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CN111829600A - Measuring device and measuring method for micro-upgrade flow - Google Patents

Measuring device and measuring method for micro-upgrade flow Download PDF

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CN111829600A
CN111829600A CN201910324671.6A CN201910324671A CN111829600A CN 111829600 A CN111829600 A CN 111829600A CN 201910324671 A CN201910324671 A CN 201910324671A CN 111829600 A CN111829600 A CN 111829600A
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fluid
current
flow
coil
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CN111829600B (en
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陈兴隆
吕伟峰
李思源
韩海水
俞宏伟
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Petrochina Co Ltd
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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01FMEASURING VOLUME, VOLUME FLOW, MASS FLOW OR LIQUID LEVEL; METERING BY VOLUME
    • G01F1/00Measuring the volume flow or mass flow of fluid or fluent solid material wherein the fluid passes through a meter in a continuous flow
    • G01F1/56Measuring the volume flow or mass flow of fluid or fluent solid material wherein the fluid passes through a meter in a continuous flow by using electric or magnetic effects
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N15/00Investigating characteristics of particles; Investigating permeability, pore-volume or surface-area of porous materials
    • G01N15/08Investigating permeability, pore-volume, or surface area of porous materials
    • G01N15/082Investigating permeability by forcing a fluid through a sample

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Abstract

The application discloses metering device and metering method of little upgrading flow, and this metering device includes: the orifice plate comprises a fluid inlet, a fluid outlet and a transverse channel positioned between the fluid inlet and the fluid outlet, the fluid inlet and the transverse channel are connected through a main channel, a first side channel and a second side channel, and the transverse channel and the fluid outlet are connected through a third side channel and a fourth side channel; the magnetic induction device comprises a coil, a conductive circuit and a magnet, wherein the coil and the magnet are arranged in the transverse channel, one end of the conductive circuit is connected with the coil, and the other end of the conductive circuit is connected with the current detection circuit; the current detection circuit is used for detecting the magnitude of induced current generated in the conducting circuit and the frequency of change of the current direction; induced current is generated in the conductive path when the magnet is pushed by the fluid to reciprocate in the transverse passage in a direction perpendicular to the coil; and a calculation device for calculating the flow rate of the fluid according to the magnitude of the induced current and the frequency of the change in the direction of the current.

Description

微升级流量的计量装置及计量方法Measuring device and measuring method for micro-upgrade flow

技术领域technical field

本申请涉及流量测量技术领域,尤其涉及一种微升级流量的计量装置及计量方法。The present application relates to the technical field of flow measurement, and in particular, to a metering device and a metering method for micro-upgraded flow.

背景技术Background technique

当前,常规计量方法仍是毫升级别的量筒类装置观察方法以及电子天平称量方法。量筒类装置观察方法受界面干扰等影响,其误差始终在0.2ml以上;电子天平称量方法则要求流体密度必须有更精准的测量,对不同种类的油相而言,其计量精度并不高于量筒计量方法。At present, the conventional measurement method is still the observation method of the measuring cylinder-like device at the milliliter level and the electronic balance weighing method. The observation method of measuring cylinder devices is affected by interface interference, and its error is always above 0.2ml; the electronic balance weighing method requires more accurate measurement of fluid density, and its measurement accuracy is not high for different types of oil phases. in the measuring cylinder method.

随着超低渗、特低渗油藏开发研究的逐渐深入,实验中对微小体积流量的准确计量展现出越来越大的难度,常规计量方法难以满足对于测量精度的需求。在岩心实验中,常规岩心内的流体体积由6毫升(ml)左右降低至2ml左右,而相同实验的流程死体积并未降低,因而计量误差大幅升高。此外,尽管计算岩心内流体体积所需的入口、出口管线内体积可以计算,出口回压器流体量可计量,但是受压缩性的影响,不同压力条件下的体积量不易校准,这也进一步导致计量误差增大。With the gradual deepening of the development and research of ultra-low permeability and ultra-low permeability reservoirs, the accurate measurement of small volume flow in experiments has become more and more difficult, and conventional measurement methods are difficult to meet the requirements for measurement accuracy. In the core experiment, the fluid volume in the conventional core was reduced from about 6 milliliters (ml) to about 2 ml, but the dead volume of the process in the same experiment did not decrease, so the measurement error was greatly increased. In addition, although the volume in the inlet and outlet pipelines required to calculate the volume of the fluid in the core can be calculated, and the volume of the fluid in the outlet back pressure can be measured, it is not easy to calibrate the volume under different pressure conditions due to the influence of compressibility, which further leads to The measurement error increases.

在常规微观孔隙模型实验中,由于模型体内流体总量很少,其范围在1微升(μL)~200μL之间,体积计量几乎无法实现,因此通常采用面积法进行测量,或者通过计算估计不同状态的流体量,但是这种方法也受到流体是否可识别的影响,而且无法计量流动过程中流量变化情况。受这种技术状况的制约,常规微观试验多以观察现象的定位分析为主,无法定量分析始终困扰着研究人员。In conventional microscopic pore model experiments, since the total amount of fluid in the model body is very small, and its range is between 1 microliter (μL) and 200 μL, volume measurement is almost impossible, so the area method is usually used for measurement, or different calculation estimates are used. The amount of fluid in the state, but this method is also affected by whether the fluid is identifiable, and it cannot measure the flow change during the flow. Restricted by this technical situation, conventional microscopic experiments mostly focus on the localization analysis of observed phenomena, and the inability of quantitative analysis has always troubled researchers.

