CN1102682C - Functional Chinese medical stone fibres and its making method - Google Patents
Functional Chinese medical stone fibres and its making method Download PDFInfo
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- CN1102682C CN1102682C CN99100243A CN99100243A CN1102682C CN 1102682 C CN1102682 C CN 1102682C CN 99100243 A CN99100243 A CN 99100243A CN 99100243 A CN99100243 A CN 99100243A CN 1102682 C CN1102682 C CN 1102682C
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- 239000004575 stone Substances 0.000 title claims abstract description 72
- 238000000034 method Methods 0.000 title claims description 15
- 229920000297 Rayon Polymers 0.000 claims abstract description 32
- 239000000835 fiber Substances 0.000 claims abstract description 27
- 238000009987 spinning Methods 0.000 claims abstract description 18
- 239000004744 fabric Substances 0.000 claims abstract description 17
- 238000005516 engineering process Methods 0.000 claims abstract description 6
- 238000012545 processing Methods 0.000 claims abstract description 3
- 239000003292 glue Substances 0.000 claims description 17
- 239000003595 mist Substances 0.000 claims description 14
- 238000004519 manufacturing process Methods 0.000 claims description 11
- 239000007788 liquid Substances 0.000 claims description 9
- 238000007670 refining Methods 0.000 claims description 9
- 239000002994 raw material Substances 0.000 claims description 6
- 239000000463 material Substances 0.000 claims description 5
- 230000008569 process Effects 0.000 claims description 5
- 241000209094 Oryza Species 0.000 claims description 4
- 235000007164 Oryza sativa Nutrition 0.000 claims description 4
- 239000002253 acid Substances 0.000 claims description 4
- 239000003513 alkali Substances 0.000 claims description 4
- 238000001914 filtration Methods 0.000 claims description 4
- 235000009566 rice Nutrition 0.000 claims description 4
- 239000004113 Sepiolite Substances 0.000 claims description 3
- 238000013019 agitation Methods 0.000 claims description 3
- 238000004090 dissolution Methods 0.000 claims description 3
- 239000012535 impurity Substances 0.000 claims description 3
- 229910052745 lead Inorganic materials 0.000 claims description 3
- 235000012054 meals Nutrition 0.000 claims description 3
- 229910052753 mercury Inorganic materials 0.000 claims description 3
- 238000002156 mixing Methods 0.000 claims description 3
- 229910052624 sepiolite Inorganic materials 0.000 claims description 3
- 235000019355 sepiolite Nutrition 0.000 claims description 3
- 238000001179 sorption measurement Methods 0.000 claims description 3
- 238000005406 washing Methods 0.000 claims description 3
- 238000000227 grinding Methods 0.000 claims description 2
- 239000000126 substance Substances 0.000 claims description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 2
- 230000036541 health Effects 0.000 abstract description 6
- 239000004753 textile Substances 0.000 abstract description 6
- 239000011573 trace mineral Substances 0.000 abstract description 6
- 235000013619 trace mineral Nutrition 0.000 abstract description 6
- 229910052761 rare earth metal Inorganic materials 0.000 abstract description 5
- 238000000554 physical therapy Methods 0.000 abstract description 2
- 238000002360 preparation method Methods 0.000 abstract 2
- 230000002349 favourable effect Effects 0.000 abstract 1
- 239000000843 powder Substances 0.000 abstract 1
- 230000000694 effects Effects 0.000 description 5
- 238000012360 testing method Methods 0.000 description 5
- 229910000831 Steel Inorganic materials 0.000 description 4
- 230000008901 benefit Effects 0.000 description 4
- 239000010959 steel Substances 0.000 description 4
- 230000004071 biological effect Effects 0.000 description 3
- 230000000144 pharmacologic effect Effects 0.000 description 3
- 229920000742 Cotton Polymers 0.000 description 2
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 description 2
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 2
- 238000006477 desulfuration reaction Methods 0.000 description 2
- 230000023556 desulfurization Effects 0.000 description 2
- 230000004089 microcirculation Effects 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 238000005554 pickling Methods 0.000 description 2
- 230000005855 radiation Effects 0.000 description 2
- 102000005606 Activins Human genes 0.000 description 1
