[go: up one dir, main page]

CN111076979B - Gas-liquid split-flow multifunctional sampling and measuring device and use method thereof - Google Patents

Gas-liquid split-flow multifunctional sampling and measuring device and use method thereof Download PDF

Info

Publication number
CN111076979B
CN111076979B CN202010066836.7A CN202010066836A CN111076979B CN 111076979 B CN111076979 B CN 111076979B CN 202010066836 A CN202010066836 A CN 202010066836A CN 111076979 B CN111076979 B CN 111076979B
Authority
CN
China
Prior art keywords
liquid inlet
sampling
liquid
control valve
cover
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
CN202010066836.7A
Other languages
Chinese (zh)
Other versions
CN111076979A (en
Inventor
林国美
杨志明
韩雷
周剑
杨莉华
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
China People's Liberation Army Joint Service Support Force Quartermaster Energy Quality Supervision Station
Nanjing Bolong Instrument Technology Co ltd
Original Assignee
China People's Liberation Army Joint Service Support Force Quartermaster Energy Quality Supervision Station
Nanjing Bolong Instrument Technology Co ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by China People's Liberation Army Joint Service Support Force Quartermaster Energy Quality Supervision Station, Nanjing Bolong Instrument Technology Co ltd filed Critical China People's Liberation Army Joint Service Support Force Quartermaster Energy Quality Supervision Station
Priority to CN202010066836.7A priority Critical patent/CN111076979B/en
Publication of CN111076979A publication Critical patent/CN111076979A/en
Application granted granted Critical
Publication of CN111076979B publication Critical patent/CN111076979B/en
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00Sampling; Preparing specimens for investigation
    • G01N1/02Devices for withdrawing samples
    • G01N1/10Devices for withdrawing samples in the liquid or fluent state
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01KMEASURING TEMPERATURE; MEASURING QUANTITY OF HEAT; THERMALLY-SENSITIVE ELEMENTS NOT OTHERWISE PROVIDED FOR
    • G01K13/00Thermometers specially adapted for specific purposes
    • G01K13/12Thermometers specially adapted for specific purposes combined with sampling devices for measuring temperatures of samples of materials
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N9/00Investigating density or specific gravity of materials; Analysing materials by determining density or specific gravity
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00Sampling; Preparing specimens for investigation
    • G01N1/02Devices for withdrawing samples
    • G01N1/10Devices for withdrawing samples in the liquid or fluent state
    • G01N2001/1031Sampling from special places

Landscapes

  • Physics & Mathematics (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Hydrology & Water Resources (AREA)
  • Sampling And Sample Adjustment (AREA)

Abstract

本发明一种气液分流式多功能取样测量装置及其使用方法,涉及的是用于液体取样的设备,利用该设备进行取样测量的使用方法。气液分流式多功能取样测量装置包括瓶体和上方的取样盖;瓶体和取样盖之间通过螺纹或卡扣密封连接。利用气液分流式多功能取样测量装置具有液体取样、密封存储样品和液体密度、温度测量的功能。本发明一种气液分流式多功能取样测量装置,其构思巧妙、使用方便,具有良好的使用检测效果,通过不同的状态设置具有多种用途,具有很好的使用灵活性和应用推广价值。

The present invention discloses a gas-liquid shunt type multifunctional sampling and measuring device and a method of using the device, which relates to a device for liquid sampling and a method of using the device for sampling and measurement. The gas-liquid shunt type multifunctional sampling and measuring device comprises a bottle body and a sampling cover on top; the bottle body and the sampling cover are sealed and connected by threads or snaps. The gas-liquid shunt type multifunctional sampling and measuring device has the functions of liquid sampling, sealed storage of samples, and liquid density and temperature measurement. The gas-liquid shunt type multifunctional sampling and measuring device of the present invention is ingenious in design, easy to use, has good detection effect, has multiple uses through different state settings, and has good flexibility of use and application promotion value.

