CN1135940C - Tobacco-swelling biological additive and its prepn. and application - Google Patents
Tobacco-swelling biological additive and its prepn. and application Download PDFInfo
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- CN1135940C CN1135940C CNB021135452A CN02113545A CN1135940C CN 1135940 C CN1135940 C CN 1135940C CN B021135452 A CNB021135452 A CN B021135452A CN 02113545 A CN02113545 A CN 02113545A CN 1135940 C CN1135940 C CN 1135940C
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- Prior art keywords
- tobacco
- degrading enzyme
- additive
- swelling
- biological additive
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- 239000000654 additive Substances 0.000 title claims abstract description 34
- 230000000996 additive effect Effects 0.000 title claims abstract description 26
- 241000208125 Nicotiana Species 0.000 claims abstract description 93
- 235000002637 Nicotiana tabacum Nutrition 0.000 claims abstract description 93
- 102000004190 Enzymes Human genes 0.000 claims abstract description 20
- 108090000790 Enzymes Proteins 0.000 claims abstract description 20
- 230000000593 degrading effect Effects 0.000 claims abstract description 20
- CIWBSHSKHKDKBQ-JLAZNSOCSA-N Ascorbic acid Chemical compound OC[C@H](O)[C@H]1OC(=O)C(O)=C1O CIWBSHSKHKDKBQ-JLAZNSOCSA-N 0.000 claims abstract description 12
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 9
- 229920001277 pectin Polymers 0.000 claims abstract description 8
- 235000010987 pectin Nutrition 0.000 claims abstract description 8
- 239000001814 pectin Substances 0.000 claims abstract description 8
- 229920002472 Starch Polymers 0.000 claims abstract description 7
- 239000000835 fiber Substances 0.000 claims abstract description 7
- 235000019698 starch Nutrition 0.000 claims abstract description 7
- 239000008107 starch Substances 0.000 claims abstract description 7
- ZZZCUOFIHGPKAK-UHFFFAOYSA-N D-erythro-ascorbic acid Natural products OCC1OC(=O)C(O)=C1O ZZZCUOFIHGPKAK-UHFFFAOYSA-N 0.000 claims abstract description 6
- 102000004317 Lyases Human genes 0.000 claims abstract description 6
- 108090000856 Lyases Proteins 0.000 claims abstract description 6
- 229930003268 Vitamin C Natural products 0.000 claims abstract description 6
- 150000004676 glycans Chemical class 0.000 claims abstract description 6
- 229920001282 polysaccharide Polymers 0.000 claims abstract description 6
- 239000005017 polysaccharide Substances 0.000 claims abstract description 6
- 235000019154 vitamin C Nutrition 0.000 claims abstract description 6
- 239000011718 vitamin C Substances 0.000 claims abstract description 6
- 238000002360 preparation method Methods 0.000 claims abstract description 4
- 235000019504 cigarettes Nutrition 0.000 claims description 21
- 238000000034 method Methods 0.000 claims description 14
- 239000000047 product Substances 0.000 claims description 14
- 239000000463 material Substances 0.000 claims description 11
- 230000008569 process Effects 0.000 claims description 11
- 102000038379 digestive enzymes Human genes 0.000 claims description 10
- 108091007734 digestive enzymes Proteins 0.000 claims description 10
- 102000030523 Catechol oxidase Human genes 0.000 claims description 5
- 108010031396 Catechol oxidase Proteins 0.000 claims description 5
- 101710138460 Leaf protein Proteins 0.000 claims description 5
- 239000003607 modifier Substances 0.000 claims description 5
- 239000007921 spray Substances 0.000 claims description 5
- 238000004090 dissolution Methods 0.000 claims description 3
- 239000000706 filtrate Substances 0.000 claims description 3
- 239000002904 solvent Substances 0.000 claims description 3