- 108010059616 Activins Proteins 0.000 description 1
- 241000894006 Bacteria Species 0.000 description 1
- 241000973497 Siphonognathus argyrophanes Species 0.000 description 1
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 1
- 206010043189 Telangiectasia Diseases 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 230000009471 action Effects 0.000 description 1
- 239000000488 activin Substances 0.000 description 1
- 238000004458 analytical method Methods 0.000 description 1
- 230000003110 anti-inflammatory effect Effects 0.000 description 1
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- 239000003908 antipruritic agent Substances 0.000 description 1
- 238000003556 assay Methods 0.000 description 1
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- 230000001473 noxious effect Effects 0.000 description 1
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- 230000035790 physiological processes and functions Effects 0.000 description 1
- 229920000642 polymer Polymers 0.000 description 1
- 230000001737 promoting effect Effects 0.000 description 1
- 230000008929 regeneration Effects 0.000 description 1
- 238000011069 regeneration method Methods 0.000 description 1
- 210000003296 saliva Anatomy 0.000 description 1
- 239000011734 sodium Substances 0.000 description 1
- 229910052938 sodium sulfate Inorganic materials 0.000 description 1
- 235000011152 sodium sulphate Nutrition 0.000 description 1
- 230000001954 sterilising effect Effects 0.000 description 1
- 238000004659 sterilization and disinfection Methods 0.000 description 1
- 239000011593 sulfur Substances 0.000 description 1
- 229910052717 sulfur Inorganic materials 0.000 description 1
- 208000009056 telangiectasis Diseases 0.000 description 1
- 238000009941 weaving Methods 0.000 description 1
- 239000011701 zinc Substances 0.000 description 1
- NWONKYPBYAMBJT-UHFFFAOYSA-L zinc sulfate Chemical compound [Zn+2].[O-]S([O-])(=O)=O NWONKYPBYAMBJT-UHFFFAOYSA-L 0.000 description 1
- 229960001763 zinc sulfate Drugs 0.000 description 1
- 229910000368 zinc sulfate Inorganic materials 0.000 description 1
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- Artificial Filaments (AREA)
Abstract
The present invention relates to a medical stone function fiber and a preparation method thereof, which belongs to the field of textiles. Medical stone miro-powder accounting for 0.001 to 30 wt% of a fiber is prepared into a medical stone refined solution by a special processing technology, and then the medical stone refined solution is added to viscose during the preparation process of viscose fibers to prepare the medical stone function fiber by spinning with an approximate conventional technology. The fiber contains a plurality of trace elements and rare-earth elements of medical stone, and thus, the fabrics made of the fiber have favorable physiotherapy and health care functions on human bodies.
Description
The present invention relates to a kind of functional fibre, especially functional Chinese medical stone fibres and manufacture method thereof belong to field of textiles.
Viscose fiber fabric has advantages such as good hygroscopicity, dyeability and low price because of it, be the main raw material of textile industry always, and its fabric extremely consumers in general is welcome.Along with the development of textile industry and the raising of people's living standard, people more and more pay attention to the health of human body self, a kind of " infrared multifunctional fiber and manufacture method " (publication number CN1123849A) disclosed so have the fabric of functions such as various health cares, the physiotherapy Chinese invention patent that quietly sells well on market, this method is to add some to have functional materials such as special fuel factor, magnetic effect and infra-red radiation in fibre-forming polymer, and the fabric that fiber process is become has the good health care effect.But do not find to contain the functional fibre of medical stone as yet.
The purpose of this invention is to provide a kind of functional Chinese medical stone fibres and manufacture method thereof with unique biological effect and magical pharmacological effect, the fabric that is made into functional Chinese medical stone fibres can play better health-care physiotherapeutic effect to wearer's human body, thereby further adapts to the demand in market.
