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CN110803697A - Graphitization and purification integrated furnace - Google Patents

Graphitization and purification integrated furnace Download PDF

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Publication number
CN110803697A
CN110803697A CN201911099136.1A CN201911099136A CN110803697A CN 110803697 A CN110803697 A CN 110803697A CN 201911099136 A CN201911099136 A CN 201911099136A CN 110803697 A CN110803697 A CN 110803697A
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CN
China
Prior art keywords
acquisition module
furnace
graphitization
purification integrated
isolation
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201911099136.1A
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Chinese (zh)
Inventor
尹朝洁
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Anhui Honglang Carbon Technology Co Ltd
Original Assignee
Anhui Honglang Carbon Technology Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Anhui Honglang Carbon Technology Co Ltd filed Critical Anhui Honglang Carbon Technology Co Ltd
Priority to CN201911099136.1A priority Critical patent/CN110803697A/en
Publication of CN110803697A publication Critical patent/CN110803697A/en
Pending legal-status Critical Current

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    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B32/00Carbon; Compounds thereof
    • C01B32/15Nano-sized carbon materials
    • C01B32/182Graphene
    • C01B32/194After-treatment
    • C01B32/196Purification
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B32/00Carbon; Compounds thereof
    • C01B32/15Nano-sized carbon materials
    • C01B32/182Graphene
    • C01B32/184Preparation

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Nanotechnology (AREA)
  • Inorganic Chemistry (AREA)
  • Carbon And Carbon Compounds (AREA)

Abstract

The invention discloses a graphitization and purification integrated furnace which comprises a furnace body, wherein a furnace body of the furnace body is made of special corrosion-resistant and high-temperature-resistant materials. Because the invention adopts special corrosion-resistant and high-temperature-resistant materials, the invention can deal with various working conditions, can be directly graphitized and purified, and has strong popularization value.

Description

Graphitization and purification integrated furnace
Technical Field
The invention relates to a graphitization and purification integrated furnace.
Background
The demand of the market for graphite materials is higher and higher, so the common graphite materials need further treatment. The treatment of ordinary graphite is mainly divided into two aspects, namely graphitization and purification.
The graphitization treatment method is high-temperature calcination, and the graphitization can improve the performance of the graphite material and discharge a small amount of impurities. The purification treatment method is that the purification gas is introduced to fully contact with the common graphite in a high-temperature environment, and the purification gas reacts with impurities contained in the common graphite material to generate gas and is discharged in the contact process, so that the aim of purifying the material is fulfilled.
Currently, for example, the semiconductor industry, consumes large quantities of high purity graphite materials in the manufacture of semiconductors. The functions of the existing high-temperature furnace in the market are single, and only graphitization or purification can be carried out. The pure graphitization high-temperature furnace cannot rapidly discharge impurities, the whole structure of the furnace is not corrosion-resistant and cannot be directly purified, the pure graphitization furnace cannot rapidly discharge impurities, and the furnace temperature is too low to be directly graphitized.
Disclosure of Invention
The invention aims to overcome the technical problems and provide a graphitization and purification integrated furnace.
In order to achieve the purpose, the invention adopts the following technical scheme:
the utility model provides an integrative stove of graphitization purification, includes the stove body, the furnace body of stove body adopts special anticorrosive high temperature resistant material, can arrange the miscellaneous fast, owing to adopt special anticorrosive high temperature resistant material, consequently can deal with various operating modes, can directly graphitization add the purification.
Further, the furnace body further comprises a monitoring operation system, the monitoring operation system comprises a system host and a thermocouple acquisition module, the thermocouple acquisition module is installed on the furnace body, and the acquired temperature is sent to the system host through an RS485 bus.
Further, the model of the thermocouple acquisition module is DAM 3038.
Further, the temperature measuring point and the head of the thermocouple acquisition module are insulated.
Further, control operation system still includes switching signal collection module, switching signal collection module includes that AC switch inputs isolation transmitter and isolation digital input module, the switch alarm signal of stove body passes through AC switch inputs isolation transmitter transform and is direct current signal, and AC switch inputs isolation transmitter and transmits and keep apart digital input module, keep apart digital input module and send for the system host computer through the RS485 bus again.
Further, the alternating current switch input isolation transmitter is S4431 in model number.
Further, the model of the isolation digital quantity input module is DAM 3013D.
Furthermore, the monitoring operation system further comprises a direct current signal acquisition module, the direct current signal acquisition module comprises a data acquisition card and a high-frequency differential isolator transmitter, the high-frequency differential isolator transmitter acquires a voltage signal of the rectifier and transmits the voltage signal to the data acquisition card, and the data acquisition card is converted into a digital signal through A/D and then inputs the digital signal to the system host.
Further, the model of the data acquisition card is PCI 8620.
The invention adopts special corrosion-resistant and high-temperature-resistant materials, can deal with various working conditions, can be directly graphitized and purified, and has strong popularization value.
Drawings
FIG. 1: the invention discloses a wiring schematic diagram of a thermocouple acquisition module.
FIG. 2: the invention discloses a wiring schematic diagram of a direct current signal acquisition module.
Detailed Description
The present invention will be described in detail below with reference to the accompanying drawings and examples.
The first embodiment is as follows:
the utility model provides an integrative stove of graphitization purification, includes the stove body, the furnace body of stove body adopts special anticorrosive high temperature resistant material, can arrange the miscellaneous fast, owing to adopt special anticorrosive high temperature resistant material, consequently can deal with various operating modes, can directly graphitization add the purification.
Example two:
the difference from the first embodiment is that the furnace body further comprises a monitoring operation system, as shown in fig. 1, the monitoring operation system comprises a system host and a thermocouple acquisition module, the thermocouple acquisition module is installed on the furnace body, and the acquired temperature is sent to the system host through an RS485 bus. The model of the thermocouple acquisition module is DAM3038, and the temperature measuring point and the head of the thermocouple acquisition module are insulated, so that the influence of a complex field working environment is avoided, and good stability and safety are ensured.
Example three:
the difference from the second embodiment is that the monitoring operation system further comprises a switch signal acquisition module, the switch signal acquisition module comprises an alternating current switch input isolation transmitter and an isolation digital quantity input module, a switch alarm signal of the furnace body is converted into a direct current signal through the alternating current switch input isolation transmitter, the alternating current switch input isolation transmitter transmits the direct current signal to the isolation digital quantity input module, and the isolation digital quantity input module transmits the direct current signal to the system host through an RS485 bus. The type of the alternating current switch input isolation transmitter is S4431, and the type of the isolation digital quantity input module is DAM 3013D.
Example four:
the difference from the third embodiment is that, as shown in fig. 2, the monitoring operation system further includes a dc signal acquisition module, the dc signal acquisition module includes a data acquisition card and a high-frequency differential isolator transmitter, the high-frequency differential isolator transmitter acquires a voltage signal of the rectifier and transmits the voltage signal to the data acquisition card, and the data acquisition card converts the voltage signal into a digital signal through an a/D and inputs the digital signal to the system host. The model of the data acquisition card is PCI8620, and the model of the high-frequency differential isolator transmitter is S1105H.
Finally, it should be noted that: the above embodiments are only used to illustrate the present invention and do not limit the technical solutions described in the present invention; thus, while the present invention has been described in detail with reference to the foregoing embodiments, it will be understood by those skilled in the art that various changes may be made and equivalents may be substituted; all such modifications and variations are intended to be included herein within the scope of this disclosure and the present invention and protected by the following claims.

