CN118615743A - A freezing concentration device - Google Patents
A freezing concentration device Download PDFInfo
- Publication number
- CN118615743A CN118615743A CN202411098564.3A CN202411098564A CN118615743A CN 118615743 A CN118615743 A CN 118615743A CN 202411098564 A CN202411098564 A CN 202411098564A CN 118615743 A CN118615743 A CN 118615743A
- Authority
- CN
- China
- Prior art keywords
- heater
- cover
- stock solution
- container
- solid
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 238000007710 freezing Methods 0.000 title claims abstract description 39
- 230000008014 freezing Effects 0.000 title claims abstract description 39
- 239000007788 liquid Substances 0.000 claims abstract description 65
- 239000007787 solid Substances 0.000 claims abstract description 28
- 239000000203 mixture Substances 0.000 claims abstract description 14
- 238000000926 separation method Methods 0.000 claims abstract description 10
- 238000000746 purification Methods 0.000 claims abstract description 9
- 239000002537 cosmetic Substances 0.000 claims abstract description 6
- 230000007613 environmental effect Effects 0.000 claims abstract description 6
- 235000013305 food Nutrition 0.000 claims abstract description 6
- 238000004090 dissolution Methods 0.000 claims abstract description 5
- 239000011550 stock solution Substances 0.000 claims abstract 19
- 239000000243 solution Substances 0.000 claims abstract 17
- 239000003814 drug Substances 0.000 claims abstract 4
- 238000000034 method Methods 0.000 claims description 12
- 238000010438 heat treatment Methods 0.000 claims description 8
- 238000009413 insulation Methods 0.000 claims description 8
- 235000013336 milk Nutrition 0.000 claims description 4
- 239000008267 milk Substances 0.000 claims description 4
- 210000004080 milk Anatomy 0.000 claims description 4
- 230000001681 protective effect Effects 0.000 claims description 4
- 235000016213 coffee Nutrition 0.000 claims description 3
- 235000013353 coffee beverage Nutrition 0.000 claims description 3
- 239000000419 plant extract Substances 0.000 claims description 3
- 239000013535 sea water Substances 0.000 claims description 3
- 235000013322 soy milk Nutrition 0.000 claims description 3
- 239000000126 substance Substances 0.000 claims description 3
- 235000013616 tea Nutrition 0.000 claims description 3
- 238000004065 wastewater treatment Methods 0.000 claims description 3
- 235000014101 wine Nutrition 0.000 claims description 3
- 230000001105 regulatory effect Effects 0.000 claims 3
- 241001122767 Theaceae Species 0.000 claims 1
- 235000015203 fruit juice Nutrition 0.000 claims 1
- 230000000717 retained effect Effects 0.000 description 8
- 238000001816 cooling Methods 0.000 description 7
- 239000003507 refrigerant Substances 0.000 description 5
- 239000007791 liquid phase Substances 0.000 description 3
- 239000003566 sealing material Substances 0.000 description 3
- 244000269722 Thea sinensis Species 0.000 description 2
- 235000013361 beverage Nutrition 0.000 description 2
- 238000002425 crystallisation Methods 0.000 description 2
- 230000008025 crystallization Effects 0.000 description 2
- 238000005485 electric heating Methods 0.000 description 2
- 239000012530 fluid Substances 0.000 description 2
- 235000011389 fruit/vegetable juice Nutrition 0.000 description 2
- 241000411851 herbal medicine Species 0.000 description 2
- 230000000750 progressive effect Effects 0.000 description 2
- 235000010469 Glycine max Nutrition 0.000 description 1
- 244000068988 Glycine max Species 0.000 description 1
- 101001121408 Homo sapiens L-amino-acid oxidase Proteins 0.000 description 1
- 102100026388 L-amino-acid oxidase Human genes 0.000 description 1
- 101100233916 Saccharomyces cerevisiae (strain ATCC 204508 / S288c) KAR5 gene Proteins 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D9/00—Crystallisation
- B01D9/02—Crystallisation from solutions
- B01D9/04—Crystallisation from solutions concentrating solutions by removing frozen solvent therefrom
Landscapes
- Chemical & Material Sciences (AREA)
- Crystallography & Structural Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Physical Water Treatments (AREA)
Abstract
Description
技术领域Technical Field
本发明属于冷冻浓缩技术领域，具体为一种冷冻浓缩装置。The invention belongs to the technical field of freeze concentration, and in particular relates to a freeze concentration device.