Description

Gas-liquid split-flow type multifunctional sampling and measuring device and application method thereof
Technical Field
The invention discloses a gas-liquid split-flow type multifunctional sampling and measuring device and a using method thereof, and relates to equipment for liquid sampling and a using method for sampling and measuring by using the equipment.
Background
In many occasions, liquid needs to be sampled, especially in various places for storing oil liquid and liquid chemicals, the representativeness of oil sampling can directly influence the representativeness of oil quality inspection results. In the existing sampler, the diameter of the mouth is different, the sampling speed is different, but sampling and exhausting are the same in sampling, for example, sampling is carried out in a gasoline tank, an empty sampler is opened, a gasoline sample enters the sampler from a sampler port, gas in the sampler is blown out of the sampler port and discharged, and one liter of gasoline sample fed by one liter of sampler is subjected to opposite flushing, blowing and volatilization of one liter of gas. Tests show that the density of a gasoline sample is increased by one to three thousandths through the sampler, and the vapor pressure of the gasoline is lower, so that the problem is that the sampling and measuring density of the gasoline is detected by the sampler, firstly, the sampling is carried out by pouring the gasoline sample into an oil sample bottle, secondly, the density is measured by pouring the gasoline sample into a measuring cylinder from the oil sample bottle, and thirdly, the gasoline sample has the volatilization loss of light components in the three links, and the flash points of jet fuel and diesel oil are higher, so that the judgment on the quality of the oil is often inaccurate, and therefore, a new sampler is necessary to meet the sampling requirement.
Disclosure of Invention
The invention provides a gas-liquid split-type multifunctional sampling and measuring device, which can effectively overcome the defects of the existing equipment, realize accurate sampling without sample fall and volatilization, accurately measure the metering quality results such as metering density of oil liquid and the like, is suitable for accurate sampling of petrochemical liquid and environment-friendly water quality, and has good use and popularization effects.
The gas-liquid split-flow type multifunctional sampling and measuring device comprises a bottle body and a sampling cover above the bottle body, wherein the bottle body is connected with the sampling cover in a sealing manner through threads or buckles.
The sampling cover comprises a circular cover body, a sliding through hole is formed in the center of the cover body, and a circular arc-shaped liquid inlet through groove or a circular arc-shaped liquid inlet through hole is formed in the side face of the sliding through hole; when the liquid inlet through hole is formed, the liquid inlet through hole is provided with a plurality of through holes with the same size, and the through holes are arranged in an arc manner along the center of the cover body, and the arc of the liquid inlet through groove or the liquid inlet through hole is a minor arc; A cover boss is arranged on the periphery of a liquid inlet through groove or a liquid inlet through hole, a liquid inlet control valve is inserted below the cover by taking the sliding through hole as a central shaft sleeve, a partition plate is arranged at the lower end of the liquid inlet control valve, a hollow exhaust channel is arranged in the center of the upper part of the partition plate, when the upper surface tension force of the partition plate is close to the cover boss, the liquid inlet through groove or the liquid inlet through hole is closed, the axial section of the liquid inlet control valve is in an inverted T shape, an inverted T-shaped exhaust control valve is inserted in the exhaust channel, the top end of the exhaust control valve extends out of the exhaust channel and is fixedly connected with a rope control device, the lower end of the rope control device is in threaded connection with the exhaust channel on the liquid inlet control valve through threads, a liquid inlet control valve plate matched with the liquid inlet through groove or the liquid inlet through hole on the cover is sleeved on the upper surface or the lower surface of the cover by taking the sliding through hole as an axle center, a plurality of circular arc-shaped through holes which correspond to the liquid inlet through groove or the liquid inlet through hole are arranged on the liquid inlet control valve plate, when the liquid inlet through groove is arranged on the cover, the liquid inlet control valve plate is in the shape, the liquid inlet through groove corresponding to the circular arc-shaped through groove or the liquid inlet through hole is arranged on the cover, and the liquid inlet control valve can rotate, and the liquid inlet through hole can be controlled by the speed on the valve plate.
When the liquid inlet control valve plate is arranged below the cover body, the liquid inlet control valve plate is arranged between the cover body and the partition plate of the liquid inlet control valve.
The top at the bottle still has the bottle boss with the baffle matched with of feed liquor control valve, when the lower surface of baffle contacted with the bottle boss under the action of gravity, the baffle can play sealed effect, sealed bottle boss top sample liquid.
A strip-shaped liquid inlet groove or a continuous liquid inlet hole is formed in the side face of the bottom of the boss of the bottle body, sample liquid flows in along the wall of the bottle body through the liquid inlet groove or the liquid inlet hole, impact force during inflow is relieved, splashed liquid drops are prevented from being generated, and sampling precision is affected.
The rope control device comprises a rope hook, a pipe cap, a spring sleeve, a push rod and a locking pipe, wherein a hook groove with a hook-shaped opening in axial section is formed in the middle of the spring sleeve, the pipe cap is installed at the upper end of the spring sleeve, a spring is arranged in a cavity of the spring sleeve, one end of the spring is propped against the inner wall of the pipe cap, the other end of the spring pushes against the K-shaped push rod, an exhaust control valve is fixedly connected to the tail end of the K-shaped push rod and is fixed by a side screw, the rope hook enters the hook groove in a state that the exhaust control valve is closed, is clamped in the middle of the K-shaped push rod, the locking pipe is arranged at the lower part of the opening of the spring sleeve, the upper adjusting locking pipe can block the unhooking of the rope hook, the tail end of the spring sleeve is connected with the liquid inlet control valve through threads and is fixed by the side screw, the spring sleeve is communicated with the exhaust pipe, and the top end of the rope hook penetrates through the pipe cap and is connected with a sampling rope.
