CN111812232A - Fragrance product fragrance molecule content proportion, fragrance molecule color management and map display method - Google Patents
Fragrance product fragrance molecule content proportion, fragrance molecule color management and map display method Download PDFInfo
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- CN111812232A CN111812232A CN202010618364.1A CN202010618364A CN111812232A CN 111812232 A CN111812232 A CN 111812232A CN 202010618364 A CN202010618364 A CN 202010618364A CN 111812232 A CN111812232 A CN 111812232A
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- fragrance
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- 239000003205 fragrance Substances 0.000 title claims abstract description 57
- 238000000034 method Methods 0.000 title claims abstract description 19
- 238000010438 heat treatment Methods 0.000 claims abstract description 18
- 238000000926 separation method Methods 0.000 claims abstract description 14
- XLUXHEZIGIDTCC-UHFFFAOYSA-N acetonitrile;ethyl acetate Chemical compound CC#N.CCOC(C)=O XLUXHEZIGIDTCC-UHFFFAOYSA-N 0.000 claims abstract description 12
- 238000000605 extraction Methods 0.000 claims abstract description 8
- 238000007865 diluting Methods 0.000 claims abstract description 6
- 239000012528 membrane Substances 0.000 claims abstract description 6
- 238000002156 mixing Methods 0.000 claims abstract description 6
- 230000010355 oscillation Effects 0.000 claims abstract description 6
- 229920006395 saturated elastomer Polymers 0.000 claims abstract description 6
- 238000005303 weighing Methods 0.000 claims abstract description 6
- 238000001914 filtration Methods 0.000 claims abstract description 3
- 238000001228 spectrum Methods 0.000 claims description 6
- 238000001514 detection method Methods 0.000 claims description 5
- 238000001819 mass spectrum Methods 0.000 claims description 5
- 239000007788 liquid Substances 0.000 abstract 2
- 230000000694 effects Effects 0.000 description 6
- 238000007689 inspection Methods 0.000 description 6
- 239000002304 perfume Substances 0.000 description 3
- 230000007547 defect Effects 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
Classifications
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/04—Preparation or injection of sample to be analysed
- G01N30/06—Preparation
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/26—Conditioning of the fluid carrier; Flow patterns
- G01N30/28—Control of physical parameters of the fluid carrier
- G01N30/30—Control of physical parameters of the fluid carrier of temperature
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/62—Detectors specially adapted therefor
- G01N30/72—Mass spectrometers
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- Physics & Mathematics (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Analytical Chemistry (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- General Physics & Mathematics (AREA)
- Immunology (AREA)
- Pathology (AREA)
- Other Investigation Or Analysis Of Materials By Electrical Means (AREA)
Abstract
The invention relates to the technical field of display information, in particular to a fragrance product fragrance molecule content ratio, fragrance molecule color management and map display method, which comprises the following steps of selecting a sample to be detected for sample treatment: accurately weighing about 0.2-0.3 g of essence into a 15mL colorimetric tube with a plug, adding 0.5-0.7mL of saturated chlorinated solution, diluting to a scale by using an acetonitrile-ethyl acetate extracting solution, wherein the mixing ratio of the acetonitrile-ethyl acetate is 10:90, performing oscillation extraction, taking supernate, filtering the supernate through a microporous filter membrane, and detecting by using an image chromatography-mass spectrometer; heating the extraction liquid obtained in the first step to 180-200 ℃, and introducing the extraction liquid into a chromatographic column for separation; detecting the solution separated in the second step by a gas chromatography-mass spectrometer; and drawing a color pattern and a molecule contained proportion pattern according to the contained molecule type. The aroma content and the proportion of all products are clear. The data is scientific and accurate. The problem of how to more accurately select the fragrance product suitable for the consumer and understand the favorite reason for a certain fragrance is solved.
Description
Technical Field
The invention relates to the technical field of information display, in particular to a fragrance product fragrance molecule content ratio, fragrance molecule color management and map display method.
Background
The fragrance product is an effective raw material for manufacturing perfume and is widely applied in life, but the prior fragrance product has the following defects:
1. the current descriptions of perfumes and fragrances for fragrance types are simply a few names listed;
2. the information of each channel for the same product is inconsistent;
3. there is no scientific and data description of the scent of the product.
Therefore, consumers and users cannot know the accurate fragrance type and smell of a bottle of perfume and a fragrance product, and in order to solve the problems, a fragrance molecular content ratio, fragrance molecular color management and map display method of the fragrance product is provided.
Disclosure of Invention
The invention aims to solve the defects in the prior art, and provides a fragrance product fragrance molecule content ratio, fragrance molecule color management and map display method.
