CN112595696B - In situ characterization method for bonding interface state under irradiation conditions - Google Patents
In situ characterization method for bonding interface state under irradiation conditions Download PDFInfo
- Publication number
- CN112595696B CN112595696B CN202011459774.2A CN202011459774A CN112595696B CN 112595696 B CN112595696 B CN 112595696B CN 202011459774 A CN202011459774 A CN 202011459774A CN 112595696 B CN112595696 B CN 112595696B
- Authority
- CN
- China
- Prior art keywords
- bonding interface
- failure
- laser
- situ
- state
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
- 238000012512 characterization method Methods 0.000 title claims abstract description 27
- 238000011065 in-situ storage Methods 0.000 title claims abstract description 21
- 238000001514 detection method Methods 0.000 claims abstract description 15
- 238000005070 sampling Methods 0.000 claims abstract description 11
- 238000004458 analytical method Methods 0.000 claims abstract description 10
- 238000000034 method Methods 0.000 claims abstract description 10
- 239000000853 adhesive Substances 0.000 claims abstract description 8
- 230000001070 adhesive effect Effects 0.000 claims abstract description 8
- 230000001052 transient effect Effects 0.000 claims description 16
- 230000015556 catabolic process Effects 0.000 claims description 7
- 238000006731 degradation reaction Methods 0.000 claims description 7
- 238000010183 spectrum analysis Methods 0.000 claims description 7
- 238000013178 mathematical model Methods 0.000 claims description 6
- 238000004611 spectroscopical analysis Methods 0.000 claims description 6
- 230000001678 irradiating effect Effects 0.000 claims description 5
- 238000003325 tomography Methods 0.000 claims description 5
- 238000012545 processing Methods 0.000 claims description 3
- 230000005855 radiation Effects 0.000 abstract description 7
- 230000007774 longterm Effects 0.000 abstract description 3
- 238000010249 in-situ analysis Methods 0.000 abstract 1
- 238000011160 research Methods 0.000 description 7
- 230000007547 defect Effects 0.000 description 6
- 238000007689 inspection Methods 0.000 description 5
- 238000005516 engineering process Methods 0.000 description 3
- 239000000463 material Substances 0.000 description 3
- 238000003491 array Methods 0.000 description 2
- 238000005266 casting Methods 0.000 description 2
- 238000013016 damping Methods 0.000 description 2
- 238000006073 displacement reaction Methods 0.000 description 2
- 238000002474 experimental method Methods 0.000 description 2
- 230000008014 freezing Effects 0.000 description 2
- 238000007710 freezing Methods 0.000 description 2
- 239000007787 solid Substances 0.000 description 2
- 238000012546 transfer Methods 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000013461 design Methods 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 230000000704 physical effect Effects 0.000 description 1
- 230000002265 prevention Effects 0.000 description 1
- 239000011253 protective coating Substances 0.000 description 1
- 238000007789 sealing Methods 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
Classifications
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N21/00—Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
- G01N21/62—Systems in which the material investigated is excited whereby it emits light or causes a change in wavelength of the incident light
- G01N21/63—Systems in which the material investigated is excited whereby it emits light or causes a change in wavelength of the incident light optically excited
Landscapes
- Health & Medical Sciences (AREA)
- Nuclear Medicine, Radiotherapy & Molecular Imaging (AREA)
- Physics & Mathematics (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Analytical Chemistry (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- General Physics & Mathematics (AREA)
- Immunology (AREA)
- Pathology (AREA)
- Investigating Or Analyzing Materials By The Use Of Ultrasonic Waves (AREA)
- Analysing Materials By The Use Of Radiation (AREA)
Abstract
本发明涉及粘接界面状态的原位表征方法，具体涉及一种辐照条件下粘接界面状态的原位表征方法。本发明的目的是解决现有方法中存采用射线探伤方法时，依赖辐射源等大型专用设备，服役现场的展开受到空间限制，使用便利性不足，采用超声探伤方法时，辐照条件下对人员防护要求高且难以满足长期使用的要求，采用结构动力学分析时，传感器及其粘贴用胶粘剂的辐射耐受性需专门研究的技术问题，提供一种辐照条件下粘接界面状态的原位表征方法。该方法以涉及辐照条件的核电设备等为主要应用对象，通过粘接界面取样、典型状态的标定、服役现场非接触原位检测等步骤，实现了非接触、无人化、简单、安全可靠、及时的粘接界面状态表征。The invention relates to an in-situ characterization method for bonding interface states, in particular to an in-situ characterization method for bonding interface states under irradiation conditions. The purpose of the present invention is to solve the problem that when the radiographic flaw detection method is adopted in the existing method, the large-scale special equipment such as radiation source is relied on, the deployment of the service site is limited by space, and the convenience of use is insufficient. The protection requirements are high and it is difficult to meet the requirements of long-term use. When structural dynamics analysis is used, the radiation resistance of the sensor and its adhesive adhesive needs to be specially studied. Provide an in-situ analysis of the bonding interface state under irradiation conditions. Characterization method. The method takes nuclear power equipment involving irradiation conditions as the main application object, and realizes non-contact, unmanned, simple, safe and reliable through the steps of bonding interface sampling, calibration of typical state, and non-contact in-situ detection at the service site. , Timely characterization of bonding interface state.
