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CN110803960A - Broccoli planting fertilizer capable of reducing plant diseases and insect pests - Google Patents

Broccoli planting fertilizer capable of reducing plant diseases and insect pests Download PDF

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Publication number
CN110803960A
CN110803960A CN201911363820.6A CN201911363820A CN110803960A CN 110803960 A CN110803960 A CN 110803960A CN 201911363820 A CN201911363820 A CN 201911363820A CN 110803960 A CN110803960 A CN 110803960A
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CN
China
Prior art keywords
broccoli
fertilizer
sepiolite
microcrystalline cellulose
chitosan
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Pending
Application number
CN201911363820.6A
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Chinese (zh)
Inventor
高云中
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Anhui Cloud Ecological Agriculture Development Co Ltd
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Anhui Cloud Ecological Agriculture Development Co Ltd
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Priority to CN201911363820.6A priority Critical patent/CN110803960A/en
Publication of CN110803960A publication Critical patent/CN110803960A/en
Pending legal-status Critical Current

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    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05DINORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C; FERTILISERS PRODUCING CARBON DIOXIDE
    • C05D9/00Other inorganic fertilisers
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05GMIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G3/00Mixtures of one or more fertilisers with additives not having a specially fertilising activity

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Inorganic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Pest Control & Pesticides (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)

Abstract

The invention discloses a broccoli planting fertilizer capable of reducing plant diseases and insect pests, which comprises 500 parts of 100-one-wall water, 20-30 parts of sepiolite, 10-15 parts of nano silicon dioxide, 1-3 parts of nano titanium dioxide, 1-3 parts of graphene oxide, 1-3 parts of bacterial cellulose, 0.1-0.5 part of sodium polystyrene sulfonate, 0.1-0.5 part of microcrystalline cellulose, and also comprises polyallylamine, humic acid and chitosan. Wherein the sepiolite is preferably chitosan in which magnesium ions in the skeleton are replaced by hydrogen ions, the microcrystalline cellulose is preferably microcrystalline cellulose with the ultimate degree of polymerization of 100-150, and the chitosan is preferably chitosan with the degree of deacetylation of 90-95%. The product obtained by the invention can form an organic-inorganic composite film layer on the surface of the broccoli, can play a role of effectively slowly releasing fertilizer, and can prevent the invasion of plant diseases and insect pests to plants.

