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CN111229132A - An Improved Fine Powder Catalyst Metering and Dispensing Device - Google Patents

An Improved Fine Powder Catalyst Metering and Dispensing Device Download PDF

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CN111229132A
CN111229132A CN202010112334.3A CN202010112334A CN111229132A CN 111229132 A CN111229132 A CN 111229132A CN 202010112334 A CN202010112334 A CN 202010112334A CN 111229132 A CN111229132 A CN 111229132A
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flange
metering
hole
catalyst
disc
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CN111229132B (en
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张宏
魏兆成
李巍
张文涛
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Dalian University of Technology
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Dalian University of Technology
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/0015Feeding of the particles in the reactor; Evacuation of the particles out of the reactor
    • B01J8/002Feeding of the particles in the reactor; Evacuation of the particles out of the reactor with a moving instrument
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J4/00Feed or outlet devices; Feed or outlet control devices
    • B01J4/001Feed or outlet devices as such, e.g. feeding tubes
    • B01J4/007Feed or outlet devices as such, e.g. feeding tubes provided with moving parts
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J4/00Feed or outlet devices; Feed or outlet control devices
    • B01J4/02Feed or outlet devices; Feed or outlet control devices for feeding measured, i.e. prescribed quantities of reagents

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Filling Or Emptying Of Bunkers, Hoppers, And Tanks (AREA)

Abstract

The utility model provides an improved fine powder form catalyst measurement dosing unit, belongs to machinery, includes middle part flange, bottom flange, filter equipment, spiral agitator, metering element, unloading subassembly, drive shaft, axle supporting component, drive arrangement. Middle part flange device is on bottom flange upper portion, and the bottom flange is split type structure, and filter equipment arranges in middle part flange upper portion, and the spiral agitator is supported and drives rotatoryly by the driveshaft, and its inside centre bore that is equipped with, measurement subassembly from the top down arranges floating cover plate, floating disc, measurement dish, wear-resisting dish in proper order, and the unloading subassembly comprises copper lantern ring, packing, self-aligning bearing, elastic coupling by flange body support shaft subassembly. The invention has compact structure, and reduces the processing difficulty of the bottom flange of a key part while realizing the accurate measurement of the fine powder catalyst. In addition, the influence of the coaxiality error of the driving shaft on the operation of the device is reduced by eliminating the principle error of the coaxiality of the driving shaft and enhancing the adaptability of the operation of the device to the coaxiality error.

Description

一种改进的细粉状催化剂计量配给装置An Improved Fine Powder Catalyst Metering and Dispensing Device

技术领域technical field

本发明属于机械领域,涉及一种改进的细粉状催化剂计量配给装置,主要应用于催化剂精确计量供给的气体烯烃聚合反应中,还涉及一种关键件底部法兰便于制造的催化剂计量配给装置,更涉及一种对驱动轴同轴度误差适应性好的催化剂计量配给装置。The invention belongs to the field of machinery, and relates to an improved fine powder catalyst metering and distributing device, which is mainly used in the gas olefin polymerization reaction in which the catalyst is accurately metered and supplied, and also relates to a catalyst metering and distributing device whose bottom flange of a key part is easy to manufacture, It also relates to a catalyst metering and distributing device with good adaptability to the coaxiality error of the drive shaft.

背景技术Background technique

在涉及大量烯烃聚合反应的石油化工行业,能否长期稳定计量配给催化剂直接决定产品的质量和持续生产率。国内用于连续聚合反应的催化剂配给装置,已基本实现催化剂的计量供给,但装置关键件加工难度高、催化剂计量供给持续性差仍是两大技术性难题。In the petrochemical industry involving a large number of olefin polymerization reactions, the long-term stable metering of catalysts directly determines product quality and sustained productivity. The domestic catalyst distribution device for continuous polymerization has basically realized the metered supply of catalyst, but the high processing difficulty of key parts of the device and the poor continuity of catalyst metered supply are still two major technical problems.

200610064918.8专利,公开了一种催化剂配给装置,该装置结构紧凑、装拆方便并可实现催化剂的精确调节。但装置关键件底部法兰3要求加工精度高成为其推广使用的一大障碍。其结构如图1所示。The 200610064918.8 patent discloses a catalyst dispensing device, which has a compact structure, is easy to assemble and disassemble, and can realize precise adjustment of the catalyst. However, the high machining accuracy required for the bottom flange 3 of the key part of the device has become a major obstacle to its popularization and use. Its structure is shown in Figure 1.

200780045808.X专利,公开了一种国内广泛使用的进口催化剂配给装置,其通过旋转的螺旋搅拌器203带动计量盘205旋转,实现催化剂的计量供给,螺旋搅拌器203由与其配合的驱动轴217传递扭矩。但装置螺旋搅拌器203、计量盘205两者的驱动方式存在缺陷。其结构如图2所示。The 200780045808.X patent discloses an imported catalyst distribution device widely used in China, which drives the metering disc 205 to rotate through the rotating screw agitator 203 to realize the metering supply of the catalyst, and the screw agitator 203 is transmitted by the drive shaft 217 matched with it. torque. However, there are defects in the driving methods of the screw agitator 203 and the metering disc 205 . Its structure is shown in Figure 2.

(1)搅拌器203同时传递扭矩和切向力给计量盘205,附加的切向力会导致驱动轴217同轴度误差不断增大。(1) The agitator 203 transmits torque and tangential force to the metering disc 205 at the same time, and the additional tangential force will cause the coaxiality error of the drive shaft 217 to increase continuously.

