CN113368535B - Micromolecular biomass extraction and purification equipment - Google Patents
Micromolecular biomass extraction and purification equipment Download PDFInfo
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- 238000000605 extraction Methods 0.000 title claims abstract description 90
- 239000002028 Biomass Substances 0.000 title claims abstract description 16
- 238000000746 purification Methods 0.000 title claims abstract description 10
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- 238000002156 mixing Methods 0.000 claims abstract description 8
- 239000012295 chemical reaction liquid Substances 0.000 claims abstract description 7
- 239000002904 solvent Substances 0.000 claims abstract description 6
- 239000002994 raw material Substances 0.000 claims abstract description 5
- 238000005192 partition Methods 0.000 claims description 19
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 11
- 150000003384 small molecules Chemical class 0.000 claims description 7
- 238000003756 stirring Methods 0.000 claims description 4
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- VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 description 2
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- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D11/00—Solvent extraction
- B01D11/04—Solvent extraction of solutions which are liquid
- B01D11/0492—Applications, solvents used
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Abstract
Description
技术领域technical field
本发明涉及一种萃取领域,具体是一种小分子生物质萃取提纯设备。The invention relates to the field of extraction, in particular to a small molecular biomass extraction and purification device.
背景技术Background technique
根据国际能源机构(IEA)的定义,生物质(biomass)是指通过光合作用而形成的各种有机体,包括所有的动植物和微生物。生物质能则是太阳能以化学能形式储存在生物质中的能量形式,它一直是人类赖以生存的重要能源之一,是仅次于煤炭、石油、天然气之后第四大能源,在整个能源系统中占有重要的地位。According to the definition of the International Energy Agency (IEA), biomass refers to various organisms formed through photosynthesis, including all animals, plants and microorganisms. Biomass energy is the energy form of solar energy stored in biomass in the form of chemical energy. It has always been one of the important energy sources for human survival. It is the fourth largest energy source after coal, oil and natural gas. plays an important role in the system.
在对生物质的使用过程中,现有技术用到萃取的方式对溶液内部的生物质材料进行提取分离,主要操作方式为人工萃取的方式;In the process of using the biomass, the prior art uses the extraction method to extract and separate the biomass material inside the solution, and the main operation method is the manual extraction method;
但是,人工萃取的过程中,萃取液的分隔面难以辨析,进而使得溶剂被混入萃取液的内部,进而造成萃取液受到污染。However, in the process of artificial extraction, it is difficult to distinguish the separation surface of the extraction liquid, so that the solvent is mixed into the interior of the extraction liquid, and the extraction liquid is polluted.
发明内容SUMMARY OF THE INVENTION
本发明的目的在于提供一种小分子生物质萃取提纯设备,以解决上述背景技术中提出的萃取液在人工操作的过程中受到污染的问题。The purpose of the present invention is to provide a small molecule biomass extraction and purification equipment, so as to solve the problem of contamination of the extraction solution in the process of manual operation proposed in the above-mentioned background art.