- 238000003756 stirring Methods 0.000 claims description 3
- 230000000284 resting effect Effects 0.000 claims description 2
- 239000003795 chemical substances by application Substances 0.000 abstract description 4
- 230000008901 benefit Effects 0.000 abstract description 3
- 150000008442 polyphenolic compounds Chemical class 0.000 abstract description 3
- 235000013824 polyphenols Nutrition 0.000 abstract description 3
- 230000000391 smoking effect Effects 0.000 abstract description 3
- 102000004169 proteins and genes Human genes 0.000 abstract description 2
- 108090000623 proteins and genes Proteins 0.000 abstract description 2
- 239000000470 constituent Substances 0.000 abstract 1
- 239000004615 ingredient Substances 0.000 abstract 1
- 230000001590 oxidative effect Effects 0.000 abstract 1
- 239000000203 mixture Substances 0.000 description 7
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 6
- 230000008859 change Effects 0.000 description 6
- 230000000694 effects Effects 0.000 description 6
- 238000005516 engineering process Methods 0.000 description 6
- 239000000126 substance Substances 0.000 description 6
- 238000004519 manufacturing process Methods 0.000 description 4
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 description 3
- 229960004424 carbon dioxide Drugs 0.000 description 3
- 235000011089 carbon dioxide Nutrition 0.000 description 3
- 230000002950 deficient Effects 0.000 description 3
- 238000011161 development Methods 0.000 description 3
- 239000003546 flue gas Substances 0.000 description 3
- 239000003205 fragrance Substances 0.000 description 3
- 239000007789 gas Substances 0.000 description 3
- FYGHSUNMUKGBRK-UHFFFAOYSA-N 1,2,3-trimethylbenzene Chemical compound CC1=CC=CC(C)=C1C FYGHSUNMUKGBRK-UHFFFAOYSA-N 0.000 description 2
- HYFLWBNQFMXCPA-UHFFFAOYSA-N 1-ethyl-2-methylbenzene Chemical compound CCC1=CC=CC=C1C HYFLWBNQFMXCPA-UHFFFAOYSA-N 0.000 description 2
- LCZUOKDVTBMCMX-UHFFFAOYSA-N 2,5-Dimethylpyrazine Chemical compound CC1=CN=C(C)C=N1 LCZUOKDVTBMCMX-UHFFFAOYSA-N 0.000 description 2
- HUMNYLRZRPPJDN-UHFFFAOYSA-N benzaldehyde Chemical compound O=CC1=CC=CC=C1 HUMNYLRZRPPJDN-UHFFFAOYSA-N 0.000 description 2
- 229910002092 carbon dioxide Inorganic materials 0.000 description 2
- 238000013461 design Methods 0.000 description 2
- 230000002779 inactivation Effects 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 239000002304 perfume Substances 0.000 description 2
- 238000012545 processing Methods 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- 235000013599 spices Nutrition 0.000 description 2
- 239000011269 tar Substances 0.000 description 2
- 238000012360 testing method Methods 0.000 description 2
- -1 (2H) furans ketone Chemical class 0.000 description 1
- IANQTJSKSUMEQM-UHFFFAOYSA-N 1-benzofuran Chemical class C1=CC=C2OC=CC2=C1 IANQTJSKSUMEQM-UHFFFAOYSA-N 0.000 description 1
- 239000001934 2,5-dimethylpyrazine Substances 0.000 description 1
- WRMNZCZEMHIOCP-UHFFFAOYSA-N 2-phenylethanol Chemical class OCCC1=CC=CC=C1 WRMNZCZEMHIOCP-UHFFFAOYSA-N 0.000 description 1
- CIBKSMZEVHTQLG-UHFFFAOYSA-N 5-Ethyl-2,3-dimethylpyrazine Chemical compound CCC1=CN=C(C)C(C)=N1 CIBKSMZEVHTQLG-UHFFFAOYSA-N 0.000 description 1
- 244000061458 Solanum melongena Species 0.000 description 1
- 235000002597 Solanum melongena Nutrition 0.000 description 1
- 150000001298 alcohols Chemical class 0.000 description 1
- 150000001413 amino acids Chemical class 0.000 description 1
- 230000002738 anti-smoking effect Effects 0.000 description 1
- 125000003118 aryl group Chemical group 0.000 description 1
- 230000004888 barrier function Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000033228 biological regulation Effects 0.000 description 1