The bottom of the K-shaped ejector rod is provided with a groove for assisting in exhausting, so that the gas in the bottle body can be conveniently and rapidly exhausted.
The bottle be cylindrical bottle, further, the bottle by cylindrical bottle and disk form bottle end sealing connection form, the bottle end adopt nickel alloy, it is compared in stainless steel, can not produce the reaction with fluid for the fluid is rotten after long-time storage.
The bottle body and the sampling cover are preferably connected in a threaded sealing way.
The invention can also replace the sampling cover by the sealing cover to store the sample liquid in the bottle body in a sealing way.
The sealing cover is provided with an upper cover, the middle part of the upper cover is provided with a threaded hole, the upper surface of the upper cover is screwed with an adjusting knob through the threaded hole, a hard plate is filled in the sealing cover, and a sealing ring is tightly attached to the lower part of the hard plate.
The bottle body is made of transparent materials, is preferably glass, is further preferably toughened glass, and can effectively prevent external impact and bear the extrusion of sample liquid to the bottle body and prevent deformation.
The gas-liquid split-flow type multifunctional sampling and measuring device has the functions of liquid sampling, sealed storage of samples, liquid density and temperature measurement.
The liquid sampling comprises sampling a bottom sample, sampling a sample and sampling a whole course;
The method for taking liquid bottom samples and sample application by utilizing the gas-liquid split-flow type multifunctional sampling and measuring device comprises the following steps:
the cover body fixedly provided with the rope control device is connected with the bottle body in a sealing way;
rotating the liquid inlet control valve plate to a preset position according to the liquid inlet speed requirement;
The rope hook is clamped into the K-shaped ejector rod, and the rope hook and the K-shaped ejector rod are in a locking state;
the portable sampling rope is utilized, and the gas-liquid split-type multifunctional sampling measuring device is stably placed in a container to be sampled;
after the sampling measuring device is lowered to a preset depth, rapidly lifting the sampling rope for a certain distance, lowering the sampling rope to a original position, pushing the K-shaped ejector rod to move downwards by using a spring in the spring sleeve, and popping up and unlocking the rope hook;
The liquid inlet control valve moves downwards under the action of gravity to separate from the cover boss, is tightly attached to the sealed bottle boss, and simultaneously, the exhaust control valve moves downwards to open the exhaust channel, sample liquid enters through the liquid inlet through groove or the liquid inlet through hole on the side surface of the sliding through hole, and smoothly flows into the strip-shaped liquid inlet groove or the continuous liquid inlet hole on the side surface of the bottle boss along the partition plate on the liquid inlet control valve, and the sample liquid flows in along the bottle wall of the bottle through the liquid inlet groove or the liquid inlet hole to slow down the impact force during inflow;
The gas to be discharged in the bottle body is discharged through the exhaust through pipe at the center of the partition plate, and the gas is further discharged upwards through the gap in the spring sleeve;
After the gas is completely discharged and the bottle body is filled with sample liquid, the sampling rope is lifted and the sampling container is lifted.
A method for taking a whole-course sample by a gas-liquid split-flow type multifunctional sampling and measuring device comprises the following steps:
the sampling cover fixedly provided with the rope control device is connected with the bottle body in a sealing way;
according to the requirement of the speed of liquid inlet, rotating an adjusting groove formed on a liquid inlet adjusting plate to a preset position;
the rope hook is clamped into the K-shaped ejector rod, the rope hook and the K-shaped ejector rod are in a locking state, and the locking pipe is adjusted downwards to keep the hook groove normally open;
The sampling rope is extracted by hands, and the gas-liquid split-flow type multifunctional liquid sampler is stably placed in a container to be sampled;
after the sampler is lowered to a depth close to the bottom of the container, rapidly lifting the sampling rope for a certain distance, lowering the sampling rope to a original position, pushing the K-shaped ejector rod to move downwards by using a spring in the spring sleeve, and popping up and unlocking the rope hook;
The through hole shaft moves downwards under the action of gravity, the liquid inlet control valve plate descends, the liquid inlet channel I and the exhaust chamber are opened, sample liquid enters through the liquid inlet channel I on the cover body and smoothly flows in along the drainage disc, and the sample liquid slowly flows in along the bottle wall of the bottle body through the liquid inlet groove or the liquid inlet hole on the drainage disc, so that the impact force during inflow is slowed down;
the gas to be discharged in the bottle body is discharged through the exhaust through pipe of the through hole shaft, and the gas is further discharged upwards through the gap in the spring sleeve;
When the bottle body is subjected to liquid feeding and air discharging, the sampling rope is lifted upwards at a constant speed, the container to be sampled is directly lifted out completely, and when the container is completely taken out, the bottle body cannot be filled with the sample liquid injected into the bottle body (if the bottle body is full, the sampling of the whole layer of sample is failed, and the sampling rope is required to be resampled until the bottle body is not filled with the sample liquid).
The method for sealing and storing the sample by using the gas-liquid split-flow type multifunctional sampling and measuring device comprises the following steps:
Taking down the sampling cover in the gas-liquid split-type multifunctional sampling and measuring device for sampling the liquid sample, replacing the sealing cover, connecting the sealing cover with the bottle body, rotating the adjusting knob of the sealing cover downwards, and ejecting the hard plate downwards for a certain distance to enable the hard plate to press the bottle body.
When the liquid sample in the storage is required to be taken out, the adjusting knob of the sealing cover is firstly rotated upwards, the hard plate is loosened upwards for a certain distance, and then the sealing cover can be easily unscrewed and the sample liquid can be taken out.
The method for testing the density or temperature of the stored sample in the bottle body by using the gas-liquid split-flow type multifunctional sampling and measuring device comprises the following steps:
