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CN111228159A - Polypeptide anti-wrinkle firming activation water and preparation process thereof - Google Patents

Polypeptide anti-wrinkle firming activation water and preparation process thereof Download PDF

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CN111228159A
CN111228159A CN202010263093.2A CN202010263093A CN111228159A CN 111228159 A CN111228159 A CN 111228159A CN 202010263093 A CN202010263093 A CN 202010263093A CN 111228159 A CN111228159 A CN 111228159A
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polypeptide
firming
wrinkle
activated water
stirring
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张迪
欧伦
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Shanghai Zhifu Technology Co Ltd
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Shanghai Zhifu Technology Co Ltd
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9728Fungi, e.g. yeasts
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/64Proteins; Peptides; Derivatives or degradation products thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/64Proteins; Peptides; Derivatives or degradation products thereof
    • A61K8/645Proteins of vegetable origin; Derivatives or degradation products thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A61K8/922Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9706Algae
    • A61K8/9722Chlorophycota or Chlorophyta [green algae], e.g. Chlorella
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • A61K8/9789Magnoliopsida [dicotyledons]
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/59Mixtures
    • A61K2800/592Mixtures of compounds complementing their respective functions
    • A61K2800/5922At least two compounds being classified in the same subclass of A61K8/18

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Abstract

The polypeptide anti-wrinkle firming activation water comprises the following components in percentage by mass: a material: 65-75% of deionized water, 3-8% of glycerol, 0-1% of antioxidant, 0-0.5% of tremella fruiting body extract and 0-1.5% of thickening agent; b, material B: 1-5% of 1, 2-pentanediol; c, material C: 0-1% of an emollient; d, material: 0-11% of a skin conditioner, 0-1% of a humectant, 0-1% of a solubilizer and 0-0.5% of an aromatic; 0-1% of polypeptide. Dissolving the water-soluble silicon wax, cooling to below 40 ℃, and then adding the material C, the material D and the polypeptide components. The water-soluble silicon wax is better dissolved, the phenomenon that a material body becomes a semi-dim state is avoided, the purity of activated water is better, and polypeptide components can effectively remove wrinkles.

Description

Polypeptide anti-wrinkle firming activation water and preparation process thereof
Technical Field
The invention belongs to the technical field of cosmetics, and particularly relates to polypeptide anti-wrinkle firming activation water and a preparation process thereof.
Background
The development of the modern times and the innovation and progress of the technology lead the cosmetic industry to develop rapidly, meanwhile, the requirements of people on cosmetic products are continuously improved, various functional, dosage forms and cosmetic products with unique appearances attract the eyes of consumers, and water cosmetics in cosmetic variety dosage forms always occupy an important position. From "Shenxian water" of SK-II to "Tian Yi water" of Europe to the appearance of various unique appearance waters nowadays, it deeply attracts consumers. Water cosmetics always occupy important market share, the competition of water cosmetics is more intense, and the water cosmetics with unique appearance can effectively attract the eyes of consumers. However, the water cosmetics in the prior art have poor purity and are difficult to effectively resist and remove wrinkles.
Disclosure of Invention
1. Technical problem to be solved by the invention
The invention aims to solve the problems that the water cosmetics in the prior art are poor in purity and difficult to effectively resist and remove wrinkles.
2. Technical scheme
In order to achieve the purpose, the technical scheme provided by the invention is as follows:
the invention relates to polypeptide anti-wrinkle firming activated water which comprises the following components in parts by mass:
a material: 65-75% of deionized water, 3-8% of glycerol, 0-1% of antioxidant, 0-0.5% of tremella fruiting body extract and 0-1.5% of thickening agent;
b, material B: 1-5% of 1, 2-pentanediol;
c, material C: 0-1% of an emollient;
d, material: 0-11% of a skin conditioner, 0-1% of a humectant, 0-1% of a solubilizer and 0-0.5% of an aromatic;
0-1% of polypeptide.