(2)随着计量盘与非旋转组件接触面215和接触面503低摩擦材料层的磨损,搅拌器203传递扭矩增大;因轴向密封件227为弹性元件,因此同轴度误差引起的驱动轴217的角度倾斜会使驱动轴217装配的安全销承受多余的剪切力;不断增大的传递扭矩、多余的剪切力会使安全销过早过载剪断,使固体供给装置提前失去安全保护。(2) With the wear of the low-friction material layer of the contact surface 215 and the contact surface 503 of the metering disc and the non-rotating component, the torque transmitted by the agitator 203 increases; because the axial seal 227 is an elastic element, the concentricity error is caused by The inclined angle of the drive shaft 217 will cause the safety pin assembled with the drive shaft 217 to bear excess shearing force; the increasing transmission torque and excess shearing force will cause the safety pin to be prematurely overloaded and cut off, causing the solid supply device to lose its safety in advance. Protect.

不断增大的同轴度误差引发的弹性元件盘根227磨损、安全销的过早剪断将直接降低装置的长期运转可靠性。The wear of the elastic element packing 227 and the premature shearing of the safety pin caused by the ever-increasing coaxiality error will directly reduce the long-term operation reliability of the device.

由此可见,降低催化剂计量配给装置关键件加工难度、提升装置长期运转可靠性是当前固体催化剂加料装置的两大发展趋势。为降低装置关键件底部法兰的加工难度并同时提升催化剂持续计量配给的能力,本发明提出了一种更适合国产化推广的改进的细粉状催化剂计量配给装置。It can be seen that reducing the processing difficulty of the key parts of the catalyst metering and dispensing device and improving the long-term operation reliability of the device are the two major development trends of the current solid catalyst feeding device. In order to reduce the processing difficulty of the bottom flange of the key parts of the device and at the same time improve the ability of continuous metering and distribution of the catalyst, the present invention proposes an improved metering and distribution device for fine powder catalyst which is more suitable for localization and promotion.

发明内容SUMMARY OF THE INVENTION

针对现有技术中存在的难题。本发明提供一种改进的催化剂计量配给装置,其降低了关键件底部法兰的加工难度,通过改进螺旋搅拌器、计量盘的驱动结构以及改善传动轴的支撑提升了装置运转对驱动轴同轴度误差的适应性,由此增强了催化剂持续计量配给的能力。For the problems existing in the prior art. The invention provides an improved catalyst metering and distributing device, which reduces the processing difficulty of the bottom flange of key parts, improves the drive structure of the screw agitator, the metering disc and improves the support of the drive shaft, and improves the coaxiality of the device operation to the drive shaft. This improves the ability of the catalyst to continue metering.

为了达到上述目的,本发明采用的技术方案为:In order to achieve the above object, the technical scheme adopted in the present invention is:

一种改进的细粉状催化剂计量配给装置,包括中部法兰1、底部法兰2、过滤装置3、螺旋搅拌器5、计量组件6、下料组件9、驱动轴12、轴支撑组件、驱动装置。An improved fine powder catalyst metering and distributing device, comprising a middle flange 1, a bottom flange 2, a filter device 3, a screw agitator 5, a metering component 6, a blanking component 9, a drive shaft 12, a shaft support component, a drive device.

所述的中部法兰1装置于底部法兰2的上部,是催化剂的中间过渡容器。The middle flange 1 is installed on the upper part of the bottom flange 2 and is an intermediate transition container for the catalyst.

所述的底部法兰2为分体式结构,由吊耳201、法兰本体202、轴承固定板203、微调螺钉204、螺柱205、下支板206组合装配而成。具体结构为:所述吊耳201对称焊接于法兰本体202圆周表面;所述法兰本体202开有两个下料孔;所述轴承固定板203布置于底部法兰2中部,轴承固定板203与螺柱205实现孔轴配合;除轴承固定板203通过微调螺钉204保持合适的轴向位置外,其余各部分均焊为一体。The bottom flange 2 is a split structure, which is assembled and assembled by a lifting lug 201 , a flange body 202 , a bearing fixing plate 203 , a fine adjustment screw 204 , a stud 205 , and a lower support plate 206 . The specific structure is as follows: the lifting lugs 201 are symmetrically welded to the circumferential surface of the flange body 202; the flange body 202 is provided with two blanking holes; the bearing fixing plate 203 is arranged in the middle of the bottom flange 2, and the bearing fixing plate 203 and the stud 205 realize hole-shaft fit; except that the bearing fixing plate 203 maintains a proper axial position through the fine-tuning screw 204, the rest of the parts are welded into one.

所述的过滤装置3布置于中部法兰1上部。The filter device 3 is arranged on the upper part of the middle flange 1 .

所述的螺旋搅拌器5由驱动轴12支撑并带动旋转,其底平面与耐磨盘604留有适当间隙;螺旋搅拌器5内部设有中心孔,其内孔上部与驱动轴12直接配合,其内孔下部为一段锥形孔。其下部圆周方向有2个用于存放驱动销7的销孔。对应地,与螺旋搅拌器5下部配合的计量盘603,其上部开有2个容纳驱动销7的凹槽6031。The screw agitator 5 is supported and driven to rotate by the drive shaft 12, and there is an appropriate gap between the bottom plane and the wear-resistant disc 604; the screw agitator 5 is provided with a central hole inside, and the upper part of the inner hole is directly matched with the drive shaft 12, The lower part of the inner hole is a section of conical hole. There are two pin holes for storing the drive pins 7 in the circumferential direction of the lower part. Correspondingly, two grooves 6031 for accommodating the driving pins 7 are formed in the upper part of the metering plate 603 matched with the lower part of the screw agitator 5 .