背景技术Background Art
现有技术中的冷冻浓缩方法是：利用稀溶液与冰在冰点以下时的固液相关系来实现的一种浓缩技术。主要有两种方式：悬浮结晶冷冻浓缩法和渐进冷冻浓缩法。悬浮结晶冷冻浓缩法的原理是：在对稀溶液进行冷冻时，不断排除在液体中悬浮的自由小冰晶，使液体浓度增加的方法。渐进冷冻浓缩法的原理是：在对稀溶液进行冷冻时，随着冰层在冷却面的生成和成长，固、液界面附近的溶质被排除到液相侧，导致液相中溶质质量浓度逐渐升高的浓缩方法。现有的冷冻浓缩方法的设备结构复杂、设备成本和生产成本高、且效率不高。The freeze concentration method in the prior art is a concentration technology that utilizes the solid-liquid phase relationship between a dilute solution and ice below the freezing point. There are two main methods: suspended crystallization freeze concentration and progressive freeze concentration. The principle of the suspended crystallization freeze concentration method is that when a dilute solution is frozen, the free small ice crystals suspended in the liquid are continuously removed to increase the liquid concentration. The principle of the progressive freeze concentration method is that when a dilute solution is frozen, as the ice layer is generated and grows on the cooling surface, the solute near the solid-liquid interface is removed to the liquid phase side, resulting in a concentration method in which the mass concentration of the solute in the liquid phase gradually increases. The existing freeze concentration method has a complex equipment structure, high equipment cost and production cost, and low efficiency.
发明内容Summary of the invention
为解决现有技术存在的问题，本发明的主要目的是提出一种冷冻浓缩装置。In order to solve the problems existing in the prior art, the main purpose of the present invention is to provide a freezing concentration device.
为解决上述技术问题，根据本发明的一个方面，本发明提供了如下技术方案：To solve the above technical problems, according to one aspect of the present invention, the present invention provides the following technical solutions:
一种冷冻浓缩装置，包括：A freezing concentration device, comprising:
原液容器和加热器；加热器安装在原液容器的盖子上；A raw liquid container and a heater; the heater is mounted on a cover of the raw liquid container;
稀溶液注入原液容器后，盖上盖子保持原液容器的容器开口朝上，把装置送进冷冻设备，稀溶液冷冻成固体（冰体）或固液混合体（冰体+浓溶液）后，把装置移出冷冻设备，并将原液容器的容器开口朝下进行放置，通过加热器对固体或固液混合体传递热量进行溶解分离，分段留取溶液，符合目标浓度的溶液留取备用，不符合目标浓度的溶液，使用所述冷冻浓缩装置继续冷冻和溶解，实现稀溶液浓缩。After the dilute solution is injected into the original liquid container, the lid is closed to keep the container opening of the original liquid container facing upward, and the device is sent to the freezing equipment. After the dilute solution is frozen into a solid (ice body) or a solid-liquid mixture (ice body + concentrated solution), the device is removed from the freezing equipment and placed with the container opening of the original liquid container facing downward. The solid or solid-liquid mixture is dissolved and separated by transferring heat through a heater, and the solution is retained in sections. The solution that meets the target concentration is retained for use, and the solution that does not meet the target concentration is continued to be frozen and dissolved using the freeze concentration device to achieve concentration of the dilute solution.
作为本发明所述的一种冷冻浓缩装置的优选方案，其中：加热器为一个或多个；加热器可以为发热元件（如电热元件等），也可以采用热量媒介（如流体等）作为加热器。As a preferred embodiment of the freezing concentration device described in the present invention, there are one or more heaters; the heater can be a heating element (such as an electric heating element, etc.), or a heat medium (such as a fluid, etc.) can be used as the heater.
作为本发明所述的一种冷冻浓缩装置的优选方案，其中：加热器设置在原液容器的中心轴线位置或其周围区域。As a preferred embodiment of the freezing concentration device described in the present invention, the heater is arranged at the central axis position of the raw liquid container or its surrounding area.
作为本发明所述的一种冷冻浓缩装置的优选方案，其中：原液容器的盖子上设置有溶液出口。As a preferred embodiment of the freezing concentration device described in the present invention, a solution outlet is provided on the cover of the stock liquid container.