可见,现有计量方法测量微升级流量的难度及误差较大,难以满足当前对于微升级流量的计量要求。It can be seen that the existing measurement methods have great difficulties and errors in measuring the micro-upgrade flow, and it is difficult to meet the current measurement requirements for the micro-upgrade flow.

发明内容SUMMARY OF THE INVENTION

第一方面,本申请实施例提供一种微升级流量的计量装置,用以减小微升级流量的计量误差,提高计量精度。该计量装置包括:In a first aspect, an embodiment of the present application provides a metering device for micro-upgrade flow, which is used to reduce the measurement error of micro-upgrade flow and improve the measurement accuracy. The metering device includes:

孔道板8,包括流体入口7、流体出口15和位于流体入口7、流体出口15之间的横向通道12,流体入口7和横向通道12之间通过主流道9、第一侧流道10和第二侧流道11连接,第一侧流道10与主流道9之间的夹角,与第二侧流道11与主流道9之间的夹角相同,横向通道12与流体出口15之间通过第三侧流道32与第四侧流道33连接,横向通道12的宽度大于流体入口7的宽度;磁感应装置,包括线圈16、导电线路34和磁体13,线圈16和磁体13设置于横向通道12内部,导电线路34的一端与线圈16连接,另一端与电流检测电路19连接;电流检测电路19,用于检测导电线路34中产生的感应电流的大小及电流方向改变的频率;所述感应电流在磁体13受流体推动而在横向通道12中沿与线圈16垂直的方向做往复运动时在导电线路34中产生;计算设备21,根据感应电流的大小和电流方向改变的频率计算流体的流量。The orifice plate 8 includes a fluid inlet 7, a fluid outlet 15, and a transverse channel 12 between the fluid inlet 7 and the fluid outlet 15. Between the fluid inlet 7 and the transverse channel 12, the main channel 9, the first side channel 10 and the first side channel 12 pass through. The two side flow channels 11 are connected, the angle between the first side flow channel 10 and the main flow channel 9 is the same as the angle between the second side flow channel 11 and the main flow channel 9, and the angle between the lateral channel 12 and the fluid outlet 15 is the same. The third side flow channel 32 is connected to the fourth side flow channel 33, and the width of the transverse channel 12 is greater than the width of the fluid inlet 7; the magnetic induction device includes the coil 16, the conductive line 34 and the magnet 13, and the coil 16 and the magnet 13 are arranged in the transverse direction. Inside the channel 12, one end of the conductive line 34 is connected to the coil 16, and the other end is connected to the current detection circuit 19; the current detection circuit 19 is used to detect the magnitude of the induced current generated in the conductive line 34 and the frequency at which the current direction changes; the The induced current is generated in the conductive line 34 when the magnet 13 is pushed by the fluid and reciprocates in the transverse channel 12 in a direction perpendicular to the coil 16; the computing device 21 calculates the flow rate of the fluid according to the magnitude of the induced current and the frequency at which the direction of the current changes. flow.

第二方面,本申请实施例提供一种应用于如第一方面所述的微升级流量的计量装置的计量方法,该方法包括:In a second aspect, an embodiment of the present application provides a metering method applied to the metering device for micro-upgrade flow as described in the first aspect, the method comprising:

检测流体推动磁体做切割线圈的往复运动时,在导电线路中产生的感应电流的大小、电流方向改变的频率;根据感应电流的大小及电流方向改变的频率计算流体的流量。When the fluid pushes the magnet to do the reciprocating motion of the cutting coil, the magnitude of the induced current generated in the conductive line and the frequency of the change of the current direction are detected; the flow rate of the fluid is calculated according to the magnitude of the induced current and the frequency of the change of the current direction.

本申请实施例中提供的微升级流量的计量装置可以直接安装在岩心微观模型的入口或出口处,排除了管线、回压控制装置内死体积的干扰以及压缩系数变化的干扰,提升了超低渗、特低渗岩心实验的精度,同时,本申请利用电磁感应原理,建立了感知磁体往复运动的微电流检测方法,也解决了常规微观试验无法定量计量微升级流量的难题。The micro-upgrade flow metering device provided in the embodiment of the present application can be directly installed at the inlet or outlet of the core microscopic model, which eliminates the interference of the dead volume in the pipeline and the back pressure control device and the interference of the change of the compression coefficient, and improves the ultra-low At the same time, the application uses the principle of electromagnetic induction to establish a micro-current detection method for sensing the reciprocating motion of the magnet, and also solves the problem that conventional micro-tests cannot quantitatively measure the flow of micro-level upgrades.

附图说明Description of drawings

为了更清楚地说明本申请实施例或现有技术中的技术方案,下面将对实施例或现有技术描述中所需要使用的附图作简单地介绍,显而易见地,下面描述中的附图仅仅是本申请的一些实施例,对于本领域普通技术人员来讲,在不付出创造性劳动的前提下,还可以根据这些附图获得其他的附图。在附图中:In order to more clearly illustrate the embodiments of the present application or the technical solutions in the prior art, the following briefly introduces the accompanying drawings required for the description of the embodiments or the prior art. Obviously, the drawings in the following description are only These are some embodiments of the present application. For those of ordinary skill in the art, other drawings can also be obtained based on these drawings without any creative effort. In the attached image:

图1为本申请实施例中提供的一种微升级流量的计量装置的原理示意图;1 is a schematic diagram of the principle of a metering device for micro-upgrade flow provided in an embodiment of the application;

图2为本申请实施例中提供的微升级流量的计量装置中孔道板的结构示意图;FIG. 2 is a schematic structural diagram of an orifice plate in the metering device for micro-upgrade flow provided in the embodiment of the application;

图3为本申请实施例中提供的另一种微升级流量的计量装置的原理示意图;3 is a schematic diagram of the principle of another micro-upgrade flow metering device provided in an embodiment of the application;