Preferably, the polypeptides include palmitoyl pentapeptide-4, palmitoyl tripeptide-5, dipeptide diaminobutyrylbenzylamide diacetate, acetyl tetrapeptide-2, acetyl hexapeptide-8, tripeptide-10 citrulline, tripeptide-1, and tetradecylaminobutylamidobutanamide butyrate trifluoroacetate.
Preferably, the antioxidant in the material A is p-hydroxyacetophenone.
Preferably, the thickener comprises xanthan gum, hydroxyethyl cellulose and polyethylene glycol-90M, and the mass ratio of the xanthan gum to the hydroxyethyl cellulose to the polyethylene glycol-90M is 1: 1: 1-1: 2: 3.
preferably, the emollient in material C is bis-PEG-18 methyl ether dimethylsilane.
Preferably, the moisturizing agent in the material D is panthenol, the solubilizing agent is PEG-40 hydrogenated castor oil, the aromatic is essence, and the skin conditioner is dipotassium glycyrrhizinate, alpine edelweiss extract, citric acid, potassium sorbate, sodium benzoate, chlorella extract, arginine ferulate, hydrolyzed pea protein, glucose, sodium chloride, disodium succinate, sunflower seed oil, rosemary leaf extract, hydrolyzed RNA, whey protein and wild soybean protein.
A preparation process of polypeptide anti-wrinkle firming activation water comprises the following steps:
s100, preparing materials, namely respectively preparing a material A, a material B, a material C, a material D and polypeptide with required mass fractions;
s200, heating, namely adding the material A into a main pot, heating to 85 ℃, and keeping the temperature and stirring for 30 minutes;
s300, mixing materials for the first time, cooling the main pot processed in the step S200 to 60 ℃, and adding a material B;
s400, mixing materials for the second time, namely cooling the water phase pot after the first mixing to 40 ℃, and adding the material C, the material D and the polypeptide;
s500, primary stirring, namely, performing heat preservation stirring on the main pot after the secondary mixing;
and S600, stirring for the second time, and stirring and cooling the primary stirred main pot to obtain the activated water.
Preferably, the following components: the heat preservation stirring time in the step S500 is 30 minutes, and the heat preservation temperature is 40 ℃.
Preferably, the step S600 further includes filtering.
Preferably, a water-soluble silicon wax is further added in the step S300.
3. Advantageous effects
Compared with the prior art, the technical scheme provided by the invention has the following beneficial effects:
the invention relates to polypeptide anti-wrinkle firming activated water which comprises the following components in parts by mass: a material: 65-75% of deionized water, 3-8% of glycerol, 0-1% of antioxidant, 0-0.5% of tremella fruiting body extract and 0-1.5% of thickening agent; b, material B: 1-5% of 1, 2-pentanediol; c, material C: 0-1% of an emollient; d, material: 0-11% of a skin conditioner, 0-1% of a humectant, 0-1% of a solubilizer and 0-0.5% of an aromatic; 0-1% of polypeptide. Dissolving the water-soluble silicon wax, cooling to below 40 ℃, and then adding the material C, the material D and the polypeptide components. The water-soluble silicon wax is better dissolved, the phenomenon that a material body becomes a semi-dim state is avoided, the purity of activated water is better, and polypeptide components can effectively remove wrinkles.
Drawings
Fig. 1 is a flow chart of a preparation process of polypeptide anti-wrinkle firming activated water.
Detailed Description
In order to facilitate an understanding of the invention, the invention will now be described more fully hereinafter with reference to the accompanying drawings, in which several embodiments of the invention are shown, but which may be embodied in many different forms and are not limited to the embodiments described herein, but rather are provided for the purpose of providing a more thorough disclosure of the invention.
Unless defined otherwise, all technical and scientific terms used herein have the same meaning as commonly understood by one of ordinary skill in the art to which this invention belongs; the terminology used herein in the description of the invention is for the purpose of describing particular embodiments only and is not intended to be limiting of the invention; as used herein, the term "and/or" includes any and all combinations of one or more of the associated listed items.