- 230000003592 biomimetic effect Effects 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 239000012496 blank sample Substances 0.000 description 1
- RNOOHTVUSNIPCJ-UHFFFAOYSA-N butan-2-yl prop-2-enoate Chemical class CCC(C)OC(=O)C=C RNOOHTVUSNIPCJ-UHFFFAOYSA-N 0.000 description 1
- 239000001569 carbon dioxide Substances 0.000 description 1
- 239000011285 coke tar Substances 0.000 description 1
- 238000002485 combustion reaction Methods 0.000 description 1
- 239000002131 composite material Substances 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 235000009508 confectionery Nutrition 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- DOIRQSBPFJWKBE-UHFFFAOYSA-N dibutyl phthalate Chemical class CCCCOC(=O)C1=CC=CC=C1C(=O)OCCCC DOIRQSBPFJWKBE-UHFFFAOYSA-N 0.000 description 1
- 239000012895 dilution Substances 0.000 description 1
- 238000010790 dilution Methods 0.000 description 1
- 238000007598 dipping method Methods 0.000 description 1
- 238000011156 evaluation Methods 0.000 description 1
- 238000002309 gasification Methods 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 230000003993 interaction Effects 0.000 description 1
- 150000002576 ketones Chemical class 0.000 description 1
- 230000014759 maintenance of location Effects 0.000 description 1
- 230000007246 mechanism Effects 0.000 description 1
- ZAZKJZBWRNNLDS-UHFFFAOYSA-N methyl tetradecanoate Chemical class CCCCCCCCCCCCCC(=O)OC ZAZKJZBWRNNLDS-UHFFFAOYSA-N 0.000 description 1
- CAWHJQAVHZEVTJ-UHFFFAOYSA-N methylpyrazine Chemical compound CC1=CN=CC=N1 CAWHJQAVHZEVTJ-UHFFFAOYSA-N 0.000 description 1
- 230000000813 microbial effect Effects 0.000 description 1
- 231100000252 nontoxic Toxicity 0.000 description 1
- 230000003000 nontoxic effect Effects 0.000 description 1
- QNGNSVIICDLXHT-UHFFFAOYSA-N para-ethylbenzaldehyde Natural products CCC1=CC=C(C=O)C=C1 QNGNSVIICDLXHT-UHFFFAOYSA-N 0.000 description 1
- DTUQWGWMVIHBKE-UHFFFAOYSA-N phenylacetaldehyde Chemical class O=CCC1=CC=CC=C1 DTUQWGWMVIHBKE-UHFFFAOYSA-N 0.000 description 1
- 230000008092 positive effect Effects 0.000 description 1
- 230000001007 puffing effect Effects 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 239000000523 sample Substances 0.000 description 1
- 230000001953 sensory effect Effects 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 230000004936 stimulating effect Effects 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 230000008961 swelling Effects 0.000 description 1
- 235000019505 tobacco product Nutrition 0.000 description 1
Landscapes
- Manufacture Of Tobacco Products (AREA)
Abstract
The present invention relates to a biological additive for expanding tobacco, a preparation method thereof and an application thereof. The constituents and contents comprise 0.1 to 10% of protein degrading enzyme of tobacco leaf, 1.0 to 10% of starch degrading enzyme, 0.2 to 10% of pectin degrading enzyme, 0.5 to 20% of polysaccharide degrading enzyme, 0.5 to 20% of fibre modifying agent, 0.1 to 5% of polyphenol oxidative degrading enzyme, 0.1 to 10% of desmolase, 0.1 to 5% of vitamin C and water as the rest. The biological additive is added after moisture regaining and chopping of tobacco, namely that the provided biological additive for expanding tobacco of the present invention is added before expansion, the addition of the biological additive is from 0.2 to 5 wt% of the tobacco shreds, and the adding temperature is from 30 to 50 DEG C. The present invention has the advantages of no negative influence on tobacco and effective function of reducing the unfavorable ingredients of smoking.