图4为本申请实施例中提供的微升级流量的计量装置的结构示意图;4 is a schematic structural diagram of a metering device for micro-upgrade flow provided in an embodiment of the application;

图5为本申请实施例中提供的应用于微升级流量的计量装置的计量方法的流程图;5 is a flowchart of a metering method applied to a metering device for micro-upgrade flow provided in an embodiment of the application;

图6为本申请实施例中提供的应用于常规微观实验的微升级流量的计量装置的孔道板的尺寸示意图;6 is a schematic view of the size of the orifice plate of the metering device for micro-level flow rate applied to conventional microscopic experiments provided in the embodiment of the application;

图7为本申请实施例中提供的常规微观实验中微升级流量的计量装置的安装位置示意图;7 is a schematic diagram of the installation position of the metering device for micro-upgrade flow in the conventional microscopic experiment provided in the embodiment of the application;

图8为本申请实施例中提供的应用于岩心驱替实验的微升级流量的计量装置的孔道板的尺寸示意图;FIG. 8 is a schematic view of the dimensions of the orifice plate of the metering device for micro-upgrade flow rate applied to the core-flooding experiment provided in the embodiment of the application;

图9为本申请实施例中提供的岩心驱替实验中微升级流量的计量装置的安装位置示意图。FIG. 9 is a schematic diagram of the installation position of the metering device for micro-upgrade flow in the core-flooding experiment provided in the embodiment of the present application.

附图标号reference number

1:细管 2:突扩管1: Thin tube 2: Sudden expansion tube

3:总流量矢量 4:主方向分量3: Total flow vector 4: Main direction component

5:涡分量 6:侧向分量5: Eddy component 6: Lateral component

7:流体入口 8:孔道板7: Fluid inlet 8: Orifice plate

9:主流道 10:第一侧流道9: Main runner 10: First side runner

11:第二侧流道 12:横向通道11: Second side channel 12: Lateral channel

13:磁体 14:位置标识13: Magnet 14: Position marker

15:流体出口 16:线圈15: Fluid Outlet 16: Coil

17:电流表 18:基板17: Ammeter 18: Substrate

19:电流检测电路 20:放大电路19: Current detection circuit 20: Amplifier circuit

21:计算设备 22:流量输出显示窗口21: Computing device 22: Flow output display window

23:入口 24:微观可视模型23: Entrance 24: Microscopic Visual Model

25:微升级流量的计量装置 26:孔隙部分25: Metering device for microliter flow rate 26: Pore section

27:出口 28:驱替装置27: Exit 28: Displacement device

29:夹持器 30:低渗岩心29: Holder 30: Low permeability core

31:回压及接收装置 32:第三侧流道31: Back pressure and receiving device 32: Third side flow channel

33:第四侧流道 34:导电线路33: Fourth side runner 34: Conductive line

具体实施方式Detailed ways

为使本申请实施例的目的、技术方案和优点更加清楚明白,下面结合附图对本申请实施例做进一步详细说明。在此,本申请的示意性实施例及其说明用于解释本申请,但并不作为对本申请的限定。In order to make the purposes, technical solutions and advantages of the embodiments of the present application more clearly understood, the embodiments of the present application will be further described in detail below with reference to the accompanying drawings. Here, the exemplary embodiments and descriptions of the present application are used to explain the present application, but are not intended to limit the present application.

本申请利用微流控技术,设计了微米级通道,通过不同通道流速微调实现了固体微颗粒在横向孔道内往复运动;由磁感应原理可知,微磁体往复运动将在环绕的导电线圈内产生微电流,监测该电流方向变换频率即可计算出进出孔道内的流量值。下面将对本申请的方法原理进行简要介绍。The application uses microfluidic technology to design micron-scale channels, and realizes the reciprocating motion of solid micro-particles in the transverse channel by fine-tuning the flow rate of different channels; it can be known from the principle of magnetic induction that the reciprocating motion of the micro-magnet will generate a micro-current in the surrounding conductive coil. , and monitoring the current direction conversion frequency can calculate the flow value in and out of the channel. The principle of the method of the present application will be briefly introduced below.

参阅图1,由流体在细管1进入突扩管2结构的流道内的运动可知,总流量矢量3进入突扩管2后分散成主方向分量4和侧向分量6,并在管径突然增加的端面主流道两侧形成涡分量5,此处压力较低,流体易于在此处滞留。显然若在突扩管2内有一无法流出的较小固体,其将运移在此低压处,最为稳定。Referring to Fig. 1, it can be seen from the movement of the fluid in the flow channel where the thin tube 1 enters the sudden expanding tube 2 structure, the total flow vector 3 is dispersed into the main direction component 4 and the lateral component 6 after entering the sudden expanding tube 2, and the The vortex component 5 is formed on both sides of the main flow channel of the increased end face, where the pressure is lower, and the fluid is easy to stay here. Obviously, if there is a small solid that cannot flow out in the sudden expansion pipe 2, it will migrate at this low pressure and be the most stable.