为实现上述目的,本发明提供如下技术方案:To achieve the above object, the present invention provides the following technical solutions:
一种小分子生物质萃取提纯设备,包括L型架,还包括:A small-molecule biomass extraction and purification equipment, comprising an L-shaped frame, and further comprising:
盛放装置,用作为装置提供原料;A holding device, which is used as a device to provide raw materials;
管路装置,盛放装置与管路装置相互导通,用作反应液的输送;The pipeline device, the holding device and the pipeline device communicate with each other, which are used for the transportation of the reaction liquid;
萃取装置,萃取装置与管路装置的尾部相互导通安装,用作对萃取液进行分隔式萃取;Extraction device, the tail of the extraction device and the pipeline device are connected to each other and are used for separate extraction of the extraction liquid;
动力装置,动力装置安装在萃取装置的表面,用作对萃取过程中中间滚筒的翻滚混合;The power unit, which is installed on the surface of the extraction unit, is used for tumbling mixing of the intermediate drum during the extraction process;
隔板装置,所述隔板装置安装在萃取装置的中间部位内部,用作将萃取完成的萃取液和溶剂分隔开;A partition device, which is installed inside the middle part of the extraction device and used to separate the extraction liquid and the solvent after extraction;
萃取装置包括安装在导管底部的萃取箱体,萃取箱体的内部安装有搅拌浮球,萃取箱体的中间部位安装有隔板装置,萃取箱体的底部安装有出口装置;The extraction device includes an extraction box installed at the bottom of the conduit, a stirring float is installed inside the extraction box, a partition device is installed in the middle of the extraction box, and an outlet device is installed at the bottom of the extraction box;
隔板装置包括固定在萃取箱体一侧的气缸,气缸的顶部安装有气缸杆,气缸杆的顶部安装有隔板装置,隔板装置包括安装在气缸杆表面的隔板,隔板的两侧安装有滑套,隔板的侧边安装有伸缩基座,伸缩基座的表面安装有伸缩杆,伸缩杆的一侧安装有滑块,滑块的一侧安装有布帘,隔板的中间安装有纱网。The partition device includes a cylinder fixed on one side of the extraction box, a cylinder rod is installed on the top of the cylinder, and a partition device is installed on the top of the cylinder rod, and the partition device includes a partition installed on the surface of the cylinder rod. A sliding sleeve is installed, a telescopic base is installed on the side of the clapboard, a telescopic rod is installed on the surface of the telescopic base, a slider is installed on one side of the telescopic rod, a cloth curtain is installed on one side of the slider, and the middle of the clapboard is installed. Installed with gauze.
优选的,盛放装置包括固定在L型架一侧的桶体,桶体的内部盛放有待处理液,桶体的侧壁安装有气泵,桶体的内侧安装有出口管。Preferably, the holding device includes a barrel fixed on one side of the L-shaped frame, the inside of the barrel contains the liquid to be treated, the side wall of the barrel is installed with an air pump, and the inner side of the barrel is installed with an outlet pipe.
优选的,管路装置包括安装在纵向支架板内部的弯管,弯管的一侧与出口管导通连接,弯管的另一侧与第二套环导通安装。Preferably, the pipeline device includes an elbow installed inside the longitudinal support plate, one side of the elbow is connected to the outlet pipe, and the other side of the elbow is connected to the second collar.
优选的,动力装置包括固定在L型架一侧的撑杆,撑杆的顶部安装有电机,电机的输出端安装有套环,套环的内部安装有第一转轴,套环与第二套环之间固定有外框架,外框架的内部设置有管路,管路与第二套环相互导通,外框架的底部安装有导管。Preferably, the power device includes a strut fixed on one side of the L-shaped frame, a motor is installed on the top of the strut, a collar is installed at the output end of the motor, a first rotating shaft is installed inside the collar, and the collar is connected to the second sleeve. An outer frame is fixed between the rings, a pipeline is arranged inside the outer frame, the pipeline and the second collar communicate with each other, and a conduit is installed at the bottom of the outer frame.
在上述技术方案的基础上,本发明还提供以下可选技术方案:On the basis of the above technical solutions, the present invention also provides the following optional technical solutions:
优选的,出口装置包括安装在萃取箱体侧边的管道,管道的内部安装有进水孔,管道的表面安装有旋钮,旋钮的内部开设有流通管道,旋钮的另一侧安装有出水管道。Preferably, the outlet device includes a pipe installed on the side of the extraction box, a water inlet hole is installed inside the pipe, a knob is installed on the surface of the pipe, a circulation pipe is opened inside the knob, and a water outlet pipe is installed on the other side of the knob.
相较于现有技术,本发明的有益效果如下:Compared with the prior art, the beneficial effects of the present invention are as follows:
本装置包括:盛放装置,用作为装置提供原料;管路装置,盛放装置与管路装置相互导通,用作反应液的输送;萃取装置,萃取装置与管路装置的尾部相互导通安装,用作对萃取液进行分隔式萃取;动力装置,动力装置安装在萃取装置的表面,用作对萃取过程中中间滚筒的翻滚混合,隔板装置;通过各个装置之间的配合使用实现了当混合液在萃取的过程中可以利用隔板将萃取层与溶剂层隔开,避免了萃取液的污染现象。The device includes: a holding device, which is used as a device to provide raw materials; a pipeline device, where the holding device and the pipeline device communicate with each other and are used for conveying the reaction liquid; an extraction device, where the tail of the extraction device and the pipeline device communicate with each other Installation, used for separation extraction of the extraction liquid; power device, the power device is installed on the surface of the extraction device, used for the tumbling mixing of the intermediate drum during the extraction process, the partition device; through the cooperation between the various devices to achieve when mixing During the extraction process of the liquid, a separator can be used to separate the extraction layer from the solvent layer, so as to avoid the contamination of the extraction liquid.
