dry yeast and 1-2% aroma-producing active dry yeast; keep the temperature at 28-30°C and ferment for 8-10 days; then distill and produce wine The temperature is generally controlled below 30°C, and the mixed alcohol content of middle-distilled wine and wine reaches 50°C; clay pottery pieces are added to the wine, sealed, and aged in a cool place for half a year; the supernatant is sucked up by siphon method and filtered; the orthogonal test is adopted According to the method, the main components of alcohol content, total sugar and total acid that affect the taste are selected as the experimental factors, and the sisal wine is prepared; after inspection and bottling, the finished sisal wine is obtained.
本发明利用剑麻柄等废弃物发酵制酒,达到综合利用剑麻柄等废弃物的目的,技术参数和结果今人满意,预期本发明的工作及成果,将会产生社会和经济双重效益。The present invention utilizes sisal stalks and other wastes to ferment wine to achieve the purpose of comprehensive utilization of sisal stalks and other wastes. The technical parameters and results are satisfactory. It is expected that the work and results of the present invention will produce social and economic double benefits.
附图说明Description of drawings
附图为本发明的工艺流程图。Accompanying drawing is process flow chart of the present invention.
具体实施方式Detailed ways
1、原料:新鲜剑麻柄,酿酒高活性干酵母、生香活性干酵母、砂糖糖浆、S02、纯净水。1. Raw materials: fresh sisal stalk, brewing high active dry yeast, aroma producing active dry yeast, sugar syrup, S0 2 , purified water.
2、切块、蒸煮:2. Cut into pieces and cook:
高压蒸煮:将剑麻柄切成碎块,称取10千克剑麻块放入高压锅中,添加约20升蒸馏水,蒸煮约3小时。High-pressure cooking: Cut the sisal handle into pieces, weigh 10 kg of sisal pieces and put them into a pressure cooker, add about 20 liters of distilled water, and cook for about 3 hours.
3、冷却、榨汁:蒸煮后冷却,然后切碎榨汁。3. Cooling and juicing: Cool after steaming, then chop and squeeze the juice.
4、调整成分:用糖浆调整剑麻汁总糖达17%,用柠檬酸调剑麻汁pH值为4左右,然后加入50毫克/升的S02。4. Adjust the ingredients: adjust the total sugar of the sisal juice to 17% with syrup, adjust the pH value of the sisal juice to about 4 with citric acid, and then add 50 mg/liter of S0 2 .
5、接种:先用75%酒精对接种瓶口进行消毒,再接种5%酿酒活性干酵母和1%生香活性干酵母,接种后发酵液的体积不超过发酵容积的3/4。5. Inoculation: Disinfect the mouth of the inoculation bottle with 75% alcohol, and then inoculate 5% brewing active dry yeast and 1% aroma-producing active dry yeast. The volume of the fermentation liquid after inoculation should not exceed 3/4 of the fermentation volume.
6、发酵:发酵温度保持28~30℃,并注意通风排气。若发现温度过高,及时降温发酵前期还要常搅动发酵液以补充空气,促进酵母增殖.当发酵2天后,发酵液含糖量降低,应补充糖浆,使发酵液含糖量达17%左右,然后密闭发酵罐,促进酵母进行酒精发酵。当发酵进入第8天后,发酵液呈现淡米黄色,清澈透明时,停止发酵。6. Fermentation: Keep the fermentation temperature at 28-30°C, and pay attention to ventilation and exhaust. If the temperature is found to be too high, lower the temperature in time and stir the fermentation liquid frequently in the early stage of fermentation to replenish air and promote yeast proliferation. After 2 days of fermentation, the sugar content of the fermentation liquid decreases, and syrup should be added to make the sugar content of the fermentation liquid reach about 17%. , and then close the fermenter to promote the yeast to carry out alcoholic fermentation. After the 8th day of fermentation, the fermented liquid was light beige, clear and transparent, and the fermentation was stopped.
7、蒸馏:将发酵完毕的醪液过滤后,装入蒸馏釜中,注意装料量不要超过蒸馏釜的2/3,蒸馏时要做到前猛中平后急,即开始温度要高,开始出酒时则可以缓和,待接近尾声时则需加大温度。勿使出酒温度过高,一般控制在30℃以下。出酒时,先接酒头,单放;中馏酒接酒混合酒度达50°待酒精含量达5%左右时,即断花摘酒。7. Distillation: After filtering the fermented mash, put it into the distillation kettle, and pay attention to the filling volume not exceeding 2/3 of the distillation kettle. When the wine starts to be released, it can be relaxed, and when it is near the end, the temperature needs to be increased. Do not make the temperature of the wine too high, generally controlled below 30 ℃. When the wine is served, first pick the head of the wine and put it alone; when the middle-distilled wine is mixed with the wine, the alcohol content reaches 50°, and when the alcohol content reaches about 5%, the wine is broken and picked.
8、陈酿:在酒中加入土陶片,密封,在阴凉处贮藏半年后,用虹吸法吸取上清液,过滤。8. Aging: Add earthen pottery slices to the wine, seal it, store it in a cool place for half a year, use siphon method to absorb the supernatant, and filter.
9、调配:采用正交试验法对剑麻酒进行调配。选择影响口感的酒度、总糖、总酸主要成分为试验因素,采用正交试验调配成试样,经品评打分,级差分析,确定最佳配方。9. Blending: The sisal wine was blended by using the orthogonal test method. Alcohol content, total sugar, and total acid, which affect the taste, were selected as the main components of the test, and the samples were prepared by orthogonal experiments, and the best formula was determined through evaluation, scoring, and differential analysis.
10、调配后,检验、装瓶后即为剑麻酒成品。10. After blending, inspection and bottling, it is the finished sisal wine.
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| CNB2005100686572A CN1332015C (en) | 2005-04-26 | 2005-04-26 | Formula and technology of preparing distilled spirit by fermentation of sisal hemp stem |
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| CNB2005100686572A CN1332015C (en) | 2005-04-26 | 2005-04-26 | Formula and technology of preparing distilled spirit by fermentation of sisal hemp stem |
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| CN1718709A CN1718709A (en) | 2006-01-11 |
| CN1332015C true CN1332015C (en) | 2007-08-15 |
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Families Citing this family (5)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CA2824956C (en) | 2011-01-18 | 2015-05-05 | Claremont Collection Handelsgesellschaft Mbh | Method of obtaining hemp plant juice and use of same for the production of beverages |
| DE202011001759U1 (en) * | 2011-01-18 | 2011-04-21 | Bisterfeld Von Meer, Galathea Ute | Juice from the hemp plant |
| CN104726286A (en) * | 2015-04-15 | 2015-06-24 | 中国热带农业科学院热带生物技术研究所 | Method for brewing wine by means of fermenting sisal stems |
| CN105505717A (en) * | 2016-01-08 | 2016-04-20 | 山西双林富农林开发有限公司 | Health-care wine made of fruit stems of xanthoceras sorbifolium bunge and making method thereof |
| CN106309278B (en) * | 2016-08-31 | 2020-05-08 | 澳宝化妆品(惠州)有限公司 | Agave fermentation product for anti-aging cosmetics and preparation method and application thereof |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN1490045A (en) * | 2003-09-05 | 2004-04-21 | 清华大学 | Sisal extract and its preparation method and use |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN1490045A (en) * | 2003-09-05 | 2004-04-21 | 清华大学 | Sisal extract and its preparation method and use |
Non-Patent Citations (1)
| Title |
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| 浅谈剑麻及其制品的应用 莫百春,中国纤检,第6期 2003 * |
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