根据上述原理,本申请实施例设计了一种微升级流量的计量装置的孔道板8,该孔道板8的材质可以为聚二甲硅氧烷(PDMS)。参见图2,该孔道板8包括流体入口7、流体出口15和位于流体入口7、流体出口15之间的横向通道12。流体入口7和横向通道12之间通过主流道9、第一侧流道10和第二侧流道11连接,第一侧流道10与主流道9之间的夹角,与第二侧流道11与主流道9之间的夹角相同,横向通道12与流体出口15之间通过第三侧流道32与第四侧流道33连接,横向通道12的宽度大于流体入口7的宽度。其中,第一侧流道10的出口宽度是主流道9出口宽度的一半;第二侧流道11的出口宽度是主流道9出口宽度的一半。According to the above principles, the embodiment of the present application designs an orifice plate 8 of a metering device for a micro-level flow rate, and the material of the orifice plate 8 may be polydimethylsiloxane (PDMS). Referring to FIG. 2 , the orifice plate 8 includes a fluid inlet 7 , a fluid outlet 15 and a transverse channel 12 between the fluid inlet 7 and the fluid outlet 15 . The fluid inlet 7 and the transverse channel 12 are connected by the main channel 9, the first side channel 10 and the second side channel 11. The angle between the first side channel 10 and the main channel 9 is the same as the second side channel. The angle between the channel 11 and the main channel 9 is the same. The transverse channel 12 and the fluid outlet 15 are connected to the fourth side channel 33 through the third side channel 32 . The width of the transverse channel 12 is greater than that of the fluid inlet 7 . Wherein, the outlet width of the first side channel 10 is half of the outlet width of the main channel 9 ; the outlet width of the second side channel 11 is half the outlet width of the main channel 9 .

结合图1所示的原理可知,当流体由流体入口7进入,由主流道9、第一侧流道10和第二侧流道11进入直径突然增加的横向通道12内,参阅图2,此时在横向通道12内的04和04’位置压力最低。磁体13,即如图所示的磁性球,有在此处稳定的倾向,受在02和02’流出流量的分流量的作用,磁体13偏移04和04’位置。若磁体13处于03和03’位置有堵塞出口侧流道倾向时,02和02’流出流量的分流量将其驱离。由此在横向通道12内,磁体13在入口流体流动的作用下,其将在01和02的范围内或01和02’的范围内或02和02’的范围内往复运动。According to the principle shown in FIG. 1 , when the fluid enters from the fluid inlet 7 , the main channel 9 , the first side channel 10 and the second side channel 11 enter the transverse channel 12 with a sudden increase in diameter. Referring to FIG. 2 , this The pressure is lowest at positions 04 and 04' in the transverse channel 12. The magnet 13, i.e. the magnetic ball as shown in the figure, has a tendency to be stable here, offset by the 04 and 04' positions due to the partial flow of the outgoing flow at 02 and 02'. If the magnets 13 at positions 03 and 03' tend to block the outlet side flow passages, the partial flow of the outflow flow from 02 and 02' drives them away. Thus within the transverse channel 12, the magnet 13 will reciprocate in the range 01 and 02 or 01 and 02' or 02 and 02' under the action of the inlet fluid flow.

考虑到磁体13可能在01和02的范围内或01和02’的范围内或02和02’的范围内往复运动,在本申请实施例中,线圈16以入口主流道9为分界,两侧分别缠绕,即线圈16在图2中的01和02,以及01和02’的范围内分别缠绕,这样,当磁体13在01和02的范围内运动时,可以在01和02范围内的线圈16中产生感应电流;当磁体13在01和02’的范围内运动时,可以在01和02’范围内的线圈16中产生感应电流。Considering that the magnet 13 may reciprocate within the range of 01 and 02, the range of 01 and 02', or the range of 02 and 02', in the embodiment of the present application, the coil 16 takes the inlet main channel 9 as a boundary, and two sides Wound separately, that is, the coil 16 is wound in the range of 01 and 02, and 01 and 02' in FIG. 2, respectively, so that when the magnet 13 moves in the range of 01 and 02, the coil in the range of 01 and 02 can be wound. An induced current is generated in 16; when the magnet 13 moves in the range of 01 and 02', an induced current can be generated in the coil 16 in the range of 01 and 02'.

需要说明的是,当磁体13在初始条件下产生运动后,会受到惯性影响持续运动,其不会稳定在某个位置。如若因孔道粗糙导致磁体13受较大阻力停止运动,则可以利用人为改变线圈16电流方向及强度的方法,使磁体13脱离该停止位置。It should be noted that, after the magnet 13 moves under the initial condition, it will continue to move under the influence of inertia, and it will not be stable in a certain position. If the magnet 13 stops moving due to the roughness of the hole, the magnet 13 can be removed from the stop position by artificially changing the current direction and intensity of the coil 16 .

显然磁体13在横向通道12内的运动范围及往复频率与流速正相关,流速越高,磁体13横向运动的范围越大且往复频率越快。Obviously, the movement range and reciprocating frequency of the magnet 13 in the transverse channel 12 are positively related to the flow velocity. The higher the flow velocity, the larger the lateral movement range of the magnet 13 and the faster the reciprocating frequency.

为实现微升级的流量计量,图2中孔道板8的孔道尺寸在微米(μm)尺度。根据测量需要,调整孔道尺寸,即可设计制作出不同流量范围的微升级流量的计量装置25。In order to achieve micro-scale flow measurement, the size of the orifice of the orifice plate 8 in FIG. 2 is in the micrometer (μm) scale. According to the measurement needs, the size of the orifice can be adjusted to design and manufacture the metering device 25 for micro-upgrade flow with different flow ranges.

此外,本申请实施例提供的微升级流量的计量装置25还利用了电磁感应原理。如图3所示,当磁体13在线圈16内做运动时,随着磁通量的增加或减少将产生感应电流,灵敏的电流表17将检测到相对应的电流方向及幅值变化。In addition, the metering device 25 for the micro-upgrade flow provided by the embodiment of the present application also utilizes the principle of electromagnetic induction. As shown in FIG. 3 , when the magnet 13 moves in the coil 16 , an induced current will be generated as the magnetic flux increases or decreases, and the sensitive ammeter 17 will detect the corresponding current direction and amplitude change.