Example 1
Referring to the attached figure 1, the polypeptide anti-wrinkle firming activated water comprises the following components in percentage by mass:
a material: deionized water 75%, glycerin 8%, antioxidant 1%, tremella sporophore extract 0.. 5% and thickener 1.5%;
b, material B: 5% of 1, 2-pentanediol;
c, material C: 1% of an emollient;
d, material: 10% of skin conditioner, 1% of humectant, 1% of solubilizer and 0.5% of aromatic;
0.1 percent of polypeptide.
Preferably, the polypeptides include palmitoyl pentapeptide-4, palmitoyl tripeptide-5, dipeptide diaminobutyrylbenzylamide diacetate, acetyl tetrapeptide-2, acetyl hexapeptide-8, tripeptide-10 citrulline, tripeptide-1, and tetradecylaminobutylamidobutanamide butyrate trifluoroacetate.
Preferably, the antioxidant in the material A is p-hydroxyacetophenone.
Preferably, the thickener comprises xanthan gum, hydroxyethyl cellulose and polyethylene glycol-90M, and the mass ratio of the xanthan gum to the hydroxyethyl cellulose to the polyethylene glycol-90M is 1: 1: 1-1: 2: 3.
preferably, the emollient in material C is bis-PEG-18 methyl ether dimethylsilane.
Preferably, the moisturizing agent in the material D is panthenol, the solubilizing agent is PEG-40 hydrogenated castor oil, the aromatic is essence, and the skin conditioner is dipotassium glycyrrhizinate, alpine edelweiss extract, citric acid, potassium sorbate, sodium benzoate, chlorella extract, arginine ferulate, hydrolyzed pea protein, glucose, sodium chloride, disodium succinate, sunflower seed oil, rosemary leaf extract, hydrolyzed RNA, whey protein and wild soybean protein.
A preparation process of polypeptide anti-wrinkle firming activation water comprises the following steps:
s100, preparing materials, namely respectively preparing a material A, a material B, a material C, a material D and polypeptide with required mass fractions;
s200, heating, namely adding the material A into a main pot, heating to 85 ℃, and keeping the temperature and stirring for 30 minutes;
s300, mixing materials for the first time, cooling the main pot processed in the step S200 to 60 ℃, and adding a material B;
s400, mixing materials for the second time, namely cooling the water phase pot after the first mixing to 40 ℃, and adding the material C, the material D and the polypeptide;
s500, primary stirring, namely, performing heat preservation stirring on the main pot after the secondary mixing;
and S600, stirring for the second time, and stirring and cooling the primary stirred main pot to obtain the activated water.
Preferably, the following components: the heat preservation stirring time in the step S500 is 30 minutes, and the heat preservation temperature is 40 ℃.
Preferably, the step S600 further includes filtering.
Preferably, in step S300, water-soluble silicone wax is further added, the temperature is reduced from 80 ℃ to 60 ℃, the temperature is reduced to below 40 ℃ after the water-soluble silicone wax is dissolved, and then the material C, the material D and the polypeptide component are added. The water-soluble silicon wax is better dissolved, the phenomenon that a material body becomes a semi-dim state is avoided, the purity of activated water is better, and polypeptide components can effectively remove wrinkles. If the temperature is directly lowered to 40 ℃ or less, the water-soluble silicone wax is hardly dissolved, and the material becomes a semi-hazy state.
Example 2
Referring to the attached figure 1, the polypeptide anti-wrinkle firming activated water comprises the following components in percentage by mass:
a material: deionized water 75%, glycerin 8%, antioxidant 1%, tremella sporophore extract 0.. 5% and thickener 1.5%;
b, material B: 5% of 1, 2-pentanediol;
c, material C: 1% of an emollient;
d, material: 10% of skin conditioner, 1% of humectant, 1% of solubilizer and 0.5% of aromatic;
0.3 percent of polypeptide.