And opening the bottle body containing the sample liquid, and putting the bottle body into a glass densimeter.
When the temperature needs to be measured, the glass thermometer is put into the glass thermometer.
The gas-liquid split-type multifunctional sampling and measuring device is ingenious in conception, convenient to use, good in use and detection effect, and has multiple purposes through different state settings, and good in use flexibility and application popularization value.
Drawings
The invention will be further described with reference to the accompanying drawings in which:
FIG. 1 is a schematic diagram of a gas-liquid split-type multifunctional sampling and measuring device according to the present invention.
Fig. 2 is a schematic structural diagram of a sampling cover and a rope control device in the gas-liquid split-type multifunctional sampling and measuring device of the invention.
Fig. 3 is a schematic cross-sectional structure of a sampling cap in the gas-liquid split-flow type multifunctional sampling and measuring device of the present invention.
Fig. 4 is a schematic top view of a sampling cover in the gas-liquid split-type multifunctional sampling and measuring device according to the present invention.
Fig. 5 is a schematic structural diagram of a liquid inlet control valve plate in the gas-liquid split-type multifunctional sampling and measuring device of the invention.
FIG. 6 is a schematic cross-sectional view of a seal cover in a gas-liquid split-flow type multifunctional sampling measurement device according to the present invention.
Detailed Description
The invention is described in further detail below with reference to fig. 1-6.
Referring to fig. 1, the gas-liquid split-type multifunctional sampling and measuring device comprises a bottle body 1 and a sampling cover above the bottle body 1, wherein the bottle body 1 and the sampling cover are connected through threads or a buckle seal.
The sampling cover comprises a circular cover body 2, a sliding through hole 3 is formed in the center of the cover body 2, and a circular arc-shaped liquid inlet through groove or liquid inlet through hole 4 is formed in the side face of the sliding through hole 3; when the liquid inlet through hole is formed, the liquid inlet through hole is provided with a plurality of through holes with the same size, and the through holes are arranged in an arc manner along the center of the cover body, and the arc of the liquid inlet through groove or the liquid inlet through hole is a minor arc; the periphery of the liquid inlet through groove or the liquid inlet through hole 4 is provided with a cover boss 2-1, a liquid inlet control valve 5 is inserted below the cover 2 by taking the sliding through hole 3 as a central shaft sleeve, the lower end of the liquid inlet control valve 5 is provided with a partition plate 5-1, a hollow exhaust passage 5-2 is arranged at the center above the partition plate 5-1, when the upper surface of the partition plate 5-1 is tightly adhered to the cover boss 2-1 upwards by tension force, the liquid inlet through groove or the liquid inlet through hole 4 is closed, the axial section of the liquid inlet control valve 5 is in an inverted T shape, an inverted T-shaped exhaust control valve 6 is inserted in the exhaust passage 5-2, the top end of the exhaust control valve 6 extends out of the exhaust passage 5-2 and is fixedly connected with a rope control device, the lower end of the rope control device is in threaded connection with the exhaust passage 5-2 on the liquid inlet control valve 5 through threads, a liquid inlet control valve plate 7 matched with the liquid inlet through groove or the liquid inlet through hole 2-1 on the cover 2 is sleeved on the upper surface or the lower surface of the cover 2 by taking the sliding through hole 3 as an axle center, the liquid inlet control valve plate 7 is arranged on the cover 2 in a circular arc shape corresponding to the size of the liquid inlet through hole 7 on the cover plate 7 when the liquid inlet control valve plate 2 is in a circular arc shape, the liquid inlet control valve plate 7 is arranged in a circular shape corresponding to the size of the liquid inlet through hole 7 on the valve plate is arranged in a circular shape, the closing degree of the liquid inlet through groove or the liquid inlet through hole on the cover body 2 can be effectively controlled, so that the liquid inlet speed is controlled.
When the liquid inlet control valve plate 7 is arranged below the cover body 2, the liquid inlet control valve plate 7 is arranged between the cover body 2 and the partition plate 5-1 of the liquid inlet control valve 5.
The upper part of the bottle body 1 is also provided with a bottle body boss 1-1 matched with a baffle plate 5-1 of the liquid inlet control valve 5, and when the lower surface of the baffle plate 5-1 contacts with the bottle body boss 1-1 under the action of gravity, the baffle plate 5-1 can play a role in sealing, so as to seal sample liquid in the bottle body boss 1-1.
A strip-shaped liquid inlet groove 1-2 or a continuous liquid inlet hole is formed in the side face of the bottom of the bottle body boss 1-1, sample liquid flows in along the bottle wall of the bottle body 1 through the liquid inlet groove 1-2 or the liquid inlet hole, impact force during inflow is relieved, splashing liquid drops are prevented from being generated, and sampling precision is affected.
The rope control device comprises a rope hook 11, a pipe cap 12, a spring 13, a spring sleeve 14, a K-shaped ejector rod 18 and a lock tube 16, wherein a hook groove 17 with a hook-shaped opening in axial section is formed in the middle of the spring sleeve 14, the pipe cap 12 is arranged at the upper end of the spring sleeve 14, the spring 13 is arranged in a cavity of the spring sleeve 14, one end of the spring 13 abuts against the inner wall of the pipe cap 12, the other end of the spring 13 pushes the K-shaped ejector rod 18, an exhaust control valve 6 is fixedly connected to the tail end of the K-shaped ejector rod 18 through a side screw 18-2, the rope hook 11 enters the hook groove 17 and is clamped in the middle of the K-shaped ejector rod 18 when the exhaust control valve 6 is closed, the lock tube 16 is arranged at the lower part of the opening of the spring sleeve 14, the lock tube 16 can block the rope hook 11 from unhooking, the tail end of the spring sleeve 14 is connected with the liquid inlet control valve 5 through threads and is fixed through the side screw 5-3, the top end of the rope hook 11 is communicated with an exhaust pipe 12, and a sampling rope 19 is connected to the tail end of the rope.
The bottom of the K-shaped ejector rod 18 is provided with a groove 18-1 for assisting in exhausting, so that the gas in the bottle body 1 can be conveniently and rapidly exhausted.