Medical stone is a kind of natural medicine ore, because of wherein containing multiple and closely bound up trace element and the rare earth element of health, and has the pharmacological effect of unique biological effect and mystery.Since the sixties in this century, health drink that medical stone makes, health care device etc. appear utilizing in beginning successively.The present invention changes people drew trace element and rare earth element in the past from mouth convention, various trace elements in the high-quality medical stone and rare earth element after handling, special process are joined in the viscose glue, through firm being adsorbed on the cellulose macromolecule after the spinning, this fiber being become a kind ofly can produce the new type functional textile raw material of unique biological effect and magical pharmacological action human body.
The object of the present invention is achieved like this: this functional Chinese medical stone fibres is in the viscose manufacture process, makes after the refined liquid of interpolation medical stone micro mist, is characterized in that medical stone micro mist weight accounts for the 0.001-30% of fibre weight.
The manufacture method of this functional Chinese medical stone fibres is as follows:
1, the processing of medical stone micro mist
The medical stone raw material through washing, meal, dedusting, removal of impurities, is crushed to granularity 300-500 purpose medical stone micro mist with pulverizer machinery again;
2, the medical stone micro mist is refining
The medical stone micro mist dropped in alkali lye that concentration is the 5-160 grams per liter or the water soaked 24-56 hour, after mechanical agitation, use wherein harmful element such as Hg, Pb of chemical fibre material, micro porous filtration material or the filtering of sepiolite adsorption technology again, the refining liquid of medical stone;
3, the manufacturing of functional Chinese medical stone fibres viscose glue
In the yellow end of a period of viscose glue or course of dissolution the refining liquid of 2 gained medical stones is evenly added in the viscose glue, after 2-5 hour abundant mixing and grinding, making viscosity is the 30-60 functional Chinese medical stone fibres viscose glue with medical stone function of second;
4, the spinning of functional Chinese medical stone fibres
The functional Chinese medical stone fibres viscose glue is filtered the back to be increased 1-3 layer poplin cloth filter cloth and filters through conventional three roads, again behind conventional spinning acid bath, with spinning speed 40-70 rice/minute (than the low 10-20 rice of normal spinning speed/minute) carry out spinning, get functional Chinese medical stone fibres.
The mensuration of viscose riscosity adopts the general normal beam technique of the industry, and its principle is to utilize the steel ball of certain mass, and the speed that descends in viscosity tube is measured its viscosity, and institute's elapsed time is directly proportional with viscosity, so viscose riscosity shows with the time stopwatch.Concrete assay method is: behind the viscose glue sample thermometric that will just fetch, pour drying into and in the clean viscosity tube, the liquid level of viscose glue is flat with the horizontal saliva of test tube mouth, concave and convex phenomenon can not be arranged, and vertically put into rack for test tube.Steel ball is put into test tube mouth center, start stopwatch simultaneously, observe steel ball and arrive pipe during the end, steel ball decline required time number second is write down in stopwatch immediately.Add or deduct temperature correction value, promptly get viscose riscosity.
Below in conjunction with following embodiment the present invention is further described, scope of the present invention is not subjected to the restriction of present embodiment.
The inventor manufactures experimently medical stone function viscose staple fibre:
Product specification: 1.67 dtexs are cut length for 38 millimeters
Raw material: cotton pulp, Changbai Mountain high-quality medical stone
Medical stone micro mist addition: account for 0.1% of the fine weight of first.
Make as follows:
1, with Changbai Mountain high-quality medical stone raw material through washing, meal, dedusting, removal of impurities, being ground into granularity with pulverizer again is 300 purpose medical stone micro mists;
2, the medical stone micro mist is dropped in the alkali lye that concentration is 100 grams per liters and soaked 48 hours, after mechanical agitation, remove wherein harmful elements such as Hg, Pb with the sepiolite adsorption technology again and get medical stone and make with extra care liquid;
3, in the viscose glue course of dissolution the refining liquid of medical stone is evenly added in the viscose glue, make the functional Chinese medical stone fibres viscose glue with medical stone function after mixing, grind through 4 hours, its index is:
First fibre: 8.80-9.10%
Contain alkali: 5.40-5.80%
Viscosity: 40 seconds
Degree of ripeness: 8.0-9.0 milliliter;
4, the functional Chinese medical stone fibres viscose glue is increased by 2 layers of poplin cloth filter cloth after conventional three roads filter and filter, behind conventional spinning acid bath, carry out spinning again, get medical stone function viscose staple fibre.