Preferably, the polypeptides include palmitoyl pentapeptide-4, palmitoyl tripeptide-5, dipeptide diaminobutyrylbenzylamide diacetate, acetyl tetrapeptide-2, acetyl hexapeptide-8, tripeptide-10 citrulline, tripeptide-1, and tetradecylaminobutylamidobutanamide butyrate trifluoroacetate.
Preferably, the antioxidant in the material A is p-hydroxyacetophenone.
Preferably, the thickener comprises xanthan gum, hydroxyethyl cellulose and polyethylene glycol-90M, and the mass ratio of the xanthan gum to the hydroxyethyl cellulose to the polyethylene glycol-90M is 1: 1: 1-1: 2: 3.
preferably, the emollient in material C is bis-PEG-18 methyl ether dimethylsilane.
Preferably, the moisturizing agent in the material D is panthenol, the solubilizing agent is PEG-40 hydrogenated castor oil, the aromatic is essence, and the skin conditioner is dipotassium glycyrrhizinate, alpine edelweiss extract, citric acid, potassium sorbate, sodium benzoate, chlorella extract, arginine ferulate, hydrolyzed pea protein, glucose, sodium chloride, disodium succinate, sunflower seed oil, rosemary leaf extract, hydrolyzed RNA, whey protein and wild soybean protein.
A preparation process of polypeptide anti-wrinkle firming activation water comprises the following steps:
s100, preparing materials, namely respectively preparing a material A, a material B, a material C, a material D and polypeptide with required mass fractions;
s200, heating, namely adding the material A into a main pot, heating to 85 ℃, and keeping the temperature and stirring for 30 minutes;
s300, mixing materials for the first time, cooling the main pot processed in the step S200 to 60 ℃, and adding a material B;
s400, mixing materials for the second time, namely cooling the water phase pot after the first mixing to 40 ℃, and adding the material C, the material D and the polypeptide;
s500, primary stirring, namely, performing heat preservation stirring on the main pot after the secondary mixing;
and S600, stirring for the second time, and stirring and cooling the primary stirred main pot to obtain the activated water.
Preferably, the following components: the heat preservation stirring time in the step S500 is 30 minutes, and the heat preservation temperature is 40 ℃.
Preferably, the step S600 further includes filtering.
Preferably, a water-soluble silicon wax is further added in the step S300.
Example 3
Referring to the attached figure 1, the polypeptide anti-wrinkle firming activated water comprises the following components in percentage by mass:
a material: deionized water 75%, glycerin 8%, antioxidant 1%, tremella sporophore extract 0.. 5% and thickener 1.5%;
b, material B: 5% of 1, 2-pentanediol;
c, material C: 1% of an emollient;
d, material: 10% of skin conditioner, 1% of humectant, 1% of solubilizer and 0.5% of aromatic;
0.5 percent of polypeptide.
Preferably, the polypeptides include palmitoyl pentapeptide-4, palmitoyl tripeptide-5, dipeptide diaminobutyrylbenzylamide diacetate, acetyl tetrapeptide-2, acetyl hexapeptide-8, tripeptide-10 citrulline, tripeptide-1, and tetradecylaminobutylamidobutanamide butyrate trifluoroacetate.
Preferably, the antioxidant in the material A is p-hydroxyacetophenone.
Preferably, the thickener comprises xanthan gum, hydroxyethyl cellulose and polyethylene glycol-90M, and the mass ratio of the xanthan gum to the hydroxyethyl cellulose to the polyethylene glycol-90M is 1: 1: 1-1: 2: 3.
preferably, the emollient in material C is bis-PEG-18 methyl ether dimethylsilane.
Preferably, the moisturizing agent in the material D is panthenol, the solubilizing agent is PEG-40 hydrogenated castor oil, the aromatic is essence, and the skin conditioner is dipotassium glycyrrhizinate, alpine edelweiss extract, citric acid, potassium sorbate, sodium benzoate, chlorella extract, arginine ferulate, hydrolyzed pea protein, glucose, sodium chloride, disodium succinate, sunflower seed oil, rosemary leaf extract, hydrolyzed RNA, whey protein and wild soybean protein.