The bottle body 1 be cylindrical bottle, further, bottle 1 by cylindrical bottle and round slice bottle end 20 sealing connection form, bottle end 20 adopt nickel alloy, it is compared in the stainless steel, can not produce the reaction with fluid for the fluid is rotten after long-time storage.
The bottle body 1 and the sampling cover are preferably connected in a threaded sealing way.
The invention can also replace the sampling cover by the sealing cover to store the sample liquid in the bottle body 1 in a sealing way.
The sealing cover is provided with an upper cover 9, a threaded hole is formed in the middle of the upper cover 9, an adjusting knob 10 is screwed on the upper surface of the upper cover 9 through the threaded hole, a hard plate 8 is padded in the sealing cover, and a sealing ring 21 is tightly attached to the lower side of the hard plate 8.
The bottle body 1 is made of transparent materials, is preferably glass, is more preferably toughened glass, and can effectively prevent external impact and bear the extrusion of sample liquid to the bottle body and prevent deformation.
The gas-liquid split-flow type multifunctional sampling and measuring device has the functions of liquid sampling, sealed storage of samples, liquid density and temperature measurement.
The method for sampling liquid by using the gas-liquid split-flow type multifunctional sampling and measuring device comprises the following steps:
the cover body 2 fixedly provided with the rope control device is connected with the bottle body 1 in a sealing way;
according to the requirement of the speed of liquid feeding, the liquid feeding control valve plate 7 is rotated to a preset position;
the rope hook 11 is clamped into the K-shaped ejector rod 18, and the rope hook 11 and the K-shaped ejector rod 18 are in a locking state;
the portable sampling rope 19 is utilized, and the gas-liquid split-type multifunctional sampling measuring device is stably placed in a container to be sampled;
After the sampling measuring device is lowered to a preset depth, rapidly lifting the sampling rope 19 for a certain distance, lowering the sampling rope to a original position, pushing the K-shaped ejector rod 18 to move downwards by using the spring 13 in the spring sleeve 14, and popping up and unlocking the rope hook 11;
The liquid inlet control valve 5 moves downwards under the action of gravity to separate from the cover boss 2-1, the bottle boss 1-1 is tightly sealed, the exhaust control valve 6 descends, the exhaust channel 5-2 is opened, sample liquid enters through the liquid inlet through groove or the liquid inlet through hole 4 on the side surface of the sliding through hole 3, and smoothly flows into the strip-shaped liquid inlet groove 1-2 or continuous liquid inlet holes on the side surface of the bottle boss 1-1 along the partition plate 5-1 on the liquid inlet control valve 5, and the sample liquid flows in along the bottle wall of the bottle 1 through the liquid inlet groove 1-2 or the liquid inlet holes, so that the impact force during inflow is slowed down;
The gas to be discharged in the bottle body 1 is discharged through the exhaust pipe 5-2 at the center of the baffle plate 5-1, and the gas is further discharged upwards through the gap in the spring sleeve 14;
after the gas is completely discharged and the bottle body 1 is filled with sample liquid, the sampling rope 19 is lifted up, and the sampling container is lifted up.
The liquid sampling comprises sampling a bottom sample, sampling a sample and sampling a whole course;
The method for taking liquid bottom samples and sample application by utilizing the gas-liquid split-flow type multifunctional sampling and measuring device comprises the following steps:
the sampling cover fixedly provided with the rope control device is connected with the bottle body in a sealing way;
according to the requirement of the speed of liquid inlet, rotating an adjusting groove formed on a liquid inlet adjusting plate to a preset position;
the rope hook is clamped into the K-shaped ejector rod, the rope hook and the K-shaped ejector rod are in a locking state, and the locking pipe is adjusted downwards to keep the hook groove normally open;
The sampling rope is extracted by hands, and the gas-liquid split-flow type multifunctional liquid sampler is stably placed in a container to be sampled;
after the sampler is lowered to a depth close to the bottom of the container, rapidly lifting the sampling rope for a certain distance, lowering the sampling rope to a original position, pushing the K-shaped ejector rod to move downwards by using a spring in the spring sleeve, and popping up and unlocking the rope hook;
The through hole shaft moves downwards under the action of gravity, the liquid inlet control valve plate descends, the liquid inlet channel I and the exhaust chamber are opened, sample liquid enters through the liquid inlet channel I on the cover body and smoothly flows in along the drainage disc, and the sample liquid slowly flows in along the bottle wall of the bottle body through the liquid inlet groove or the liquid inlet hole on the drainage disc, so that the impact force during inflow is slowed down;
the gas to be discharged in the bottle body is discharged through the exhaust through pipe of the through hole shaft, and the gas is further discharged upwards through the gap in the spring sleeve;
When the bottle body is subjected to liquid feeding and air discharging, the sampling rope is lifted upwards at a constant speed, the container to be sampled is directly lifted out completely, and when the container is completely taken out, the bottle body cannot be filled with the sample liquid injected into the bottle body (if the bottle body is full, the sampling of the whole layer of sample is failed, and the sampling rope is required to be resampled until the bottle body is not filled with the sample liquid).
The method for sealing and storing the sample by using the gas-liquid split-flow type multifunctional sampling and measuring device comprises the following steps:
taking down the sampling cover in the gas-liquid split-type multifunctional sampling and measuring device for sampling the liquid sample, replacing the sealing cover 9, connecting the sealing cover with the bottle body 1, rotating the adjusting knob 10 of the sealing cover downwards, and ejecting the hard plate 8 downwards for a certain distance to enable the hard plate 8 to press the bottle body 1.
When the liquid sample in the storage is required to be taken out, the adjusting knob 10 of the sealing cover is firstly rotated upwards, the hard plate 8 is loosened upwards for a certain distance, and the sealing cover can be easily unscrewed and the sample liquid can be taken out.
The method for testing the density or temperature of the stored sample in the bottle body by using the gas-liquid split-flow type multifunctional sampling and measuring device comprises the following steps:
and opening the bottle body 1 containing the sample liquid, and putting the bottle body into a glass densimeter.
When the temperature needs to be measured, the glass thermometer is put into the glass thermometer.