作为本发明所述的一种冷冻浓缩装置的优选方案，其中：溶液出口上还设置有溶液出口阀。As a preferred embodiment of the freezing concentration device described in the present invention, a solution outlet valve is also provided on the solution outlet.
作为本发明所述的一种冷冻浓缩装置的优选方案，其中：所述装置还包括：隔热装置，用于套装于原液容器外实现隔热。隔热装置是一个备选装置，根据冷冻浓缩的需要选择使用。As a preferred solution of the freeze concentration device of the present invention, the device further comprises: a heat insulation device, which is used to be mounted outside the raw liquid container to achieve heat insulation. The heat insulation device is an alternative device, which is selected and used according to the needs of freeze concentration.
作为本发明所述的一种冷冻浓缩装置的优选方案，其中：所述装置还备有待用的备用盖，备用盖没有安装加热器；当冷冻过程的温度非常低，会影响加热器时，在冷冻过程使用备用盖；稀溶液注入原液容器后，盖上备用盖保持原液容器的容器开口朝上，把装置送进冷冻设备，稀溶液冷冻成固态后，把装置移出冷冻设备，打开并撤去备用盖，根据原液容器盖子上的加热器的方位，在固体上制造出可放进加热器的通道，然后盖上安装有加热器的盖子。As a preferred embodiment of the freezing concentration device described in the present invention, the device is also equipped with a standby cover, which is not equipped with a heater; when the temperature of the freezing process is very low and will affect the heater, the standby cover is used in the freezing process; after the dilute solution is injected into the raw liquid container, the standby cover is covered to keep the container opening of the raw liquid container facing upward, and the device is sent into the freezing equipment. After the dilute solution is frozen into a solid state, the device is removed from the freezing equipment, the standby cover is opened and removed, and according to the orientation of the heater on the cover of the raw liquid container, a channel for placing the heater is made on the solid, and then the cover with the heater installed is covered.
作为本发明所述的一种冷冻浓缩装置的优选方案，其中：原液容器的盖子外侧还设置有支脚，用于加热溶解时实现对原液容器的支撑。As a preferred embodiment of the freezing concentration device described in the present invention, the outer side of the cover of the stock liquid container is also provided with supporting feet for supporting the stock liquid container during heating and dissolution.
作为本发明所述的一种冷冻浓缩装置的优选方案，其中：原液容器的盖子上设置有隔热层。As a preferred embodiment of the freezing concentration device described in the present invention, a heat insulating layer is provided on the lid of the stock liquid container.
作为本发明所述的一种冷冻浓缩装置的优选方案，其中：原液容器的盖子上设置有电源插座、调温开关，电源线和控制线连接电源插座、调温开关，在电源插座、调温开关上设置有保护盖。As a preferred embodiment of the freezing concentration device described in the present invention, a power socket and a thermostat are arranged on the lid of the raw liquid container, a power cord and a control cord are connected to the power socket and the thermostat, and a protective cover is arranged on the power socket and the thermostat.
作为本发明所述的一种冷冻浓缩装置的优选方案，其中：盖子与原液容器之间还设置有密封材料。As a preferred embodiment of the freezing concentration device described in the present invention, a sealing material is provided between the cover and the raw liquid container.
为解决上述技术问题，根据本发明的另一个方面，本发明提供了如下技术方案：To solve the above technical problem, according to another aspect of the present invention, the present invention provides the following technical solution:
一种上述的冷冻浓缩装置在食品、化妆品、生物医药、环保处理等领域的应用。An application of the above-mentioned freezing concentration device in the fields of food, cosmetics, biomedicine, environmental protection treatment, etc.
一种上述的冷冻浓缩装置在牛奶、酒类、果汁、咖啡、茶、饮料、豆奶、化学药液、中草药液、植物提取物、海水提纯、废水处理等领域的应用。The above-mentioned freezing concentration device is used in the fields of milk, wine, juice, coffee, tea, beverages, soy milk, chemical liquid, Chinese herbal medicine liquid, plant extract, seawater purification, wastewater treatment, etc.
一种上述的冷冻浓缩装置在热敏性原料的冷冻浓缩和分离提纯领域的应用。An application of the above-mentioned freezing concentration device in the field of freezing concentration and separation and purification of heat-sensitive raw materials.