所述的计量组件6包括浮动盖板601、浮动盘602、计量盘603、耐磨盘604。并从上到下依次布置,除计量盘603外,其余组件均为非旋转组件。具体结构为:所述浮动盖板601与法兰本体202固定;浮动盘602下表面覆有非金属耐磨材料;浮动盖板601与浮动盘602之间设有弹簧自动补偿装置,可保证运转过程中浮动盘602与计量盘603紧密贴合;所述计量盘603由螺旋搅拌器5通过驱动销7带动旋转;所述耐磨盘604装置于法兰本体202底部,其上表面覆有非金属耐磨材料。The metering assembly 6 includes a floating cover plate 601 , a floating disk 602 , a metering disk 603 , and a wear-resistant disk 604 . They are arranged in sequence from top to bottom. Except for the metering disc 603, the other components are non-rotating components. The specific structure is as follows: the floating cover plate 601 is fixed with the flange body 202; the lower surface of the floating plate 602 is covered with non-metallic wear-resistant materials; a spring automatic compensation device is arranged between the floating cover plate 601 and the floating plate 602, which can ensure the operation During the process, the floating disk 602 is closely attached to the metering disk 603; the metering disk 603 is driven to rotate by the screw agitator 5 through the driving pin 7; the wear-resistant disk 604 is installed at the bottom of the flange body 202, and its upper surface is covered with Metal wear-resistant material.

所述的下料组件9由法兰本体202支撑,装设于法兰本体202下料孔处。The blanking assembly 9 is supported by the flange body 202 and installed at the blanking hole of the flange body 202 .

所述的驱动轴12为两段阶梯轴,轴肩位于驱动轴中部,用于确定锥形导套8轴向位置。驱动轴12依次穿过螺旋搅拌器5内孔、法兰本体202中心孔、轴承13内孔,在末端通过联轴器14与减速机15输出轴连接,驱动轴12尾端设有存放安全销4的贯通销孔。The drive shaft 12 is a two-stage stepped shaft, and the shaft shoulder is located in the middle of the drive shaft to determine the axial position of the tapered guide sleeve 8 . The drive shaft 12 passes through the inner hole of the screw agitator 5, the central hole of the flange body 202, and the inner hole of the bearing 13 in sequence, and is connected to the output shaft of the reducer 15 through the coupling 14 at the end. The end of the drive shaft 12 is provided with a storage safety pin 4 through pin holes.

所述的轴支撑组件包括铜套环10、盘根11、轴承13、联轴器14。其中:所述铜套环10、盘根11装设于法兰本体202中心孔,并与驱动轴12形成过盈配合;所述轴承13安放在轴承固定板203上,所述联轴器上半部分加工有用于存放安全销4的U形槽141。The shaft support assembly includes a copper collar 10 , a packing 11 , a bearing 13 , and a coupling 14 . Wherein: the copper collar 10 and the packing 11 are installed in the center hole of the flange body 202, and form an interference fit with the drive shaft 12; the bearing 13 is placed on the bearing fixing plate 203, and the coupling The half is machined with a U-shaped groove 141 for storing the safety pin 4 .

所述的驱动装置包括安全销4、驱动销7、减速机15、电机16。所述安全销4装配在驱动轴12末端的贯通销孔内,可起到过载保护作用;驱动销7与螺旋搅拌器5下部圆柱体的销孔配合;减速机15和驱动轴12通过联轴器14、安全销4实现扭矩传递。所述电机16与减速机15连接。The driving device includes a safety pin 4 , a driving pin 7 , a reducer 15 , and a motor 16 . The safety pin 4 is assembled in the through pin hole at the end of the drive shaft 12, which can play an overload protection function; the drive pin 7 is matched with the pin hole of the lower cylinder of the screw agitator 5; the reducer 15 and the drive shaft 12 pass through the coupling shaft The actuator 14 and the safety pin 4 realize torque transmission. The motor 16 is connected to the reducer 15 .

进一步地,为在催化剂计量配给准确的同时降低底部法兰2的加工难度,所述底部法兰2各组成部件,法兰本体202由高精度机床保证加工精度,可保证其上下表面的平行度,以及下表面与下料组件9接触部分的局部粗糙度,其余组件按经济精度加工。装置试车前各部分简单装配,试车时根据运转需要调节底部法兰2各部分装配。所述轴承固定板203每个侧面各钻有两个螺纹孔,螺纹孔邻近竖直棱边布置;所述微调螺钉204与轴承固定板203侧壁的螺纹孔配合;所述螺柱205与轴承固定板203配合性质为间隙配合;通过调节微调螺钉204,可避免轴承13卡死,保证驱动轴12的回转精度。通过调节微调螺钉204确定组件合适位置后,再精确固定、焊为一体。Further, in order to reduce the processing difficulty of the bottom flange 2 while the catalyst metering is accurate, each component of the bottom flange 2 and the flange body 202 are processed by a high-precision machine tool to ensure the processing accuracy, which can ensure the parallelism of its upper and lower surfaces. , and the local roughness of the lower surface in contact with the blanking component 9, and the remaining components are processed with economical precision. Each part of the device is simply assembled before the test run, and the assembly of each part of the bottom flange 2 is adjusted according to the operation needs during the test run. Two threaded holes are drilled on each side of the bearing fixing plate 203, and the threaded holes are arranged adjacent to the vertical edges; the fine adjustment screw 204 is matched with the threaded hole on the side wall of the bearing fixing plate 203; the stud 205 is connected to the bearing The fitting property of the fixing plate 203 is clearance fit; by adjusting the fine adjustment screw 204 , the bearing 13 can be prevented from being stuck and the rotation accuracy of the drive shaft 12 can be ensured. After the proper position of the assembly is determined by adjusting the fine adjustment screw 204, it is then precisely fixed and welded into one.