根据上述电磁感应原理,如图4所示,本申请实施例设计了一种微升级流量的计量装置的磁感应装置、电流检测电路19及计算设备21。其中,该磁感应装置包括线圈16、导电线路34和磁体13,线圈16和磁体13设置于横向通道12(图4中未示出)内部,导电线路34的一端与线圈16连接,另一端与电流检测电路19连接。电流检测电路19,用于检测导电线路34中产生的感应电流的大小及电流方向改变的频率;感应电流在磁体13受流体推动而在横向通道12中沿与线圈16垂直的方向做往复运动时在导电线路34中产生。计算设备21,根据感应电流的大小和电流方向改变的频率计算流体的流量。According to the above electromagnetic induction principle, as shown in FIG. 4 , the embodiment of the present application designs a magnetic induction device, a current detection circuit 19 and a computing device 21 of a metering device for micro-upgrade flow. The magnetic induction device includes a coil 16, a conductive line 34, and a magnet 13. The coil 16 and the magnet 13 are arranged inside the transverse channel 12 (not shown in FIG. 4). One end of the conductive line 34 is connected to the coil 16, and the other end is connected to the current The detection circuit 19 is connected. The current detection circuit 19 is used to detect the magnitude of the induced current generated in the conductive line 34 and the frequency at which the direction of the current changes; when the magnet 13 is pushed by the fluid and reciprocates in the transverse channel 12 in a direction perpendicular to the coil 16 Produced in conductive traces 34 . The computing device 21 calculates the flow rate of the fluid according to the magnitude of the induced current and the frequency of changing the direction of the current.

其中,磁感应装置包括两个线圈16和两个导电线路34,每个线圈16与一个导电线路34连接;其中一个线圈16设置于横向通道12中,处于第一侧流道10与主流道9之间的位置;另一个线圈16设置于横向通道12中,处于第二侧流道11与主流道9之间的位置。孔道板8设置在基板18上,为了稳固线圈16,可以将线圈缠绕在基板18上,并利用液体胶固化在基板18上。The magnetic induction device includes two coils 16 and two conductive lines 34, each coil 16 is connected to one conductive line 34; one of the coils 16 is arranged in the transverse channel 12, between the first side channel 10 and the main channel 9 The other coil 16 is arranged in the transverse channel 12 at the position between the second side flow channel 11 and the main flow channel 9 . The orifice plate 8 is disposed on the base plate 18 . In order to stabilize the coil 16 , the coil can be wound on the base plate 18 and cured on the base plate 18 by liquid glue.

其中,磁体13的材质可以为钕铁硼磁体。磁体13的形状可以为正方体、长方体或球体等。但考虑到球体运动时的摩擦较小,可以优先选择球体作为磁体13的形状。The material of the magnet 13 may be a neodymium iron boron magnet. The shape of the magnet 13 may be a cube, a rectangular parallelepiped, a sphere, or the like. However, considering that the friction of the sphere is relatively small, the shape of the sphere can be preferably selected as the magnet 13 .

参见图4,为本申请实施例提供的微升级流量的计量装置的整体结构示意图。在该计量装置中的电流检测电路19包括放大电路20,该放电电路20与导电线路34连接,用于放大导电线路34中的感应电流。放大电路34可以采用三极管多级放大方法,可检测纳安(NA)级的电流变化情况。本申请实施例中磁体13微小,且线圈16的数量受体积限制较少,其电流变化幅度在微安级以下,因此为了提高测量的精度,在导电线路34与电流检测设备之间可以设置放大电路20。放电电路20的结构及连接方法是成熟的现有技术,在此不再赘述。Referring to FIG. 4 , it is a schematic diagram of the overall structure of the metering device for micro-upgrade flow provided by the embodiment of the present application. The current detection circuit 19 in the metering device includes an amplification circuit 20 connected to the conductive line 34 for amplifying the induced current in the conductive line 34 . The amplifying circuit 34 can adopt the triode multi-stage amplifying method, and can detect the current change of the nano-ampere (NA) level. In the embodiment of the present application, the magnet 13 is small, and the number of coils 16 is less limited by the volume, and its current variation range is below the microamp level. Therefore, in order to improve the measurement accuracy, an amplifier can be set between the conductive line 34 and the current detection device. circuit 20. The structure and connection method of the discharge circuit 20 are mature in the prior art, and will not be repeated here.

在本申请实施例的一种实现方式中,为了使用户明确流量的大小,如图4所示,可以为计算设备21设置流量输出显示窗22,用户可通过该显示窗22来了解当前流量的大小。In an implementation manner of the embodiment of the present application, in order for the user to know the size of the flow, as shown in FIG. size.

本申请实施例中提供的微升级流量的计量装置可以直接安装在岩心微观模型的入口或出口处,排除了管线、回压控制装置内死体积的干扰以及压缩系数变化的干扰,提升了超低渗、特低渗岩心实验的精度,同时,本申请利用电磁感应原理,建立了感知磁体往复运动的微电流检测方法,也解决了常规微观试验无法定量计量微升级流量的难题。The micro-upgrade flow metering device provided in the embodiment of the present application can be directly installed at the inlet or outlet of the core microscopic model, which eliminates the interference of the dead volume in the pipeline and the back pressure control device and the interference of the change of the compression coefficient, and improves the ultra-low At the same time, the application uses the principle of electromagnetic induction to establish a micro-current detection method for sensing the reciprocating motion of the magnet, and also solves the problem that conventional micro-tests cannot quantitatively measure the flow of micro-level upgrades.

