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CN111166686A - Hyaluronic acid toner - Google Patents

Hyaluronic acid toner Download PDF

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Publication number
CN111166686A
CN111166686A CN201811336862.6A CN201811336862A CN111166686A CN 111166686 A CN111166686 A CN 111166686A CN 201811336862 A CN201811336862 A CN 201811336862A CN 111166686 A CN111166686 A CN 111166686A
Authority
CN
China
Prior art keywords
hyaluronic acid
toner
cross
concentration
mass volume
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201811336862.6A
Other languages
Chinese (zh)
Inventor
孔葵生
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Wuxi Huoban Cosmetic Technology Co ltd
Original Assignee
Wuxi Huoban Cosmetic Technology Co ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Wuxi Huoban Cosmetic Technology Co ltd filed Critical Wuxi Huoban Cosmetic Technology Co ltd
Priority to CN201811336862.6A priority Critical patent/CN111166686A/en
Publication of CN111166686A publication Critical patent/CN111166686A/en
Pending legal-status Critical Current

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Classifications

    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73Polysaccharides
    • A61K8/735Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/02Cosmetics or similar toiletry preparations characterised by special physical form
    • A61K8/04Dispersions; Emulsions
    • A61K8/046Aerosols; Foams
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/965Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of inanimate origin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin

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  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Public Health (AREA)
  • Veterinary Medicine (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
  • Epidemiology (AREA)
  • Birds (AREA)
  • Emergency Medicine (AREA)
  • Chemical & Material Sciences (AREA)
  • Dispersion Chemistry (AREA)
  • Dermatology (AREA)
  • Cosmetics (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)

Abstract

The present invention discloses a moisturizing spray toner comprising cross-linked hyaluronic acid or one of its salts in a concentration of 1% to 4% by mass volume, the cross-linking carried out providing the possibility of obtaining a gel based on cross-linked hyaluronic acid having a so-called cohesive structure; a concentration of the sea sludge extract in the form of an average size of less than or equal to 200 microns is between 5% and 60% by mass volume; the moisturizing spray toner has viscoelasticity such that tan δ at a frequency of 1Hz is less than or equal to 0.60. The moisturizing spray toner disclosed by the invention is mainly prepared from sea sludge extract, hydrolyzed hyaluronic acid, hyaluronic acid and propylene glycol, and is used for concentrating on water replenishing and moisturizing, and micromolecule hydrolyzed sodium hyaluronate penetrates through layers of barriers and penetrates into the bottom layer of the skin to inject source activity into the skin. The surface layer of the macromolecular hyaluronic acid locks water and preserves moisture, prevents water loss, replenishes water internally and preserves moisture externally.