A preparation process of polypeptide anti-wrinkle firming activation water comprises the following steps:
s100, preparing materials, namely respectively preparing a material A, a material B, a material C, a material D and polypeptide with required mass fractions;
s200, heating, namely adding the material A into a main pot, heating to 85 ℃, and keeping the temperature and stirring for 30 minutes;
s300, mixing materials for the first time, cooling the main pot processed in the step S200 to 60 ℃, and adding a material B;
s400, mixing materials for the second time, namely cooling the water phase pot after the first mixing to 40 ℃, and adding the material C, the material D and the polypeptide;
s500, primary stirring, namely, performing heat preservation stirring on the main pot after the secondary mixing;
and S600, stirring for the second time, and stirring and cooling the primary stirred main pot to obtain the activated water.
Preferably, the following components: the heat preservation stirring time in the step S500 is 30 minutes, and the heat preservation temperature is 40 ℃.
Preferably, the step S600 further includes filtering.
Preferably, a water-soluble silicon wax is further added in the step S300.
Example 4
Referring to the attached figure 1, the polypeptide anti-wrinkle firming activated water comprises the following components in percentage by mass:
a material: deionized water 75%, glycerin 8%, antioxidant 1%, tremella sporophore extract 0.. 5% and thickener 1.5%;
b, material B: 5% of 1, 2-pentanediol;
c, material C: 1% of an emollient;
d, material: 10% of skin conditioner, 1% of humectant, 1% of solubilizer and 0.5% of aromatic;
0.7 percent of polypeptide.
Preferably, the polypeptides include palmitoyl pentapeptide-4, palmitoyl tripeptide-5, dipeptide diaminobutyrylbenzylamide diacetate, acetyl tetrapeptide-2, acetyl hexapeptide-8, tripeptide-10 citrulline, tripeptide-1, and tetradecylaminobutylamidobutanamide butyrate trifluoroacetate.
Preferably, the antioxidant in the material A is p-hydroxyacetophenone.
Preferably, the thickener comprises xanthan gum, hydroxyethyl cellulose and polyethylene glycol-90M, and the mass ratio of the xanthan gum to the hydroxyethyl cellulose to the polyethylene glycol-90M is 1: 1: 1-1: 2: 3.
preferably, the emollient in material C is bis-PEG-18 methyl ether dimethylsilane.
Preferably, the moisturizing agent in the material D is panthenol, the solubilizing agent is PEG-40 hydrogenated castor oil, the aromatic is essence, and the skin conditioner is dipotassium glycyrrhizinate, alpine edelweiss extract, citric acid, potassium sorbate, sodium benzoate, chlorella extract, arginine ferulate, hydrolyzed pea protein, glucose, sodium chloride, disodium succinate, sunflower seed oil, rosemary leaf extract, hydrolyzed RNA, whey protein and wild soybean protein.
A preparation process of polypeptide anti-wrinkle firming activation water comprises the following steps:
s100, preparing materials, namely respectively preparing a material A, a material B, a material C, a material D and polypeptide with required mass fractions;
s200, heating, namely adding the material A into a main pot, heating to 85 ℃, and keeping the temperature and stirring for 30 minutes;
s300, mixing materials for the first time, cooling the main pot processed in the step S200 to 60 ℃, and adding a material B;
s400, mixing materials for the second time, namely cooling the water phase pot after the first mixing to 40 ℃, and adding the material C, the material D and the polypeptide;
s500, primary stirring, namely, performing heat preservation stirring on the main pot after the secondary mixing;
and S600, stirring for the second time, and stirring and cooling the primary stirred main pot to obtain the activated water.
Preferably, the following components: the heat preservation stirring time in the step S500 is 30 minutes, and the heat preservation temperature is 40 ℃.
Preferably, the step S600 further includes filtering.
Preferably, a water-soluble silicon wax is further added in the step S300.