附图说明Description of drawings
图1为本发明的一个实施例中的机架整体结构示意图。FIG. 1 is a schematic diagram of the overall structure of a rack in an embodiment of the present invention.
图2为本发明的一个实施例中的隔板装置结构示意图。FIG. 2 is a schematic structural diagram of a partition device in an embodiment of the present invention.
图3为本发明的一个实施例中的出水装置结构示意图。FIG. 3 is a schematic structural diagram of a water outlet device in an embodiment of the present invention.
附图标记注释:1L型架、2撑杆、3电机、4第一转轴、5套环、6外框架、7导管、8萃取箱体、9隔板装置、10搅拌浮球、11气缸杆、12气缸、13第二套环、14弯管、15纵向支架板、16气泵、17出口管、18桶体、19待处理液、20隔板、21滑套、22伸缩基座、23伸缩杆、24纱网、25滑块、26布帘、27管道、28进水孔、29旋钮、30流通管道、31出水管道。Reference number notes: 1L frame, 2 struts, 3 motor, 4 first shaft, 5 collar, 6 outer frame, 7 conduit, 8 extraction box, 9 partition device, 10 stirring float, 11 cylinder rod , 12 cylinders, 13 second collars, 14 elbows, 15 longitudinal support plates, 16 air pumps, 17 outlet pipes, 18 barrels, 19 liquid to be treated, 20 partitions, 21 sliding sleeves, 22 telescopic bases, 23 telescopic Rod, 24 gauze, 25 slider, 26 curtain, 27 pipe, 28 water inlet, 29 knob, 30 circulation pipe, 31 water outlet pipe.
具体实施方式Detailed ways
在本发明的描述中,需要理解的是,术语 “上”、“下”、“顶”、“底”、“左”、“右”等指示的方位或位置关系为基于附图所示的方位或位置关系,仅是为了便于描述本发明和简化描述,而不是指示或暗示所指的装置或元件必须具有特定的方位、以特定的方位构造和操作,因此不能理解为对本发明的限制。In the description of the present invention, it should be understood that the orientations or positional relationships indicated by the terms "upper", "lower", "top", "bottom", "left", "right", etc. are based on those shown in the accompanying drawings The orientation or positional relationship is only for the convenience of describing the present invention and simplifying the description, rather than indicating or implying that the referred device or element must have a specific orientation, be constructed and operated in a specific orientation, and therefore should not be construed as a limitation of the present invention.
此外,术语“第一”、“第二”仅用于描述目的,而不能理解为指示或暗示相对重要性或者隐含指明所指示的技术特征的数量。由此,限定有“第一”、“第二”的特征可以明示或者隐含地包括一个或者更多个该特征。在本发明的描述中,“多个”的含义是两个或两个以上,除非另有明确具体的限定。In addition, the terms "first" and "second" are only used for descriptive purposes, and should not be construed as indicating or implying relative importance or implying the number of indicated technical features. Thus, a feature defined as "first" or "second" may expressly or implicitly include one or more of that feature. In the description of the present invention, "plurality" means two or more, unless otherwise expressly and specifically defined.