(1), spinning technology parameter:
Ejection drawing-off: 1.10%
Cold drawing-off: 1.20%
Hot drawing-off: 1.35%
Spin speed: 60 meters/minute
(2), spinning bath is formed:
Sulfuric acid: 120-125 grams per liter
Zinc sulfate: 12-13 grams per liter
Sodium sulphate: 320-330 grams per liter
Acid bath drop: less than 5 grams per liters
(3), refining process condition:
Refining speed: 3 meters/minute
Pickling concentration: 1.0-1.5 grams per liter
Pickling temperature:. normal temperature
Desulfurization bath concentration: 4.5-5.5 grams per liter
Desulfurization bath temperature: 70-75 ℃
Gained medical stone function viscose staple fibre physical index such as table 1 after testing.(table 1 is seen the literary composition back)
Equal accord with Q/the JLHXW.W05-1998 of above-mentioned every quality index " functional Chinese medical stone fibres " company standard.
Trace element and ree content such as table 2 in this medical stone function viscose staple fibre of relevant department's check and analysis.(table 2 is seen the literary composition back)
The inventor tries embodiment gained medical stone function viscose staple fibre to spin in certain textile mills, the spinnability of check functional Chinese medical stone fibres, once succeed, spinning is smoothly by operations such as comb and parallel cotton fibers prior to spinning, drafting, rove, spun yarns, and the gained yarn qualities all reaches the special communique 50% following level of Ubbelohde.Spin fabrics such as 32 yarn test weaving underwears making, underpants with this functional Chinese medical stone fibres, this fabric removes has the general fibre fabrics feel soft, and drapability is good, and hygroscopicity is strong, and good permeability is outside the advantage such as comfortable and easy to wear.Owing to have trace element and the rare earth element that contains in the medical stone in this fabric, can absorb the energy of surrounding environment and human body self radiation, and the bio-energy and the human body that are translated into the human body beneficial form RESONANCE ABSORPTION, the human activin cell, blood circulation is accelerated, produce thermogenetic effect, make telangiectasis, strengthen microvascular self-disciplining motion, thereby microcirculation improvement promotes normal metabolic level and physiological function, at any time get rid of microcirculation disorder, eliminate muscular fatigue, promote regeneration, delay senility.The various harmful peroxide that metabolism is come out on the adsorbable human body skin of functional Chinese medical stone fibres draws noxious material in rubbish and the human body surrounding air environment simultaneously, prevents that effectively illness finds its way in by the mouth.Human body directly contacts this functional Chinese medical stone fibres fabric, and skin is prevented effects such as canceration, plum bacterium, antipruritic, sterilization, anti-inflammatory, deodorizing in addition.Therefore, this functional Chinese medical stone fibres has good health-care physiotherapeutic effect, has stepped a new step for promoting viscose to change to the functional form direction, and range of application is very extensive, will produce good social benefit and economic benefit after applying.Table 1: medical stone function viscose staple fibre quality inspection report
JX/CJ-JY-12 A wire gauge lattice: 1.67dtex
| Lot number project result | 12-3-5 | ||
| Do fracture strength (cN/dtex) | 2.45 | ||
| Wet breaking strength (cN/dtex) | 1.44 | ||
| Dried elongation at break (%) | 20.6 | ||
| Line density deviation ratio (%) | 0 | ||
| Length variation rate (%) | -3.6 | ||