Description
Affiliated technical field
The present invention relates to tobacco additive agent, more particularly the present invention relates to a kind of bio-additive of expanding tobacco.The invention still further relates to a kind of preparation method of described bio-additive and the application in production of cigarettes thereof simultaneously
Background technology
Along with global anti-smoking campaign grows to even greater heights, low harm cigarette becomes development trend; Expanding tobacco is one of most important material of making low harm cigarette.Because tobacco is after expanding, density reduces, and the tobacco leaf volume increases, and filling power increases, thereby can reduce the consumption of pipe tobacco in the cigarette, plays and reduces the tobacco leaf consumption, reduces the purpose of tar, has very big economic benefit.The pipe tobacco of Unit Weight increases greatly with the contact area of air after expanding, burn rate is accelerated, and ratio of combustion is more complete, tobacco consumption that can every mouthful of suction of corresponding minimizing, tar content in the flue gas is obviously reduced, thereby in the exploitation of low-coke tar cigarette, have positive effect.Therefore, from the tobacco expansion process technology development of the later stage sixties rapidly, we can say that expanded cut tobacco has become is important in the modern cigarette product prescription design, indispensable effective means and strong weapon.
Carbon dioxide expanding tobacco technology is a new technology that developed in recent years.Because CO
2The source is abundant, and is cheap, colourless, nontoxic, harmless, gasification point is very low and expansion rate can reach more than 80%, so CO worldwide
2Expansion technique development and universal very fast.The CO that built up and gone into operation at present of Yunnan Province only
2The dry-ice expanding line has 6, has formed considerable commercial production scale in China.Be equipped with cigarette producer both at home and abroad all mixed expanded cut tobacco different proportion in its cigarette product, and set up the expanded cut tobacco production line, expanded cut tobacco becomes the important foundation raw material of cigarette producer.
But, expanding tobacco is but bigger because of autostimulation, shrivelled gas is heavy, cigarette perfume (or spice) is light, abundant etc. defective, makes the flue gas of cigarette product be subjected to very big dilution, and fragrance matter is affected, and assorted gas appears, mouthfeel is relatively poor, and the solid sense of the rich and flue gas of cigarette perfume (or spice) also obviously descends, and these all become the bottleneck that restriction cigarette product quality improves.Therefore, how improving the interior quality of expanded cut tobacco, it is played a greater role in cigarette product, have bigger availability, is the great problem of pendulum in face of each cigarette producer and vast cigarette worker.It also is urgency technical barrier to be solved of tobacco business.
Summary of the invention
In order to overcome the deficiencies in the prior art part, the objective of the invention is provides a kind of tobacco-swelling biological additive, thereby promotes the suction quality of expanding tobacco significantly under the constant situation of the every physical index of expanding tobacco guaranteeing.
Another object of the present invention is to provide a kind of method for preparing tobacco-swelling biological additive.
The present invention also aims to provide the application of a kind of tobacco-swelling biological additive in cigarette producing process.
Technical scheme: except as otherwise noted, the percentage that is adopted among the present invention is percetage by weight.
Tobacco-swelling biological additive provided by the invention, its component and content are:
Tobacco leaf protein digestive enzyme 0.1～10%
Starch degrading enzyme 1.0-10%
Pectin degrading enzyme 0.2-10%
Polysaccharide degrading enzyme 0.5-20%
Fibre modifier 0.5-20%
Polyphenol oxidase digestive enzyme 0.1-5%
Desmolase 0.1-10%
Vitamin C 0.1-5%
Water fills up 100%
The preparation method of tobacco-swelling biological additive provided by the invention, this method comprises the step of following order:
(1) material shown in will filling a prescription is that dissolution with solvents is mixed with water;
(2) stir, filter;
(3) filtrate is finished product.
The invention provides the application process of tobacco-swelling biological additive in cigarette producing process, may further comprise the steps:
(1) add---after tobacco moisture regain chopping, promptly before tobacco expanding, just add expanding tobacco additive provided by the invention, addition is 0.2%～5% of a pipe tobacco weight, adding temperature is 30 ℃～50 ℃, interpolation equipment sprays interpolation with spray pattern, can adopt the atomising device of band flowmeter;
(2) store---be stored in 30 ℃～50 ℃ of temperature after the interpolation, under the environment of 60% humidity, pipe tobacco moisture content keeps 19%～25%, and the resting period is 2～5 hours.