Claims (9)

1. The utility model provides an integrative stove of graphitization purification, includes the stove body, its characterized in that: the furnace body of the furnace body is made of special corrosion-resistant and high-temperature-resistant materials.
2. The graphitization purification integrated furnace of claim 1, wherein: the furnace body further comprises a monitoring operation system, the monitoring operation system comprises a system host and a thermocouple acquisition module, the thermocouple acquisition module is installed on the furnace body, and the acquired temperature is sent to the system host through an RS485 bus.
3. The graphitization purification integrated furnace of claim 1, wherein: the model of the thermocouple acquisition module is DAM 3038.
4. The graphitization purification integrated furnace of claim 1, wherein: the temperature measuring point and the head of the thermocouple acquisition module are insulated.
5. The graphitization purification integrated furnace of claim 2, wherein: the monitoring operation system further comprises a switch signal acquisition module, the switch signal acquisition module comprises an alternating current switch input isolation transmitter and an isolation digital quantity input module, a switch alarm signal of the furnace body is converted into a direct current signal through the alternating current switch input isolation transmitter, the alternating current switch input isolation transmitter transmits the direct current signal to the isolation digital quantity input module, and the isolation digital quantity input module transmits the direct current signal to the system host through an RS485 bus.
6. The graphitization purification integrated furnace of claim 5, wherein: the type of the alternating current switch input isolation transmitter is S4431.
7. The graphitization purification integrated furnace of claim 5, wherein: the model of the isolation digital quantity input module is DAM 3013D.
8. The graphitization purification integrated furnace of claim 2, wherein: the monitoring operation system further comprises a direct current signal acquisition module, the direct current signal acquisition module comprises a data acquisition card and a high-frequency differential isolator transmitter, the high-frequency differential isolator transmitter acquires voltage signals of the rectifier and transmits the voltage signals to the data acquisition card, and the data acquisition card converts the voltage signals into digital signals through A/D and then inputs the digital signals to the system host.
9. The graphitization purification integrated furnace of claim 8, wherein: the model of the data acquisition card is PCI 8620.
CN201911099136.1A 2019-11-12 2019-11-12 Graphitization and purification integrated furnace Pending CN110803697A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201911099136.1A CN110803697A (en) 2019-11-12 2019-11-12 Graphitization and purification integrated furnace

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201911099136.1A CN110803697A (en) 2019-11-12 2019-11-12 Graphitization and purification integrated furnace

Publications (1)

Publication Number Publication Date
CN110803697A true CN110803697A (en) 2020-02-18

Family

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Family Applications (1)

Application Number Title Priority Date Filing Date
CN201911099136.1A Pending CN110803697A (en) 2019-11-12 2019-11-12 Graphitization and purification integrated furnace

Country Status (1)

Country Link
CN (1) CN110803697A (en)

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2009038650A1 (en) * 2007-09-21 2009-03-26 Siemens Energy & Automation, Inc. Systems and/or devices for providing an isolated analog output or analog input
CN102126721A (en) * 2011-04-27 2011-07-20 深圳市贝特瑞新能源材料股份有限公司 Purification and graphitization method of graphite material
US8009078B1 (en) * 2010-03-18 2011-08-30 General Electric Company Configurable analog input channel with galvanic isolation
CN204508817U (en) * 2015-03-27 2015-07-29 长沙格翎电池材料有限公司 A kind of graphite furnace temperature measuring apparatus

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2009038650A1 (en) * 2007-09-21 2009-03-26 Siemens Energy & Automation, Inc. Systems and/or devices for providing an isolated analog output or analog input
US8009078B1 (en) * 2010-03-18 2011-08-30 General Electric Company Configurable analog input channel with galvanic isolation
CN102126721A (en) * 2011-04-27 2011-07-20 深圳市贝特瑞新能源材料股份有限公司 Purification and graphitization method of graphite material
CN204508817U (en) * 2015-03-27 2015-07-29 长沙格翎电池材料有限公司 A kind of graphite furnace temperature measuring apparatus

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Application publication date: 20200218