进一步地,为避免现有技术中安全销4因承受多余剪切力而过早折断,所述安全销4从贯通销孔的伸出部分在U形槽141的中部。Further, in order to prevent the safety pin 4 from being prematurely broken due to excessive shearing force in the prior art, the protruding part of the safety pin 4 from the through pin hole is in the middle of the U-shaped groove 141 .

进一步地,为消除现有技术中驱动轴12相对于底部法兰2中心孔同轴度的原理误差。所述螺旋搅拌器5下部圆周体的销孔为对称销孔,对应地,与螺旋搅拌器5下部配合的计量盘603上部凹槽6031为对称式。此外,所述螺旋搅拌器5内部锥形孔与锥形导套8形成同轴度精度高的锥面配合。Further, in order to eliminate the principle error of the coaxiality of the drive shaft 12 relative to the central hole of the bottom flange 2 in the prior art. The pin holes of the lower circumferential body of the spiral agitator 5 are symmetrical pin holes, and correspondingly, the upper groove 6031 of the metering plate 603 matched with the lower part of the spiral agitator 5 is symmetrical. In addition, the inner conical hole of the spiral stirrer 5 and the conical guide sleeve 8 form a conical surface with high coaxiality precision.

进一步地,为增强装置运转对同轴度误差的适应性。所述轴承13为调心轴承,可对驱动轴12的同轴度误差进行补偿;所述联轴器14为梅花形弹性联轴器,可补偿驱动轴12与减速机15输出轴的相对偏移。Further, in order to enhance the adaptability of the device operation to the coaxiality error. The bearing 13 is a self-aligning bearing, which can compensate the coaxiality error of the drive shaft 12; the coupling 14 is a plum-shaped elastic coupling, which can compensate the relative deviation of the drive shaft 12 and the output shaft of the reducer 15. shift.

相比现有技术,本发明的有益效果在于:所述的催化剂计量配给装置结构紧凑,在实现细粉状催化剂精确计量的同时降低了关键件底部法兰的加工难度。此外,通过消除驱动轴同轴度原理误差和增强装置运转对同轴度误差的适应性,大大降低了驱动轴同轴度误差对于装置运转的影响。Compared with the prior art, the present invention has the beneficial effects that the catalyst metering and distributing device has a compact structure, which reduces the processing difficulty of the bottom flange of the key part while realizing the precise metering of the fine powder catalyst. In addition, by eliminating the principle error of the coaxiality of the drive shaft and enhancing the adaptability of the operation of the device to the coaxiality error, the influence of the coaxiality error of the drive shaft on the operation of the device is greatly reduced.

附图说明Description of drawings

图1为从200610064918.8专利复制的现有技术的催化剂计量配给装置局部剖视示意图;Fig. 1 is the partial cross-sectional schematic diagram of the catalyst metering and dispensing device of the prior art copied from the 200610064918.8 patent;

图2为从200780045808.X专利复制的现有技术的催化剂计量配给装置的剖面图;Figure 2 is a cross-sectional view of a prior art catalyst metering and dispensing device copied from the 200780045808.X patent;

图3为本发明结构总体局部剖视示意图;FIG. 3 is a schematic partial cross-sectional view of the overall structure of the present invention;

图4为计量部分放大剖面图;Figure 4 is an enlarged cross-sectional view of the metering part;

图5为分体式底部法兰结构示意图;Figure 5 is a schematic diagram of the split bottom flange structure;

图6为轴承固定板断面图;Figure 6 is a sectional view of the bearing fixing plate;

图7为剪切销与U形槽配合示意图;Figure 7 is a schematic diagram of the cooperation between the shear pin and the U-shaped groove;

图8(a)为计量盘的主视图;Figure 8(a) is a front view of the metering disc;

图8(b)为计量盘的俯视图;Figure 8(b) is a top view of the metering plate;

图中:1中部法兰;2底部法兰,201吊耳,202法兰本体,203轴承固定板,204微调螺钉,205螺柱,206下支板;3过滤装置;4安全销;5螺旋搅拌器;6计量组件,601浮动盖板,602浮动盘,603计量盘,6031凹槽,604耐磨盘;7驱动销;8锥形导套;9下料组件;10铜套环;11盘根;12驱动轴;13轴承;14联轴器,141 U形槽;15减速机;16电机。In the picture: 1 middle flange; 2 bottom flange, 201 lifting lugs, 202 flange body, 203 bearing fixing plate, 204 fine adjustment screw, 205 stud, 206 lower support plate; 3 filter device; 4 safety pin; 5 screw Agitator; 6 metering components, 601 floating cover plate, 602 floating disc, 603 metering disc, 6031 groove, 604 wear-resistant disc; 7 drive pins; 8 conical guide bushes; 9 blanking components; 10 copper collars; 11 Packing; 12 drive shafts; 13 bearings; 14 couplings, 141 U-slots; 15 reducers; 16 motors.

具体实施方式Detailed ways

为了进一步解释本发明的技术方案,下面结合附图来对本发明进行详细阐述。In order to further explain the technical solutions of the present invention, the present invention will be described in detail below with reference to the accompanying drawings.

如图1所示,一种改进的细粉状催化剂计量配给装置主要由中部法兰1、底部法兰2、过滤装置3、螺旋搅拌器5、计量组件6、下料组件9、驱动轴12、轴支撑组件、驱动装置组成。As shown in Figure 1, an improved fine powder catalyst metering and distributing device is mainly composed of a middle flange 1, a bottom flange 2, a filter device 3, a screw agitator 5, a metering component 6, a blanking component 9, and a drive shaft 12. , shaft support components, drive components.