在本发明中,除非另有明确的规定和限定,术语“安装”、“相连”、“连接”、“固定”等术语应做广义理解,例如,可以是固定连接,也可以是可拆卸连接,或成一体;可以是机械连接,也可以是电连接;可以是直接相连,也可以通过中间媒介间接相连,可以是两个元件内部的连通或两个元件的相互作用关系。对于本领域的普通技术人员而言,可以根据具体情况理解上述术语在本发明中的具体含义。In the present invention, unless otherwise expressly specified and limited, the terms "installed", "connected", "connected", "fixed" and other terms should be understood in a broad sense, for example, it may be a fixed connection or a detachable connection , or integrated; it can be a mechanical connection or an electrical connection; it can be a direct connection or an indirect connection through an intermediate medium, and it can be the internal connection of the two elements or the interaction relationship between the two elements. For those of ordinary skill in the art, the specific meanings of the above terms in the present invention can be understood according to specific situations.
下面结合具体实施方式对本专利的技术方案作进一步详细地说明。The technical solution of the present patent will be described in further detail below in conjunction with specific embodiments.
在一个实施例中,如图1所示,包括L型架1,还包括:In one embodiment, as shown in FIG. 1, it includes an L-shaped frame 1, and also includes:
盛放装置,用作为装置提供原料;A holding device, which is used as a device to provide raw materials;
管路装置,所述盛放装置与管路装置相互导通,用作反应液的输送;The pipeline device, the holding device and the pipeline device are connected to each other, and are used for the transportation of the reaction liquid;
萃取装置,所述萃取装置与管路装置的尾部相互导通安装,用作对萃取液进行分隔式萃取;an extraction device, the extraction device and the tail of the pipeline device are installed in communication with each other, and are used for separate extraction of the extraction liquid;
动力装置,所述动力装置安装在萃取装置的表面,用作对萃取过程中中间滚筒的翻滚混合;a power device, which is installed on the surface of the extraction device and used for tumbling mixing of the intermediate drum during the extraction process;
隔板装置9,所述隔板装置9安装在萃取装置的中间部位内部,用作将萃取完成的萃取液和溶剂分隔开;Separator device 9, the separator device 9 is installed inside the middle part of the extraction device, and is used to separate the extraction liquid and the solvent after the extraction is completed;
采用动力装置控制萃取装置进行旋转,进而实现内部液体的混合,当萃取工作完成以后,利用隔板装置将液面分割开来,进而将生物质从管路装置引出至盛放装置的内部,作为一个实施例,附图中给出的各个部件的左右上下位置只是一种排布方式,具体的位置根据具体需要设定;The power device is used to control the rotation of the extraction device, so as to realize the mixing of the internal liquid. When the extraction work is completed, the liquid level is divided by the baffle device, and the biomass is led out from the pipeline device to the inside of the holding device as a In one embodiment, the left, right, up and down positions of each component given in the accompanying drawings are just an arrangement, and the specific positions are set according to specific needs;
在一个实施例中,如图1所示,该机构可以选择金属桶,塑料桶等桶装结构,具体不限制,在本实施例中,优选的,盛放装置包括固定在L型架1一侧的桶体18,桶体的主要作用是对萃取原液进行收装的装置;桶体18的内部盛放有待处理液19,桶体18的侧壁安装有气泵16,气泵16装置的作用是使得桶体的内部形成正压,进而使得装置内部可以排出反应液,桶体18的内侧安装有出口管17,出口管17的作用是向装置的内部灌注反应液;In one embodiment, as shown in FIG. 1 , the mechanism can choose a barrel structure such as a metal barrel, a plastic barrel, etc., which is not particularly limited. The