Claims (6)

1.一种气液分流式多功能取样测量装置,其特征在于:包括瓶体和上方的取样盖;瓶体和取样盖之间通过螺纹或卡扣密封连接;1. A gas-liquid split-flow multifunctional sampling and measuring device, characterized in that: it comprises a bottle body and a sampling cover on the upper side; the bottle body and the sampling cover are sealed and connected by a thread or a buckle; 所述的取样盖包括圆形的盖体,在盖体的中心处开设有滑动通孔,滑动通孔的侧面开设有圆弧形的进液通槽或进液通孔;在为进液通孔时,进液通孔具有多个等尺寸的通孔沿盖体的中心进行圆弧排列,进液通槽或进液通孔的圆弧为劣弧;在进液通槽或进液通孔的外围设有盖体凸台;在盖体的下方以滑动通孔为中心轴套插有进液控制阀,进液控制阀的下端具有隔板,在隔板上方的中心处具有中空的排气通道,当隔板的上表面受拉力向上贴紧密封盖体凸台时,关闭进液通槽或进液通孔,进液控制阀的轴向剖面为倒置的T形;在排气通道内装插有倒置的T形的排气控制阀,排气控制阀的顶端伸出排气通道并与绳控装置固定连接,绳控装置的下端通过螺纹与进液控制阀上的排气通道螺纹连接;在盖体的上表面或下表面以滑动通孔为轴心套装有与盖体上进液通槽或进液通孔相配套的进液控制阀板,在盖体上为进液通槽时,进液控制阀板上设置有与之对应的多个等尺寸的圆弧形排列的通孔,在盖体为进液通孔时,进液控制阀板上设置有与之对应的圆弧形的通槽,通过以滑动通孔为轴心转动进液控制阀板,能够有效控制盖体上进液通槽或进液通孔的闭合度,进而控制进液速度;The sampling cover comprises a circular cover body, a sliding through hole is provided at the center of the cover body, and an arc-shaped liquid inlet groove or liquid inlet hole is provided on the side of the sliding through hole; when it is a liquid inlet through hole, the liquid inlet through hole has a plurality of holes of equal size arranged in an arc along the center of the cover body, and the arc of the liquid inlet groove or the liquid inlet through hole is a minor arc; a cover body boss is provided on the periphery of the liquid inlet groove or the liquid inlet through hole; a liquid inlet control valve is inserted into a shaft sleeve with the sliding through hole as the center below the cover body, a partition is provided at the lower end of the liquid inlet control valve, and a hollow exhaust channel is provided at the center above the partition, when the upper surface of the partition is pulled upward and pressed against the sealing cover body boss, the liquid inlet groove or the liquid inlet through hole is closed, and the axial section of the liquid inlet control valve is an inverted T-shape; in the exhaust channel An inverted T-shaped exhaust control valve is installed, the top end of the exhaust control valve extends out of the exhaust channel and is fixedly connected to the rope control device, and the lower end of the rope control device is threadedly connected to the exhaust channel on the liquid inlet control valve through a thread; a liquid inlet control valve plate matching the liquid inlet groove or the liquid inlet hole on the cover body is sleeved on the upper surface or the lower surface of the cover body with the sliding through hole as the axis. When the cover body is the liquid inlet groove, the liquid inlet control valve plate is provided with a plurality of arc-shaped through holes of equal size corresponding thereto; when the cover body is the liquid inlet through hole, the liquid inlet control valve plate is provided with a corresponding arc-shaped through groove. By rotating the liquid inlet control valve plate with the sliding through hole as the axis, the closing degree of the liquid inlet groove or the liquid inlet through hole on the cover body can be effectively controlled, thereby controlling the liquid inlet speed; 在进液控制阀板装在盖体下方时,进液控制阀板安装在盖体与进液控制阀的隔板之间;When the liquid inlet control valve plate is installed under the cover body, the liquid inlet control valve plate is installed between the cover body and the partition of the liquid inlet control valve; 在瓶体的上方还具有与进液控制阀的隔板相配合的瓶体凸台,当隔板的下表面在重力作用下与瓶体凸台接触时,隔板能够起到密封作用,密封瓶体凸台上方的样液;A bottle body boss matched with the partition of the liquid inlet control valve is provided above the bottle body. When the lower surface of the partition contacts the bottle body boss under the action of gravity, the partition can play a sealing role to seal the sample liquid above the bottle body boss. 在瓶体凸台底部的侧面开设有条状的进液槽或连续的进液孔,样液通过进液槽或进液孔沿着瓶体的瓶壁流入,减缓流入时的冲击力,防止产生飞溅的液滴,影响取样精度。A strip-shaped liquid inlet groove or a continuous liquid inlet hole is opened on the side of the bottom of the bottle body boss. The sample liquid flows into the bottle body along the bottle wall through the liquid inlet groove or the liquid inlet hole, which reduces the impact force during the inflow and prevents splashing droplets from affecting the sampling accuracy. 2.根据权利要求1所述的一种气液分流式多功能取样测量装置,其特征在于:所述的绳控装置由绳钩、管帽、弹簧、弹簧套管、K形顶杆、锁管组成;弹簧套管的中部有轴向剖面为钩形开口的钩槽;弹簧套管上端安装有管帽、弹簧套管的腔内装有弹簧,弹簧的一端顶着管帽的内壁,另一端推压K形顶杆,K形顶杆的尾端固定连接有排气控制阀,并以侧面螺丝固定;在排气控制阀关闭的状态下,绳钩进入钩槽,卡在K形顶杆中部,弹簧套管开口的下部设有锁管,上调锁管可挡住绳钩脱钩,弹簧套管的尾端通过螺纹与进液控制阀连接,并以侧面螺丝固定,弹簧套管与排气通管相通,绳钩的顶端穿过管帽并连接有取样绳;2. A gas-liquid shunting multifunctional sampling and measuring device according to claim 1, characterized in that: the rope control device consists of a rope hook, a pipe cap, a spring, a spring sleeve, a K-shaped push rod, and a locking tube; the middle part of the spring sleeve has a hook groove with an axial cross-section of a hook-shaped opening; a pipe cap is installed on the upper end of the spring sleeve, and a spring is installed in the cavity of the spring sleeve, one end of the spring presses against the inner wall of the pipe cap, and the other end pushes the K-shaped push rod, and the tail end of the K-shaped push rod is fixedly connected to the exhaust control valve and fixed with a side screw; when the exhaust control valve is closed, the rope hook enters the hook groove and is stuck in the middle of the K-shaped push rod, and a locking tube is provided at the lower part of the opening of the spring sleeve, and the upward adjustment of the locking tube can prevent the rope hook from being unhooked, and the tail end of the spring sleeve is connected to the liquid inlet control valve through a thread and fixed with a side screw, the spring sleeve is communicated with the exhaust through-pipe, and the top end of the rope hook passes through the pipe cap and is connected to the sampling rope; 所述的K形顶杆的底部具有用于辅助排气的沟槽,方便快速排出瓶体内的气体。