Description
Technical Field
The invention relates to an in-situ characterization method of a bonding interface state, in particular to an in-situ characterization method of a bonding interface state under an irradiation condition.
Background
The bonding structure is formed by bonding different materials, and can simultaneously realize the functions of bearing, sealing, heat prevention and the like in the field of engineering structures. Due to the discontinuous characteristic of the geometric configuration and the strong discontinuity property of the physical property, the bonding interface has the defects of high mechanical stress, microcrack of the bonding interface and the like.
For the bonding interface of nuclear power pipeline structure and protective coating, the generation of defects such as microcracks can cause the deviation of service state and design state, and seriously affect the service reliability, so the in-situ characterization of the bonding interface state under the irradiation condition becomes the basic requirement for carrying out integrity analysis and avoiding structural failure.
The existing in-situ characterization method for the bonding interface state mainly comprises three methods, namely ray inspection, ultrasonic inspection and structural dynamics analysis.
And (3) ray flaw detection: the method is characterized in that the bonding interface between a lining layer of the casting type solid engine and a grain is researched by adopting a ray tomography technology, and the difference of the bonding interface state before and after a freezing experiment and defect identification are analyzed. The defects are that radiographic inspection depends on large-scale special equipment such as a radiation source, the expansion of a service site is limited by space, and the use convenience is insufficient.
Ultrasonic flaw detection: a reference block is designed, and the non-ideal condition of the CuW/Cu (CrCu) joint surface of the contact is researched by utilizing ultrasonic flaw detection. The ultrasonic flaw detection method has the defects that the ultrasonic flaw detection is mainly carried out by hand, the requirement on personnel protection under the irradiation condition is high, and the requirement on long-term use is difficult to meet.
Structural dynamics analysis: based on the structural dynamics characteristics such as natural frequency, damping ratio and the like, the correlation between the bonding interface state of the concrete material and the coarse aggregate and the transfer function of the concrete structure is researched. The method has the disadvantages that a structural dynamics analysis method needs to stick a sensor array such as a displacement sensor or a strain sensor near a bonding interface, and the radiation tolerance of the sensor and an adhesive for sticking the sensor needs to be specially researched.
Disclosure of Invention
The invention aims to solve the problems that when the existing in-situ characterization method of the bonding interface state under the irradiation condition adopts a ray inspection method, the expansion of a service site is limited by space and the use convenience is insufficient due to the dependence on large-scale special equipment such as a radiation source and the like; when the ultrasonic flaw detection method is adopted, the requirement on personnel protection under the irradiation condition is high and the requirement on long-term use is difficult to meet; when structural dynamics analysis is adopted, the technical problem that the radiation tolerance of the sensor and the adhesive for sticking the sensor needs special research is solved, and an in-situ characterization method of the state of a sticking interface under an irradiation condition is provided.
In order to solve the technical problems, the technical solution provided by the invention is as follows:
an in-situ characterization method for the bonding interface state under irradiation condition is characterized by comprising the following steps:
1) adhesive interface sampling
Cutting and sampling the typical state part of the irradiated real component bonding interface according to the irradiation failure mechanism and the degradation rule of the target bonding interface, preparing the table and certificate in the typical state by using the sampled product, recording the number of the table and certificate as n, numbering each piece as 1, 2 and … n, wherein n is more than or equal to 3;
2) calibrating a typical state
2.1) Signal analysis based on laser-induced transient Grating Spectroscopy
Irradiating the surface certificate 1 prepared in the step 1) by using the laser-induced transient grating, obtaining a spectrogram of the surface certificate 1 by using spectral analysis equipment, carrying out non-contact pickup on characteristic signals in the spectrogram, marking characteristic signal data in a typical state as DI-1, and marking laser parameters used by the laser-induced transient grating as PaI;
2.2) defining failure classes
2.2.1) scanning and three-dimensional reconstruction of the bonding interface of the surface certificate 1 by adopting a micro-focus tomography device, marking the reconstructed bonding interface with a state according to a target bonding interface irradiation failure mechanism and a degradation rule, and defining the failure grade as Da-1;
2.2.2) the same way as in step 2.1), step 2.2.1) is used to traverse the remaining table certificates, marking the typical state signature data as DI-i (i ═ 2, 3, … n), corresponding to the definition of a failure level Da-i (i ═ 2, 3, … n);
2.2.3) fitting all failure levels Da-i and typical state characteristic signal data DI-i, and establishing a correlation mathematical model M;
3) non-contact in-situ detection of service site
3.1) laser-induced transient Grating Spectroscopy characterizing A target
After the laser induced transient grating is set by the laser parameter PaI marked in the step 2.1), irradiating the characterization target, obtaining a spectrogram of the characterization target by using a spectrum analysis device, carrying out non-contact pickup on a characteristic signal in the spectrogram, and marking the characteristic signal data as DTest-1;
3.2) feature Signal processing
And (3) obtaining a failure grade representing a target by using the correlation mathematical model M obtained in the step 2.2.3) and taking the characteristic signal data DTest-1 as input.
Further, in step 1), the irradiation failure mechanism is the only failure mode introduced in the sampling process.
Further, in the step 1), n is more than or equal to 5.
Compared with the prior art, the invention has the following beneficial effects:
1. the in-situ characterization method for the bonding interface state under the irradiation condition provided by the invention takes nuclear power equipment and the like related to the irradiation condition as main application objects, and realizes non-contact, unmanned, simple, safe, reliable and timely bonding interface state characterization through the steps of bonding interface sampling, typical state calibration, service field non-contact in-situ detection and the like.
2. Compared with a radiographic inspection method which adopts a radiographic tomography technology to research the bonding interface between the lining layer of the casting type solid engine and the grain and analyzes the difference of the states of the bonding interface before and after a freezing experiment and defect identification, the characterization method provided by the invention does not need to rely on other large-scale special equipment, and is convenient to implement.
3. Compared with the ultrasonic flaw detection which utilizes the ultrasonic flaw detection to research the non-ideal condition of the CuW/Cu (CrCu) joint surface of the contact of the reference block, the ultrasonic flaw detection does not need to be carried out by hands.
4. Compared with structural dynamics analysis of the correlation between the state of the bonding interface of the concrete material and the coarse aggregate and the transfer function of the concrete structure from the aspects of structural dynamics such as natural frequency, damping ratio and the like, the characterization method is simpler, and special research on the radiation tolerance of sensor arrays such as a displacement sensor or a strain sensor and the like adhered to the vicinity of the bonding interface and the adhesive for adhering the sensor arrays is not needed.
Detailed Description
The present invention will be further described with reference to the following examples.
An in-situ characterization method of a bonding interface state under an irradiation condition comprises the following steps:
1) adhesive interface sampling
According to the research conclusion of the irradiation failure mechanism, the degradation rule and the like of the target bonding interface, cutting and sampling are carried out on the typical state part of the irradiated real component bonding interface, the table certificate in the typical state is prepared by using the sampled product, other failure modes except the irradiation failure mechanism cannot be introduced in the sampling process, the number of the table certificate is recorded as n, the number of each table certificate is 1, 2 and … n, wherein n is more than or equal to 3, and preferably n is more than or equal to 5;
2) calibrating a typical state
2.1) Signal analysis based on laser-induced transient Grating Spectroscopy
Irradiating the surface certificate 1 prepared in the step 1) by using the laser-induced transient grating, obtaining a spectrogram of the surface certificate 1 by using spectral analysis equipment, carrying out non-contact pickup on characteristic signals in the spectrogram, marking characteristic signal data in a typical state as DI-1, and marking laser parameters used by the laser-induced transient grating as PaI;
2.2) defining failure classes
2.2.1) scanning and three-dimensional reconstruction of the bonding interface of the surface certificate 1 by adopting a micro-focus tomography device, carrying out state marking on the reconstructed bonding interface according to research conclusions such as a target bonding interface irradiation failure mechanism, a degradation rule and the like, and defining the failure grade as Da-1;
2.2.2) the same way as in step 2.1), step 2.2.1) is used to traverse the remaining table certificates, marking the typical state signature data as DI-i (i ═ 2, 3, … n), corresponding to the definition of a failure level Da-i (i ═ 2, 3, … n);
2.2.3) fitting all failure levels Da-i and typical state characteristic signal data DI-i, and establishing a correlation mathematical model M;
3) non-contact in-situ detection of service site
3.1) laser-induced transient Grating Spectroscopy characterizing A target
After the laser induced transient grating is set by the laser parameter PaI marked in the step 2.1), the characterization target is irradiated, a spectrogram of the characterization target is obtained by using a spectrum analysis device, a characteristic signal in the spectrogram is picked up in a non-contact mode, and characteristic signal data is marked as DTest-1.
3.2) feature Signal processing
And (3) obtaining a failure grade representing a target by using the correlation mathematical model M obtained in the step 2.2.3) and taking the characteristic signal data DTest-1 as input.
The laser-induced transient grating and the spectral analysis equipment related to the steps belong to general technologies and equipment, and research conclusions such as target bonding interface irradiation failure mechanism, degradation rule and the like belong to the existing industry knowledge and are executed according to general technical specifications and technical requirements for representing targets.
Finally, it should be noted that: the above embodiments are only used for illustrating the technical solutions of the present invention, and not for limiting the same, and it is obvious for a person skilled in the art to modify the specific technical solutions described in the foregoing embodiments or to substitute part of the technical features, and these modifications or substitutions do not make the essence of the corresponding technical solutions depart from the scope of the technical solutions protected by the present invention.
Claims (3)
1. An in-situ characterization method for a bonding interface state under an irradiation condition is characterized by comprising the following steps:
1) adhesive interface sampling
Cutting and sampling the typical state part of the irradiated real component bonding interface according to the irradiation failure mechanism and the degradation rule of the target bonding interface, preparing the table and certificate in the typical state by using the sampled product, recording the number of the table and certificate as n, numbering each piece as 1, 2 and … n, wherein n is more than or equal to 3;
2) calibrating a typical state
2.1) Signal analysis based on laser-induced transient Grating Spectroscopy
Irradiating the surface certificate 1 prepared in the step 1) by using the laser-induced transient grating, obtaining a spectrogram of the surface certificate 1 by using spectral analysis equipment, carrying out non-contact pickup on characteristic signals in the spectrogram, marking characteristic signal data in a typical state as DI-1, and marking laser parameters used by the laser-induced transient grating as PaI;
2.2) defining failure classes
2.2.1) scanning and three-dimensional reconstruction of the bonding interface of the surface certificate 1 by adopting a micro-focus tomography device, marking the reconstructed bonding interface with a state according to a target bonding interface irradiation failure mechanism and a degradation rule, and defining the failure grade as Da-1;
2.2.2) the same way as in step 2.1), step 2.2.1) is used to traverse the remaining table certificates, marking the typical state signature data as DI-i (i ═ 2, 3, … n), corresponding to the definition of a failure level Da-i (i ═ 2, 3, … n);
2.2.3) fitting all failure levels Da-i and typical state characteristic signal data DI-i, and establishing a correlation mathematical model M;
3) non-contact in-situ detection of service site
3.1) laser-induced transient Grating Spectroscopy characterizing A target
After the laser induced transient grating is set by the laser parameter PaI marked in the step 2.1), irradiating the characterization target, obtaining a spectrogram of the characterization target by using a spectrum analysis device, carrying out non-contact pickup on a characteristic signal in the spectrogram, and marking the characteristic signal data as DTest-1;
3.2) feature Signal processing
And (3) obtaining a failure grade representing a target by using the correlation mathematical model M obtained in the step 2.2.3) and taking the characteristic signal data DTest-1 as input.
2. The in-situ characterization method of the bonding interface state under irradiation condition according to claim 1, characterized in that: in the step 1), the irradiation failure mechanism is the only failure mode introduced in the sampling process.