In order to achieve the purpose, the invention adopts the following technical scheme:
designing a fragrance molecule content ratio, fragrance molecule color management and spectrum display method of fragrance products, and performing component detection by using a gas chromatography-mass spectrometer, wherein the method comprises the following steps:
firstly, selecting a sample to be detected for sample treatment: accurately weighing about 0.2-0.3 g of essence into a 15mL colorimetric tube with a plug, adding 0.5-0.7mL of saturated chlorinated solution, diluting to a scale by using an acetonitrile-ethyl acetate extracting solution, wherein the mixing ratio of the acetonitrile-ethyl acetate is 10:90, performing oscillation extraction, taking supernate, filtering the supernate through a microporous filter membrane, and detecting by using an image chromatography-mass spectrometer;
secondly, heating the extract obtained in the first step to 180-200 ℃, and introducing the extract into a chromatographic column for separation, wherein the chromatographic column is any one of an HP-5MS chromatographic column and a DB-WAXUI3 chromatographic column;
thirdly, detecting the solution separated in the second step by a gas chromatograph-mass spectrometer, so as to obtain the molecular content proportion of the detected solution and obtain the optimal mass spectrum parameters of the detected solution;
fourthly, drawing a color pattern and a molecule contained proportion pattern according to the contained molecule type;
fifthly, inputting the corresponding product name of the drawn information into a computer according to the pattern information drawn in the fourth step;
and sixthly, inputting the name of the product to be inquired into the computer, and displaying the related information of the product to be inquired.
Preferably, when the second step is performed by introducing into the chromatographic column for separation, the temperature of the chromatographic column is first raised to 75-80 ℃ and maintained for 1min, then the temperature is raised to 180 ℃ by the program of 5-6 ℃ per min, then the temperature is raised to 200 ℃ by 1-1.5 ℃ per min, and then the temperature is raised to 260-270 ℃ by 12-15 ℃ per min and maintained for 5 min.
Preferably, the pattern drawn in the fourth step must be clear and transparent for easy observation.
Preferably, the related information of the product to be queried in the sixth step includes encyclopedic information of the contained molecule type, article content related to the molecule type, a product available for supply corresponding to the molecule type, supplier information, and official data provided by a supplier, and the rechecking and checking with the official data of each brand are realized to perform secondary checking of the data.
The fragrance molecule content proportion, fragrance molecule color management and map display method of the fragrance product provided by the invention has the beneficial effects that: the aroma content and the proportion of all products are clear. The data is scientific and accurate. The problem that the fragrance cannot be described by words for a long time is solved, and the fragrance can be digitalized and visualized. The problem of how to more accurately select the fragrance product suitable for the consumer and understand the favorite reason for a certain fragrance is solved.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments.
The embodiment I of the method for fragrance molecule content ratio, fragrance molecule color management and spectrum display of the fragrance product is characterized in that a gas chromatography-mass spectrometer is used for component detection, and the method comprises the following steps:
firstly, selecting a sample to be detected for sample treatment: accurately weighing about 0.2 g of essence in a 15mL colorimetric tube with a plug, adding 0.5mL of saturated chlorinated solution, diluting to a scale with an acetonitrile-ethyl acetate extracting solution, wherein the mixing ratio of the acetonitrile-ethyl acetate is 10:90, performing oscillation extraction, taking supernate, passing the supernate through a microporous filter membrane, and detecting by using a GC-MS (gas chromatography-mass spectrometer);
secondly, heating the extract obtained in the first step to 180 ℃, and introducing the extract into a chromatographic column for separation, wherein the chromatographic column is any one of an HP-5MS chromatographic column and a DB-WAXUI3 chromatographic column; when the separation is carried out by introducing into a chromatographic column, firstly heating the chromatographic column to 75 ℃ and keeping the temperature for 1min, then heating to 180 ℃ by a program of 5 ℃/min, then heating to 200 ℃ by 1 ℃/min, then heating to 260 ℃ by 12 ℃/min, keeping the temperature for 5min, and the separation effect is good.
Thirdly, detecting the solution separated in the second step by a gas chromatograph-mass spectrometer, so as to obtain the molecular content proportion of the detected solution and obtain the optimal mass spectrum parameters of the detected solution;
fourthly, drawing a color pattern and a molecule contained proportion pattern according to the contained molecule type; the pattern drawn in the fourth step must be clear and bright, so that the observation is convenient, the observation effect is better, and the trouble of the user is solved.
Fifthly, inputting the corresponding product name of the drawn information into a computer according to the pattern information drawn in the fourth step;
and sixthly, inputting the name of the product to be inquired into the computer, namely displaying the related information of the product to be inquired, wherein the related information of the product to be inquired in the sixth step comprises encyclopedia information of the contained molecular type, article content related to the molecular type, the product which can be supplied corresponding to the molecular type, supplier information and official data provided by the supplier, and the rechecking inspection of the official data of each brand is realized, the secondary inspection of the data is performed, and the data is diverse, so that a user can conveniently know the condition.