Description

Hyaluronic acid toner
Technical Field
The invention belongs to the technical field of skin care products, and particularly relates to hyaluronic acid toner.
Background
Aging is a natural phenomenon faced by any individual, inevitably accompanied by reduction of cell activities of the human body, the completion of the metabolism function of the skin needs a large amount of water, like the human body, water shortage is the most important factor in skin aging, the water taken by the human body every day is poor in circulation to the face, the content is far from enough, and the water shortage of the skin causes many symptoms, such as death, skin growth, and the like, so that the skin needs to be refreshed. The toner, also called firming lotion, astringent, etc., has the effects of re-cleaning to restore the pH value of the skin surface, conditioning the stratum corneum, making the skin absorb better and preparing for the use of a care product.
Most of the skin toner in the existing formula has the effects of sterilization and astringency by adding alcohol, but can bring different degrees of stimulation to sensitive skin and dry skin, and as many as twenty-three kinds of raw materials are added in the existing formula, so that the skin toner can not be used by any skin.
Technical scheme
The invention mainly solves the technical problem of providing moisturizing spraying toner which is in the form of viscous viscoelastic gel and is characterized in that the toner comprises cross-linked hyaluronic acid or salt thereof, the concentration of the cross-linked hyaluronic acid or salt thereof is 1-3% by mass and volume, and the cross-linked hyaluronic acid is cross-linked with propylene glycol diglycidyl ether; the concentration of the sea sludge extract is 10% to 60% by mass volume, the sea sludge extract is in ultrafine form, having an average size of 10 μm or more and 200 μm or less, wherein the toner exhibits viscoelasticity such that tan δ at a frequency of 1Hz is 0.60 or less, and has been sterilized at a humid temperature.
Optionally, wherein the hyaluronic acid or one of its salts has a molecular weight between 2.5 x 105 dalton and 4 x 106 dalton.
Optionally, wherein the concentration of the cross-linked hyaluronic acid or one of its salts is between 1.5% and 2.5% mass volume percent.
Optionally, wherein the concentration of the sea sludge extract is between 10 and 50% mass volume percent.
Optionally, wherein the concentration of the sea sludge extract is between 20% and 40% mass volume percent.
The invention has the beneficial effects that:
the moisturizing spray toner disclosed by the invention is mainly prepared from sea sludge extract, hydrolyzed hyaluronic acid, hyaluronic acid and propylene glycol, and is used for concentrating on water replenishing and moisturizing, and micromolecule hydrolyzed sodium hyaluronate penetrates through layers of barriers and penetrates into the bottom layer of the skin to inject source activity into the skin. The surface layer of the macromolecular hyaluronic acid locks water and preserves moisture, prevents water loss, replenishes water internally and preserves moisture externally.
Examples
The following detailed description of the preferred embodiments of the present invention is provided to enable those skilled in the art to more readily understand the advantages and features of the present invention, and to clearly and unequivocally define the scope of the present invention.
Absorbable infill materials exist in the skin aesthetic market, for example, and can be made with products containing sea sludge extracts, these being suspended in an aqueous phase which may contain polymers like cellulose carboxymethyl cellulose, especially for use on the face, they exhibit a high level of biocompatibility, and for these products, few side effects or complications are reported, from the point of view of absorption, the rapid removal of the aqueous phase from the treatment area, the sea sludge extracts being degraded and metabolized by macrophages over time.
The object of the invention described below is to propose a new bioabsorbable moisturizing spray toner for cosmetic and aesthetic purposes, with specific characteristics of viscoelasticity, filling and long-term performance. The toner is characterized in that it is in the form of a particular cohesive viscoelastic gel, crosslinked hyaluronic acid or a salt thereof, at a concentration of between 1% and 4% (mass/volume), the crosslinking providing a gel based on crosslinked hyaluronic acid having a so-called cohesive structure, a concentration of sea sludge extract of between 5% and 60% (mass/volume), said sea sludge extract being in the form of an average size of less than or equal to 200 μm; the injectable sterile aqueous toner has viscoelastic properties such that TaN δ is less than or equal to 0.60 at a frequency of 1 Hz.
Surprisingly, according to the conditions of the present invention, it can be seen that this toner has a significant capacity to generate volume in the tissue over a long period of time, through a synergistic effect between the cross-linked hyaluronic acid and the sea sludge extract, which, from a mechanical point of view, greatly enhances the elasticity of the gel, so that it is able to generate volume by inducing a significant force/pressure on the tissue to correct the defective site to be whitened. Cross-linked hyaluronic acid itself provides viscoelastic properties, i.e. elasticity, but viscosity may also bring the gel consistency close to tissue, thus compensating for the very strong elasticity and lack of viscosity. On the other hand, crosslinked hyaluronic acid, under the conditions of the present invention, will greatly reduce the migration of the sea mud extract, remaining in the gel, due to the strong cohesion of the crosslinked hyaluronic acid. The strong limitation of the migration of the cohesive type (crosslinked hyaluronic acid with low absorption kinetics) offers the possibility of a gel with a long-term improved volume-forming capacity and of reducing side effects such as the appearance of so-called hard areas felt by the patient. Among the preferred salts of hyaluronic acid according to the invention, mention will be made of salts of hyaluronic acid with cations, for example monovalent or divalent salts, for example sodium, potassium, magnesium, calcium, manganese salts, sodium salts being particularly preferred. The cohesion of the gel based on cross-linked hyaluronic acid is a main and required specific feature of the present invention, the gel should not disperse rapidly when it is introduced into water, that is, the gel with non-viscous properties is called "biphasic" gel (gel based on cross-linked hyaluronic acid, which cannot sustain sea silt extract, thus avoiding migration).
The present invention generally comprises a concentration of cross-linked hyaluronic acid, or salt thereof, of between 1% and 4% (mass/volume), preferably between 1% and 3% (mass/volume). According to a particularly preferred alternative, the concentration of cross-linked hyaluronic acid or one of its salts is between 1.5% and 2.5% (mass/volume), or alternatively, the concentration of cross-linked hyaluronic acid or one of its salts may be between 1.5% and 3% (mass/volume) or between 1% and 2.5% (mass/volume), advantageously, the aqueous toner according to the invention comprises hyaluronic acid or one of its salts, the molecular mass of which is preferably between 2.5 × 105Da and 4 × 106 Da. According to a particularly preferred option, the molecular mass is between 1X 106Da and 3X 106Da, and in addition the molecular mass is between 1X 106Da and 2.5X 106Da, or between 2.5X 105Da and 3X 106 Da. The compounds of sea sludge extract have been used as biomaterials in various medical products for many years, the present invention generally comprising a concentration of sea sludge extract of between 5 and 60% (mass/volume), preferably between 10 and 50% (mass/volume), preferably between 20 and 40% (mass/volume), the sea sludge extract having an average size of less than or equal to 200 μm, preferably less than 50 μm, preferably greater than 10 μm. It has been observed that the viscosity and elastic properties of the formulations of the invention are best when the parameter TaN δ or TaN δ corresponding to the ratio [ viscosity modulus G ]/elastic modulus G' is less than or equal to 0.60, P, at a frequency of 1Hz, which can be referred to as less than or equal to 0.58. It has turned out that the elastic properties of the toner according to the invention with respect to its viscosity should be sufficiently large to be able to avoid sedimentation of the sea sludge extract.
Another object of the invention is to have a better life time compared to the formulations of the prior art, a better aesthetic effect is obtained by the capacity of the cross-linked hyaluronic acid to maintain the sea sludge extract in the injection zone for a long time and the capacity of the sea sludge extract to impart remarkable mechanical/rheological properties, so that the gain in skin lightening in the clinical situation of the toner according to the invention may be several months. On the other hand, the ability of sea mud extract to stimulate endogenous collagen production is an important factor of the present invention, and slow absorption of products in the tissue will be accompanied by collagen production (volume and elasticity production), which will provide the possibility of long-term participation in whitening.
The sequence of the above embodiments is only for convenience of description and does not represent the advantages and disadvantages of the embodiments.
Finally, it should be noted that: the above examples are only intended to illustrate the technical solution of the present invention, but not to limit it; although the present invention has been described in detail with reference to the foregoing embodiments, it will be understood by those of ordinary skill in the art that: the technical solutions described in the foregoing embodiments may still be modified, or some technical features may be equivalently replaced; and such modifications or substitutions do not depart from the spirit and scope of the corresponding technical solutions of the embodiments of the present invention.