| Overcut fibre (%) | 0.2 | ||
| Over-length fibre (mg/100g) | 2.8 | ||
| Residual sulfur content (mg/100g) | 10.1 | ||
| Fault (mg/100g) | 2.35 | ||
| Greasy dirt yellowish fiber (mg/100g) | 0 | ||
| Do the strong coefficient of variation (CV) (%) | 11.32 | ||
| Whiteness (%) | 77.5 | ||
| Oil content (%) | 0.18 | ||
| Regain (%) | 11.23 | ||
| Grade | The top grade product |
Table 2: analyze lot number: 98A082
| Sample presentation number | Analyze number | Constituent content ω (B)/10 -6 |
| V B Zn Cu Mn Co Mo Mg Ca Fe | ||
| 1 | 1633 | 0.79 0.88 17.37 6.24 1.06 ＜0.01 0.12 42.77 91.17 70.28 |
| Ni Sr Cd Ba Be Cr Ti K Na | ||
| 0.34 0.76 0.14 2.25 ＜0.05 4.09 ＜0.10 141 223 |
Claims (2)
1, a kind of functional Chinese medical stone fibres is to make add the refined liquid of medical stone micro mist in the viscose manufacture process after, it is characterized in that medical stone micro mist weight accounts for the 0.001-30% of fibre weight.
2, a kind of manufacture method of functional Chinese medical stone fibres as claimed in claim 1 is characterized in that manufacture method is as follows:
(1), the processing of medical stone micro mist
The medical stone raw material through washing, meal, dedusting, removal of impurities, is crushed to granularity 300-500 purpose medical stone micro mist with pulverizer machinery again;
(2), the medical stone micro mist is refining
The medical stone micro mist dropped in alkali lye that concentration is the 5-160 grams per liter or the water soaked 24-56 hour, after mechanical agitation, use wherein harmful element such as Hg, Pb of chemical fibre material, micro porous filtration material or the filtering of sepiolite adsorption technology again, the refining liquid of medical stone;
(3), the manufacturing of functional Chinese medical stone fibres viscose glue
In the yellow end of a period of viscose glue or course of dissolution the refining liquid of (2) gained medical stone is evenly added in the viscose glue, after 2-5 hour abundant mixing and grinding, making viscosity is the 30-60 functional Chinese medical stone fibres viscose glue with medical stone function of second;
(4), the spinning of functional Chinese medical stone fibres
The functional Chinese medical stone fibres viscose glue is filtered the back to be increased 1-3 layer poplin cloth filter cloth and filters through conventional three roads, again behind conventional spinning acid bath, with spinning speed 40-70 rice/minute (than the low 10-20 rice of normal spinning speed/minute) carry out spinning, get functional Chinese medical stone fibres.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN99100243A CN1102682C (en) | 1999-01-25 | 1999-01-25 | Functional Chinese medical stone fibres and its making method |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN99100243A CN1102682C (en) | 1999-01-25 | 1999-01-25 | Functional Chinese medical stone fibres and its making method |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN1262354A CN1262354A (en) | 2000-08-09 |
| CN1102682C true CN1102682C (en) | 2003-03-05 |
Family
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN99100243A Expired - Lifetime CN1102682C (en) | 1999-01-25 | 1999-01-25 | Functional Chinese medical stone fibres and its making method |
Country Status (1)
| Country | Link |
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| CN (1) | CN1102682C (en) |
Families Citing this family (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1266319C (en) * | 2004-08-04 | 2006-07-26 | 雷新琦 | Multi-component multifunction health-care yarn with kender, negative and medical stone and its health-care textile |