所述中部法兰1是催化剂的中间过渡容器,装置于底部法兰2的上部。The middle flange 1 is an intermediate transition vessel for the catalyst, and is installed on the upper part of the bottom flange 2 .

所述底部法兰2为分体式结构,由吊耳201、法兰本体202、轴承固定板203、微调螺钉204、螺柱205、下支板206组合装配而成。具体结构为:所述吊耳201对称焊接于法兰本体202圆周表面;所述法兰本体202开有两个下料孔,当计量盘601上的计量孔与下料孔相对时,催化剂在重力作用下从计量孔掉落到下料组件9内。为保证催化剂计量准确,法兰本体202由高精度机床保证加工精度,由此保证其上下表面的平行度,以及下表面与下料组件接触部分的局部粗糙度,其余各组件按经济精度加工;所述轴承固定板203设置在底部法兰2中部,其侧壁钻有螺纹孔(4个侧壁共钻有8个螺纹孔),螺纹孔邻近竖直棱边布置;所述微调螺钉204与轴承固定板203侧壁的螺纹孔配合;所述螺柱205与轴承固定板203配合性质为间隙配合,以实现微调螺钉204可调节;除轴承固定板203通过微调螺钉204保持合适的轴向位置外,其余各部分均焊为一体,焊缝位置参见图5。The bottom flange 2 is a split structure, which is assembled and assembled by a lifting lug 201 , a flange body 202 , a bearing fixing plate 203 , a fine adjustment screw 204 , a stud 205 , and a lower support plate 206 . The specific structure is as follows: the lifting lugs 201 are symmetrically welded to the circumferential surface of the flange body 202; the flange body 202 is provided with two feeding holes. Under the action of gravity, it falls into the unloading assembly 9 from the metering hole. In order to ensure the accurate measurement of the catalyst, the flange body 202 is processed by a high-precision machine tool to ensure the processing accuracy, thereby ensuring the parallelism of its upper and lower surfaces, and the local roughness of the contact part between the lower surface and the blanking component, and the remaining components are processed with economic precision; The bearing fixing plate 203 is arranged in the middle of the bottom flange 2, and its side walls are drilled with threaded holes (4 side walls have 8 threaded holes in total), and the threaded holes are arranged adjacent to the vertical edges; The threaded holes on the side wall of the bearing fixing plate 203 are matched; the stud 205 and the bearing fixing plate 203 are matched in a clearance fit, so that the fine-tuning screw 204 can be adjusted; In addition, the rest of the parts are welded as a whole, and the position of the welding seam is shown in Figure 5.

所述的过滤装置3布置于中部法兰1上部,可防止大颗粒催化剂堵塞计量组件。The filtering device 3 is arranged on the upper part of the middle flange 1, which can prevent the large particle catalyst from clogging the metering component.

具体地,过滤能力大于催化剂加料速率。Specifically, the filtration capacity is greater than the catalyst feed rate.

所述的螺旋搅拌器5由驱动轴12支撑并带动旋转,主要起松动催化剂作用。其底平面与耐磨盘604留有适当间隙;其内孔上部与驱动轴12直接配合;其内部中心孔下部为一段锥形孔,该锥形孔与锥形导套8形成锥面配合,利用锥面配合同轴度精度高的特点,可减小运转过程中驱动轴12的同轴度误差;其下部圆周方向设于存放驱动销7的2个对称销孔。驱动销7对称布置可消除装置运转时驱动轴12相对于底部法兰2中心孔同轴度的原理误差。The screw agitator 5 is supported by the drive shaft 12 and driven to rotate, and mainly plays the role of loosening the catalyst. There is a proper gap between the bottom plane and the wear-resistant disc 604; the upper part of the inner hole is directly matched with the drive shaft 12; the lower part of the inner center hole is a section of tapered hole, and the tapered hole and the tapered guide sleeve 8 form a tapered fit, The coaxiality error of the drive shaft 12 during operation can be reduced by utilizing the characteristics of the high precision of the conical surface matching the coaxiality; The symmetrical arrangement of the drive pins 7 can eliminate the principle error of the coaxiality of the drive shaft 12 relative to the central hole of the bottom flange 2 when the device is running.

所述的计量组件6包括浮动盖板601、浮动盘602、计量盘603、耐磨盘604。并从上到下依次布置,除计量盘603外,其余组件均为非旋转组件。其中:浮动盖板601与法兰本体202固定为一体;浮动盘602下表面覆有耐磨材料;浮动盖板601与浮动盘602之间设有弹簧自动补偿装置,可使运转过程中浮动盘602与计量盘603紧密贴合,避免催化剂强制加料现象;计量盘603由螺旋搅拌器5带动旋转,其上部对称开有2个容纳驱动销7的凹槽6031;耐磨盘604固定于法兰本体202底部,其与计量盘603下表面接触面覆有非金属耐磨材料。The metering assembly 6 includes a floating cover plate 601 , a floating disk 602 , a metering disk 603 , and a wear-resistant disk 604 . They are arranged in sequence from top to bottom. Except for the metering disc 603, the other components are non-rotating components. Among them: the floating cover plate 601 and the flange body 202 are fixed as a whole; the lower surface of the floating plate 602 is covered with wear-resistant materials; a spring automatic compensation device is arranged between the floating cover plate 601 and the floating plate 602, which can make the floating plate 602 during operation. 602 is closely attached to the metering plate 603 to avoid the forced feeding of catalyst; the metering plate 603 is driven to rotate by the screw agitator 5, and the upper part of the metering plate 603 is symmetrically opened with two grooves 6031 for accommodating the driving pins 7; the wear-resistant plate 604 is fixed on the flange The bottom of the main body 202 is covered with a non-metal wear-resistant material on its contact surface with the lower surface of the metering disc 603 .