Example 5
Referring to the attached figure 1, the polypeptide anti-wrinkle firming activated water comprises the following components in percentage by mass:
a material: deionized water 75%, glycerin 8%, antioxidant 1%, tremella sporophore extract 0.. 5% and thickener 1.5%;
b, material B: 5% of 1, 2-pentanediol;
c, material C: 1% of an emollient;
d, material: 10% of skin conditioner, 1% of humectant, 1% of solubilizer and 0.5% of aromatic;
1% of polypeptide.
Preferably, the polypeptides include palmitoyl pentapeptide-4, palmitoyl tripeptide-5, dipeptide diaminobutyrylbenzylamide diacetate, acetyl tetrapeptide-2, acetyl hexapeptide-8, tripeptide-10 citrulline, tripeptide-1, and tetradecylaminobutylamidobutanamide butyrate trifluoroacetate.
Preferably, the antioxidant in the material A is p-hydroxyacetophenone.
Preferably, the thickener comprises xanthan gum, hydroxyethyl cellulose and polyethylene glycol-90M, and the mass ratio of the xanthan gum to the hydroxyethyl cellulose to the polyethylene glycol-90M is 1: 1: 1-1: 2: 3.
preferably, the emollient in material C is bis-PEG-18 methyl ether dimethylsilane.
Preferably, the moisturizing agent in the material D is panthenol, the solubilizing agent is PEG-40 hydrogenated castor oil, the aromatic is essence, and the skin conditioner is dipotassium glycyrrhizinate, alpine edelweiss extract, citric acid, potassium sorbate, sodium benzoate, chlorella extract, arginine ferulate, hydrolyzed pea protein, glucose, sodium chloride, disodium succinate, sunflower seed oil, rosemary leaf extract, hydrolyzed RNA, whey protein and wild soybean protein.
A preparation process of polypeptide anti-wrinkle firming activation water comprises the following steps:
s100, preparing materials, namely respectively preparing a material A, a material B, a material C, a material D and polypeptide with required mass fractions;
s200, heating, namely adding the material A into a main pot, heating to 85 ℃, and keeping the temperature and stirring for 30 minutes;
s300, mixing materials for the first time, cooling the main pot processed in the step S200 to 60 ℃, and adding a material B;
s400, mixing materials for the second time, namely cooling the water phase pot after the first mixing to 40 ℃, and adding the material C, the material D and the polypeptide;
s500, primary stirring, namely, performing heat preservation stirring on the main pot after the secondary mixing;
and S600, stirring for the second time, and stirring and cooling the primary stirred main pot to obtain the activated water.
Preferably, the stirring time at the temperature maintained in step S500 is 30 minutes, and the temperature maintained is 40 ℃.
Preferably, the step S600 further includes filtering.
Preferably, a water-soluble silicon wax is further added in the step S300.
Comparative example 1
The activated water of the comparative example comprises the following components in percentage by mass:
a material: deionized water 75%, glycerin 8%, antioxidant 1%, tremella sporophore extract 0.. 5% and thickener 1.5%;
b, material B: 5% of 1, 2-pentanediol;
c, material C: 1% of an emollient;
d, material: 10% of skin conditioner, 1% of humectant, 1% of solubilizer and 0.5% of aromatic.
Preferably, the polypeptides include palmitoyl pentapeptide-4, palmitoyl tripeptide-5, dipeptide diaminobutyrylbenzylamide diacetate, acetyl tetrapeptide-2, acetyl hexapeptide-8, tripeptide-10 citrulline, tripeptide-1, and tetradecylaminobutylamidobutanamide butyrate trifluoroacetate.
Preferably, the antioxidant in the material A is p-hydroxyacetophenone.
Preferably, the thickener comprises xanthan gum, hydroxyethyl cellulose and polyethylene glycol-90M, and the mass ratio of the xanthan gum to the hydroxyethyl cellulose to the polyethylene glycol-90M is 1: 1: 1-1: 2: 3.
preferably, the emollient in material C is bis-PEG-18 methyl ether dimethylsilane.