一种上述的冷冻浓缩装置在牛奶、酒类、果汁、咖啡、茶、饮料、豆浆、豆奶、化学药液、中草药液、植物提取物、海水提纯、废水处理等的冷冻浓缩和分离提纯领域的应用。The above-mentioned freezing concentration device is used in the fields of freezing concentration and separation and purification of milk, wine, juice, coffee, tea, beverages, soybean milk, soy milk, chemical liquid, Chinese herbal medicine liquid, plant extract, seawater purification, wastewater treatment, etc.
本发明的有益效果如下：The beneficial effects of the present invention are as follows:
本发明提出一种冷冻浓缩装置，包括原液容器和加热器，加热器安装在原液容器的盖子上；稀溶液注入原液容器后，盖上盖子保持原液容器的容器开口朝上，把装置送进冷冻库，稀溶液冷冻成固体或固液混合体后，把装置移出冷库，并将原液容器的容器开口朝下进行放置，通过加热器对固体或固液混合体传递热量进行溶解分离，分段留取溶液，符合目标浓度的溶液留取备用，不符合目标浓度的溶液，使用所述冷冻浓缩装置继续冷冻和溶解，实现稀溶液浓缩。本发明提高了冷冻浓缩和分离提纯的效率，设备和操作简单，便于在食品、化妆品、生物医药、环保处理等领域的应用。The present invention proposes a freeze concentration device, including a raw liquid container and a heater, wherein the heater is installed on the lid of the raw liquid container; after the dilute solution is injected into the raw liquid container, the lid is covered to keep the container opening of the raw liquid container facing upward, and the device is sent to a freezer. After the dilute solution is frozen into a solid or a solid-liquid mixture, the device is removed from the cold storage, and the container opening of the raw liquid container is placed downward, and the solid or solid-liquid mixture is transferred to heat by the heater for dissolution and separation, and the solution is retained in sections, and the solution that meets the target concentration is retained for standby use, and the solution that does not meet the target concentration is continuously frozen and dissolved using the freeze concentration device to achieve dilute solution concentration. The present invention improves the efficiency of freeze concentration and separation and purification, and the equipment and operation are simple, which is convenient for application in the fields of food, cosmetics, biomedicine, environmental protection treatment, etc.
附图说明BRIEF DESCRIPTION OF THE DRAWINGS
为了更清楚地说明本发明实施例或现有技术中的技术方案，下面将对实施例或现有技术描述中所需要使用的附图作简单地介绍，显而易见地，下面描述中的附图仅仅是本发明的一些实施例，对于本领域普通技术人员来讲，在不付出创造性劳动的前提下，还可以根据这些附图示出的结构获得其他的附图。In order to more clearly illustrate the embodiments of the present invention or the technical solutions in the prior art, the drawings required for use in the embodiments or the description of the prior art will be briefly introduced below. Obviously, the drawings described below are only some embodiments of the present invention. For ordinary technicians in this field, other drawings can be obtained based on the structures shown in these drawings without paying creative work.
图1为本发明冷冻浓缩装置容器开口朝上的切面示意图。FIG1 is a schematic cross-sectional view of a freeze concentration device according to the present invention with the container opening facing upward.
图2为本发明冷冻浓缩装置容器套装隔热装置开口朝下的切面示意图。FIG. 2 is a schematic cross-sectional view of a container of a freeze concentration device according to the present invention, with the heat insulation device having an opening facing downward.
图3为本发明冷冻浓缩装置不含原液容器的结构示意图。FIG3 is a schematic structural diagram of the freeze concentration device of the present invention without a stock liquid container.
图中，1-原液容器，3-加热器，4-盖子，5-溶液出口，6-密封材料，7-固体，8-保护盖，9-电源插座，10-调温开关，11-隔热装置。In the figure, 1-original liquid container, 3-heater, 4-lid, 5-solution outlet, 6-sealing material, 7-solid, 8-protective cover, 9-power socket, 10-temperature control switch, 11-thermal insulation device.
本发明目的的实现、功能特点及优点将结合实施例，参照附图做进一步说明。The realization of the purpose, functional features and advantages of the present invention will be further explained in conjunction with embodiments and with reference to the accompanying drawings.