Claims (5)

1. A moisturizing spray toner in the form of a viscous viscoelastic gel, characterized in that the toner comprises cross-linked hyaluronic acid or a salt thereof at a concentration of 1% to 3% by mass volume, the cross-linked hyaluronic acid being cross-linked with propylene glycol diglycidyl ether; the concentration of the sea sludge extract is 10% to 60% by mass volume, the sea sludge extract is in ultrafine form, having an average size of 10 μm or more and 200 μm or less, wherein the toner exhibits viscoelasticity such that tan δ at a frequency of 1Hz is 0.60 or less, and has been sterilized at a humid temperature.
2. The moisturizing spray toner of claim 1, wherein: wherein the hyaluronic acid or one of its salts has a molecular weight between 2.5 x 105 dalton and 4 x 106 dalton.
3. The moisturizing spray toner of claim 1, wherein: wherein the concentration of the cross-linked hyaluronic acid or one of its salts is between 1.5% and 2.5% mass volume percent.
4. The moisturizing spray toner of claim 1, wherein: wherein the concentration of the sea sludge extract is between 10 and 50% mass volume percent.
5. The moisturizing spray toner of claim 1, wherein: wherein the concentration of the sea sludge extract is between 20% and 40% mass volume percent.
CN201811336862.6A 2018-11-12 2018-11-12 Hyaluronic acid toner Pending CN111166686A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201811336862.6A CN111166686A (en) 2018-11-12 2018-11-12 Hyaluronic acid toner

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201811336862.6A CN111166686A (en) 2018-11-12 2018-11-12 Hyaluronic acid toner

Publications (1)

Publication Number Publication Date
CN111166686A true CN111166686A (en) 2020-05-19

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP3769750A1 (en) * 2019-07-24 2021-01-27 Amorepacific Corporation A hyaluronic acid composition for external use on skin and its use

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104703582A (en) * 2012-10-08 2015-06-10 安特易斯有限公司 Sterile aqueous formulation for injection comprising cross-linked hyaluronic acid and hydroxyapatite for cosmetic use

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104703582A (en) * 2012-10-08 2015-06-10 安特易斯有限公司 Sterile aqueous formulation for injection comprising cross-linked hyaluronic acid and hydroxyapatite for cosmetic use

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
山东福瑞达生物工程有限公司: "颐莲玻尿酸补水喷雾", 《国产非特殊用途化妆品备案信息服务平台》, 16 July 2018 (2018-07-16), pages 1 - 2 *

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP3769750A1 (en) * 2019-07-24 2021-01-27 Amorepacific Corporation A hyaluronic acid composition for external use on skin and its use
CN112294690A (en) * 2019-07-24 2021-02-02 株式会社爱茉莉太平洋 Hyaluronic acid skin external preparation composition

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