The bottom of the K-shaped ejector pin is provided with a groove for assisting exhaust, so as to facilitate and quickly discharge the gas in the bottle. 3.根据权利要求1所述的一种气液分流式多功能取样测量装置,其特征在于:所述的瓶体为圆柱形瓶体,所述的瓶体由圆柱形的瓶身和圆片状的瓶底密封连接而成,所述的瓶底采用镍合金;3. A gas-liquid split-flow multifunctional sampling and measuring device according to claim 1, characterized in that: the bottle body is a cylindrical bottle body, the bottle body is formed by sealingly connecting a cylindrical bottle body and a disc-shaped bottle bottom, and the bottle bottom is made of nickel alloy; 瓶体和取样盖之间通过螺纹密封连接。The bottle body and the sampling cover are connected by thread sealing. 4.根据权利要求1所述的一种气液分流式多功能取样测量装置,其特征在于:密封盖替换取样盖,将瓶体内的样液密封存储;4. A gas-liquid split flow multifunctional sampling and measuring device according to claim 1, characterized in that: the sealing cover replaces the sampling cover to seal and store the sample liquid in the bottle; 所述的密封盖具有上盖,上盖的中部开设有螺纹孔,上盖的上表面通过螺纹孔旋接有调节旋钮,在密封盖内垫装有硬质板材,硬质板材的下方紧贴有密封圈。The sealing cover has an upper cover, a threaded hole is opened in the middle of the upper cover, an adjusting knob is screwed on the upper surface of the upper cover through the threaded hole, a hard plate is padded inside the sealing cover, and a sealing ring is tightly attached to the lower part of the hard plate. 5.利用权利要求2中所述的气液分流式多功能取样测量装置进行液体取样的方法,其特征在于:5. A method for liquid sampling using the gas-liquid split flow multifunctional sampling and measuring device as claimed in claim 2, characterized in that: 液体取样包括取底样和取点样;Liquid sampling includes bottom sampling and spot sampling; 利用气液分流式多功能取样测量装置进行液体取底样和取点样的方法为:The method of taking liquid bottom sample and spot sample by using gas-liquid split flow multifunctional sampling and measuring device is as follows: 将固定安装有绳控装置的盖体与瓶体进行密封连接;The cover body on which the rope control device is fixedly installed is sealedly connected to the bottle body; 按照进液的速度要求,将进液控制阀板旋转至预定位置;According to the liquid inlet speed requirement, rotate the liquid inlet control valve plate to the predetermined position; 绳钩卡入K形顶杆内,绳钩与K形顶杆处于锁止状态;The rope hook is inserted into the K-shaped top rod, and the rope hook and the K-shaped top rod are in a locked state; 利用手提取样绳,并平稳地将气液分流式多功能取样测量装置放入待取样的容器中;Use your hands to extract the sample rope and steadily place the gas-liquid split-flow multifunctional sampling and measuring device into the container to be sampled; 待取样测量装置下放至预定深度后,急速将取样绳上提一段距离,并下放至原定位置,利用弹簧套管内的弹簧推动K形顶杆向下运动,将绳钩弹出解锁;After the sampling and measuring device is lowered to the predetermined depth, the sampling rope is quickly lifted up for a distance and lowered to the original position. The spring in the spring sleeve is used to push the K-shaped push rod downward to pop out the rope hook and unlock it. 进液控制阀在重力的作用下向下运动离开盖体凸台,贴紧密封瓶体凸台,同时排气控制阀下行,开启排气通道,样液通过滑动通孔侧面的进液通槽或进液通孔进入,顺着进液控制阀上的隔板平缓地流入瓶体凸台侧面的条状的进液槽或连续的进液孔,样液通过进液槽或进液孔沿着瓶体的瓶壁流入,减缓流入时的冲击力;The liquid inlet control valve moves downward under the action of gravity, leaving the cover body boss and tightly sealing the bottle body boss. At the same time, the exhaust control valve moves downward to open the exhaust channel. The sample liquid enters through the liquid inlet groove or the liquid inlet hole on the side of the sliding through hole, and flows smoothly into the strip-shaped liquid inlet groove or the continuous liquid inlet hole on the side of the bottle body boss along the partition on the liquid inlet control valve. The sample liquid flows in along the bottle wall of the bottle body through the liquid inlet groove or the liquid inlet hole, which reduces the impact force when flowing in. 瓶体内的待排出的气体通过隔板中心处的排气通道排出,气体通过弹簧套管内的空隙向上排出;The gas to be discharged in the bottle is discharged through the exhaust channel at the center of the partition, and the gas is discharged upward through the gap in the spring sleeve; 待气体完全排出,瓶体内灌满样液后,拎取取样绳,拎出取样的容器即可。After the gas is completely discharged and the bottle is filled with sample liquid, pick up the sampling rope and take out the sampling container. 6.利用权利要求4中所述的气液分流式多功能取样测量装置进行密封存储样品的方法,其特征在于:6. A method for sealing and storing samples using the gas-liquid split-flow multifunctional sampling and measuring device as claimed in claim 4, characterized in that: 将已完成液体样品取样的气液分流式多功能取样测量装置中的取样盖取下,换上密封盖,将密封盖与瓶体连接,再将密封盖的调节旋钮向下旋转,将硬质板材向下顶出一段距离,使硬质板材压紧瓶体;Remove the sampling cover of the gas-liquid split-flow multifunctional sampling and measuring device that has completed the liquid sample sampling, replace it with a sealing cover, connect the sealing cover to the bottle body, and then rotate the adjustment knob of the sealing cover downward to push the hard plate downward for a distance so that the hard plate presses the bottle body; 在需要将存储内的液体样品取出时,先将密封盖的调节旋钮向上旋转,将硬质板材向上松出一段距离,即可轻松地将密封盖旋松并取出样液。When it is necessary to take out the liquid sample in the storage, first rotate the adjusting knob of the sealing cover upwards, loosen the hard plate upwards for a distance, and then the sealing cover can be easily loosened and the sample liquid can be taken out.
CN202010066836.7A 2020-01-20 2020-01-20 Gas-liquid split-flow multifunctional sampling and measuring device and use method thereof Active CN111076979B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN202010066836.7A CN111076979B (en) 2020-01-20 2020-01-20 Gas-liquid split-flow multifunctional sampling and measuring device and use method thereof

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN202010066836.7A CN111076979B (en) 2020-01-20 2020-01-20 Gas-liquid split-flow multifunctional sampling and measuring device and use method thereof

Publications (2)

Publication Number Publication Date
CN111076979A CN111076979A (en) 2020-04-28
CN111076979B true CN111076979B (en) 2025-04-18

Family

ID=70324016

Family Applications (1)

Application Number Title Priority Date Filing Date
CN202010066836.7A Active CN111076979B (en) 2020-01-20 2020-01-20 Gas-liquid split-flow multifunctional sampling and measuring device and use method thereof

Country Status (1)

Country Link
CN (1) CN111076979B (en)

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN203824799U (en) * 2014-05-13 2014-09-10 江苏爵格工业设备有限公司 Airtight sampling device
CN107515173A (en) * 2017-09-29 2017-12-26 南京博龙仪器科技有限公司 A kind of full-service fluid sampling colour comparatour and its application method
CN211504797U (en) * 2020-01-20 2020-09-15 南京博龙仪器科技有限公司 Gas-liquid shunting type multifunctional sampling measuring device

Family Cites Families (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN203310654U (en) * 2013-02-21 2013-11-27 舟山市检验检疫科学技术研究院 Oil product bottom water sampler of vertical shore tank
EP3151965B1 (en) * 2014-06-04 2021-02-24 Edan Instruments, Inc. Sample collection and analysis devices

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN203824799U (en) * 2014-05-13 2014-09-10 江苏爵格工业设备有限公司 Airtight sampling device
CN107515173A (en) * 2017-09-29 2017-12-26 南京博龙仪器科技有限公司 A kind of full-service fluid sampling colour comparatour and its application method
CN211504797U (en) * 2020-01-20 2020-09-15 南京博龙仪器科技有限公司 Gas-liquid shunting type multifunctional sampling measuring device

Also Published As

Publication number Publication date
CN111076979A (en) 2020-04-28

Similar Documents

Publication Publication Date Title
US8578754B2 (en) Adsorbed gas content measuring instrument and its testing method
FR2601451A1 (en) PERMEAMETER RELATIVE GAS-LIQUID AUTOMATISE
CN205300978U (en) Water sample collector
CN111076979B (en) Gas-liquid split-flow multifunctional sampling and measuring device and use method thereof
US8061221B2 (en) Liquid sampling apparatus
CN111076978B (en) A gas-liquid split-flow multifunctional liquid sampler and its use method
CN211504797U (en) Gas-liquid shunting type multifunctional sampling measuring device
CN205981783U (en) Prevent disturbance and proclaim oneself formula liquid sampling device device
CN211504795U (en) Gas-liquid shunting type multifunctional liquid sampler
US4150560A (en) Measuring cell for the continuous determination of a liquid, especially a beverage flowing through a pipe
CN211504796U (en) Sampling cover of gas-liquid shunting type multifunctional liquid sampler
US3028759A (en) Method and apparatus for obtaining average samples of liquid in tanks
CN211717840U (en) Bottle bottom liquid feeding mechanism of gas-liquid shunting type multifunctional liquid sampler
CN205175742U (en) Barreled liquid sampling device instrument
CN201199237Y (en) Ammonia nitrogen measuring chamber
CN106289876A (en) Fluid sampling device and sampling method thereof
CN115855572B (en) Unmanned aerial vehicle for monitoring water quality of lake and reservoir
JPH06144491A (en) Filling apparatus
CN100476160C (en) Automatic continuous sampler for oil well
FR2708341A1 (en) Method for dosing, in particular micro-dosing of a liquid; application to obtaining controlled dilutions, in particular nanovolumetric dilutions.
CN220729720U (en) Grain and oil inspection sampling device
US3442138A (en) Particulate solid sampling device
CN223332679U (en) Liquid oxygen analysis sampling device
US2198324A (en) Temperature determining apparatus and sampler for liquid containers
US2746298A (en) Specific gravity measuring apparatus

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
GR01 Patent grant
GR01 Patent grant