本申请实施例还提供了一种应用于如前述的微升级流量的计量装置的计量方法,如图5所示,该方法包括:The embodiment of the present application also provides a metering method applied to the aforementioned micro-upgraded flow metering device. As shown in FIG. 5 , the method includes:

步骤501、检测流体推动磁体做切割线圈的往复运动时,在导电线路中产生的感应电流的大小、电流方向改变的频率。Step 501: Detect the magnitude of the induced current and the frequency at which the current direction changes when the fluid pushes the magnet to perform the reciprocating motion of the cutting coil.

步骤502、根据感应电流的大小及电流方向改变的频率计算流体的流量。Step 502: Calculate the flow rate of the fluid according to the magnitude of the induced current and the frequency at which the direction of the current changes.

在本申请实施例的一种实现方式中,根据感应电流的大小及电流方向改变的频率计算流体的流量,包括:根据公式S=aebI计算磁体在一次往复运动中的路程S,其中,a、b为常数,I为感应电流的幅值;根据公式q=meS计算单次流量q,其中,m为孔道相关的常数;根据公式Q=nq计算流体的流量Q,其中,n为电流方向改变的频率。In an implementation manner of the embodiment of the present application, calculating the flow rate of the fluid according to the magnitude of the induced current and the frequency of changing the direction of the current includes: calculating the distance S of the magnet in one reciprocating motion according to the formula S=ae bI , where a , b are constants, I is the amplitude of the induced current; calculate the single flow q according to the formula q=me S , where m is the constant related to the channel; calculate the flow rate Q of the fluid according to the formula Q=nq, where n is the current The frequency with which the direction changes.

其中,常数a、b可以根据下述方法确定:Among them, the constants a and b can be determined according to the following methods:

预设流体的流速,利用不同恒定流速的流体流经微升级流量的计量装置,采集与不同流速对应的感应电流的大小及电流方向改变的频率;根据与不同流速对应的感应电流的大小及电流方向改变的频率确定常数a、b。The flow rate of the fluid is preset, and the fluid with different constant flow rates is used to flow through the micro-level flow metering device to collect the magnitude of the induced current corresponding to the different flow rates and the frequency at which the current direction changes; according to the magnitude and current of the induced current corresponding to the different flow rates The frequency of the direction change determines the constants a, b.

m与孔道的直径、主流道与侧流道之间的夹角、流道的长度、横向通道的宽度等孔道结构有关。因此,在制作出本申请所述的微升级流量的计量装置之后,再根据孔道结构,以固定流量进行实验确定参数m。m is related to the channel structure such as the diameter of the channel, the angle between the main channel and the side channel, the length of the channel, and the width of the lateral channel. Therefore, after the metering device for the micro-upgrade flow rate described in the present application is manufactured, the parameter m is determined experimentally with a fixed flow rate according to the pore structure.

本申请实施例中提供的微升级流量的计量装置可以直接安装在岩心微观模型的入口或出口处,排除了管线、回压控制装置内死体积的干扰以及压缩系数变化的干扰,提升了超低渗、特低渗岩心实验的精度,同时,本申请利用电磁感应原理,建立了感知磁体往复运动的微电流检测方法,也解决了常规微观试验无法定量计量微升级流量的难题。The micro-upgrade flow metering device provided in the embodiment of the present application can be directly installed at the inlet or outlet of the core microscopic model, which eliminates the interference of the dead volume in the pipeline and the back pressure control device and the interference of the change of the compression coefficient, and improves the ultra-low At the same time, the application uses the principle of electromagnetic induction to establish a micro-current detection method for sensing the reciprocating motion of the magnet, and also solves the problem that conventional micro-tests cannot quantitatively measure the flow of micro-level upgrades.

下面将结合具体的尺寸介绍一种应用于常规微观实验中的微升级流量的计量装置,以及一种应用于岩心驱替实验中的微升级流量的计量装置。The following will introduce a metering device for micro-up flow rate applied in conventional microscopic experiments, and a metering device for micro-up flow rate applied in core flooding experiments in combination with specific dimensions.

1、应用于常规微观实验中的微升级流量的计量装置1. A metering device for micro-level flow in conventional microscopic experiments

适合微观可视模型的微升级流量的计量装置的设计尺寸见图6。其外形尺寸为3毫米(mm)×6mm×2mm,孔道厚度均为40微米(μm)。经过计算可知,计量装置的孔道内总空间体积约为0.2微升(μL)。40μm的孔道PDMS模型制作方法及流程是成熟技术,在此不再赘述。The design dimensions of the metering device for micro-upgrade flow suitable for the microscopic visual model are shown in Figure 6. Its external dimensions are 3 millimeters (mm) × 6 mm × 2 mm, and the thickness of the channels is 40 micrometers (μm). After calculation, it can be known that the total space volume in the channel of the metering device is about 0.2 microliter (μL). The fabrication method and process of the 40 μm pore PDMS model is a mature technology, and will not be repeated here.

磁感应装置中的线圈16可以采用12μm直径的铜线,当使用的磁体13的形状为球型时,磁性球体的直径介于30~35μm之间。The coil 16 in the magnetic induction device can be a copper wire with a diameter of 12 μm. When the shape of the used magnet 13 is spherical, the diameter of the magnetic sphere is between 30 and 35 μm.

在进行常规微观实验时,可以依照如图7所示的两个微升级流量的计量装置25安装的位置之一进行安装,即该微升级流量的计量装置25可以安装在入口端23或出口端27均可。在微观可视模型24中,该计量装置25直接放置在微观可视模型24内部。When performing conventional microscopic experiments, it can be installed according to one of the two installation positions of the metering devices 25 for micro-upgrade flow as shown in FIG. 27 are available. In the microscopic visualization model 24 , the metering device 25 is placed directly inside the microscopic visualization model 24 .