Beneficial effect
1. test data shows that tobacco-swelling biological additive of the present invention has the shallow lake amount that reduces in the tobacco leaf, reduce the protein content in the tobacco leaf, reduce the pectin content in the tobacco leaf, change the part fibre structure of tobacco leaf cell, sugared content transforms the remarkable efficacy of the polyphenols in the tobacco leaf to reasonable level in the regulation and control tobacco leaf; Adding biologic product can not bring negative effect can reduce the composition that is unfavorable for suction quality again to tobacco simultaneously, the present invention has filtered out effect biological products preferably, and it is made up the mature and stable prescription of composite formation, started the biology direction of tobacco additive agent.
2. not to resemble the conventional chemical addition agent it will just be ignored, develops as one pleases after adding tobacco to bio-additive the present invention, but when some compositions are degraded to a certain degree, will utilize the hot conditions of back one step that it is carried out inactivation treatment after 2-5 hour in effect, stop its effect.So, our additive be to aim at this technology of CO2 expanded cut tobacco and design, can not break away from foregoing expansion process condition, i.e. (moisture in cut tobacco: 19%-25%, pipe tobacco temperature: 20 ℃-50 ℃, swelling temperature: 280 ℃-350 ℃), thus with the biological tobacco additive of developing at present substantial breakthrough is arranged.
3. the quality of expanded cut tobacco still depends on the quality of raw tobacco material to a great extent, and the raw tobacco material that is used as expanded cut tobacco mostly is junior tobacco.Therefore the purpose of bio-modification additive is: add biologic product in pipe tobacco after tobacco moisture regain chopping, utilize the suit advantage of microbial activities of moisture regain storage silk this section pipe tobacco in period high humidity and relative higher temperature, biologic product can be to greatest extent to being unfavorable for the composition biodegrade of suction quality in the tobacco, quality behind the expanding tobacco is correspondingly increased substantially, after achieving the above object, pipe tobacco is admitted to the high temperature expansion stage, utilize hot conditions that bio-additive is carried out inactivation treatment, finish its mission, thereby reach depth of interaction and the effect range of controlling additive fully, keep the stability of tobacco product.
4. domestic most of cigarette enterprise all adopts CO
2As inflating medium, and pipe tobacco all do not deal with before expansion, directly carries out expandedly, only adopts the mode of interpolation table essence to modify in the expansion process back that finishes to pipe tobacco.The present invention has made important improvement to original processing technological flow, starts with from the expand chemical composition change of front and back pipe tobacco and the variation of aroma component, at CO
2The process characteristic of dry-ice expanding is promptly: the low-temperature/high-pressure dipping (79 ℃/2.83MPa) and high temperature puffing and the back pipe tobacco fragrance loss that expands bigger, stimulating increases, defectives such as mouthfeel is undesirable, change traditional expanded cut tobacco perfuming processing mode, before tobacco expanding, impose special bio-additive, make in the pipe tobacco of expanded front and back the material that changes not quite but produce breath of poor quality obtain degraded, reduce the material that is unfavorable for suction quality, the defective of expanded cut tobacco is eliminated, and quality promotes towards target direction.Promptly just it was carried out bioactivation before tobacco expanding and handle, pipe tobacco moisture regain back humiture is higher, helps biologic product performance maximum activity, and the quality of tobacco grade is improved, and therefore, the pipe tobacco that is equivalent to make good use of is done raw material, has just obtained good expansion thread naturally.
5. break through the limitation of traditional flavoring and casing mode, analyze and research from the interior change mechanism aspect of tobacco, the composition that is unfavorable for suction quality in the tobacco is effectively improved and degraded, and the quality that makes expanding tobacco transforms towards the direction that helps improving quality.Thereby can improve its availability greatly, the present invention organically combines up-to-date bio-modification technology and biomimetic chemistry etc. for one, has broad application prospects and potentiality to be exploited.
Fig. 1 is an expanded cut tobacco additive treating process chart of the present invention.
The specific embodiment
Can further be well understood to the present invention by specific embodiments of the invention given below and comparing embodiment.But they are not limitation of the invention.