| CN101974796A (en) * | 2010-10-02 | 2011-02-16 | 山东海龙股份有限公司 | Method for preparing medical stone cellulose fiber |
| CN103726117B (en) * | 2012-02-26 | 2016-03-16 | 昆山华阳新材料股份有限公司 | Composite medical fiber |
| CN105442074B (en) * | 2015-12-25 | 2018-07-20 | 罗莱生活科技股份有限公司 | A method of preparing the viscose rayon containing medical stone |
| CN109518304A (en) * | 2018-10-29 | 2019-03-26 | 南通市苏中纺织有限公司 | A kind of preparation method and applications of crystal fibre |
| CN109537103A (en) * | 2018-10-29 | 2019-03-29 | 南通市苏中纺织有限公司 | A kind of preparation method and applications of crystal fibre |
| CN109652864A (en) * | 2018-10-29 | 2019-04-19 | 南通市苏中纺织有限公司 | A kind of preparation method and applications of crystal fibre |
| CN117468109A (en) * | 2023-09-13 | 2024-01-30 | 山东盛和纺织股份有限公司 | A kind of medical stone/regenerated cellulose composite functional fiber and its preparation method |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4775585A (en) * | 1983-01-21 | 1988-10-04 | Kanebo Ltd./Kanto Chemical Co. | Polymer article having an antibacterial property containing zeolite particles therein and the processes for producing same |
| CN1054257A (en) * | 1991-04-06 | 1991-09-04 | 舒克孝 | Flesh-keeping film (bag) |
| CN1103412A (en) * | 1993-11-30 | 1995-06-07 | 沟口龙一 | Synthetic resin particles and products containing edible stone, preparation and application of same |
| CN1211642A (en) * | 1997-05-28 | 1999-03-24 | 石美秀 | Fiber product made of elvan |
-
1999
- 1999-01-25 CN CN99100243A patent/CN1102682C/en not_active Expired - Lifetime
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4775585A (en) * | 1983-01-21 | 1988-10-04 | Kanebo Ltd./Kanto Chemical Co. | Polymer article having an antibacterial property containing zeolite particles therein and the processes for producing same |
| CN1054257A (en) * | 1991-04-06 | 1991-09-04 | 舒克孝 | Flesh-keeping film (bag) |
| CN1103412A (en) * | 1993-11-30 | 1995-06-07 | 沟口龙一 | Synthetic resin particles and products containing edible stone, preparation and application of same |
| CN1211642A (en) * | 1997-05-28 | 1999-03-24 | 石美秀 | Fiber product made of elvan |
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| CN1262354A (en) | 2000-08-09 |
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Applicant after: Fu Wancai Applicant after: Dong Pingwei Applicant after: Lin Xinghua Applicant after: Yang Wenhui Applicant after: Yu Bo Applicant after: Liu Shi Applicant after: Shen Guifang Applicant after: Liu Chunyan Applicant after: Sui Baokang Applicant after: Jin Shujie Applicant after: Li Hongqin Applicant after: Yang Shiying Applicant after: Zhang Liyan Applicant after: Zheng Cijun Applicant after: Song Zhiguo Applicant after: Zhang Fengmin Applicant before: Fu Wancai Applicant before: Dong Pingwei Applicant before: Lin Xinghua Applicant before: Yang Wenhui Applicant before: Yu Bo Applicant before: Liu Shi Applicant before: Shen Guifang Applicant before: Sui Baokang Applicant before: Jin Shujie Applicant before: Li Hongqin Applicant before: Yang Shiying Applicant before: Zhang Liyan Applicant before: Zheng Chengjun Applicant before: Song Zhiguo Applicant before: Zhang Fengmin |
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Free format text: CORRECT: APPLICANT; FROM: FU WANCAI; SUI BAOKANG; JIN SHUJIE; LI HONGQIN; YANG SHIYING; ZHANG LIYAN; ZHENG CHENGJUN; SONG ZHIGUO; ZHANG FENGMIN; DONG PINGWEI; LIN XINGHUA; YANG WENHUI; YU BO; LIU SHI; SHEN GUIFANG TO: FU WANCAI; SUI BAOKANG; JIN SHUJIE; LI HONGQIN; YANG SHIYING; ZHANG LIYAN; ZHENG CIJUN; SONG ZHIGUO; ZHANG FENGMIN; DONG PINGWEI; LIN XINGHUA; YANG WENHUI; YU BO; LIU SHI; SHEN GUIFANG; LIU CHUNYAN |
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