具体实施方式DETAILED DESCRIPTION
下面将结合实施例中的技术方案进行清楚、完整地描述，显然，所描述的实施例仅仅是本发明的一部分实施例，而不是全部的实施例。基于本发明中的实施例，本领域普通技术人员在没有作出创造性劳动前提下所获得的所有其他实施例，都属于本发明保护的范围。The following will be described clearly and completely in conjunction with the technical solutions in the embodiments. Obviously, the described embodiments are only part of the embodiments of the present invention, not all of the embodiments. Based on the embodiments of the present invention, all other embodiments obtained by ordinary technicians in this field without creative work are within the scope of protection of the present invention.
本发明提出一种冷冻浓缩装置，与现有冷冻浓缩设备的技术方案不同，其技术方案是把热源设置在稀溶液冷冻成固体（或者固液混合体）后的特定方位，通过溶解分离实现冷冻浓缩，提高了冷冻浓缩和分离提纯的效率，设备和操作简单，便于在食品、化妆品、生物医药、环保处理等领域的应用。The present invention proposes a freeze concentration device, which is different from the technical solution of the existing freeze concentration equipment. The technical solution is to set the heat source at a specific position after the dilute solution is frozen into a solid (or a solid-liquid mixture), and realize freeze concentration through dissolution separation, thereby improving the efficiency of freeze concentration and separation and purification. The equipment and operation are simple, and it is convenient for application in the fields of food, cosmetics, biomedicine, environmental protection treatment, etc.
为了更清晰的表达特定方位的概念，给出如下两个举例方案：In order to express the concept of specific orientation more clearly, the following two examples are given:
（1）一个圆柱体状冷冻装置：稀溶液在这个装置中冷冻成固体或固液混合体。在对稀溶液进行冷冻时，冷媒位于装置中的稀溶液容器的外面，冷却面是靠近冷媒的容器壁面。设置热源时要设置在特定方位区域，是向着固体或固液混合体从冷却面出发离开冷却面方向的区域。在本装置中，固体或固液混合体的中心轴线周围的区域就在这个区域的范围内：即，冰体内的中心轴线周围的区域，除靠近冷却面形成的溶质含量低的固体层外都符合，可以在此区域设置一个热源（加热棒），或者设置多个热源（多根热源棒）。(1) A cylindrical freezing device: a dilute solution is frozen into a solid or a solid-liquid mixture in this device. When freezing a dilute solution, the refrigerant is located outside the dilute solution container in the device, and the cooling surface is the container wall close to the refrigerant. When setting a heat source, it should be set in a specific orientation area, which is the area in the direction from the solid or solid-liquid mixture away from the cooling surface. In this device, the area around the central axis of the solid or solid-liquid mixture is within the scope of this area: that is, the area around the central axis of the ice body, except for the solid layer with low solute content formed close to the cooling surface, meets the requirements. One heat source (heating rod) or multiple heat sources (multiple heat source rods) can be set in this area.
（2）一个圆柱体状冷冻装置：这个装置中，冷媒是从密封的管道从中心轴线的区域通过装置的，在对稀溶液进行冷冻成固体或固液混合体时，冷却面是冷媒管的外壁。设置热源时要设置在特定方位区域，是向着固体或固液混合体从冷却面出发离开冷却面方向的区域，即：热源的设置可以设置在靠近容器外壁周围附近区域的冰体内，也可以设置在容器外壁外。而在固体（冰体）内，靠近冷媒管道外壁（冷却面）形成的溶质含量低的固体层，不在所述的特定方位范围。(2) A cylindrical freezing device: In this device, the refrigerant passes through the device from the central axis area through a sealed pipe. When freezing a dilute solution into a solid or a solid-liquid mixture, the cooling surface is the outer wall of the refrigerant tube. When setting the heat source, it should be set in a specific orientation area, which is the area in the direction of the solid or solid-liquid mixture leaving the cooling surface, that is, the heat source can be set in the ice body near the outer wall of the container, or it can be set outside the outer wall of the container. The solid layer with low solute content formed in the solid (ice body) near the outer wall (cooling surface) of the refrigerant pipe is not within the specific orientation range.