Description

Broccoli planting fertilizer capable of reducing plant diseases and insect pests
Technical Field
The invention relates to the field of agricultural fertilizers, in particular to a fertilizer for planting broccoli, which can reduce plant diseases and insect pests.
Background
Broccoli, also known as cauliflower, is a 1-2 year old herbaceous plant. The broccoli is rich in nutrition, contains protein, sugar, fat, vitamins and carotene, has the nutritional ingredients at the head of similar vegetables, and is known as 'vegetable crown'.
The broccoli is suitable for being planted on loam and sandy loam which are good in irrigation and drainage, deep in plough layer, loose and fertile in soil and strong in water and fertility preservation, and needs sufficient fertilizer in the whole growth process, wherein the nitrogen-phosphorus-potassium ratio of the broccoli is 14: 5: and 8, in the growth process of the flower ball, the broccoli has more requirements on trace elements such as boron, molybdenum, magnesium and the like, so that the yield and the quality can be obviously improved by applying a proper trace element foliar fertilizer before budding.
1. Illumination: the requirements of broccoli on illumination are not very strict, but sufficient illumination is favored in the growth process, the plants grow strongly when the illumination is sufficient, strong nutriments can be formed, photosynthesis and nutrient accumulation are facilitated, the flower balls are compact and compact, the color is bright green, the quality is good, and the growth and development of the broccoli are not facilitated due to excessively strong sunlight in summer.
2. Temperature: in the range of 5-20 deg.C, the higher the temperature, the faster the growth and development of broccoli. The optimum germination temperature is 20-25 ℃, and the optimum growth temperature in the seedling stage is 15-20 ℃. The broccoli has strong cold resistance and heat resistance, the growth temperature in the rosette stage is 20-22 ℃, the development temperature of the curd is 15-18 ℃, the quality of the curd is easy to deteriorate when the temperature is higher than 25 ℃, but the curd can still slowly grow at the low temperature of 5 ℃ or even below as long as the curd is not frozen.
The temperature requirements for vernalization completion of different varieties and different seedling ages are greatly different, so that the selection of varieties in annual cultivation is very important.
3. Water content: the water demand of the broccoli is large in the whole growth process, particularly, the broccoli cannot lack water in the vigorous growth period and the ball formation period, and the yield is reduced even if the broccoli is drought for a short time. Diseases such as black rot, black spot and the like are easily caused by heavy rain in the seedling stage or overhigh soil humidity. The soil humidity in the formation period of the flower ball can meet the growth requirement only when the field water capacity is about 70-80%.
4. Soil: the broccoli has low requirements on soil conditions, but if the broccoli is too lean, the plant is dysplastic, the yield and the quality are low, and if the soil is too fertile, the flower buds are loose and the flower moss is hollow. The broccoli is suitable for being planted on loam and sandy loam which are good in irrigation and drainage, deep in plough layer, loose and fertile in soil and strong in water retention and fertility preservation. The pH value of the soil is adapted to 5.5-8, but 6 is the best. The broccoli needs sufficient fertilizer in the whole growth process, and the N, P, K ratio of the broccoli is 14: 5: 8. the nitrogen requirement is relatively high in the seedling stage, and the P, K requirement is relatively increased after flower buds begin to differentiate.
However, in the field of broccoli planting, different fertilizers are continuously researched to supplement nutrient elements lacking in broccoli, and the influence on illumination, moisture, temperature and the like of the broccoli after fertilization, particularly after foliar fertilizer application, is ignored, and the influence on pest and disease resistance of the broccoli after fertilizer application is not concerned.
Disclosure of Invention
The invention aims to provide a fertilizer for planting broccoli capable of reducing plant diseases and insect pests, and aims to solve the problems that after foliar fertilizer is applied in the prior art, factors such as illumination, moisture and temperature required by growth of broccoli are adversely affected, and improvement of disease and insect pest resistance of products cannot be realized.
In order to achieve the purpose, the invention provides the following technical scheme:
a fertilizer for broccoli planting capable of reducing plant diseases and insect pests comprises the following raw materials in percentage by species:
100 portions of water, 20 to 30 portions of sepiolite, 10 to 15 portions of nano silicon dioxide, 1 to 3 portions of nano titanium dioxide, 1 to 3 portions of graphene oxide, 1 to 3 portions of bacterial cellulose, 0.1 to 0.5 portion of sodium polystyrene sulfonate and 0.1 to 0.5 portion of microcrystalline cellulose.