所述的下料组件9由法兰本体202支撑,装设于法兰本体202下料孔处。可带动催化剂连续进入反应容器。The blanking assembly 9 is supported by the flange body 202 and installed at the blanking hole of the flange body 202 . The catalyst can be driven into the reaction vessel continuously.

所述的驱动轴12为两段阶梯轴,轴肩位于驱动轴中部,可确定锥形导套8的轴向位置。驱动轴12上部支撑有螺旋搅拌器,并依次穿过螺旋搅拌器5内孔、法兰本体202中心孔,在中部由轴承13支撑,在末端通过联轴器14与减速机15输出轴连接,驱动轴12尾端设有存放安全销4的贯通销孔。The drive shaft 12 is a two-stage stepped shaft, and the shaft shoulder is located in the middle of the drive shaft, which can determine the axial position of the tapered guide sleeve 8 . The upper part of the drive shaft 12 is supported with a helical agitator, and passes through the inner hole of the helical agitator 5 and the center hole of the flange body 202 in turn, is supported by the bearing 13 in the middle, and is connected to the output shaft of the reducer 15 through the coupling 14 at the end, The rear end of the drive shaft 12 is provided with a through pin hole for storing the safety pin 4 .

所述的轴支撑组件包括铜套环10、盘根11、轴承13、联轴器14。其中:铜套环10、盘根11装设于法兰本体202中心孔,并与驱动轴12形成过盈配合;轴承13为调心轴承,安放在轴承固定板203上,其调心性能可对驱动轴12同轴度误差进行补偿;联轴器14上半部分加工有用于存放安全销4的U形槽141。The shaft support assembly includes a copper collar 10 , a packing 11 , a bearing 13 , and a coupling 14 . Among them: the copper collar 10 and the packing 11 are installed in the center hole of the flange body 202, and form an interference fit with the drive shaft 12; the bearing 13 is a self-aligning bearing, which is placed on the bearing fixing plate 203, and its self-aligning performance can be improved Compensate for the coaxiality error of the drive shaft 12 ; the upper half of the coupling 14 is machined with a U-shaped groove 141 for storing the safety pin 4 .

所述的驱动装置包括安全销4、驱动销7、减速机15、电机16。装配在驱动轴12末端贯通销孔内的安全销4起过载保护作用,其伸出部分位于U形槽141中部,以保证安全销4仅受纯扭矩,避免承受多余剪切力;驱动销7与螺旋搅拌器5下部圆柱体的销孔配合;减速机15和驱动轴12通过联轴器14、安全销4实现扭矩传递。The driving device includes a safety pin 4 , a driving pin 7 , a reducer 15 , and a motor 16 . The safety pin 4 assembled in the through pin hole at the end of the drive shaft 12 plays an overload protection role, and its protruding part is located in the middle of the U-shaped groove 141 to ensure that the safety pin 4 only receives pure torque and avoids excessive shear force; the drive pin 7 It is matched with the pin hole of the lower cylinder of the screw agitator 5; the reducer 15 and the drive shaft 12 realize torque transmission through the coupling 14 and the safety pin 4.

具体地,通过调节微调螺钉204,可避免轴承13卡死,保证驱动轴12的回转精度。所述调心轴承13的内圈、球、保持架可相对外圈进行一定角度的旋转,具有自动调心能力,其调心能力可以对同轴度误差进行补偿。参见图5,因轴承固定板203与螺柱205实现的孔轴配合均为间隙配合,参见图6,因此可通过调节轴承固定板203侧壁的8个微调螺钉204,调节调心轴承13内外圈的相对倾斜程度,使内外圈相对倾斜程度在允许范围内,避免轴承卡死,以实现调心轴承13的自动调心功能,最终保证驱动轴12的回转精度。Specifically, by adjusting the fine adjustment screw 204, the bearing 13 can be prevented from being stuck, and the rotation accuracy of the drive shaft 12 can be ensured. The inner ring, the ball and the cage of the self-aligning bearing 13 can rotate at a certain angle relative to the outer ring, and have the ability of self-aligning, and the self-aligning ability can compensate the coaxiality error. Referring to FIG. 5 , because the hole-shaft fit achieved by the bearing fixing plate 203 and the stud 205 is a clearance fit, referring to FIG. 6 , the inner and outer parts of the self-aligning bearing 13 can be adjusted by adjusting the eight fine-tuning screws 204 on the side wall of the bearing fixing plate 203 The relative inclination of the rings keeps the relative inclination of the inner and outer rings within the allowable range to avoid the bearing from being stuck, so as to realize the self-aligning function of the self-aligning bearing 13 and finally ensure the rotation accuracy of the drive shaft 12 .

优选地,所述联轴器14为梅花形弹性联轴器,其通过凸爪与弹性元件之间的挤压传递动力,弹性元件产生的弹性变形可补偿连接两轴相对偏移,实现减振缓冲。因此该型联轴器可削弱减速机15输出轴与驱动轴12相对偏移对驱动轴12同轴度误差的影响。Preferably, the coupling 14 is a plum-shaped elastic coupling, which transmits power through the extrusion between the convex claw and the elastic element, and the elastic deformation generated by the elastic element can compensate for the relative offset of the two connecting shafts, so as to reduce vibration buffer. Therefore, this type of coupling can weaken the influence of the relative offset between the output shaft of the reducer 15 and the drive shaft 12 on the coaxiality error of the drive shaft 12 .