The second embodiment is a fragrance product fragrance molecule content proportion, fragrance molecule color management and spectrum display method, and component detection is performed by using a gas chromatography-mass spectrometer, and the method is characterized by comprising the following steps:
firstly, selecting a sample to be detected for sample treatment: accurately weighing about 0.25 g of essence into a 15mL colorimetric tube with a plug, adding 0.6mL of saturated chlorinated solution, diluting to a scale with an acetonitrile-ethyl acetate extracting solution, wherein the mixing ratio of the acetonitrile-ethyl acetate is 10:90, performing oscillation extraction, taking supernate, passing the supernate through a microporous filter membrane, and detecting by using a GC-MS instrument;
secondly, heating the extract obtained in the first step to 190 ℃, and introducing the extract into a chromatographic column for separation, wherein the chromatographic column is any one of an HP-5MS chromatographic column and a DB-WAXUI3 chromatographic column; when the separation is carried out by introducing into a chromatographic column, firstly heating the chromatographic column to 78 ℃ and keeping the temperature for 1min, then heating to 180 ℃ by a program of 5.5 ℃ per min, then heating to 200 ℃ by 1.3 ℃ per min, then heating to 270 ℃ by a program of 13 ℃ per min, keeping the temperature for 5min, and having good separation effect.
Thirdly, detecting the solution separated in the second step by a gas chromatograph-mass spectrometer, so as to obtain the molecular content proportion of the detected solution and obtain the optimal mass spectrum parameters of the detected solution;
fourthly, drawing a color pattern and a molecule contained proportion pattern according to the contained molecule type; the pattern drawn in the fourth step must be clear and bright, so that the observation is convenient, the observation effect is better, and the trouble of the user is solved.
Fifthly, inputting the corresponding product name of the drawn information into a computer according to the pattern information drawn in the fourth step;
and sixthly, inputting the name of the product to be inquired into the computer, namely displaying the related information of the product to be inquired, wherein the related information of the product to be inquired in the sixth step comprises encyclopedia information of the contained molecular type, article content related to the molecular type, the product which can be supplied corresponding to the molecular type, supplier information and official data provided by the supplier, and the rechecking inspection of the official data of each brand is realized, the secondary inspection of the data is performed, and the data is diverse, so that a user can conveniently know the condition.
The third embodiment of the invention provides a fragrance molecule content proportion, fragrance molecule color management and spectrum display method of fragrance products, and component detection is carried out by using a gas chromatography-mass spectrometer, and the method is characterized by comprising the following steps:
firstly, selecting a sample to be detected for sample treatment: accurately weighing about 0.3 g of essence in a 15mL colorimetric tube with a plug, adding 0.7mL of saturated chlorinated solution, diluting to a scale with an acetonitrile-ethyl acetate extracting solution, wherein the mixing ratio of the acetonitrile-ethyl acetate is 10:90, performing oscillation extraction, taking supernate, passing the supernate through a microporous filter membrane, and detecting by using a GC-MS instrument;
secondly, heating the extract obtained in the first step to 200 ℃, and introducing the extract into a chromatographic column for separation, wherein the chromatographic column is any one of an HP-5MS chromatographic column and a DB-WAXUI3 chromatographic column; when the separation is carried out by introducing into a chromatographic column, firstly heating the chromatographic column to 80 ℃ and keeping the temperature for 1min, then heating to 180 ℃ by a program of 6 ℃/min, then heating to 200 ℃ by 1.5 ℃/min, then heating to 270 ℃ by 15 ℃/min, keeping the temperature for 5min, and the separation effect is good.
Thirdly, detecting the solution separated in the second step by a gas chromatograph-mass spectrometer, so as to obtain the molecular content proportion of the detected solution and obtain the optimal mass spectrum parameters of the detected solution;
fourthly, drawing a color pattern and a molecule contained proportion pattern according to the contained molecule type; the pattern drawn in the fourth step must be clear and bright, so that the observation is convenient, the observation effect is better, and the trouble of the user is solved.
Fifthly, inputting the corresponding product name of the drawn information into a computer according to the pattern information drawn in the fourth step;
and sixthly, inputting the name of the product to be inquired into the computer, namely displaying the related information of the product to be inquired, wherein the related information of the product to be inquired in the sixth step comprises encyclopedia information of the contained molecular type, article content related to the molecular type, the product which can be supplied corresponding to the molecular type, supplier information and official data provided by the supplier, and the rechecking inspection of the official data of each brand is realized, the secondary inspection of the data is performed, and the data is diverse, so that a user can conveniently know the condition.
The above description is only for the preferred embodiment of the present invention, but the scope of the present invention is not limited thereto, and any person skilled in the art should be considered to be within the technical scope of the present invention, and the technical solutions and the inventive concepts thereof according to the present invention should be equivalent or changed within the scope of the present invention.