The technical scheme of the invention introduces sepiolite, nano silicon dioxide, nano titanium dioxide, graphene oxide, bacterial cellulose and microcrystalline cellulose, firstly, the molecular structures of the bacterial cellulose and the microcrystalline cellulose also have a large amount of active polar functional groups such as hydroxyl, when the product is sprayed on the surface of broccoli, the product can be well compatible with the surface of broccoli, and a gelled structure is formed on the surface, meanwhile, the sepiolite, the nano silicon dioxide, the nano titanium dioxide and the graphene oxide all contain polar functional groups such as hydroxyl, carboxyl and the like which can form hydrogen bond acting force with the gelled structure, so that an organic-inorganic composite gel layer is constructed on the surface of the broccoli, the gel layer is transparent and light, the normal photosynthesis of the broccoli can not be blocked, and due to the existence of sodium polystyrene sulfonate, a benzene ring can be mutually attracted and adsorbed with a conjugated region of the graphene oxide, the graphene oxide layers are mutually repelled due to the same negative charges, so that the interlayer spacing is widened, and a diffusion channel of air and water vapor is formed in the composite gel layer, so that the normal respiration of the broccoli cannot be influenced; in addition, the organic-inorganic composite gel layer keeps good mechanical strength, and the effect of plant diseases and insect pests on broccoli can be effectively prevented; the free radicals generated by the nano titanium dioxide under the action of sunlight can also have good effect of resisting microorganisms such as bacteria and the like; with the prolonging of the service life of the product, the bacterial cellulose and the microcrystalline cellulose are gradually degraded and directly absorbed by broccoli as nutrient components, thereby playing a role in fertilizer efficiency; moreover, the composite gel layer can play a good heat preservation and insulation effect, the plants can be maintained at a relatively high temperature at night, the plant metabolism reduction caused by high temperature can be avoided in the daytime, the excessive transpiration effect is realized, an independent small greenhouse is formed, and the broccoli can grow rapidly.
Further, the modified polyallylamine aqueous solution also comprises polyallylamine with the water mass of 1-5%.
The technical scheme of the invention introduces polyallylamine which can absorb carbon dioxide generated by plant respiration at night, and the carbon dioxide is released after sunlight irradiation in the day and can be directly used as nutrient for photosynthesis to play a good regulating role.
Further, the sepiolite is sepiolite in which magnesium ions in the framework are replaced by hydrogen ions.
Further, the sepiolite is sepiolite in which magnesium ions in the framework are completely replaced by hydrogen ions.
According to the technical scheme, the sepiolite with the magnesium ions replaced by the hydrogen ions in the framework is utilized, and Si-O functional groups are converted into Si-OH after the sepiolite is replaced, so that the hydrogen bond acting force between the sepiolite and other components is enhanced, the mechanical performance of the gel is further improved, and the attack of insect pests is avoided.
Furthermore, the humic acid fertilizer also comprises humic acid with the water mass of 1-10%.
Further, the microcrystalline cellulose is microcrystalline cellulose with the limiting degree of polymerization of 100-150.
Further, the microcrystalline cellulose is microcrystalline cellulose with the limiting degree of polymerization of 120-150.
Further, the water-soluble chitosan-chitosan composite material also comprises chitosan with the water mass of 1-5%.
Further, the chitosan is chitosan with deacetylation degree of 85-95%.
Further, the chitosan is chitosan with deacetylation degree of 90-95%.
The invention introduces chitosan and further limits the deacetylation degree of the chitosan so as to control the solubility of the chitosan in water and the strength of formed gel, so that the product has good affinity and insect resistance.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
According to the weight portion, 100 portions of water, 20 to 30 portions of sepiolite, 10 to 15 portions of nano silicon dioxide, 1 to 3 portions of nano titanium dioxide, 1 to 3 portions of graphene oxide, 1 to 3 portions of bacterial cellulose, 0.1 to 0.5 portion of sodium polystyrene sulfonate and 0.1 to 0.5 portion of microcrystalline cellulose are taken in turn, after the bacterial cellulose, the microcrystalline cellulose and the water are mixed, a stirrer is used for stirring and dispersing at the speed of 500r/min of 300 portions of chitosan, the sepiolite, the nano silicon dioxide, the nano titanium dioxide, the graphene oxide and the sodium polystyrene sulfonate are added, under the condition that the ultrasonic frequency is 40 to 100kHz, the polyallylamine with the mass of 1 to 5 percent of water, the humic acid with the mass of 1 to 10 percent of water and the chitosan with the mass of 1 to 5 percent of water are added after ultrasonic dispersion is carried out for 45 to 60 minutes, under the stirring state, introducing argon at the speed of 300-;
the sepiolite is sepiolite in which magnesium ions in a framework are completely replaced by hydrogen ions; the microcrystalline cellulose is microcrystalline cellulose with the limiting polymerization degree of 100-150; the chitosan has deacetylation degree of 85-95%.
Example 1
Taking 100 parts of water, 20 parts of sepiolite, 10 parts of nano silicon dioxide, 1 part of nano titanium dioxide, 1 part of graphene oxide, 1 part of bacterial cellulose, 0.1 part of sodium polystyrene sulfonate and 0.1 part of microcrystalline cellulose in sequence, mixing the bacterial cellulose, the microcrystalline cellulose and the water, stirring and dispersing for 20min at the speed of 300r/min by using a stirrer, then adding the sepiolite, the nano silicon dioxide, the nano titanium dioxide, the graphene oxide and the sodium polystyrene sulfonate, ultrasonically dispersing for 45min under the condition that the ultrasonic frequency is 40kHz, then adding polyallylamine with the mass of 1% of water, humic acid with the mass of 1% of water and chitosan with the mass of 1% of water, introducing argon at the speed of 300mL/min under the stirring state, stirring and mixing, and then sealing and filling to obtain a product;