利用本申请提供的微升级流量的计量装置25进行常规微观实验中,流体经过微观可视模型24孔道内的流体总量得到精确计量。In conventional microscopic experiments using the metering device 25 for micro-level flow rate provided by the present application, the total amount of fluid passing through the pores of the microscopic visual model 24 is accurately measured.

此外,图7中示出的孔隙部分26为微观可视模型24的构成部分。Furthermore, the aperture portion 26 shown in FIG. 7 is a constituent part of the microscopic visual model 24 .

2、应用于岩心驱替实验中的微升级流量的计量装置2. A metering device for micro-upgrade flow in core flooding experiments

适合岩心驱替的微升级流量的计量装置的设计尺寸见图8,其外形尺寸为10mm×20mm×2mm,孔道厚度均为120μm。经过计算可知,计量装置的孔道内总空间体积约为3.6μL。Figure 8 shows the design dimensions of the micro-upgraded flow metering device suitable for core flooding. After calculation, it can be known that the total space volume in the channel of the metering device is about 3.6 μL.

磁感应装置中的线圈16同样可以采用12μm直径的铜线,当使用的磁体13的形状为球型时,磁性球体的直径介于100~115μm之间。The coil 16 in the magnetic induction device can also be a copper wire with a diameter of 12 μm. When the shape of the used magnet 13 is spherical, the diameter of the magnetic sphere is between 100 and 115 μm.

在进行岩心驱替实验时,可以依照如图9所示的两个微升级流量的计量装置25安装的位置之一进行安装,即该微升级流量的计量装置25可以安装在入口端或出口端均可,在岩石驱替实验中,该计量装置需与岩石相接触。When performing the core flooding experiment, it can be installed according to one of the two installation positions of the metering device 25 for the micro-level flow rate as shown in FIG. Either, in the rock displacement experiment, the metering device needs to be in contact with the rock.

此外,还需注意的是,在岩心驱替实验中,严格控制驱替装置的注入速度。由于微升级流量的计量装置与超低渗、特低渗的慢速渗流特点相一致,因而注入速度非常慢,例如注入泵的速度设定为0.05ml/min(50μL/min),而微升级流量的计量装置则排除了驱替装置、中间容器内流体压缩性的影响,测量值为40μL/min。In addition, it should be noted that in the core flooding experiments, the injection rate of the displacement device is strictly controlled. Since the metering device of micro-liter flow rate is consistent with the characteristics of ultra-low osmotic and ultra-low osmotic slow-speed seepage, the injection speed is very slow. The flow metering device excludes the influence of the displacement device and the fluid compressibility in the intermediate container, and the measured value is 40 μL/min.

利用本申请提供的微升级流量的计量装置进行驱替实验中,流体通过计量装置的流量得到实时计量和存储。In the displacement experiment using the metering device with a micro-upgrade flow rate provided by the present application, the flow rate of the fluid passing through the metering device is measured and stored in real time.

此外,图9中所示的驱替装置28、夹持器29、低渗岩心30、回压及接收装置31均为岩心驱替实验中的常用装置,在此不再赘述。In addition, the displacement device 28 , the holder 29 , the low-permeability core 30 , the back pressure and the receiving device 31 shown in FIG. 9 are all commonly used devices in the core displacement experiment, and will not be repeated here.

本领域内的技术人员应明白,本申请的实施例可提供为方法、系统、或计算机程序产品。因此,本申请可采用完全硬件实施例、完全软件实施例、或结合软件和硬件方面的实施例的形式。而且,本申请可采用在一个或多个其中包含有计算机可用程序代码的计算机可用存储介质(包括但不限于磁盘存储器、CD-ROM、光学存储器等)上实施的计算机程序产品的形式。As will be appreciated by those skilled in the art, the embodiments of the present application may be provided as a method, a system, or a computer program product. Accordingly, the present application may take the form of an entirely hardware embodiment, an entirely software embodiment, or an embodiment combining software and hardware aspects. Furthermore, the present application may take the form of a computer program product embodied on one or more computer-usable storage media (including, but not limited to, disk storage, CD-ROM, optical storage, etc.) having computer-usable program code embodied therein.

本申请是参照根据本申请实施例的方法、设备(系统)、和计算机程序产品的流程图和/或方框图来描述的。应理解可由计算机程序指令实现流程图和/或方框图中的每一流程和/或方框、以及流程图和/或方框图中的流程和/或方框的结合。可提供这些计算机程序指令到通用计算机、专用计算机、嵌入式处理机或其他可编程数据处理设备的处理器以产生一个机器,使得通过计算机或其他可编程数据处理设备的处理器执行的指令产生用于实现在流程图一个流程或多个流程和/或方框图一个方框或多个方框中指定的功能的装置。The present application is described with reference to flowchart illustrations and/or block diagrams of methods, apparatus (systems), and computer program products according to embodiments of the present application. It will be understood that each flow and/or block in the flowchart illustrations and/or block diagrams, and combinations of flows and/or blocks in the flowchart illustrations and/or block diagrams, can be implemented by computer program instructions. These computer program instructions may be provided to the processor of a general purpose computer, special purpose computer, embedded processor or other programmable data processing device to produce a machine such that the instructions executed by the processor of the computer or other programmable data processing device produce Means for implementing the functions specified in a flow or flow of a flowchart and/or a block or blocks of a block diagram.