可知,本发明完全具备细粉状催化剂精确计量配给能力。装置运转时,催化剂在重力作用下,经过滤装置3进入中部法兰1内,驱动装置带动螺旋搅拌器5旋转,使催化剂落到计量盘603上,在浮动盖板601和浮动盘602作用下,催化剂填满计量盘603的每个计量孔,随着螺旋搅拌器5带动计量盘603不断旋转,计量孔中的催化剂通过底部法兰2上的下料孔进入下料组件9,最后供给反应容器。It can be seen that the present invention is fully capable of accurately metering and distributing the fine powder catalyst. When the device is running, the catalyst enters the middle flange 1 through the filter device 3 under the action of gravity, and the driving device drives the screw agitator 5 to rotate, so that the catalyst falls on the metering plate 603. Under the action of the floating cover plate 601 and the floating plate 602 , the catalyst fills each metering hole of the metering disc 603, and as the screw agitator 5 drives the metering disc 603 to rotate continuously, the catalyst in the metering hole enters the blanking component 9 through the blanking hole on the bottom flange 2, and finally supplies the reaction container.

又知,底部法兰2采用分体式结构,用较低的零件精度、很少的装配劳动量,降低了底部法兰2的加工难度,达到了配给装置正常运转所需的装配精度。并可通过调节微调螺钉204,避免轴承13卡死,保证驱动轴12的回转精度。It is also known that the bottom flange 2 adopts a split structure, which reduces the processing difficulty of the bottom flange 2 and achieves the assembly accuracy required for the normal operation of the dispensing device with lower part precision and less assembly labor. The fine adjustment screw 204 can be adjusted to prevent the bearing 13 from being stuck and ensure the rotation accuracy of the drive shaft 12 .

再知,由于在梅花形弹性联轴器14的上半部分加工有U形槽141,安全销4设置在U形槽141的中部,且直接与U形槽141侧壁接触,使安全销4在传递扭矩的过程中不会因驱动轴12的同轴度误差承受多余的轴向力,避免了现有技术中安全销4存在的过载折断现象。通过改进螺旋搅拌器5和计量盘603之间的驱动结构,加之,锥形导套8与螺旋搅拌器5锥形孔形成的锥面配合具有同轴度精度高的特点,消除了现有技术中驱动轴12相对于底部法兰2中心孔同轴度的原理误差;通过采用调心轴承13和梅花形弹性联轴器14,改善了驱动轴12的支撑,提升了催化剂配给装置对驱动轴12同轴度误差的适应能力。从而,大大减弱驱动轴同轴度误差对装置运转的影响。Furthermore, since the U-shaped groove 141 is processed in the upper half of the plum-shaped elastic coupling 14, the safety pin 4 is arranged in the middle of the U-shaped groove 141, and directly contacts the side wall of the U-shaped groove 141, so that the safety pin 4 In the process of torque transmission, excess axial force will not be borne due to the coaxiality error of the drive shaft 12, which avoids the overload breaking phenomenon of the safety pin 4 in the prior art. By improving the driving structure between the screw agitator 5 and the metering disc 603, and in addition, the conical surface of the conical guide sleeve 8 and the conical surface formed by the conical hole of the screw agitator 5 have the characteristics of high coaxiality accuracy, eliminating the prior art. The principle error of the coaxiality of the middle drive shaft 12 relative to the central hole of the bottom flange 2; by using the self-aligning bearing 13 and the plum-shaped elastic coupling 14, the support of the drive shaft 12 is improved, and the catalyst distribution device to the drive shaft is improved. 12 The adaptability of the coaxiality error. Therefore, the influence of the coaxiality error of the drive shaft on the operation of the device is greatly reduced.

本发明在满足装置运转需求的情况下通过分体式加工降低了关键件底部法兰加工难度;通过改进螺旋搅拌器和计量盘的驱动结构,消除驱动轴相对于底部法兰中心孔的原理性误差;通过改变安全销的放置方式,避免安全销的过早剪断;轴支撑组件改善驱动轴支撑,提升装置对驱动轴同轴度误差的适应性。综合来看,本发明有利于增强催化剂计量配给的持续性。The invention reduces the difficulty of processing the bottom flange of key parts through split processing under the condition of meeting the operation requirements of the device; and eliminates the principle error of the driving shaft relative to the center hole of the bottom flange by improving the driving structure of the screw agitator and the metering plate ; By changing the placement method of the safety pin, the premature shearing of the safety pin is avoided; the shaft support assembly improves the support of the drive shaft, and the adaptability of the lifting device to the coaxiality error of the drive shaft. Taken together, the present invention is beneficial for enhancing the sustainability of catalyst dosing.

以上所述实施例仅表达本发明的实施方式,但并不能因此而理解为对本发明专利的范围的限制,应当指出,对于本领域的技术人员来说,在不脱离本发明构思的前提下,还可以做出若干变形和改进,这些均属于本发明的保护范围。The above-mentioned embodiments only represent the embodiments of the present invention, but should not be construed as a limitation on the scope of the present invention. It should be pointed out that for those skilled in the art, without departing from the concept of the present invention, Several modifications and improvements can also be made, which all belong to the protection scope of the present invention.