the sepiolite is sepiolite in which 50% of magnesium ions in a framework are replaced by hydrogen ions; the microcrystalline cellulose is microcrystalline cellulose with the limiting polymerization degree of 100; the chitosan is chitosan with deacetylation degree of 85%.
Example 2
According to the weight parts, 300 parts of water, 25 parts of sepiolite, 12 parts of nano silicon dioxide, 2 parts of nano titanium dioxide, 2 parts of graphene oxide, 2 parts of bacterial cellulose, 0.3 part of sodium polystyrene sulfonate and 0.3 part of microcrystalline cellulose are taken in sequence, the bacterial cellulose, the microcrystalline cellulose and the water are mixed, stirred and dispersed for 30min at the speed of 400r/min by a stirrer, then the sepiolite, the nano silicon dioxide, the nano titanium dioxide, the graphene oxide and the sodium polystyrene sulfonate are added, under the condition that the ultrasonic frequency is 50kHz, ultrasonic dispersion is carried out for 50min, then polyallylamine with the water mass of 3%, humic acid with the water mass of 5% and chitosan with the water mass are added, under the stirring state, argon gas is introduced at the speed of 400mL/min, and after stirring and mixing, sealed filling is carried out, so as to obtain a product;
the sepiolite is sepiolite in which magnesium ions in a framework are completely replaced by hydrogen ions; the microcrystalline cellulose is microcrystalline cellulose with the limiting polymerization degree of 120; the chitosan is chitosan with deacetylation degree of 90%.
Example 3
According to the weight parts, 500 parts of water, 30 parts of sepiolite, 15 parts of nano silicon dioxide, 3 parts of nano titanium dioxide, 3 parts of graphene oxide, 3 parts of bacterial cellulose, 0.5 part of sodium polystyrene sulfonate and 0.5 part of microcrystalline cellulose are taken in sequence, the bacterial cellulose, the microcrystalline cellulose and the water are mixed, stirred and dispersed for 50min at the speed of 500r/min by a stirrer, then the sepiolite, the nano silicon dioxide, the nano titanium dioxide, the graphene oxide and the sodium polystyrene sulfonate are added, under the condition that the ultrasonic frequency is 100kHz, ultrasonic dispersion is carried out for 60min, then polyallylamine with the water mass of 5 percent, humic acid with the water mass of 10 percent and chitosan with the water mass of 5 percent are added, under the stirring state, argon is introduced at the speed of 500mL/min, and after stirring and mixing, sealed filling is carried out, thus obtaining the product;
the sepiolite is sepiolite in which magnesium ions in a framework are completely replaced by hydrogen ions; the microcrystalline cellulose is microcrystalline cellulose with the limiting polymerization degree of 150; the chitosan is chitosan with deacetylation degree of 95%.
Comparative example 1
Compared with example 1, the comparative example does not add nano-silica and nano-titania, and the rest conditions are kept unchanged.
Comparative example 2
This comparative example compared to example 1, no polyallylamine was added and the remaining conditions were maintained.
Comparative example 3
In this comparative example, no chitosan was added, as compared to example 1, and the remaining conditions were maintained.
The products obtained in comparative examples 1 to 3 and examples 1 to 3 were subjected to performance tests, the specific test modes and test results are as follows:
the pH value of soil for test is 8.47, the content of alkaline hydrolysis nitrogen is 47.2mg/kg, the content of quick-acting phosphorus is 10.2mg/kg, the content of quick-acting potassium is 120mg/kg, and the content of organic matters is 20.3 g/kg; spraying the product at the beginning of the rosette stage of broccoli, controlling the spraying amount to be 200kg/hm2, and starting batch harvesting after the diameter of a flower ball is combined with an outlet standard; in the growth process, regularly observing whether pests grow on the surface of the ball every day;
during collection, 10 plants are selected to measure the diameter of the flower ball, the average value is taken, and the test results are shown in table 1:
table 1: product performance test meter
Experimental project Has no harmful insects Ball diameter/cm
Example 1 Is free of 15.6
Example 2 Is free of 16.2
Example 3 Is free of 16.9
Comparative example 1 Small amount of 11.3
Comparative example 2 Small amount of 10.6
Comparative example 3 Small amount of 11.1
The detection results in table 1 show that the product obtained by the invention has good regulation effect on the growth of broccoli after being applied to the broccoli, can effectively avoid the attack of plant diseases and insect pests, and does not have the adhesion of the plant diseases and insect pests on the surface in the growth process.
It will be evident to those skilled in the art that the invention is not limited to the details of the foregoing illustrative embodiments, and that the present invention may be embodied in other specific forms without departing from the spirit or essential attributes thereof. The present embodiments are therefore to be considered in all respects as illustrative and not restrictive, the scope of the invention being indicated by the appended claims rather than by the foregoing description, and all changes which come within the meaning and range of equivalency of the claims are therefore intended to be embraced therein, and any reference thereto is therefore intended to be embraced therein.