如图1-3所示，本发明具体实施方式提供一种冷冻浓缩装置，包括：As shown in Figures 1-3, a specific embodiment of the present invention provides a freeze concentration device, comprising:
原液容器1和加热器3；加热器3安装在原液容器1的盖子4上；A raw liquid container 1 and a heater 3; the heater 3 is mounted on a cover 4 of the raw liquid container 1;
稀溶液注入原液容器1后，盖上盖子4保持原液容器1的容器开口朝上，把装置送进冷冻库，稀溶液冷冻成固态（即冰体）后，把装置移出冷库，并将原液容器1的容器开口朝下进行放置，通过加热器3对固体进行加热溶解，根据目标溶液浓度需要分段留取溶液，符合目标浓度的溶液留取备用，不符合目标浓度的溶液，使用所述冷冻浓缩装置继续冷冻和溶解，实现稀溶液浓缩。After the dilute solution is injected into the stock liquid container 1, the lid 4 is put on to keep the container opening of the stock liquid container 1 facing upward, and the device is sent to the freezer. After the dilute solution is frozen into a solid state (i.e., an ice body), the device is moved out of the cold storage, and the container opening of the stock liquid container 1 is placed downward. The solid is heated and dissolved by the heater 3, and the solution is retained in sections according to the target solution concentration. The solution that meets the target concentration is retained for standby use, and the solution that does not meet the target concentration is continuously frozen and dissolved using the freeze concentration device to achieve concentration of the dilute solution.
在本发明的一种实施方式中，加热器3为一个或多个；加热器3可以为发热元件（如电热元件等），也可以采用作为热量媒介（如流体等）作为加热器3。In one embodiment of the present invention, there are one or more heaters 3 ; the heater 3 may be a heating element (such as an electric heating element, etc.), or a heat medium (such as a fluid, etc.) may be used as the heater 3 .
在本发明的一种实施方式中，加热器3设置在原液容器1的中心轴线位置或其周围区域。In one embodiment of the present invention, the heater 3 is disposed at the central axis position of the raw liquid container 1 or in the surrounding area thereof.
在本发明的一种实施方式中，原液容器1的盖子4上设置有溶液出口5。In one embodiment of the present invention, a solution outlet 5 is provided on the cover 4 of the raw liquid container 1 .
在本发明的一种实施方式中，溶液出口5上还设置有溶液出口阀。In one embodiment of the present invention, a solution outlet valve is further provided on the solution outlet 5 .
在本发明的一种实施方式中，所述装置还包括：隔热装置11，用于套装于原液容器1外实现隔热。隔热装置11是一个备选装置，根据冷冻浓缩的需要选择使用。In one embodiment of the present invention, the device further comprises: a heat insulating device 11, which is used to be mounted outside the raw liquid container 1 to achieve heat insulation. The heat insulating device 11 is an optional device, which is selected for use according to the needs of freeze concentration.
在本发明的一种实施方式中，所述装置还备有待用的备用盖，备用盖没有安装加热器；当冷冻过程的温度非常低，会影响加热器时，在冷冻过程使用备用盖；稀溶液注入原液容器1后，盖上备用盖保持原液容器1的容器开口朝上，把装置送进冷冻设备，稀溶液冷冻成固态后，把装置移出冷冻设备，打开并撤去备用盖，根据原液容器1的盖子4上的加热器3的方位，在固体上制造出可放进加热器3的通道，然后盖上安装有加热器3的盖子4。In one embodiment of the present invention, the device is also equipped with a spare cover for use, and the spare cover is not equipped with a heater; when the temperature of the freezing process is very low and will affect the heater, the spare cover is used in the freezing process; after the dilute solution is injected into the raw liquid container 1, the spare cover is covered to keep the container opening of the raw liquid container 1 facing upward, and the device is sent into the freezing equipment. After the dilute solution is frozen into a solid state, the device is removed from the freezing equipment, the spare cover is opened and removed, and according to the orientation of the heater 3 on the cover 4 of the raw liquid container 1, a channel for placing the heater 3 is made on the solid, and then the cover 4 with the heater 3 installed is covered.
在本发明的一种实施方式中，原液容器1的盖子4外侧还设置有支脚，用于加热溶解时实现对原液容器1的支撑。In one embodiment of the present invention, the outer side of the cover 4 of the raw liquid container 1 is also provided with supporting feet for supporting the raw liquid container 1 during heating and dissolving.
在本发明的一种实施方式中，原液容器1的盖子4上设置有隔热层。In one embodiment of the present invention, a heat insulating layer is provided on the cover 4 of the raw liquid container 1 .