在一个实施例中,如图1所示,该机构可以选择软管、钢管等管路结构,具体提不限制,在本实施例中,优选的,管路装置包括安装在纵向支架板15内部的弯管14,弯管14的作用是进行传输;弯管14的一侧与出口管17导通连接,弯管14的另一侧与第二套环13导通安装,套环13可以实现旋转和导通液体,具体可以是密封轴承等等;In one embodiment, as shown in FIG. 1 , the mechanism can select pipeline structures such as hoses, steel pipes, etc., which are not specifically limited. The function of the
在一个实施例中,如图1所示,该机构可以选择电机、转子等旋转装置,具体不限制,在本实施例中,优选的,动力装置包括固定在L型架1一侧的撑杆2,撑杆2的顶部安装有电机3,电机3是主要的动力装置;电机3的输出端安装有套环5,套环5的作用是分割转轴的转动;套环5的内部安装有第一转轴4,套环5与第二套环13之间固定有外框架6,外框架6的内部用于走管路进行液体的流通;外框架6的内部设置有管路,管路与第二套环13相互导通,外框架6的底部安装有导管7;In one embodiment, as shown in FIG. 1 , the mechanism can select a rotating device such as a motor and a rotor, which is not particularly limited. In this embodiment, preferably, the power device includes a strut fixed on one side of the L-shaped frame 1 2. A motor 3 is installed on the top of the
在一个实施例中,如图1所示,该机构可以选择玻璃萃取装置,金属萃取装置,具体不做限制,在本实施例中,优选的,萃取装置包括安装在导管7底部的萃取箱体8,萃取箱体8的内部安装有搅拌浮球10,浮球10的作用是增加混合的程度;萃取箱体8的中间部位安装有隔板装置,萃取箱体8的底部安装有出口装置。In one embodiment, as shown in FIG. 1 , the mechanism can select a glass extraction device or a metal extraction device, which is not specifically limited. In this embodiment, preferably, the extraction device includes an extraction box installed at the bottom of the conduit 7 . 8. A stirring
在一个实施例中,如图2所示,该机构可以选择滤芯,带滤孔的可关闭的面板,具体不做限制,在本实施例中,优选的,隔板装置包括固定在萃取箱体8一侧的气缸12,气缸12是推动装置;气缸12的顶部安装有气缸杆11,气缸杆11的顶部安装有隔板装置9,隔板装置9是将液面进行分隔的主要装置;隔板装置9包括安装在气缸杆11表面的隔板20,隔板20的两侧安装有滑套21,滑套21的作用是保证隔板装置在萃取桶内部的滑动;隔板20的侧边安装有伸缩基座22,伸缩基座22的表面安装有伸缩杆23,伸缩杆23的一侧安装有滑块25,滑块25带动滑块25的一侧安装的布帘26就可以实现隔断液面的效果,隔板20的中间安装有纱网24,纱网24保证了隔板装置在移动的过程中不会受到阻力。In one embodiment, as shown in FIG. 2 , the mechanism can select a filter element and a closable panel with filter holes, which is not specifically limited. 8. The
在一个实施例中,如图3所示,该机构可以选择单向阀,多向阀,螺旋塞等,具体不做限制,在本实施例中,优选的,出口装置包括安装在萃取箱体8侧边的管道27,管道27的内部安装有进水孔28,管道27的表面安装有旋钮29,通过旋钮29可以实现进水孔28、流通管道30以及出水管道31之间的导通出水;旋钮29的内部开设有流通管道30,旋钮29的另一侧安装有出水管道31。In one embodiment, as shown in FIG. 3 , the mechanism can select a one-way valve, a multi-way valve, a screw plug, etc., which is not specifically limited. In this embodiment, preferably, the outlet device includes a device installed in the extraction box. The
以上所述仅为本发明的较佳实施例而已,并不用以限制本发明,凡在本发明的精神和原则之内,所作的任何修改、等同替换、改进等,均应包含在本发明的保护范围之内。不应将权利要求中的任何附图标记视为限制所涉及的权利要求。The above descriptions are only preferred embodiments of the present invention, and are not intended to limit the present invention. Any modification, equivalent replacement, improvement, etc. made within the spirit and principle of the present invention shall be included in the scope of the present invention. within the scope of protection. Any reference signs in the claims shall not be construed as limiting the involved claim.
此外,应当理解,虽然本说明书按照实施方式加以描述,但并非每个实施方式仅包含一个独立的技术方案,说明书的这种叙述方式仅仅是为清楚起见,本领域技术人员应当将说明书作为一个整体,各实施例中的技术方案也可以经适当组合,形成本领域技术人员可以理解的其他实施方式。In addition, it should be understood that although this specification is described in terms of embodiments, not each embodiment only includes an independent technical solution, and this description in the specification is only for the sake of clarity, and those skilled in the art should take the specification as a whole , the technical solutions in each embodiment can also be appropriately combined to form other implementations that can be understood by those skilled in the art.
Claims (5)
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