Claims (10)

1. The fertilizer for broccoli planting and capable of reducing plant diseases and insect pests is characterized by comprising the following raw materials in parts by weight:
100 portions of water, 20 to 30 portions of sepiolite, 10 to 15 portions of nano silicon dioxide, 1 to 3 portions of nano titanium dioxide, 1 to 3 portions of graphene oxide, 1 to 3 portions of bacterial cellulose, 0.1 to 0.5 portion of sodium polystyrene sulfonate and 0.1 to 0.5 portion of microcrystalline cellulose.
2. The fertilizer for broccoli planting capable of reducing pests and diseases as claimed in claim 1, further comprising polyallylamine with a water mass of 1-5%.
3. The fertilizer for planting broccoli capable of reducing pests and diseases according to claim 1, wherein the sepiolite is sepiolite in which magnesium ions in the framework are replaced by hydrogen ions.
4. A broccoli planting fertilizer capable of reducing pests and diseases according to claim 3, wherein the sepiolite is a sepiolite in which magnesium ions in a framework are completely replaced by hydrogen ions.
5. The fertilizer for planting broccoli capable of reducing pests and diseases as claimed in claim 1, further comprising humic acid with a water quality of 1-10%.
6. The fertilizer for broccoli planting capable of reducing pests and diseases as claimed in claim 1, wherein the microcrystalline cellulose is microcrystalline cellulose with an ultimate degree of polymerization of 100-150.
7. The fertilizer for broccoli planting capable of reducing pests and diseases as claimed in claim 6, wherein the microcrystalline cellulose is microcrystalline cellulose with the limiting degree of polymerization of 120-150.
8. The fertilizer for broccoli planting capable of reducing pests and diseases as claimed in claim 1, wherein the fertilizer further comprises chitosan with the water mass of 1-5%.
9. A fertilizer for broccoli planting capable of reducing pests and diseases according to claim 7, wherein the chitosan has a deacetylation degree of 85-95%.
10. A fertilizer for broccoli planting according to claim 8, wherein the chitosan has a deacetylation degree of 90-95%.
CN201911363820.6A 2019-12-26 2019-12-26 Broccoli planting fertilizer capable of reducing plant diseases and insect pests Pending CN110803960A (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112479786A (en) * 2020-12-18 2021-03-12 袁新华 Organic foliar fertilizer for preventing and treating red date and coccid disease and preparation method thereof
CN113443939A (en) * 2021-07-30 2021-09-28 温炫亮 Molecular type nano silicon-titanium fertilizer and preparation method thereof

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106045770A (en) * 2016-05-31 2016-10-26 山东胜伟园林科技有限公司 Method for performing natural soil greening on low-lying saline soil by using soil conditioner containing chitosan
CN108752043A (en) * 2018-07-06 2018-11-06 佛山陵朝新材料有限公司 A kind of curing compound and preparation method thereof
CN109988462A (en) * 2019-02-25 2019-07-09 郭睿 A kind of aqueous antifoggant of automobile-used long-acting environment friendly

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106045770A (en) * 2016-05-31 2016-10-26 山东胜伟园林科技有限公司 Method for performing natural soil greening on low-lying saline soil by using soil conditioner containing chitosan
CN108752043A (en) * 2018-07-06 2018-11-06 佛山陵朝新材料有限公司 A kind of curing compound and preparation method thereof
CN109988462A (en) * 2019-02-25 2019-07-09 郭睿 A kind of aqueous antifoggant of automobile-used long-acting environment friendly

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112479786A (en) * 2020-12-18 2021-03-12 袁新华 Organic foliar fertilizer for preventing and treating red date and coccid disease and preparation method thereof
CN113443939A (en) * 2021-07-30 2021-09-28 温炫亮 Molecular type nano silicon-titanium fertilizer and preparation method thereof

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Application publication date: 20200218