Embodiment 1
Tobacco-swelling biological additive provided by the invention, its component and content are:
Tobacco leaf protein digestive enzyme 5%
Starch degrading enzyme 5%
Pectin degrading enzyme 5%
Polysaccharide degrading enzyme 10%
Fibre modifier 10%
Polyphenol oxidase digestive enzyme 10%
Desmolase 5%
Vitamin C 3%
Water fills up 100%
Embodiment 2
Tobacco leaf protein digestive enzyme 0.1%
Starch degrading enzyme 1.0%
Pectin degrading enzyme 0.2%
Polysaccharide degrading enzyme 0.5%
Fibre modifier 0.5%
Polyphenol oxidase digestive enzyme 0.1%
Desmolase 0.1%
Vitamin C 0.1%
Water fills up 100%
Embodiment 3
Tobacco leaf protein digestive enzyme 10%
Starch degrading enzyme 10%
Pectin degrading enzyme 10%
Polysaccharide degrading enzyme 20%
Fibre modifier 20%
Polyphenol oxidase digestive enzyme 5%
Desmolase 10%
Vitamin C 5%
Water fills up 100%
Embodiment 4
Be that dissolution with solvents is mixed with water with the material in embodiment 1,2,3 prescriptions respectively; Stir, filter; Filtrate is the finished product of Different Weight percentage concentration.
Application Example 1
After tobacco moisture regain chopping, expanded cut tobacco bio-additive provided by the invention is added in the pipe tobacco to every physical index of pipe tobacco with spray pattern.Project is to moisture (%) 21.5 22.8 filling value (cm before treatment samples expands in the same old way
3/ g) 6.62 6.83 whole cut rates (%) 82.0 81.7 contain the moisture (%) 12.0 12.4 that gets damp again after last rate (%) 3.4 3.5 expands
Application Example 2
Main chemical compositions situation of change before and after pipe tobacco is handled
| The pipe tobacco routine chemical components | Situation of change |
| Starch | Reduce 5-50% |
| Protein | Reduce 5-30% |
| Pectin | Reduce 3-35% |
| Polyphenols | Reduce 5-50% |
| Total reducing sugar | Reduce 5-45% |
| Reduced sugar | Increase 5-20% |
| Amino acid | Increase 5-25% |
Application Example 3
The expanding tobacco treatment samples with the contrast of main volatile aroma component in the same old way sequence number retention time compound treatment sample is contained contain in the same old way
(min) amount (%) amount (%) 1 3.35 furfurals 8.43 4.252 3.68 furfuryl alcohols 7.02 6.313 4.03 4-ring the eleventh of the twelve Earthly Branches alkene-1,3-diketone 3.28 1.514 4.19 2-butyl acrylates 1.26 1.155 4.64 australenes 0.72 0.486 4.78 2,5-dimethyl pyrazine 3.83-7 5.19 1-ethyl-2-methyl-benzene 0.68 0.628 5.55 benzaldehyde 2.09-9 5.70 1,2,3-trimethylbenzene 1.21 0.9510 6.41 phenmethylols 1.04 0.7611 6.55 phenylacetaldehydes 9.25 8.3612 7.35 2,5-dimethyl-4-hydroxyls 1.70-
-3 (2H) furans ketone 13 7.50 3-ethyls-2; 5-dimethyl pyrazine 3.36 2.0114 7.60 2,3-dimethyl-5-ethyl pyrazine 0.92-15 7.74 benzyl carbinols 3.82 1.6716 9.16 N-furfuryl group pyrroles 1.61 1.5217 9.46 3-benzofuranes 2.09 1.7318 10.21 2-isopentyl-those scholar's ketone 3.56 3.1330 20.11 neophytadienes 19.42 18.53 of 6-methylpyrazine 1.06-19 11.48 solanones 0.31 0.4420 11.80 dorinone 8.23 7.5221 12.21 carypohyllenes 3.16 2.5122 14.47 dihydroactinidiolides 7.85 6.1023 14.56 Megastigmatrienones (A) 2.96 2.4224 14.83 Megastigmatrienones (B) 13.02 10.0125 15.43 Megastigmatrienones (C) 2.87 1.5626 15.65 Megastigmatrienones (D) 10.32 7.4727 15.31 dibutyl phthalates 2.63 1.0528 17.14 methyl myristates 0.88 0.9429 18.54 eggplant
The test data of Application Example 1～3 shows, from physical index, before and after handling, pipe tobacco do not have big variation, but content from routine chemical components, pipe tobacco is handled the multiple composition of suction quality that is unfavorable in back through bio-additive and has been obtained degraded significantly, after expanding through high temperature again, react mutually between the material that some degradeds generate, form aromatic material and latent perfumery matter; Pipe tobacco has just been finished the degraded of the material that is unfavorable for suction quality and has been helped the generation of the aroma substance of suction quality in this process like this.Expanded cut tobacco and the blank sample that adds bio-additive carried out sensory evaluating smoking's evaluation, and smoking result shows: the expanded cut tobacco fragrance concentration after biologic product is handled is constant, and cigarette is fragrant fine and smooth sweet, and assorted gas is lighter, stimulates obviously to reduce, and pleasant impression is comfortable.