Claims (5)

1. An improved metering and distributing device for fine powdery catalyst, wherein a middle flange (1) is arranged at the upper part of a bottom flange (2) and is a middle transition container for the catalyst, a filtering device (3) is arranged at the upper part of the middle flange (1), and a blanking assembly (9) is supported by the bottom flange (2); the device is characterized by also comprising a bottom flange (2), a spiral stirrer (5), a metering assembly (6), a driving shaft (12), a shaft support assembly and a driving device;
the middle flange (1) is arranged at the upper part of the bottom flange (2) and is a middle transition container of the catalyst;
the bottom flange (2) is of a split structure and is formed by assembling lifting lugs (201), a flange body (202), a bearing fixing plate (203), fine adjustment screws (204) and studs (205); the lifting lugs (201) are symmetrically arranged on the circumferential surface of the flange body (202); the flange body (202) is provided with two discharging holes; the bearing fixing plate (203) is arranged in the middle of the bottom flange (2), and the bearing fixing plate (203) is matched with the stud (205) in a hole-shaft mode; all the parts except the bearing fixing plate (203) are welded into a whole except that the proper axial position is kept by the fine adjustment screw (204); the blanking assembly (9) is supported by the flange body (202) and is arranged at a blanking hole of the flange body (202);
the filtering device (3) is arranged at the upper part of the middle flange (1);
the spiral stirrer (5) is supported by a driving shaft (12) and is driven to rotate, and a proper gap is reserved between the bottom plane of the spiral stirrer and the wear-resistant disc (604); a central hole is arranged in the spiral stirrer (5), the upper part of the central hole is directly matched with the driving shaft (12), the lower part of the central hole is a section of conical hole, and the conical hole and the conical guide sleeve (8) form conical surface matching with high coaxiality and precision; 2 pin holes for storing the driving pin (7) are symmetrically formed in the circumferential direction of the lower part of the spiral stirrer (5); correspondingly, a measuring disc (603) matched with the lower part of the spiral stirrer (5) is provided with 2 symmetrical grooves (6031) for accommodating the driving pins (7) at the upper part;
the metering assembly (6) comprises a floating cover plate (601), a floating disc (602), a metering disc (603) and a wear-resisting disc (604); the components are arranged from top to bottom in sequence, and except the metering disc (603), the other components are non-rotating components; the floating cover plate (601) is fixed with the flange body (202); the lower surface of the floating disc (602) is coated with non-metallic wear-resistant material; a spring automatic compensation device is arranged between the floating cover plate (601) and the floating disc (602) and is used for ensuring that the floating disc (602) is tightly attached to the metering disc (603) in the operation process; the metering disc (603) is driven to rotate by a spiral stirrer (5) through a driving pin (7); the wear-resistant disc (604) is arranged at the bottom of the flange body (202), and the upper surface of the wear-resistant disc is coated with a non-metallic wear-resistant material;
the driving shaft (12) is provided with two sections of stepped shafts, and a shaft shoulder is positioned in the middle of the driving shaft and used for determining the axial position of the conical guide sleeve (8); a driving shaft (12) sequentially penetrates through an inner hole of the spiral stirrer (5), a central hole of the flange body (202) and an inner hole of the bearing (13), the tail end of the driving shaft is connected with an output shaft of the speed reducer (15) through a coupler (14), and a through pin hole for storing a safety pin (4) is formed in the tail end of the driving shaft (12);
the shaft support assembly comprises a copper lantern ring (10), a packing (11), a bearing (13) and a coupling (14); the copper lantern ring (10) and the packing (11) are arranged in a center hole of the flange body (202) and form interference fit with the driving shaft (12); the bearing (13) is placed on the bearing fixing plate (203), and a U-shaped groove (141) for storing the safety pin (4) is processed at the upper half part of the coupler;
the driving device comprises a safety pin (4), a driving pin (7), a speed reducer (15) and a motor (16); the safety pin (4) is assembled in a through pin hole at the tail end of the driving shaft (12) to play a role in overload protection; the speed reducer (15) and the driving shaft (12) realize torque transmission through the coupling (14) and the safety pin (4).
2. An improved metering and dispensing device for fine powdery catalyst according to claim 1, characterized in that, in order to reduce the difficulty of machining the bottom flange (2) while the catalyst metering and dispensing is accurate, the bottom flange (2) is composed of parts, the flange body (202) is machined by a high-precision machine tool with the machining precision, and the rest of the components are machined with economic precision; the device is simple in assembly of all parts before test run, and the assembly of all parts of the bottom flange is adjusted according to operation requirements during test run; two threaded holes are drilled in each side face of the bearing fixing plate (203); the fine adjustment screw (204) is matched with a threaded hole in the side wall of the bearing fixing plate (203); the stud (205) and the bearing fixing plate (203) are in clearance fit; by adjusting the fine adjustment screw (204), the bearing (13) can be prevented from being clamped, and the rotation precision of the driving shaft (12) is ensured; after the proper position of the component is determined by adjusting the fine adjustment screw (204), the component is accurately fixed and welded into a whole.
3. An improved fine powder catalyst metering device as claimed in claim 1, characterized in that the projection of the safety pin (4) from the through-pin hole is in the middle of the U-shaped groove (141).
4. An improved fine-powder catalyst metering device according to claim 1, characterized in that the bearing (13) is a self-aligning bearing for compensating for a misalignment of the drive shaft (12) in the direction of its axis.
5. An improved dosing device for catalyst in the form of fine powder according to claim 1, characterised in that said coupling (14) is a quincunx elastic coupling for compensating the relative offset of the drive shaft (12) and the output shaft of the reducer (15).
CN202010112334.3A 2020-02-24 2020-02-24 An Improved Fine Powder Catalyst Metering and Dispensing Device Active CN111229132B (en)

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CN202010112334.3A CN111229132B (en) 2020-02-24 2020-02-24 An Improved Fine Powder Catalyst Metering and Dispensing Device

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CN112316855A (en) * 2020-10-06 2021-02-05 大连理工大学 Improved micro powder metering device with adjustable sealing force on metering disc and corresponding adjusting method

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