CN111929119A - Combustion particulate matter collection and flue gas composition testing device in low pressure environment - Google Patents
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- 238000012360 testing method Methods 0.000 title claims abstract description 32
- 238000002485 combustion reaction Methods 0.000 title claims abstract description 30
- 239000013618 particulate matter Substances 0.000 title claims abstract description 14
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 title abstract description 28
- 239000003546 flue gas Substances 0.000 title abstract description 28
- 239000000203 mixture Substances 0.000 title abstract description 9
- 239000002245 particle Substances 0.000 claims abstract description 12
- 239000000779 smoke Substances 0.000 claims description 9
- 239000000470 constituent Substances 0.000 claims 3
- 239000007789 gas Substances 0.000 abstract description 63
- 238000004458 analytical method Methods 0.000 abstract description 12
- 239000004071 soot Substances 0.000 abstract description 5
- 239000000463 material Substances 0.000 description 10
- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 description 4
- 238000000034 method Methods 0.000 description 4
- 238000004140 cleaning Methods 0.000 description 3
- 230000001988 toxicity Effects 0.000 description 3
- 231100000419 toxicity Toxicity 0.000 description 3
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Abstract
本发明提供了一种低压环境下燃烧颗粒物收集及烟气成分测试装置,包括文氏管道、第一通道、第二通道和第三通道,文氏管道一端为第一进气口;第一通道一端与所述文氏管道的另一端连通,第一通道的另一端为第一出气口,第一通道在第一出气口外接热释放速率测试仪;第二通道两端之间与第一通道连通,第二通道的一端设有气体推进器,第二通道的另一端为第二出气口,第二通道在第二出气口外接气相色谱仪,第二通道连接气瓶和泄压口;第三通道一端与文氏管道连通,第三通道另一端为第二进气口,第三通道内设有多层可拆卸滤网。本发明解决了低压环境下燃烧产生的烟尘颗粒的收集、热值测试以及气体成分分析的问题。
The invention provides a device for collecting combustion particulate matter and testing flue gas components in a low-pressure environment, comprising a venturi pipe, a first channel, a second channel and a third channel. One end of the venturi pipe is a first air inlet; the first channel One end is communicated with the other end of the venturi pipe, the other end of the first channel is a first air outlet, and the first channel is connected to an external heat release rate tester at the first air outlet; One end of the second channel is provided with a gas thruster, the other end of the second channel is a second gas outlet, the second channel is connected to a gas chromatograph at the second gas outlet, and the second channel is connected to the gas cylinder and the pressure relief port; One end of the three passages is communicated with the venturi pipe, the other end of the third passage is a second air inlet, and a multi-layer detachable filter screen is arranged in the third passage. The invention solves the problems of collection, calorific value testing and gas composition analysis of soot particles produced by combustion in a low-pressure environment.
Description
技术领域technical field
本发明涉及航空材料燃烧颗粒物收集及烟气成分测试技术领域,尤其涉及一种低压环境下燃烧颗粒物收集及烟气成分测试装置。The invention relates to the technical field of aviation material combustion particulate matter collection and flue gas composition testing, in particular to a combustion particulate matter collection and flue gas composition testing device in a low-pressure environment.
背景技术Background technique
近年来,民用航空需求量增多,航空产业蓬勃发展,不断有新材料被使用在飞机制造上,这些新材料往往具有更加优异的特点,质量更轻,耐久度更持久,价格也更加合理,但与此同时其安全性也显得更加重要。考虑到民航客机巡航高度一般位于海拔8400km至12500km之间,海拔每升高9m,大气压强降低100Pa,客机飞行过程中长期处于低压环境,一旦发生热失控燃烧事件,那么新材料在低压环境下经过燃烧后产生烟气的毒害性也成为其能否被广泛应用的考虑因素。不同环境压力下,材料燃烧产物不同,其毒害性也不同,如果新材料燃烧后烟气的危害性对人体影响较大,那么在制造过程中对其使用范围会有所保留,甚至可能拒绝使用。所以对于航空材料燃烧后的烟气收集以及毒性分析就显得尤为重要。一般的烟气收集系统都在常压范围下运行,对于烟气中的颗粒物和气体并没有明显区分。考虑到民航领域的实际情况,于是设计一种针对低压环境下航空材料燃烧后的烟气收集分析系统就显得尤为重要。In recent years, the demand for civil aviation has increased, the aviation industry has flourished, and new materials have been used in aircraft manufacturing. These new materials often have more excellent characteristics, lighter weight, longer durability, and more reasonable prices, but At the same time, its security is also more important. Considering that the cruising altitude of civil aviation passenger aircraft is generally between 8400km and 12500km above sea level, the atmospheric pressure decreases by 100Pa for every 9m increase in altitude, and the passenger aircraft is in a low-pressure environment for a long time during the flight. The toxicity of the flue gas generated after combustion has also become a consideration factor for its wide application. Under different environmental pressures, the combustion products of materials are different, and their toxicity is also different. If the harmfulness of the flue gas after the combustion of the new material has a greater impact on the human body, the scope of its use will be reserved during the manufacturing process, and it may even be refused to use. . Therefore, it is particularly important for the collection of flue gas and toxicity analysis of aviation materials after combustion. General flue gas collection systems operate in the normal pressure range, and there is no obvious distinction between particulate matter and gas in flue gas. Taking into account the actual situation in the civil aviation field, it is particularly important to design a flue gas collection and analysis system for the combustion of aviation materials in a low-pressure environment.
发明内容SUMMARY OF THE INVENTION
本发明旨在解决低压条件下燃烧物烟颗粒收集及烟气在线采集及分析问题。飞机在运行环境中,舱内与舱外实际上都处于低压状态,舱内或舱外起火对机组人员、乘客的生命安全有着极大的威胁,为此需要研究低压下物质燃烧的燃烧特性,为航空材料的设计、制备及选择,以及航空应急处置能力的提高提供保障。The invention aims to solve the problems of the collection of the smoke particles of the combustion material and the on-line collection and analysis of the flue gas under the condition of low pressure. In the operating environment of the aircraft, both inside and outside the cabin are actually in a low pressure state. A fire inside or outside the cabin poses a great threat to the life safety of the crew and passengers. Therefore, it is necessary to study the combustion characteristics of material combustion under low pressure. Provide guarantee for the design, preparation and selection of aviation materials, as well as the improvement of aviation emergency response capabilities.
现有实验手段及分析技术,对于低压条件下烟气成分的测试主要是借助于烟气分析仪,而这种测试手段所测气体组分、精度都相对有限,实时检测效果较差,而且难以直接应用到低压环境中进行样品采集和分析。而具备在线高精度测试功能的色谱,目前还难以直接用于低压下烟气成分的测试。此外,对于低压下燃烧产生的颗粒物,目前还缺乏有效的收集手段,而本发明在文丘里原理上创新提出的方案,可在不影响燃烧物气体排放及热值测试的基础上,在线采集样品燃烧产生的颗粒物。而且本发明还可通过简单拆卸取样,将收集到的颗粒物进行分析测试。气体测试方面,本发明通过物理推进器对采集到的气体进行加压,从而满足色谱测试要求,实现气体的在线高精度实时采集分析。Existing experimental methods and analysis techniques mainly rely on flue gas analyzers to test flue gas components under low pressure conditions. However, the gas components and accuracy measured by this test method are relatively limited, the real-time detection effect is poor, and it is difficult to Direct application to low pressure environments for sample collection and analysis. However, chromatography with on-line high-precision testing is still difficult to directly use for the testing of flue gas components under low pressure. In addition, there is currently no effective collection method for the particulate matter produced by combustion under low pressure, and the solution proposed in the present invention based on the Venturi principle can collect samples online without affecting the gas emission and calorific value test of the combustion product. Particulate matter from combustion. Moreover, the present invention can also analyze and test the collected particles by simply disassembling and sampling. In terms of gas testing, the present invention pressurizes the collected gas through a physical thruster, thereby meeting the requirements of chromatographic testing and realizing online high-precision real-time gas collection and analysis.
本发明提供一种低压环境下燃烧颗粒物收集及烟气成分测试装置,以解决低压环境下燃烧产生的烟尘颗粒的收集、热值测试以及气体成分分析的问题。The invention provides a device for collecting combustion particulate matter and testing flue gas components in a low-pressure environment, so as to solve the problems of collecting, calorific value testing and gas component analysis of soot particles generated by combustion in a low-pressure environment.
为实现上述目的,本发明提供的低压环境下燃烧颗粒物收集及烟气成分测试装置,包括:In order to achieve the above purpose, the device for collecting combustion particulate matter and flue gas composition testing provided by the present invention in a low-pressure environment includes:
文氏管道,其一端为第一进气口;Venturi pipe, one end of which is the first air inlet;
第一通道,其一端与所述文氏管道的另一端连通,所述第一通道的另一端为第一出气口,所述第一通道在第一出气口外接热释放速率测试仪;a first channel, one end of which is communicated with the other end of the venturi pipe, the other end of the first channel is a first air outlet, and the first channel is connected to a heat release rate tester at the first air outlet;
第二通道,其两端之间与所述第一通道连通,所述第二通道的一端设有气体推进器,所述第二通道的另一端为第二出气口,所述第二通道在第二出气口外接气相色谱仪,所述第二通道连接气瓶和泄压口;The second channel is in communication with the first channel between its two ends, one end of the second channel is provided with a gas propeller, the other end of the second channel is a second gas outlet, and the second channel is located at the end of the second channel. The second gas outlet is connected to a gas chromatograph, and the second channel is connected to the gas cylinder and the pressure relief port;
第三通道,其一端与所述文氏管道连通,所述第三通道另一端为第二进气口,所述第三通道内设有多层可拆卸滤网。One end of the third channel is communicated with the venturi pipe, the other end of the third channel is a second air inlet, and a multi-layer detachable filter screen is arranged in the third channel.
进一步地,所述第一通道在文氏管道与第二通道之间设有多层滤网。Further, the first channel is provided with a multi-layer filter screen between the venturi conduit and the second channel.
进一步地,所述第一通道与第二通道通过管道连通,且在管道上设有第四阀门。Further, the first channel is communicated with the second channel through a pipeline, and a fourth valve is provided on the pipeline.
进一步地,所述第一通道在第一出气口处设有第七阀门。Further, the first passage is provided with a seventh valve at the first air outlet.
进一步地,所述第二通道在第二出气口处设有第八阀门。Further, the second passage is provided with an eighth valve at the second air outlet.
进一步地,所述第二通道与气瓶之间设有第五阀门;所述第二通道在泄压口处设有第六阀门。Further, a fifth valve is arranged between the second passage and the gas cylinder; and a sixth valve is arranged at the pressure relief port of the second passage.
进一步地,所述文氏管道在第一进气口处设有第一阀门。Further, the venturi pipeline is provided with a first valve at the first air inlet.
进一步地,所述第三通道在第二进气口处设有第三阀门;所述第三通道在多层可拆卸滤网与文氏管道之间设有第二阀门。Further, the third passage is provided with a third valve at the second air inlet; the third passage is provided with a second valve between the multi-layer detachable filter screen and the venturi pipe.
进一步地,所述多层可拆卸滤网为三层可拆卸滤网。Further, the multi-layer removable filter screen is a three-layer removable filter screen.
进一步地,所述多层可拆卸滤网的筛孔直径为0.500~4.000mm。Further, the mesh diameter of the multi-layer detachable filter screen is 0.500-4.000 mm.
与相关技术相比较,本发明提供的一种低压环境下燃烧颗粒物收集及烟气成分测试装置具有如下有益效果:Compared with the related art, a device for collecting combustion particulate matter and testing flue gas components in a low-pressure environment provided by the present invention has the following beneficial effects:
本发明使用气瓶、泄压口洗气、抽真空对烟气进行处理,使用文氏管道、多层滤网吸入并收集烟气,使用气体推进器将气体推进到气相色谱仪,可以测试低压环境下燃烧热释放速率,以及利用色谱更加精确的分析气体组成成分,并能够收集更加干净的样本气体和烟尘颗粒,解决了目前烟气测试装置无法在低压环境下对烟气进行测试以及样本气体和烟尘颗粒收集纯度不够的问题,并且能够根据需要同时或单独对燃烧产生的气体进行热释放速率测试、成分采集分析以及烟尘颗粒的采集,同时,烟尘颗粒采集使用三层可拆卸滤网,可根据需求,使用不同孔径的滤网。该烟气收集及测试装置结构简单、成本较低,实际操作中,能够更方便的对烟气进行采集和分析,适用于与燃烧特性分析相关的科研部门、高等院校和企业进行测定。The invention uses gas cylinders, pressure relief ports to wash the gas, and vacuumizes the flue gas, uses the Venturi pipe and the multi-layer filter screen to inhale and collect the flue gas, uses the gas thruster to push the gas to the gas chromatograph, and can test the low pressure The combustion heat release rate in the environment, and the use of chromatography to analyze the gas composition more accurately, and to collect cleaner sample gas and soot particles, solve the problem that the current flue gas testing device cannot test the flue gas and sample gas in a low-pressure environment. The problem of insufficient collection purity of smoke and dust particles, and the heat release rate test, component collection and analysis, and collection of smoke and dust particles can be performed simultaneously or separately on the gas generated by combustion as required. Use filters with different apertures according to your needs. The flue gas collection and testing device is simple in structure and low in cost. In actual operation, the flue gas can be collected and analyzed more conveniently, and it is suitable for measurement in scientific research departments, universities and enterprises related to combustion characteristic analysis.
附图说明Description of drawings
图1为本发明提供的一种低压环境下燃烧颗粒物收集及烟气成分测试装置的结构示意图;1 is a schematic structural diagram of a device for collecting combustion particulate matter and flue gas composition testing in a low-pressure environment provided by the present invention;
图2为本发明提供的一种低压环境下燃烧颗粒物收集及烟气成分测试装置的可拆卸滤网示意图。FIG. 2 is a schematic diagram of a removable filter screen of a device for collecting combustion particulate matter and testing flue gas components in a low-pressure environment provided by the present invention.
图1标号:1-文氏管道;2-第一通道;3-第二通道;4-第三通道;5-第一进气口;6-第一出气口;7-第二进气口;8-第二出气口;9-多层可拆卸滤网;10-多层滤网;11-气体推进器;12-气瓶;13-泄压口;14-第一阀门;15-第二阀门;16-第三阀门;17-第四阀门;18-第五阀门;19-第六阀门;20-第七阀门;21-第八阀门。1 - Venturi pipe; 2 - first channel; 3 - second channel; 4 - third channel; 5 - first air inlet; 6 - first air outlet; 7 - second air inlet ;8-Second air outlet;9-Multilayer detachable filter; 10-Multilayer filter;11-Gas propeller; 12-Gas cylinder; 13-Pressure relief port; 14-First valve; 15-No. Two valves; 16-third valve; 17-fourth valve; 18-fifth valve; 19-sixth valve; 20-seventh valve; 21-eighth valve.
具体实施方式Detailed ways
为使本发明实施例的目的、技术方案和优点更加清楚,下面将结合本发明实施例中的附图,对本发明实施例中的技术方案进行清楚、完整地描述,显然,所描述的实施例是本发明一部分实施例,而不是全部的实施例。基于本发明中的实施例,本领域普通技术人员在没有作出创造性劳动前提下所获得的所有其他实施例,都属于本发明保护的范围。In order to make the purposes, technical solutions and advantages of the embodiments of the present invention clearer, the technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the accompanying drawings in the embodiments of the present invention. Obviously, the described embodiments These are some embodiments of the present invention, but not all embodiments. Based on the embodiments of the present invention, all other embodiments obtained by those of ordinary skill in the art without creative efforts shall fall within the protection scope of the present invention.
如图1-2所示,本发明提供了一种低压环境下燃烧颗粒物收集及烟气成分测试装置,包括文氏管道1、第一通道2、第二通道3、第三通道4、第一进气口5、第一出气口6、第二进气口7、第二出气口8、多层可拆卸滤网9、多层滤网10、气体推进器11、气瓶12、泄压口13、第一阀门14、第二阀门15、第三阀门16、第四阀门17、第五阀门18、第六阀门19、第七阀门20和第八阀门21;文氏管道1一端为第一进气口5;第一通道2一端与文氏管道1的另一端连通,第一通道2的另一端为第一出气口6,第一出气口6外接热释放速率测试仪;第二通道3两端之间与第一通道2连通,第二通道3的一端设有气体推进器11,第二通道3的另一端为第二出气口8,第二通道3在第二出气口8外接气相色谱仪,第二通道3连接气瓶12和泄压口13;第三通道4一端与文氏管道1连通,第三通道4另一端为第二进气口7,第三通道4内设有多层可拆卸滤网9。As shown in Figures 1-2, the present invention provides a device for collecting combustion particulate matter and testing flue gas components in a low-pressure environment, including a
第一通道2在文氏管道1与第二通道3之间设有多层滤网10;第一通道2与第二通道3通过管道连通,且在管道上设有第四阀门17;第一通道2在第一出气口6处设有第七阀门20;第二通道3在第二出气口8处设有第八阀门21;第二通道3与气瓶12之间设有第五阀门18;第二通道3在泄压口13处设有第六阀门19;文氏管道1在第一进气口5处设有第一阀门14;第三通道4在第二进气口7处设有第三阀门16;第三通道4在多层可拆卸滤网9与文氏管道1之间设有第二阀门15;多层可拆卸滤网9为三层可拆卸滤网。The
工作时,使用该烟气收集及测试装置进行热释放速率测试、烟尘颗粒收集、气相色谱分析,第一阀门14、第三阀门16、第七阀门20以及第八阀门21关闭,第二阀门15、第四阀门17打开,连通文氏管道1、第一通道2、第二通道3以及第三通道4,缓慢打开第五阀门18,气瓶12中气体进入文氏管道1、第一通道2、第二通道3以及第三通道4,气体进入量达到洗气要求后,关闭第五阀门18,打开第六阀门19,通过泄压口13进行泄压,对文氏管道1、第一通道2、第二通道3以及第三通道4进行清洗,清洗完毕,关闭第六阀门19,此时,文氏管道1、第一通道2、第二通道3以及第三通道4处于真空低压清洁状态,打开第一阀门14、第三阀门16,大量外界气体由第一进气口5进入,少量外界气体由第二进气口7进入,第三通道4中的气体经多层可拆卸滤网9过滤后进入文氏管道1,与通过第一进气口5进入的气体共同由文氏管道1进入第一通道2,气体经由多层滤网10过滤后,大量气体由第一出气口6进入热释放速率测试仪,经由热释放速率测试仪吸出第一通道2,少量气体进入较细的第二通道3,此时,气体推进器11最前端由第四阀门17右侧位置推进到第四阀门17左侧位置,气体被吸入第二通道3中,关闭第四阀门17,推动气体推进器11,打开第八阀门21,使气体经由第二出气口8进入气相色谱仪中。During operation, the flue gas collection and testing device is used for heat release rate test, soot particle collection, and gas chromatography analysis. The
在本实施例中不使用该烟气收集及测试装置时,可关闭第一阀门14、第三阀门16、第七阀门20以及第八阀门21,不与外界连通,避免外界气体、烟尘进入。When the flue gas collection and testing device is not used in this embodiment, the
在本实施例中,可根据使用需求,对第一阀门14、第二阀门15、第三阀门16、第四阀门17、第五阀门18、第六阀门19、第七阀门20、第八阀门21进行开关,可以单独进行气体热释放速率测试、烟尘颗粒收集、气体成分分析或任意两种功能进行搭配;第一阀门14、第二阀门15、第三阀门16、第四阀门17、第五阀门18、第六阀门19、第七阀门20、第八阀门21,阀门型号、种类以及采用手动或自动型阀门,可根据实际情况进行选择安装。In this embodiment, the
在本实施例中,多层可拆卸滤网9可跟据需求,使用0.500~4.000mm筛孔尺寸的滤网,进行拆卸后,可对烟尘颗粒进行成分、性质等分析。In this embodiment, the multi-layer
在本实施例中,气体推进器11与第二通道3无缝贴合,气密性良好,由于气体推进器11支撑,当气体推进器11粗圆柱状部分完全进入第二通道3中时,气体推进器11不会额外承受多余管壁摩擦力,使用过程中,气体推进器11细圆柱状支撑最前端不应超过第四阀门17最左端,即不应与外界环境连通。In this embodiment, the
在本实施例中,气瓶12中气体使用氩气,但不限于氩气。In this embodiment, argon is used as the gas in the
以上所述仅为本发明的实施例,并非因此限制本发明的专利范围,凡是利用本发明说明书及附图内容所作的等效结构或等效流程变换,或直接或间接运用在其它相关的技术领域,均同理包括在本发明的专利保护范围内。The above descriptions are only embodiments of the present invention, and are not intended to limit the scope of the present invention. Any equivalent structure or equivalent process transformation made by using the contents of the description and drawings of the present invention, or directly or indirectly applied to other related technologies Fields are similarly included in the scope of patent protection of the present invention.
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