Preferably, the moisturizing agent in the material D is panthenol, the solubilizing agent is PEG-40 hydrogenated castor oil, the aromatic is essence, and the skin conditioner is dipotassium glycyrrhizinate, alpine edelweiss extract, citric acid, potassium sorbate, sodium benzoate, chlorella extract, arginine ferulate, hydrolyzed pea protein, glucose, sodium chloride, disodium succinate, sunflower seed oil, rosemary leaf extract, hydrolyzed RNA, whey protein and wild soybean protein.
A preparation process of polypeptide anti-wrinkle firming activation water comprises the following steps:
s100, preparing materials, namely respectively preparing a material A, a material B, a material C and a material D with required mass fractions;
s200, heating, namely adding the material A into a main pot, heating to 85 ℃, and keeping the temperature and stirring for 30 minutes;
s300, mixing materials for the first time, cooling the main pot processed in the step S200 to 60 ℃, and adding a material B;
s400, mixing materials for the second time, namely cooling the water phase pot after the first mixing to 40 ℃, and adding the material C and the material D;
s500, primary stirring, namely, performing heat preservation stirring on the main pot after the secondary mixing;
and S600, stirring for the second time, and stirring and cooling the primary stirred main pot to obtain the activated water.
Preferably, the following components: the heat preservation stirring time in the step S500 is 30 minutes, and the heat preservation temperature is 40 ℃.
Preferably, the step S600 further includes filtering.
And (3) comparison test:
the activated water prepared in examples 1 to 5 and comparative example 1 was subjected to a test, and 50 subjects (25 to 35 years old 15, 35 to 45 years old 15 and 45 to 55 years old 20) of different ages were selected and divided into groups of comparative experiment 1, comparative experiment 2, comparative experiment 3, comparative experiment 4 and comparative experiment 5, each group of 25 to 35 years old 3, 35 to 45 years old 3 and 45 to 55 years old 4, comparative experiment 1 used the activated water prepared in example 1 and comparative example 1, comparative experiment 2 used the activated water prepared in example 2 and comparative example 1, comparative experiment 3 used the activated water prepared in example 3 and comparative example 1, comparative experiment 4 used the activated water prepared in example 4 and comparative example 1, comparative experiment 5 used the activated water prepared in example 5 and comparative example 1, and the test procedure was such that 5 groups of subjects used the activated water containing the polypeptide and the activated water containing no polypeptide on the left and right faces, respectively The effect of continuous use for one month, three months and six months and the existence rate of wrinkles (the number of existing wrinkles is larger than the number of wrinkles before use) were mainly observed, and the test results are shown in the following table:
Figure BDA0002440161760000121
in summary, the following steps:
the activated water prepared by the invention can effectively remove wrinkles after being used, and has better effects of resisting wrinkles and removing wrinkles after being continuously used.
The above-mentioned embodiments only express a certain implementation mode of the present invention, and the description thereof is specific and detailed, but not construed as limiting the scope of the present invention; it should be noted that, for those skilled in the art, without departing from the concept of the present invention, several variations and modifications can be made, which are within the protection scope of the present invention; therefore, the protection scope of the present patent shall be subject to the appended claims.

Claims (10)

1. The polypeptide anti-wrinkle firming activated water is characterized by comprising the following components in parts by mass:
a material: 65-75% of deionized water, 3-8% of glycerol, 0-1% of antioxidant, 0-0.5% of tremella fruiting body extract and 0-1.5% of thickening agent;
b, material B: 1-5% of 1, 2-pentanediol;
c, material C: 0-1% of an emollient;
d, material: 0-11% of a skin conditioner, 0-1% of a humectant, 0-1% of a solubilizer and 0-0.5% of an aromatic;
0-1% of polypeptide.
2. The polypeptide anti-wrinkle and anti-firming activated water according to claim 1, which is characterized in that: the polypeptide comprises palmitoyl pentapeptide-4, palmitoyl tripeptide-5, dipeptide diaminobutyrylbenzylamide diacetate, acetyl tetrapeptide-2, acetyl hexapeptide-8, tripeptide-10 citrulline, tripeptide-1 and tetradecyl aminobutyroylvalinamide butyric urea trifluoroacetate.