Claims (3)
1. tobacco-swelling biological additive, its component and content are:
Tobacco leaf protein digestive enzyme 0.1～10%
Starch degrading enzyme 1.0-10%
Pectin degrading enzyme 0.2-10%
Polysaccharide degrading enzyme 0.5-20%
Fibre modifier 0.5-20%
Polyphenol oxidase digestive enzyme 0.1-5%
Desmolase 0.1-10%
Vitamin C 0.1-5%
It is percetage by weight that water fills up 100% all percentages.
2. the preparation method of the described tobacco-swelling biological additive of claim 1 is characterized in that adopting the step of following order:
(1) material shown in will filling a prescription is that dissolution with solvents is mixed with water;
(2) stir, filter;
(3) filtrate is finished product.
3. the application process of the described tobacco-swelling biological additive of claim 1 in cigarette producing process may further comprise the steps:
(1) add---after tobacco moisture regain chopping, promptly before tobacco expanding, just add expanding tobacco additive provided by the invention, addition is 0.2%～5% of a pipe tobacco weight, adding temperature is 30 ℃～50 ℃, interpolation equipment sprays interpolation with spray pattern, can adopt the atomising device of band flowmeter;
(2) store---be stored in 30 ℃～50 ℃ of temperature after the interpolation, under the environment of 60% humidity, pipe tobacco moisture content keeps 19%～25%, and the resting period is 2～5 hours.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB021135452A CN1135940C (en) | 2002-03-29 | 2002-03-29 | Tobacco-swelling biological additive and its prepn. and application |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB021135452A CN1135940C (en) | 2002-03-29 | 2002-03-29 | Tobacco-swelling biological additive and its prepn. and application |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN1375244A CN1375244A (en) | 2002-10-23 |
| CN1135940C true CN1135940C (en) | 2004-01-28 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CNB021135452A Expired - Fee Related CN1135940C (en) | 2002-03-29 | 2002-03-29 | Tobacco-swelling biological additive and its prepn. and application |
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| CN (1) | CN1135940C (en) |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1319478C (en) * | 2005-07-13 | 2007-06-06 | 云南瑞升科技有限公司 | Additive for flue-cured tobacco, prepn. method and application thereof |
| CN100534337C (en) * | 2006-10-23 | 2009-09-02 | 云南瑞升烟草技术（集团）有限公司 | Additives for modifying reproduced tobacco leaves, preparation method and use method thereof |
| CN101785577B (en) * | 2008-12-26 | 2012-02-29 | 湖北中烟工业有限责任公司 | Method for reducing irritation of paper-making tobacco sheet |
| CN102669811B (en) * | 2012-05-28 | 2015-06-17 | 川渝中烟工业有限责任公司 | Method for producing cigarette expansion cut tobacco with low tar content and low harm by using microbial fermentation |
| CN104013094B (en) * | 2014-06-26 | 2016-06-08 | 福建中烟工业有限责任公司 | A kind of raising CO2The additive of expanded cut tobacco quality and the application in cigarette thereof |
| CN105614943A (en) * | 2014-10-27 | 2016-06-01 | 上海绿馨电子科技有限公司 | Tobaccos and manufacturing method thereof |
| CN110742304A (en) * | 2019-10-22 | 2020-02-04 | 红塔辽宁烟草有限责任公司 | Complex enzyme preparation for improving quality grade of expanded tobacco shreds and application thereof |
| CN117859936B (en) * | 2024-02-21 | 2025-10-24 | 江苏中烟工业有限责任公司 | A method for improving the use value of tobacco leaves air-dried in warehouse and its application |
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2002
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