在本发明的一种实施方式中，原液容器1的盖子4上设置有电源插座9、调温开关10，电源线和控制线连接电源插座9、调温开关10，在电源插座9、调温开关10上设置有保护盖8。In one embodiment of the present invention, a power socket 9 and a thermostat 10 are provided on the lid 4 of the raw liquid container 1, a power cord and a control cord are connected to the power socket 9 and the thermostat 10, and a protective cover 8 is provided on the power socket 9 and the thermostat 10.
在本发明的一种实施方式中，盖子4与原液容器1之间还设置有密封材料6。In one embodiment of the present invention, a sealing material 6 is further provided between the cover 4 and the raw liquid container 1 .
本发明具体实施方式提供的冷冻浓缩装置在使用时，把稀溶液注入原液容器1后，盖上盖子4保持原液容器1的容器开口朝上，把装置送进冷冻库，稀溶液冷冻成固态（即冰体）后，把装置移出冷库，并将原液容器1的容器开口朝下进行放置，通过支脚实现装置的安放，打开保护盖8，通过电源插座9连接电源，通过调温开关10设置加热温度，打开电源开关，通过加热器3对固体进行加热溶解，根据目标溶液浓度需要分段留取溶液，符合目标浓度的溶液留取备用，不符合目标浓度的溶液，使用所述冷冻浓缩装置继续冷冻和溶解，实现稀溶液浓缩。When the freezing concentration device provided by the specific embodiment of the present invention is used, after the dilute solution is injected into the raw liquid container 1, the lid 4 is covered to keep the container opening of the raw liquid container 1 facing upward, and the device is sent to the freezer. After the dilute solution is frozen into a solid state (i.e., an ice body), the device is moved out of the cold storage, and the container opening of the raw liquid container 1 is placed downward. The device is placed by supporting feet, the protective cover 8 is opened, the power supply is connected through the power socket 9, the heating temperature is set through the thermostat 10, the power switch is turned on, and the solid is heated and dissolved by the heater 3. The solution is retained in sections according to the target solution concentration. The solution that meets the target concentration is retained for standby use, and the solution that does not meet the target concentration is continuously frozen and dissolved using the freezing concentration device to achieve concentration of the dilute solution.
本发明提高了冷冻浓缩和分离提纯的效率，设备和操作简单，便于在食品、化妆品、生物医药、环保处理等领域的应用。The invention improves the efficiency of freeze concentration and separation and purification, has simple equipment and operation, and is convenient for application in the fields of food, cosmetics, biomedicine, environmental protection treatment, etc.
以上所述仅为本发明的优选实施例，并非因此限制本发明的专利范围，凡是在本发明的发明构思下，利用本发明说明书内容所作的等效结构变换，或直接/间接运用在其他相关的技术领域均包括在本发明的专利保护范围内。The above description is only a preferred embodiment of the present invention, and does not limit the patent scope of the present invention. All equivalent structural changes made by using the contents of the present invention specification under the inventive concept of the present invention, or direct/indirect application in other related technical fields are included in the patent protection scope of the present invention.
Claims (10)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202411098564.3A CN118615743A (en) | 2024-08-12 | 2024-08-12 | A freezing concentration device |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202411098564.3A CN118615743A (en) | 2024-08-12 | 2024-08-12 | A freezing concentration device |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN118615743A true CN118615743A (en) | 2024-09-10 |
Family
ID=92596363
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202411098564.3A Pending CN118615743A (en) | 2024-08-12 | 2024-08-12 | A freezing concentration device |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN118615743A (en) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN119034248A (en) * | 2024-10-28 | 2024-11-29 | 崇义富百乐发展有限公司 | Freezing enrichment facility |
| CN119034245A (en) * | 2024-10-28 | 2024-11-29 | 崇义富百乐发展有限公司 | Freezing enrichment facility |
| CN119034249A (en) * | 2024-10-28 | 2024-11-29 | 崇义富百乐发展有限公司 | Freezing enrichment facility |
| CN119158295A (en) * | 2024-11-19 | 2024-12-20 | 崇义富百乐发展有限公司 | A freezing concentration device |
Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20100050686A1 (en) * | 2008-06-20 | 2010-03-04 | Varian Semiconductor Equipment Associates, Inc. | Melt purification and delivery system |