3. The polypeptide anti-wrinkle and anti-firming activated water according to claim 1, which is characterized in that: the antioxidant in the material A is p-hydroxyacetophenone.
4. The polypeptide anti-wrinkle and anti-firming activated water according to claim 1, which is characterized in that: the thickening agent comprises xanthan gum, hydroxyethyl cellulose and polyethylene glycol-90M, and the mass ratio of the thickening agent to the xanthan gum to the hydroxyethyl cellulose to the polyethylene glycol-90M is 1: 1: 1-1: 2: 3.
5. the polypeptide anti-wrinkle and anti-firming activated water according to claim 1, which is characterized in that: and the emollient in the material C is bis-PEG-18 methyl ether dimethylsilane.
6. The polypeptide anti-wrinkle and anti-firming activated water according to claim 1, which is characterized in that: the moisturizing agent in the material D is panthenol, the solubilizing agent is PEG-40 hydrogenated castor oil, the aromatic agent is essence, and the skin conditioner is dipotassium glycyrrhizinate, an extract of alpine edelweiss, citric acid, potassium sorbate, sodium benzoate, an extract of green algae, arginine ferulate, hydrolyzed pea protein, glucose, sodium chloride, disodium succinate, sunflower seed oil, an extract of rosemary leaves, hydrolyzed RNA, lactalbumin and wild soybean protein.
7. The preparation process of the polypeptide anti-wrinkle firming activated water according to any one of claims 1 to 6, comprising the following steps:
s100, preparing materials, namely respectively preparing a material A, a material B, a material C, a material D and polypeptide with required mass fractions;
s200, heating, namely adding the material A into a main pot, heating to 85 ℃, and keeping the temperature and stirring for 30 minutes;
s300, mixing materials for the first time, cooling the main pot processed in the step S200 to 60 ℃, and adding a material B;
s400, mixing materials for the second time, namely cooling the water phase pot after the first mixing to 40 ℃, and adding the material C, the material D and the polypeptide;
s500, primary stirring, namely, performing heat preservation stirring on the main pot after the secondary mixing;
and S600, stirring for the second time, and stirring and cooling the primary stirred main pot to obtain the activated water.
8. The polypeptide anti-wrinkle and anti-firming activated water according to claim 7, which is characterized in that: the heat preservation stirring time in the step S500 is 30 minutes, and the heat preservation temperature is 40 ℃.
9. The polypeptide anti-wrinkle and anti-firming activated water according to claim 7, which is characterized in that: the step S600 further includes filtering.
10. The polypeptide anti-wrinkle and anti-firming activated water according to claim 7, which is characterized in that: in step S300, water-soluble silicon wax is also added.
CN202010263093.2A 2020-04-07 2020-04-07 Polypeptide anti-wrinkle firming activation water and preparation process thereof Pending CN111228159A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111991277A (en) * 2020-08-25 2020-11-27 浙江英树生物科技有限公司 Truffle substrate anti-aging care composition and preparation method and application thereof

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110101593A (en) * 2019-04-29 2019-08-09 广州科恩生物技术有限公司 A kind of anti-wrinkle cream and preparation method thereof
CN110840769A (en) * 2019-12-03 2020-02-28 河北翰林生物科技有限公司 Anti-wrinkle moisturizing skin care lotion and preparation method thereof

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110101593A (en) * 2019-04-29 2019-08-09 广州科恩生物技术有限公司 A kind of anti-wrinkle cream and preparation method thereof
CN110840769A (en) * 2019-12-03 2020-02-28 河北翰林生物科技有限公司 Anti-wrinkle moisturizing skin care lotion and preparation method thereof

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111991277A (en) * 2020-08-25 2020-11-27 浙江英树生物科技有限公司 Truffle substrate anti-aging care composition and preparation method and application thereof

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