这些计算机程序指令也可存储在能引导计算机或其他可编程数据处理设备以特定方式工作的计算机可读存储器中,使得存储在该计算机可读存储器中的指令产生包括指令装置的制造品,该指令装置实现在流程图一个流程或多个流程和/或方框图一个方框或多个方框中指定的功能。These computer program instructions may also be stored in a computer-readable memory capable of directing a computer or other programmable data processing apparatus to function in a particular manner, such that the instructions stored in the computer-readable memory result in an article of manufacture comprising instruction means, the instructions The apparatus implements the functions specified in the flow or flows of the flowcharts and/or the block or blocks of the block diagrams.

这些计算机程序指令也可装载到计算机或其他可编程数据处理设备上,使得在计算机或其他可编程设备上执行一系列操作步骤以产生计算机实现的处理,从而在计算机或其他可编程设备上执行的指令提供用于实现在流程图一个流程或多个流程和/或方框图一个方框或多个方框中指定的功能的步骤。These computer program instructions can also be loaded on a computer or other programmable data processing device to cause a series of operational steps to be performed on the computer or other programmable device to produce a computer-implemented process such that The instructions provide steps for implementing the functions specified in the flow or blocks of the flowcharts and/or the block or blocks of the block diagrams.

以上所述的具体实施例,对本申请的目的、技术方案和有益效果进行了进一步详细说明,所应理解的是,以上所述仅为本申请的具体实施例而已,并不用于限定本申请的保护范围,凡在本申请的精神和原则之内,所做的任何修改、等同替换、改进等,均应包含在本申请的保护范围之内。The specific embodiments described above further describe the purpose, technical solutions and beneficial effects of the present application in further detail. It should be understood that the above are only specific embodiments of the present application and are not intended to limit the Within the scope of protection, any modification, equivalent replacement, improvement, etc. made within the spirit and principle of this application shall be included in the protection scope of this application.

Claims (10)

1. A metering device for micro-scale flow, the metering device comprising:
the orifice plate (8) comprises a fluid inlet (7), a fluid outlet (15) and a transverse channel (12) positioned between the fluid inlet (7) and the fluid outlet (15), the fluid inlet (7) and the transverse channel (12) are connected through a main channel (9), a first side channel (10) and a second side channel (11), an included angle between the first side channel (10) and the main channel (9) is the same as that between the second side channel (11) and the main channel (9), the transverse channel (12) and the fluid outlet (15) are connected through a third side channel (32) and a fourth side channel (33), and the width of the transverse channel (12) is larger than that of the fluid inlet (7);
the magnetic induction device comprises a coil (16), a conductive circuit (34) and a magnet (13), wherein the coil (16) and the magnet (13) are arranged in the transverse channel (12), one end of the conductive circuit (34) is connected with the coil (16), and the other end of the conductive circuit is connected with the current detection circuit (19);
a current detection circuit (19) for detecting the magnitude of an induced current generated in the conductive line (34) and the frequency of change in the direction of the current; the induced current is generated in the conductive line (34) when the magnet (13) is reciprocated in the transverse channel (12) in a direction perpendicular to the coil (16) by the fluid;
and a calculation device (21) that calculates the flow rate of the fluid based on the magnitude of the induced current and the frequency at which the direction of the current changes.
2. The apparatus according to claim 1, wherein the current detection circuit (19) comprises:
and the amplifying circuit (20) is connected with the conductive line (34) and is used for amplifying the induced current in the conductive line (34).
3. The device according to claim 1, characterized in that the outlet width of the first side channel (10) is half the outlet width of the main channel (9); the outlet width of the second side runner (11) is half of the outlet width of the main runner (9).
4. A device according to claim 1 or 2, characterized in that the magnetic induction means comprise two coils (16) and two electrically conductive tracks (34), each coil (16) being connected to one electrically conductive track (34); one of the coils (16) is arranged in the transverse channel (12) at a position between the first side channel (10) and the main channel (9); another coil (16) is arranged in the transverse channel (12) at a position between the second side channel (11) and the main channel (9).
5. The device according to claim 1, characterized in that the orifice plate (8) is arranged on a base plate (18), the coil (16) being wound on the base plate (18) and being cured on the base plate (18) with a liquid glue.
6. The device according to claim 1, wherein the material of the orifice plate (8) comprises polydimethylsiloxane.
7. Device according to claim 1, characterized in that the material of the magnet (13) comprises a neodymium-iron-boron magnet.
8. A metering method applied to the metering device of the micro-upgrade flow as claimed in any one of claims 1 to 6, characterized in that the method comprises the following steps:
detecting the magnitude of induced current generated in the conducting circuit and the frequency of change of the current direction when the fluid pushes the magnet to do reciprocating motion of the cutting coil;
and calculating the flow rate of the fluid according to the magnitude of the induced current and the frequency of the change of the current direction.
9. The method of claim 8, wherein calculating the flow rate of the fluid based on the magnitude of the induced current and the frequency of the change in direction of the current comprises:
according to the formula S ═ aebICalculating the path S of the magnet in one reciprocating motion, wherein a and b are constants, and I is the amplitude of the induction current;
according to the formula q meSCalculating single flow q, wherein m is a constant related to a pore channel;
the flow rate Q of the fluid is calculated according to the formula Q nq, where n is the frequency at which the direction of the current changes.
10. The method of claim 8 or 9, wherein before calculating the flow rate of the fluid based on the magnitude of the induced current and the frequency of the change in direction of the current, the method further comprises:
presetting the flow rate of fluid, and collecting the magnitude of induced current corresponding to different flow rates and the frequency of current direction change by utilizing the flow of the fluid with different constant flow rates through a metering device for micro-upgrade flow;
the constants a, b are determined according to the magnitude of the induced current corresponding to different flow rates and the frequency of the change in the direction of the current.
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