Claims (4)
1. A fragrance molecule content proportion, fragrance molecule color management and spectrum display method of fragrance products uses a gas chromatography-mass spectrometer for component detection, and is characterized by comprising the following steps:
firstly, selecting a sample to be detected for sample treatment: accurately weighing about 0.2-0.3 g of essence into a 15mL colorimetric tube with a plug, adding 0.5-0.7mL of saturated chlorinated solution, diluting to a scale by using an acetonitrile-ethyl acetate extracting solution, wherein the mixing ratio of the acetonitrile-ethyl acetate is 10:90, performing oscillation extraction, taking supernate, filtering the supernate through a microporous filter membrane, and detecting by using an image chromatography-mass spectrometer;
secondly, heating the extract obtained in the first step to 180-200 ℃, and introducing the extract into a chromatographic column for separation, wherein the chromatographic column is any one of an HP-5MS chromatographic column and a DB-WAXUI3 chromatographic column;
thirdly, detecting the solution separated in the second step by a gas chromatograph-mass spectrometer, so as to obtain the molecular content proportion of the detected solution and obtain the optimal mass spectrum parameters of the detected solution;
fourthly, drawing a color pattern and a molecule contained proportion pattern according to the contained molecule type;
fifthly, inputting the corresponding product name of the drawn information into a computer according to the pattern information drawn in the fourth step;
and sixthly, inputting the name of the product to be inquired into the computer, and displaying the related information of the product to be inquired.
2. The fragrance product fragrance molecule content ratio, fragrance molecule color management and map display method of claim 1, wherein in the second step, when introducing into the chromatographic column for separation, the chromatographic column is heated to 75-80 ℃ for 1min, then heated to 180 ℃ by the program of 5-6 ℃ per min, then heated to 200 ℃ by 1-1.5 ℃ per min, and then heated to 260-270 ℃ by 12-15 ℃ per min for 5 min.
3. The fragrance product fragrance molecule content ratio, fragrance molecule color management and map display method of claim 1, wherein the pattern drawn in the fourth step must be clear and bright for easy observation.
4. The fragrance product fragrance molecule content ratio, fragrance molecule color management and spectrum display method of claim 1, wherein the related information of the product to be inquired in the sixth step comprises encyclopedia information of the type of the molecule contained, article content related to the type of the molecule, products available corresponding to the type of the molecule, supplier information and official data provided by the supplier, and the second check of the data is realized by rechecking the official data of each brand.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202010618364.1A CN111812232A (en) | 2020-07-01 | 2020-07-01 | Fragrance product fragrance molecule content proportion, fragrance molecule color management and map display method |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202010618364.1A CN111812232A (en) | 2020-07-01 | 2020-07-01 | Fragrance product fragrance molecule content proportion, fragrance molecule color management and map display method |
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| CN111812232A true CN111812232A (en) | 2020-10-23 |
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| CN202010618364.1A Withdrawn CN111812232A (en) | 2020-07-01 | 2020-07-01 | Fragrance product fragrance molecule content proportion, fragrance molecule color management and map display method |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115876897A (en) * | 2021-09-27 | 2023-03-31 | 汕头海关技术中心 | A method for simultaneous detection of multiple restricted fragrances in cosmetics |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CA2616164A1 (en) * | 2005-07-25 | 2007-02-01 | Metanomics Gmbh | Means and methods for analyzing a sample by means of chromatography-mass spectrometry |
| CN111122747A (en) * | 2019-12-31 | 2020-05-08 | 汕头出入境检验检疫局检验检疫技术中心 | Method for analyzing sensitized aromatic substances in cosmetics |
-
2020
- 2020-07-01 CN CN202010618364.1A patent/CN111812232A/en not_active Withdrawn
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CA2616164A1 (en) * | 2005-07-25 | 2007-02-01 | Metanomics Gmbh | Means and methods for analyzing a sample by means of chromatography-mass spectrometry |
| CN111122747A (en) * | 2019-12-31 | 2020-05-08 | 汕头出入境检验检疫局检验检疫技术中心 | Method for analyzing sensitized aromatic substances in cosmetics |
Non-Patent Citations (2)
| Title |
|---|
| 宁啸骏 等: "气相色谱-质谱联用法测定膏霜类化妆品中10种合成麝香", 《日用化学工业》 * |
| 汤学东 等: "高效液相色谱-串联质谱法测定烟用香精香料中的甲基异噻唑啉酮及其氯代物的含量", 《理化检验(化学分册)》 * |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115876897A (en) * | 2021-09-27 | 2023-03-31 | 汕头海关技术中心 | A method for simultaneous detection of multiple restricted fragrances in cosmetics |
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Application publication date: 20201023 |
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