3. The in-situ characterization method of the bonding interface state under irradiation condition according to claim 2, characterized in that: in the step 1), n is more than or equal to 5.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202011459774.2A CN112595696B (en) | 2020-12-11 | 2020-12-11 | In situ characterization method for bonding interface state under irradiation conditions |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202011459774.2A CN112595696B (en) | 2020-12-11 | 2020-12-11 | In situ characterization method for bonding interface state under irradiation conditions |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN112595696A CN112595696A (en) | 2021-04-02 |
| CN112595696B true CN112595696B (en) | 2021-10-15 |
Family
ID=75192557
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202011459774.2A Active CN112595696B (en) | 2020-12-11 | 2020-12-11 | In situ characterization method for bonding interface state under irradiation conditions |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN112595696B (en) |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101221133A (en) * | 2008-01-25 | 2008-07-16 | 天津商业大学 | Honeycomb paperboard bonding defect detection method and detection system |
| CN106338486A (en) * | 2015-09-02 | 2017-01-18 | 湖北航天化学技术研究所 | Non-destructive detection method of storage ageing performance of propellant/liner bonding interface |
| CN109239024A (en) * | 2018-09-05 | 2019-01-18 | 国网河北省电力有限公司电力科学研究院 | Composite insulator Aging level evaluation method and system |
| CN109696457A (en) * | 2019-01-10 | 2019-04-30 | 华南理工大学 | Active infrared thermal wave detection method and system towards the damage of glass curtain wall cementing structure |
Family Cites Families (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2006524813A (en) * | 2003-04-16 | 2006-11-02 | コーニンクレッカ フィリップス エレクトロニクス エヌ ヴィ | Thin film evaluation method |
| CA2651341C (en) * | 2006-05-10 | 2017-01-24 | National Research Council Of Canada | Method of assessing bond integrity in bonded structures |
-
2020
- 2020-12-11 CN CN202011459774.2A patent/CN112595696B/en active Active
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101221133A (en) * | 2008-01-25 | 2008-07-16 | 天津商业大学 | Honeycomb paperboard bonding defect detection method and detection system |
| CN106338486A (en) * | 2015-09-02 | 2017-01-18 | 湖北航天化学技术研究所 | Non-destructive detection method of storage ageing performance of propellant/liner bonding interface |
| CN109239024A (en) * | 2018-09-05 | 2019-01-18 | 国网河北省电力有限公司电力科学研究院 | Composite insulator Aging level evaluation method and system |
| CN109696457A (en) * | 2019-01-10 | 2019-04-30 | 华南理工大学 | Active infrared thermal wave detection method and system towards the damage of glass curtain wall cementing structure |
Non-Patent Citations (1)
| Title |
|---|
| 激光诱导超声表面波的实验研究;林中亚 等;《科技创新导报》;20151231;第26卷;第28-30页 * |
Also Published As
| Publication number | Publication date |
|---|---|
| CN112595696A (en) | 2021-04-02 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| Ciang et al. | Structural health monitoring for a wind turbine system: a review of damage detection methods | |
| Balayssac et al. | Non-destructive testing and evaluation of civil engineering structures | |
| Habib et al. | Structural health monitoring of bonded composite repairs–A critical comparison between ultrasonic Lamb wave approach and surface mounted crack sensor approach | |
| Raišutis et al. | The review of non-destructive testing techniques suitable for inspection of the wind turbine blades | |
| Palumbo et al. | Ultrasonic analysis and lock-in thermography for debonding evaluation of composite adhesive joints | |
| Eaton et al. | Acoustic emission source location in composite materials using Delta T Mapping | |
| Kim et al. | Performance assessment method for crack repair in concrete using PZT-based electromechanical impedance technique | |
| Banerjee et al. | A wave propagation and vibration-based approach for damage identification in structural components | |
| Diamanti et al. | Piezoelectric transducer arrangement for the inspection of large composite structures | |
| Aryan et al. | A model‐based method for damage detection with guided waves | |
| Aminzadeh et al. | Non-contact inspection methods for wind turbine blade maintenance: techno–economic review of techniques for integration with industry 4.0 | |
| Xu et al. | Identifying technology for structural damage based on the impedance analysis of piezoelectric sensor | |
| Waugh | Development of infrared techniques for practical defect identification in bonded joints | |
| Bossi et al. | Nondestructive testing of aerospace composites | |
| Lee et al. | Characterization of micro-crack propagation through analysis of edge effect in acoustic microimaging of microelectronic packages | |
| Montinaro et al. | A numerical and experimental study through laser thermography for defect detection on metal additive manufactured parts | |
| Malekimoghadam et al. | A critical review on the structural health monitoring methods of the composite wind turbine blades | |
| Liu et al. | Influence of different ultrasonic transducers on the precision of fastening force measurement | |
| Sun et al. | Non-contact detection of delamination in layered anisotropic composite materials with ultrasonic waves generated and detected by lasers | |
| CN112595696B (en) | In situ characterization method for bonding interface state under irradiation conditions | |
| Song et al. | Application of the piezoelectric materials for health monitoring in civil engineering: an overview | |
| Jeong et al. | Investitation of mobile ultrasonic propagation imager as a tool for composite wind blade quality control | |
| Kim et al. | Imaging defects in laminate composite plates using focused shear waves generated by air-coupled transducer | |
| Wang et al. | Novel damage detection techniques for structural health monitoring using a hybrid sensor | |
| Pau et al. | Simultaneous subsurface defect detection and contact parameter assessment in a wheel–rail system |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| GR01 | Patent grant | ||
| GR01 | Patent grant |