| CN102604807A (en) * | 2012-03-28 | 2012-07-25 | 雷晓明 | Novel method for making novel high-quality wine with high-medium degrees in low-temperature freezing way |
| CN109310116A (en) * | 2016-05-18 | 2019-02-05 | 艾伯茨股份有限公司 | For preparing the method and component of beverage based on frozen food |
| CN213848585U (en) * | 2020-09-27 | 2021-08-03 | 东鹏饮料(集团)股份有限公司 | Lemon stock thawing equipment |
| CN218221143U (en) * | 2022-07-15 | 2023-01-06 | 安徽亚格盛电子新材料有限公司 | Trimethyl aluminum crystallization storage tank |
| CN219844887U (en) * | 2023-04-25 | 2023-10-20 | 昆山真金食品有限公司 | Coffee liquid thawing equipment that flavor coffee beverage production was used |
-
2024
- 2024-08-12 CN CN202411098564.3A patent/CN118615743A/en active Pending
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20100050686A1 (en) * | 2008-06-20 | 2010-03-04 | Varian Semiconductor Equipment Associates, Inc. | Melt purification and delivery system |
| CN102604807A (en) * | 2012-03-28 | 2012-07-25 | 雷晓明 | Novel method for making novel high-quality wine with high-medium degrees in low-temperature freezing way |
| CN109310116A (en) * | 2016-05-18 | 2019-02-05 | 艾伯茨股份有限公司 | For preparing the method and component of beverage based on frozen food |
| CN213848585U (en) * | 2020-09-27 | 2021-08-03 | 东鹏饮料(集团)股份有限公司 | Lemon stock thawing equipment |
| CN218221143U (en) * | 2022-07-15 | 2023-01-06 | 安徽亚格盛电子新材料有限公司 | Trimethyl aluminum crystallization storage tank |
| CN219844887U (en) * | 2023-04-25 | 2023-10-20 | 昆山真金食品有限公司 | Coffee liquid thawing equipment that flavor coffee beverage production was used |
Non-Patent Citations (1)
| Title |
|---|
| 扎基•伯克著；康大成译: "《食品加工工程与技术》", 31 July 2020, 中国轻工业出版社, pages: 337 - 339 * |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN119034248A (en) * | 2024-10-28 | 2024-11-29 | 崇义富百乐发展有限公司 | Freezing enrichment facility |
| CN119034245A (en) * | 2024-10-28 | 2024-11-29 | 崇义富百乐发展有限公司 | Freezing enrichment facility |
| CN119034249A (en) * | 2024-10-28 | 2024-11-29 | 崇义富百乐发展有限公司 | Freezing enrichment facility |
| CN119034248B (en) * | 2024-10-28 | 2025-03-25 | 崇义富百乐发展有限公司 | A freezing concentration device |
| CN119158295A (en) * | 2024-11-19 | 2024-12-20 | 崇义富百乐发展有限公司 | A freezing concentration device |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN118615743A (en) | A freezing concentration device | |
| CN118634516A (en) | A freezing concentration device | |
| CN118846571A (en) | A freezing concentration device | |
| CN204582603U (en) | A kind of ultrasonic microwave combination extraction equipment | |
| CN118615742A (en) | A freeze concentration method | |
| CN118615744A (en) | A freezing concentration device | |
| CN206881200U (en) | A kind of multi-functional plant extracts separation integrated apparatus | |
| CN105476377A (en) | Drinking cup | |
| CN119034246B (en) | A freezing concentration device | |
| CN205151821U (en) | Freezing sewage treatment plant of low temperature | |
| CN119034245B (en) | A freezing concentration device | |
| CN119034244B (en) | A freeze concentration method | |
| US7976790B2 (en) | Method and apparatus for the extraction of plant constituents | |
| CN205995076U (en) | A kind of evaporating, concentrating and crystallizing kettle | |
| CN119034247B (en) | Freezing enrichment facility | |
| CN204619429U (en) | A kind of steam-type medicinal plant extraction element | |
| CN119158295A (en) | A freezing concentration device | |
| CN207062296U (en) | A kind of micro low temperature ultrasonic breaker | |
| CN119034248B (en) | A freezing concentration device | |
| CN213314781U (en) | Heat-insulation tank structure for stirring tank | |
| CN206404345U (en) | One kind centrifugation freezing and evaporating concentrating instrument | |
| CN201406395Y (en) | Temperature dual control installation for polyester polyol reaction kettle | |
| US20030141177A1 (en) | Process for re-purfying highly enriched [H2180] | |
| CN215924955U (en) | Special equipment device is cut to protease | |
| CN119034249A (en) | Freezing enrichment facility |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination |