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CN117903936A - Biological enzyme catalysis chemical reaction tank device - Google Patents

Biological enzyme catalysis chemical reaction tank device Download PDF

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Publication number
CN117903936A
CN117903936A CN202410302896.2A CN202410302896A CN117903936A CN 117903936 A CN117903936 A CN 117903936A CN 202410302896 A CN202410302896 A CN 202410302896A CN 117903936 A CN117903936 A CN 117903936A
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reaction tank
rod
contact
tank body
side end
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CN117903936B (en
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李广群
鞠瑞成
王燕蓬
郑超
王晓霞
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Shandong Baiwo Biotechnology Co ltd
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    • C12BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12MAPPARATUS FOR ENZYMOLOGY OR MICROBIOLOGY; APPARATUS FOR CULTURING MICROORGANISMS FOR PRODUCING BIOMASS, FOR GROWING CELLS OR FOR OBTAINING FERMENTATION OR METABOLIC PRODUCTS, i.e. BIOREACTORS OR FERMENTERS
    • C12M21/00Bioreactors or fermenters specially adapted for specific uses
    • C12M21/18Apparatus specially designed for the use of free, immobilized or carrier-bound enzymes
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    • C12M41/00Means for regulation, monitoring, measurement or control, e.g. flow regulation
    • C12M41/12Means for regulation, monitoring, measurement or control, e.g. flow regulation of temperature
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    • C12M41/00Means for regulation, monitoring, measurement or control, e.g. flow regulation
    • C12M41/42Means for regulation, monitoring, measurement or control, e.g. flow regulation of agitation speed
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    • C12BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12MAPPARATUS FOR ENZYMOLOGY OR MICROBIOLOGY; APPARATUS FOR CULTURING MICROORGANISMS FOR PRODUCING BIOMASS, FOR GROWING CELLS OR FOR OBTAINING FERMENTATION OR METABOLIC PRODUCTS, i.e. BIOREACTORS OR FERMENTERS
    • C12M41/00Means for regulation, monitoring, measurement or control, e.g. flow regulation
    • C12M41/48Automatic or computerized control

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Abstract

The invention discloses a biological enzyme catalysis chemical reaction tank device, which relates to the technical field of catalysis reaction tanks, and comprises a reaction tank body, wherein the top of the side end of the reaction tank body is communicated with an optimized enzyme conveying channel, a quantitative balance component is arranged in the optimized enzyme conveying channel, the side end of the top of the optimized enzyme conveying channel is communicated with an adding port, the substrate concentration is effectively improved by matching the quantitative balance component, a detector, a graphene conductive layer, a waterproof electric telescopic rod and a temperature control heating conductive block, the substrate conversion rate is conveniently improved, the improved substrate concentration is appropriately balanced and controlled according to the whole biological enzyme catalysis reaction rate, the whole catalytic reaction is prevented from being inhibited due to the excessive substrate concentration, the whole device effectively achieves catalytic balance under the regulation of the whole temperature, ph, ions and the substrate conversion rate, the whole catalytic accuracy is improved, and the influence of residual impurities in the reaction on the whole biological enzyme catalysis is reduced.

Description

一种生物酶催化化学反应罐装置A bio-enzyme catalytic chemical reaction tank device

技术领域Technical Field

本发明涉及催化反应罐技术领域,具体为一种生物酶催化化学反应罐装置。The invention relates to the technical field of catalytic reaction tanks, in particular to a bio-enzyme catalytic chemical reaction tank device.

背景技术Background technique

在催化剂作用下进行的化学反应称为催化反应。化学反应中,反应分子原有的某些化学键,必须解离并形成新的化学键,这需要一定的活化能。在某些难以发生化学反应的体系中,加入有助于反应分子化学键重排的第三种物质(催化剂)其作用可降低反应的活化能,因而能加速化学反应和控制产物的选择性及立体规整性。A chemical reaction carried out under the action of a catalyst is called a catalytic reaction. In a chemical reaction, some of the original chemical bonds of the reaction molecules must be dissociated and new chemical bonds must be formed, which requires a certain amount of activation energy. In some systems where chemical reactions are difficult to occur, the addition of a third substance (catalyst) that helps the chemical bonds of the reaction molecules to rearrange can reduce the activation energy of the reaction, thereby accelerating the chemical reaction and controlling the selectivity and stereoregularity of the product.

但现有技术中,目前在生物酶催化化学反应罐作业时,整体的反应速率得不到精准控制,一个温度或者ph的环境变量,会对整体的反应造成影响,并使得整体的底物转化率低,导致反应效果不能得到有效保障,进而可能造成反应中残存有杂质,影响生物酶作业的效率,因此就需要提出一种生物酶催化化学反应罐装置。However, in the prior art, when the bio-enzyme catalyzed chemical reactor is operating, the overall reaction rate cannot be precisely controlled. An environmental variable such as temperature or pH will affect the overall reaction and make the overall substrate conversion rate low, resulting in the reaction effect cannot be effectively guaranteed, which may cause impurities to remain in the reaction and affect the efficiency of the bio-enzyme operation. Therefore, it is necessary to propose a bio-enzyme catalyzed chemical reactor device.

发明内容Summary of the invention

本发明的目的在于提供一种生物酶催化化学反应罐装置,以解决上述背景技术提出在生物酶催化化学反应罐作业时,整体的反应速率得不到精准控制,一个温度或者ph的环境变量,会对整体的反应造成影响,并使得整体的底物转化率低,导致反应效果不能得到有效保障,进而可能造成反应中残存有杂质,影响生物酶作业的效率的问题。The object of the present invention is to provide a bio-enzyme catalyzed chemical reaction tank device to solve the problem proposed in the above-mentioned background technology that when the bio-enzyme catalyzed chemical reaction tank is operating, the overall reaction rate cannot be accurately controlled, an environmental variable of temperature or pH will affect the overall reaction and make the overall substrate conversion rate low, resulting in the reaction effect cannot be effectively guaranteed, which may cause impurities to remain in the reaction, affecting the efficiency of the bio-enzyme operation.

为实现上述目的,本发明提供如下技术方案:一种生物酶催化化学反应罐装置,包括反应罐体,所述反应罐体的侧端顶部连通有优化酶输送通道,所述优化酶输送通道的内部安装设置定量平衡组件,所述优化酶输送通道的顶部侧端连通有投加口;所述定量平衡组件包括驱动无刷电机,所述驱动无刷电机的底部安装设置定向转速调节器,所述定向转速调节器的底部轴心端安装设置棘爪轮,所述棘爪轮的底部轴心端安装设置定向转盘,所述棘爪轮的侧角边卡合连接有锥爪,所述锥爪的侧端一体成型有受力转齿卡杆,所述受力转齿卡杆的侧端表面贯穿设置中心轴柱,所述定向转盘的表面上安装设置导信接触簧片,所述受力转齿卡杆的侧端接触连接有接触杆,所述接触杆的侧端通过连接杆柱安装设置定向连接轴销,所述接触杆的侧端紧固连接有受力点触杆,所述受力点触杆的侧壁表面安装设置第一钴磁石,所述定向连接轴销的底部安装设置连接架构,所述连接架构的侧端架设安装优化酶箱,所述优化酶箱的侧壁表面紧固连接有运动控制器,所述运动控制器的侧端安装设置电动控制推杆,所述电动控制推杆的顶部安装设置第二钴磁石,所述第一钴磁石和第二钴磁石磁性连接,所述定向转盘的轴心端底部连接设置有轴向转柱,所述轴向转柱的底部周侧安装设置进料盘,所述进料盘的侧端连通有柔性伸缩轴向管,所述柔性伸缩轴向管的侧端和优化酶箱的表面连通。To achieve the above-mentioned purpose, the present invention provides the following technical solutions: a bio-enzyme catalytic chemical reaction tank device, comprising a reaction tank body, the top of the side end of the reaction tank body is connected to an optimized enzyme delivery channel, a quantitative balance component is installed inside the optimized enzyme delivery channel, and the top side end of the optimized enzyme delivery channel is connected to a dosing port; the quantitative balance component comprises a driving brushless motor, a directional speed regulator is installed at the bottom of the driving brushless motor, a ratchet wheel is installed at the bottom axial end of the directional speed regulator, a directional turntable is installed at the bottom axial end of the ratchet wheel, a cone claw is engaged with the side angle edge of the ratchet wheel, a force-bearing rotating gear clamp rod is integrally formed at the side end of the cone claw, a central shaft column is penetrated through the side end surface of the force-bearing rotating gear clamp rod, a guide contact spring is installed on the surface of the directional turntable, and the force-bearing rotating gear clamp rod is The side end is contact-connected with a contact rod, and a directional connecting pin is installed on the side end of the contact rod through a connecting rod column. The side end of the contact rod is fastened with a force-bearing point contact rod, and a first cobalt magnet is installed on the side wall surface of the force-bearing point contact rod. A connecting structure is installed at the bottom of the directional connecting pin, and an optimized enzyme box is installed on the side end of the connecting structure. A motion controller is fastened to the side wall surface of the optimized enzyme box, and an electric control push rod is installed on the side end of the motion controller. A second cobalt magnet is installed on the top of the electric control push rod, and the first cobalt magnet and the second cobalt magnet are magnetically connected. An axial rotating column is connected to the bottom of the axial end of the directional turntable, and a feed disc is installed on the bottom peripheral side of the axial rotating column. The side end of the feed disc is connected with a flexible telescopic axial tube, and the side end of the flexible telescopic axial tube is connected to the surface of the optimized enzyme box.

优选的,所述进料盘的顶壁周侧表面开设有接触滑槽,所述进料盘的表面上等距安装设置四组受压投加端,四组所述受压投加端的边侧连接设置接触簧片,所述接触簧片在接触滑槽的内部贴合安装,所述定向转盘的底部边侧紧固连接有接触伸缩触杆,所述接触伸缩触杆呈线性在接触滑槽的顶部安装设置。Preferably, a contact slide groove is provided on the peripheral surface of the top wall of the feed tray, and four groups of pressurized feeding ends are equidistantly installed on the surface of the feed tray. Contact springs are connected to the sides of the four groups of pressurized feeding ends, and the contact springs are fitted inside the contact slide groove. A contact telescopic feeler rod is fastened to the bottom side of the directional turntable, and the contact telescopic feeler rod is linearly installed on the top of the contact slide groove.

优选的,所述优化酶输送通道的侧壁表面安装设置微处理控制器,所述优化酶输送通道的顶部安装设置反馈线路架,所述反馈线路架的侧端连接有微型泵,所述微型泵的底侧端安装设置活性传感器,所述微型泵的底部连通有采样管。Preferably, a microprocessor controller is installed on the side wall surface of the optimized enzyme delivery channel, a feedback circuit frame is installed on the top of the optimized enzyme delivery channel, a micro pump is connected to the side end of the feedback circuit frame, an activity sensor is installed on the bottom side end of the micro pump, and a sampling tube is connected to the bottom of the micro pump.

优选的,所述反应罐体的另一侧端连通有进料控制阀端,所述反应罐体的底端表面上连通有出液控制阀端,所述出液控制阀端的侧端和采样管的底端连通,所述反应罐体的底部另一侧表面连通有废液处理阀端,所述反应罐体的顶部另一侧表面上分别对称连通有第一液体控制阀端和第二液体控制阀端。Preferably, the other side end of the reaction tank body is connected to a feed control valve end, the bottom surface of the reaction tank body is connected to a liquid outlet control valve end, the side end of the liquid outlet control valve end is connected to the bottom end of the sampling tube, the other side surface of the bottom of the reaction tank body is connected to a waste liquid treatment valve end, and the other side surface of the top of the reaction tank body is symmetrically connected to a first liquid control valve end and a second liquid control valve end respectively.

优选的,所述反应罐体的顶部安装设置行星控制齿轮组,所述行星控制齿轮组的轴心端顶部连接设置控制电机,所述行星控制齿轮组的内部三组行星齿轮轴心端通过连接柱紧固连接有上位转盘,所述上位转盘的顶部安装设置防护盖板。Preferably, a planetary control gear set is installed on the top of the reaction tank body, and a control motor is connected to the top of the axial end of the planetary control gear set. The axial ends of the three sets of planetary gears inside the planetary control gear set are fastened to an upper turntable through connecting columns, and a protective cover plate is installed on the top of the upper turntable.

优选的,所述上位转盘的周侧转动连接有轨道,所述轨道安装设置在反应罐体的顶部,所述防护盖板在反应罐体的顶部进行盖合安装,所述上位转盘的底部轴心端连接设置中心柱体,所述上位转盘的底部周侧连接设置分搅杆,所述中心柱体的底部周测套设安装检测仪。Preferably, the circumferential side of the upper turntable is rotatably connected to a track, the track is installed on the top of the reaction tank body, the protective cover is installed on the top of the reaction tank body, the bottom axial end of the upper turntable is connected to a central column, the bottom circumferential side of the upper turntable is connected to a stirring rod, and a detector is installed on the bottom circumferential sleeve of the central column.

优选的,所述反应罐体的底部安装设置齿轮驱动组,所述齿轮驱动组的一侧齿轮轴心端安装设置控制调节电机,所述齿轮驱动组的另一侧齿轮顶部轴心端连接安装底轴轨。Preferably, a gear drive group is installed at the bottom of the reaction tank body, a control and adjustment motor is installed at the shaft center end of the gear on one side of the gear drive group, and a bottom shaft rail is connected to the top shaft center end of the gear on the other side of the gear drive group.

优选的,所述底轴轨安装设置在反应罐体的内部底端,所述底轴轨的顶部转动连接有边侧调节反应杆。Preferably, the bottom shaft rail is installed at the inner bottom end of the reaction tank body, and the top of the bottom shaft rail is rotatably connected to a side adjustment reaction rod.

优选的,所述反应罐体的外部周测套设有保温防护壳,所述保温防护壳的内壁表面设置石墨烯导性层,所述边侧调节反应杆的外壁表面安装设置防水电动伸缩杆。Preferably, the outer peripheral cover of the reaction tank body is provided with a heat-insulating protective shell, the inner wall surface of the heat-insulating protective shell is provided with a graphene conductive layer, and the outer wall surface of the side-adjusting reaction rod is installed with a waterproof electric telescopic rod.

优选的,所述防水电动伸缩杆的侧端连接设置温控发热导电块,所述温控发热导电块和石墨烯导性层接触设置,所述反应罐体的底部周侧套设安装支撑腿架。Preferably, a temperature-controlled heating conductive block is connected to the side end of the waterproof electric telescopic rod, the temperature-controlled heating conductive block is in contact with the graphene conductive layer, and a supporting leg frame is sleeved and installed around the bottom of the reaction tank body.

与现有技术相比,本发明的有益效果是:Compared with the prior art, the present invention has the following beneficial effects:

本发明中,通过在定量平衡组件配合下,利用定向转速调节器带动棘爪轮进行转动,但此时的转动驱动前提为运动控制器接收到驱动无刷电机所需转动的驱动信号,使得电动控制推杆进行前伸,使得第一钴磁石和第二钴磁石磁性连接,便于在电动控制推杆的推动力作用下,使得受力点触杆受力进行转动,进一步使得受力转齿卡杆带动锥爪在定向连接轴销的外部进行转动,即锥爪和棘爪轮进行分离,使得棘爪轮脱落限制,接着导信接触簧片和受力转齿卡杆的表面进行接触,便于对受力转齿卡杆的受力情况信号进行传导至运动控制器中,之后棘爪轮带动定向转盘进行转动,便于当进行生物酶催化反应内部底物转化率受到影响时,发送电信号至接触伸缩触杆,使得接触伸缩触杆在定向转盘的转向带动下,进行周向调节运转,并根据所反馈的信号,进行向下延伸,便于接触伸缩触杆的底部和接触滑槽的内部接触滑动,当滑动一周圈后,接触伸缩触杆的底部和接触簧片进行接触,并利用所接触的导电触发信号输送至受压投加端中,使得其中一组在接触簧片所控制的受压投加端进行辅助优化酶投加作业,且当接触伸缩触杆形成第一周圈与接触簧片接触后,接触伸缩触杆回位,根据所反馈的底物转化率来进行后续第二周圈、第三周圈和第四周圈等接触控制操作,有效提高底物浓度,便于底物转化率提高,且所提高的底物浓度根据整体的生物酶催化反应速率进行相适宜平衡控制,避免过高的底物浓度导致整体的催化反应受到抑制,整体装置有效对生物酶的催化反应速率在整体温度、ph、离子、底物转化率的调节下,达到催化平衡,提高整体的催化精准性,降低反应中残存有杂质对整体生物酶催化产生影响。In the present invention, the directional speed regulator is used to drive the ratchet wheel to rotate under the cooperation of the quantitative balancing component. However, the rotation drive at this time is premised on the motion controller receiving the driving signal required to drive the brushless motor to rotate, so that the electric control push rod is extended forward, so that the first cobalt magnet and the second cobalt magnet are magnetically connected, so that under the driving force of the electric control push rod, the force point contact rod is forced to rotate, and further the force-bearing rotating gear clamping rod drives the cone claw to rotate outside the directional connecting shaft pin, that is, the cone claw and the ratchet wheel are separated, so that the ratchet wheel is restricted from falling off, and then the guide contact spring and the surface of the force-bearing rotating gear clamping rod are in contact, so that the force condition signal of the force-bearing rotating gear clamping rod is transmitted to the motion controller, and then the ratchet wheel drives the directional turntable to rotate, so that when the internal substrate conversion rate of the biological enzyme catalytic reaction is affected, an electrical signal is sent to the contact telescopic contact rod, so that the contact telescopic contact rod is driven by the steering of the directional turntable to perform circumferential adjustment operation, and according to the feedback signal, it is downward. The bottom of the contact telescopic feeler rod contacts the contact spring after sliding one circle, and the conductive trigger signal is transmitted to the pressurized dosing end by using the contact, so that one group of the pressurized dosing end controlled by the contact spring performs auxiliary optimization enzyme dosing operation, and when the contact telescopic feeler rod forms the first circle and contacts the contact spring, the contact telescopic feeler rod returns to its original position, and performs subsequent contact control operations such as the second circle, the third circle and the fourth circle according to the feedback substrate conversion rate, effectively improving the substrate concentration, facilitating the improvement of the substrate conversion rate, and the increased substrate concentration is appropriately balanced and controlled according to the overall bio-enzyme catalytic reaction rate, avoiding the inhibition of the overall catalytic reaction due to excessive substrate concentration, and the overall device effectively adjusts the catalytic reaction rate of the bio-enzyme under the regulation of the overall temperature, pH, ions and substrate conversion rate to achieve catalytic balance, improve the overall catalytic accuracy, and reduce the influence of impurities remaining in the reaction on the overall bio-enzyme catalysis.

2、本发明中,通过在检测仪、石墨烯导性层、防水电动伸缩杆和温控发热导电块配合下,当检测到整体的内部催化速率受环境变量影响时,防水电动伸缩杆根据所产生的温度环境变量的大小进行控制调节延伸,如温度环境变量小时,一根防水电动伸缩杆进行延伸,使得温控发热导电块和石墨烯导性层进行接触,并利用和石墨烯导性层的接触反应,来提高整体的反应环境温度量,同步在上述分搅杆和边侧调节反应杆的转动调节下,使得内部所反应物温度,可以有效进行均匀受热,避免温度变量影响整体反应速率。2. In the present invention, by cooperating with the detector, the graphene conductive layer, the waterproof electric telescopic rod and the temperature-controlled heating conductive block, when it is detected that the overall internal catalytic rate is affected by the environmental variables, the waterproof electric telescopic rod is controlled and adjusted to extend according to the size of the generated temperature environmental variables. For example, when the temperature environmental variable is small, a waterproof electric telescopic rod is extended to make the temperature-controlled heating conductive block contact the graphene conductive layer, and utilize the contact reaction with the graphene conductive layer to increase the overall reaction environment temperature. Simultaneously, under the rotation adjustment of the above-mentioned stirring rod and the side adjustment reaction rod, the temperature of the internal reactants can be effectively and evenly heated to avoid the temperature variables affecting the overall reaction rate.

3、本发明中,通过在行星控制齿轮组、分搅杆、齿轮驱动组、边侧调节反应杆配合下,利用所启动的控制电机带动行星控制齿轮组进行转动,进而使得行星控制齿轮组内部三组行星齿轮轴心端通过连接柱所紧固连接的上位转盘在反应罐体的顶部进行顺时针转动控制,同步带动分搅杆在反应罐体进行促进反应速率的转动,并通过分搅杆表面的离子控制调节器在检测仪配合下实时对反应罐体内部的反应速率进行控制,同时在控制调节电机作用下,根据检测仪所检测反馈信号,带动齿轮驱动组进行转动调节,进而带动底轴轨在反应罐体的底部内壁表面进行贴合转动,且边侧调节反应杆同步进行转动,并实时通过杆体表面所安装的ph控制器对整的反应催化速率进行调节,进一步保障整体反应的作业效率。3. In the present invention, the planetary control gear set is driven to rotate by the started control motor under the cooperation of the planetary control gear set, the sub-stirring rod, the gear drive set and the side adjustment reaction rod, so that the upper turntable to which the axial ends of the three sets of planetary gears inside the planetary control gear set are fastened through the connecting column is controlled to rotate clockwise on the top of the reaction tank body, and the sub-stirring rod is synchronously driven to rotate in the reaction tank body to promote the reaction rate, and the reaction rate inside the reaction tank body is controlled in real time through the ion control regulator on the surface of the sub-stirring rod in cooperation with the detector, and at the same time, under the action of the control and adjustment motor, according to the feedback signal detected by the detector, the gear drive set is driven to rotate and adjust, and then the bottom shaft rail is driven to rotate in contact with the bottom inner wall surface of the reaction tank body, and the side adjustment reaction rod is rotated synchronously, and the entire reaction catalytic rate is adjusted in real time through the pH controller installed on the surface of the rod body, so as to further ensure the operating efficiency of the overall reaction.

附图说明BRIEF DESCRIPTION OF THE DRAWINGS

图1为本发明一种生物酶催化化学反应罐装置中主视的结构示意图;FIG1 is a schematic diagram of the structure of a bio-enzyme catalyzed chemical reaction tank device according to the present invention from a front view;

图2为本发明一种生物酶催化化学反应罐装置中仰视的结构示意图;FIG2 is a schematic diagram of the structure of a bio-enzyme catalyzed chemical reaction tank device in the present invention when viewed from above;

图3为本发明一种生物酶催化化学反应罐装置中反应罐体的内部结构示意图;FIG3 is a schematic diagram of the internal structure of a reaction tank body in a bio-enzyme catalytic chemical reaction tank device of the present invention;

图4为本发明一种生物酶催化化学反应罐装置中反应罐体的剖视结构示意图;FIG4 is a schematic cross-sectional view of a reaction tank body in a bio-enzyme catalyzed chemical reaction tank device according to the present invention;

图5为本发明一种生物酶催化化学反应罐装置中图3中A处放大的结构示意图;FIG5 is a schematic diagram of the structure of an enlarged portion A in FIG3 of a bio-enzyme catalyzed chemical reaction tank device of the present invention;

图6为本发明一种生物酶催化化学反应罐装置中定量平衡组件的安装位置结构示意图;FIG6 is a schematic diagram of the installation position structure of a quantitative balance component in a bio-enzyme catalytic chemical reaction tank device of the present invention;

图7为本发明一种生物酶催化化学反应罐装置中定量平衡组件的结构示意图;FIG7 is a schematic structural diagram of a quantitative balance component in a bio-enzyme catalytic chemical reaction tank device of the present invention;

图8为本发明一种生物酶催化化学反应罐装置中定量平衡组件的俯视结构示意图;FIG8 is a schematic diagram of a top view of a quantitative balance assembly in a bio-enzyme catalyzed chemical reaction tank device according to the present invention;

图9为本发明一种生物酶催化化学反应罐装置中定量平衡组件的另一角度结构示意图。FIG. 9 is a schematic structural diagram of a quantitative balance component in a bio-enzyme catalyzed chemical reaction tank device according to another angle of the present invention.

图中:1、反应罐体;2、支撑腿架;3、保温防护壳;4、优化酶输送通道;5、投加口;6、微处理控制器;7、反馈线路架;8、微型泵;9、活性传感器;10、进料控制阀端;11、采样管;12、废液处理阀端;13、第一液体控制阀端;14、防护盖板;15、出液控制阀端;16、控制电机;17、控制调节电机;18、定量平衡组件;180、驱动无刷电机;181、定向转速调节器;182、棘爪轮;183、锥爪;184、受力转齿卡杆;185、中心轴柱;186、导信接触簧片;187、定向转盘;188、接触杆;189、定向连接轴销;1890、连接架构;1891、优化酶箱;1892、柔性伸缩轴向管;1893、进料盘;1894、接触滑槽;1895、接触簧片;1896、受力点触杆;1897、运动控制器;1898、电动控制推杆;1899、第一钴磁石;1801、受压投加端;1802、接触伸缩触杆;19、底轴轨;20、边侧调节反应杆;21、行星控制齿轮组;22、分搅杆;23、中心柱体;24、检测仪;25、齿轮驱动组;26、防水电动伸缩杆;27、温控发热导电块;28、石墨烯导性层。In the figure: 1, reaction tank; 2, support leg frame; 3, insulation protection shell; 4, optimized enzyme delivery channel; 5, addition port; 6, microprocessor controller; 7, feedback circuit frame; 8, micro pump; 9, activity sensor; 10, feed control valve end; 11, sampling tube; 12, waste liquid treatment valve end; 13, first liquid control valve end; 14, protective cover; 15, liquid outlet control valve end; 16, control motor; 17, control and adjustment motor; 18, quantitative balance component; 180, drive brushless motor; 181, directional speed regulator; 182, ratchet wheel; 183, cone claw; 184, force-bearing gear clamping rod; 185, central shaft column; 186, guide contact spring; 187, directional turntable; 188 , contact rod; 189, directional connecting shaft pin; 1890, connecting structure; 1891, optimized enzyme box; 1892, flexible telescopic axial tube; 1893, feed tray; 1894, contact slide; 1895, contact spring; 1896, force point contact rod; 1897, motion controller; 1898, electric control push rod; 1899, first cobalt magnet; 1801, pressurized feeding end; 1802, contact telescopic contact rod; 19, bottom shaft rail; 20, side adjustment reaction rod; 21, planetary control gear set; 22, sub-stirring rod; 23, central column; 24, detector; 25, gear drive group; 26, waterproof electric telescopic rod; 27, temperature-controlled heating conductive block; 28, graphene conductive layer.

具体实施方式Detailed ways

下面将结合本发明实施例中的附图,对本发明实施例中的技术方案进行清楚、完整地描述,显然,所描述的实施条例仅仅是本发明一部分实施例,而不是全部的实施例。基于本发明中的实施例,本领域普通技术人员在没有做出创造性劳动前提下所获得的所有其他实施例,都属于本发明保护的范围。The following will be combined with the drawings in the embodiments of the present invention to clearly and completely describe the technical solutions in the embodiments of the present invention. Obviously, the implementation regulations described are only part of the embodiments of the present invention, not all of the embodiments. Based on the embodiments of the present invention, all other embodiments obtained by ordinary technicians in this field without creative work are within the scope of protection of the present invention.

参照图1-图9所示:一种生物酶催化化学反应罐装置,包括反应罐体1,反应罐体1的侧端顶部连通有优化酶输送通道4,优化酶输送通道4的内部安装设置定量平衡组件18,优化酶输送通道4的顶部侧端连通有投加口5;定量平衡组件18包括驱动无刷电机180,驱动无刷电机180的底部安装设置定向转速调节器181,定向转速调节器181的底部轴心端安装设置棘爪轮182,棘爪轮182的底部轴心端安装设置定向转盘187,棘爪轮182的侧角边卡合连接有锥爪183,锥爪183的侧端一体成型有受力转齿卡杆184,受力转齿卡杆184的侧端表面贯穿设置中心轴柱185,定向转盘187的表面上安装设置导信接触簧片186,受力转齿卡杆184的侧端接触连接有接触杆188,接触杆188的侧端通过连接杆柱安装设置定向连接轴销189,接触杆188的侧端紧固连接有受力点触杆1896,受力点触杆1896的侧壁表面安装设置第一钴磁石1899,定向连接轴销189的底部安装设置连接架构1890,连接架构1890的侧端架设安装优化酶箱1891,优化酶箱1891的侧壁表面紧固连接有运动控制器1897,运动控制器1897的侧端安装设置电动控制推杆1898,电动控制推杆1898的顶部安装设置第二钴磁石,第一钴磁石1899和第二钴磁石磁性连接,定向转盘187的轴心端底部连接设置有轴向转柱,轴向转柱的底部周侧安装设置进料盘1893,进料盘1893的侧端连通有柔性伸缩轴向管1892,柔性伸缩轴向管1892的侧端和优化酶箱1891的表面连通。Referring to Figures 1 to 9: a bio-enzyme catalytic chemical reaction tank device, comprising a reaction tank body 1, the top of the side end of the reaction tank body 1 is connected to an optimized enzyme delivery channel 4, the inside of the optimized enzyme delivery channel 4 is installed with a quantitative balance component 18, and the top side end of the optimized enzyme delivery channel 4 is connected to a dosing port 5; the quantitative balance component 18 comprises a driving brushless motor 180, a directional speed regulator 181 is installed at the bottom of the driving brushless motor 180, a ratchet wheel 182 is installed at the bottom axial end of the directional speed regulator 181, a directional turntable 187 is installed at the bottom axial end of the ratchet wheel 182, a cone claw 183 is connected to the side corner edge of the ratchet wheel 182, and a force-bearing rotating gear clamping rod 184 is integrally formed at the side end of the cone claw 183, a central shaft column 185 is set through the side end surface of the force-bearing rotating gear clamping rod 184, a guide contact spring 186 is installed on the surface of the directional turntable 187, and the side end of the force-bearing rotating gear clamping rod 184 is contact-connected with a contact rod 188, and the contact rod 1 The side end of the contact rod 188 is provided with a directional connecting shaft pin 189 through a connecting rod column, the side end of the contact rod 188 is fastened with a force point contact rod 1896, the side wall surface of the force point contact rod 1896 is installed with a first cobalt magnet 1899, the bottom of the directional connecting shaft pin 189 is installed with a connecting frame 1890, the side end of the connecting frame 1890 is installed with an optimized enzyme box 1891, the side wall surface of the optimized enzyme box 1891 is fastened with a motion controller 1897, and the motion controller 1897 is fastened with a motion controller 1897. An electric control push rod 1898 is installed on the side end of 97, and a second cobalt magnet is installed on the top of the electric control push rod 1898. The first cobalt magnet 1899 is magnetically connected to the second cobalt magnet. An axial rotating column is connected to the bottom of the axial end of the directional turntable 187, and a feed disk 1893 is installed on the bottom circumference of the axial rotating column. The side end of the feed disk 1893 is connected to a flexible telescopic axial tube 1892, and the side end of the flexible telescopic axial tube 1892 is connected to the surface of the optimized enzyme box 1891.

根据图3、图4、图6、图7和图9所示,进料盘1893的顶壁周侧表面开设有接触滑槽1894,进料盘1893的表面上等距安装设置四组受压投加端1801,四组受压投加端1801的边侧连接设置接触簧片1895,接触簧片1895在接触滑槽1894的内部贴合安装,定向转盘187的底部边侧紧固连接有接触伸缩触杆1802,接触伸缩触杆1802呈线性在接触滑槽1894的顶部安装设置,当进行生物酶催化反应内部底物转化率受到影响时,发送电信号至接触伸缩触杆1802,使得接触伸缩触杆1802在上述定向转盘187的转向带动下,进行周向调节运转,并根据所反馈的信号,进行向下延伸,便于接触伸缩触杆1802的底部和接触滑槽1894的内部接触滑动,当滑动一周圈后,接触伸缩触杆1802的底部和接触簧片1895进行接触,并利用所接触的导电始发信号输送至受压投加端1801中,使得其中一组在接触簧片1895所控制的受压投加端1801进行辅助优化酶投加作业,且当接触伸缩触杆1802形成第一周圈与接触簧片1895接触后,接触伸缩触杆1802回位,根据所反馈的底物转化率来进行后续第二周圈、第三周圈和第四周圈等接触控制操作,有效提高底物浓度,便于底物转化率提高,且所提高的底物浓度根据整体的生物酶催化反应速率进行相适宜平衡控制,避免过高的底物浓度导致整体的催化反应受到抑制。As shown in Figures 3, 4, 6, 7 and 9, a contact chute 1894 is provided on the circumferential surface of the top wall of the feed tray 1893, and four groups of pressurized feeding ends 1801 are equidistantly installed on the surface of the feed tray 1893. The sides of the four groups of pressurized feeding ends 1801 are connected with contact springs 1895, and the contact springs 1895 are fitted inside the contact chute 1894. The bottom side of the directional turntable 187 is fastened with a contact telescopic feeler rod 1802, and the contact telescopic feeler rod 1802 is linearly installed on the top of the contact chute 1894. When the internal substrate conversion rate of the bio-enzyme catalytic reaction is affected, an electrical signal is sent to the contact telescopic feeler rod 1802, so that the contact telescopic feeler rod 1802 is driven by the steering of the above-mentioned directional turntable 187 to perform circumferential adjustment operation, and extends downward according to the feedback signal, so as to facilitate the contact telescopic feeler rod 1802 to move downward. The bottom of the contact rod 1802 contacts and slides inside the contact groove 1894. After sliding one circle, the bottom of the contact telescopic contact rod 1802 contacts the contact spring 1895, and the conductive initial signal is transmitted to the pressurized addition end 1801 by means of the contact, so that one group of the pressurized addition end 1801 controlled by the contact spring 1895 performs auxiliary optimization enzyme addition operation. After the contact telescopic contact rod 1802 forms the first circle and contacts the contact spring 1895, the contact telescopic contact rod 1802 returns to its original position, and performs subsequent contact control operations such as the second circle, the third circle and the fourth circle according to the feedback substrate conversion rate, thereby effectively increasing the substrate concentration and facilitating the improvement of the substrate conversion rate. The increased substrate concentration is appropriately balanced and controlled according to the overall enzyme catalytic reaction rate to avoid the inhibition of the overall catalytic reaction due to excessive substrate concentration.

根据图1-图4所示,优化酶输送通道4的侧壁表面安装设置微处理控制器6,优化酶输送通道4的顶部安装设置反馈线路架7,反馈线路架7的侧端连接有微型泵8,微型泵8的底侧端安装设置活性传感器9,微型泵8的底部连通有采样管11,在反馈线路架7配合下,便于将采样管11中所抽取的排出检测样本等量并按照预设时效在微型泵8的配合下进行抽取,并在活性传感器9的作用下,对所抽取样本液进行检测,之后利用反馈线路架7进行反馈至上述驱动无刷电机180中进行调节控制作业。As shown in Figures 1 to 4, a microprocessor controller 6 is installed on the side wall surface of the optimized enzyme delivery channel 4, a feedback circuit frame 7 is installed on the top of the optimized enzyme delivery channel 4, a micro pump 8 is connected to the side end of the feedback circuit frame 7, an activity sensor 9 is installed on the bottom side end of the micro pump 8, and a sampling tube 11 is connected to the bottom of the micro pump 8. With the cooperation of the feedback circuit frame 7, it is convenient to extract an equal amount of the discharge test sample drawn from the sampling tube 11 and extract it according to the preset time with the cooperation of the micro pump 8, and under the action of the activity sensor 9, the extracted sample liquid is tested, and then the feedback circuit frame 7 is used to feed back to the above-mentioned driving brushless motor 180 for adjustment and control operations.

根据图1-图4所示,反应罐体1的另一侧端连通有进料控制阀端10,反应罐体1的底端表面上连通有出液控制阀端15,出液控制阀端15的侧端和采样管11的底端连通,反应罐体1的底部另一侧表面连通有废液处理阀端12,反应罐体1的顶部另一侧表面上分别对称连通有第一液体控制阀端13和第二液体控制阀端,在进料控制阀端10的配合下,便于对进料量和进料速率进行有效控制,在出液控制阀端15的配合下,便于上述采样管11可以根据需求对出液控制阀端15所控制排出的液体样本进行采样抽取,且使得不同时间段进行多次采样控制,有效对整体的催化反应速率进行实时调节,避免整体的反应速率在温度或者ph的环境变量下,使得整体的反应造成影响。As shown in Figures 1 to 4, the other side end of the reaction tank body 1 is connected to a feed control valve end 10, the bottom surface of the reaction tank body 1 is connected to a liquid outlet control valve end 15, the side end of the liquid outlet control valve end 15 is connected to the bottom end of the sampling tube 11, the other side surface of the bottom of the reaction tank body 1 is connected to a waste liquid treatment valve end 12, and the other side surface of the top of the reaction tank body 1 is symmetrically connected to a first liquid control valve end 13 and a second liquid control valve end, respectively. With the cooperation of the feed control valve end 10, it is convenient to effectively control the feed amount and feed rate. With the cooperation of the liquid outlet control valve end 15, it is convenient for the above-mentioned sampling tube 11 to sample and extract the liquid sample discharged by the liquid outlet control valve end 15 according to demand, and multiple sampling controls are performed in different time periods, so as to effectively adjust the overall catalytic reaction rate in real time, and avoid the overall reaction rate being affected by the environmental variables of temperature or pH, which affects the overall reaction.

根据图1-图3所示,反应罐体1的顶部安装设置行星控制齿轮组21,行星控制齿轮组21的轴心端顶部连接设置控制电机16,行星控制齿轮组21的内部三组行星齿轮轴心端通过连接柱紧固连接有上位转盘,上位转盘的顶部安装设置防护盖板14,在控制电机16作用下,当进行生物酶催化反应作业时,利用所启动的控制电机16带动行星控制齿轮组21进行转动,进而使得行星控制齿轮组21内部三组行星齿轮轴心端通过连接柱所紧固连接的上位转盘在反应罐体1的顶部进行顺时针转动控制。As shown in Figures 1 to 3, a planetary control gear set 21 is installed on the top of the reaction tank body 1, and a control motor 16 is connected to the top of the axial end of the planetary control gear set 21. The axial ends of the three sets of planetary gears inside the planetary control gear set 21 are fastened to the upper turntable through connecting columns, and a protective cover plate 14 is installed on the top of the upper turntable. Under the action of the control motor 16, when the bio-enzyme catalytic reaction operation is carried out, the started control motor 16 is used to drive the planetary control gear set 21 to rotate, so that the upper turntable to which the axial ends of the three sets of planetary gears inside the planetary control gear set 21 are fastened through the connecting column is controlled to rotate clockwise on the top of the reaction tank body 1.

根据图4所示,上位转盘的周侧转动连接有轨道,轨道安装设置在反应罐体1的顶部,防护盖板14在反应罐体1的顶部进行盖合安装,上位转盘的底部轴心端连接设置中心柱体23,上位转盘的底部周侧连接设置分搅杆22,中心柱体23的底部周测套设安装检测仪24,当上位转盘进行顺时针转动时,同步带动分搅杆22在反应罐体1进行促进反应速率的转动,并通过分搅杆22表面的离子控制调节器在检测仪24配合下实时对反应罐体1内部的反应速率进行控制。As shown in Figure 4, the circumferential side of the upper turntable is connected to a track for rotation, the track is installed on the top of the reaction tank body 1, the protective cover 14 is installed on the top of the reaction tank body 1, the bottom axial end of the upper turntable is connected to the central column 23, the bottom circumferential side of the upper turntable is connected to the sub-stirring rod 22, and the bottom circumferential sleeve of the central column 23 is installed with a detector 24. When the upper turntable rotates clockwise, it synchronously drives the sub-stirring rod 22 to rotate in the reaction tank body 1 to promote the reaction rate, and the reaction rate inside the reaction tank body 1 is controlled in real time through the ion control regulator on the surface of the sub-stirring rod 22 with the cooperation of the detector 24.

根据图2-图4所示,反应罐体1的底部安装设置齿轮驱动组25,齿轮驱动组25的一侧齿轮轴心端安装设置控制调节电机17,齿轮驱动组25的另一侧齿轮顶部轴心端连接安装底轴轨19,在控制调节电机17作用下,根据检测仪24所检测反馈信号,带动齿轮驱动组25进行转动调节,进而带动底轴轨19在反应罐体1的底部内壁表面进行贴合转动。As shown in Figures 2 to 4, a gear drive group 25 is installed at the bottom of the reaction tank body 1, and a control and adjustment motor 17 is installed at the shaft center end of the gear on one side of the gear drive group 25. The shaft center end of the top gear on the other side of the gear drive group 25 is connected to the bottom shaft rail 19. Under the action of the control and adjustment motor 17, according to the feedback signal detected by the detector 24, the gear drive group 25 is driven to rotate and adjust, thereby driving the bottom shaft rail 19 to rotate in contact with the bottom inner wall surface of the reaction tank body 1.

根据图3-图5所示,底轴轨19安装设置在反应罐体1的内部底端,底轴轨19的顶部转动连接有边侧调节反应杆20,在底轴轨19进行转动时,边侧调节反应杆20同步进行转动,并实时通过杆体表面所安装的ph控制器对整的反应催化速率进行调节。As shown in Figures 3 to 5, the bottom shaft rail 19 is installed at the inner bottom end of the reaction tank body 1, and the top of the bottom shaft rail 19 is rotatably connected to the side adjustment reaction rod 20. When the bottom shaft rail 19 rotates, the side adjustment reaction rod 20 rotates synchronously, and the entire reaction catalytic rate is adjusted in real time through the pH controller installed on the surface of the rod body.

根据图1和图5所示,反应罐体1的外部周测套设有保温防护壳3,保温防护壳3的内壁表面设置石墨烯导性层28,边侧调节反应杆20的外壁表面安装设置防水电动伸缩杆26,当边侧调节反应杆20转动时,防水电动伸缩杆26同步跟随转动,并同步在检测仪24的内部实时检测反馈数据作用下,当检测到整体的内部催化速率受环境变量影响时,防水电动伸缩杆26根据所产生的温度环境变量的大小进行控制调节延伸。As shown in Figures 1 and 5, the outer peripheral sleeve of the reaction tank body 1 is provided with a thermal insulation protective shell 3, the inner wall surface of the thermal insulation protective shell 3 is provided with a graphene conductive layer 28, and the outer wall surface of the side adjustment reaction rod 20 is installed with a waterproof electric telescopic rod 26. When the side adjustment reaction rod 20 rotates, the waterproof electric telescopic rod 26 synchronously follows the rotation, and synchronously under the action of the internal real-time detection feedback data of the detector 24, when it is detected that the overall internal catalytic rate is affected by the environmental variables, the waterproof electric telescopic rod 26 is controlled and adjusted to extend according to the size of the generated temperature environmental variables.

根据图5所示,防水电动伸缩杆26的侧端连接设置温控发热导电块27,温控发热导电块27和石墨烯导性层28接触设置,反应罐体1的底部周侧套设安装支撑腿架2,如温度环境变量小时,一根防水电动伸缩杆26进行延伸,使得温控发热导电块27和石墨烯导性层28进行接触,并利用和石墨烯导性层28的接触反应,来提高整体的反应环境温度量,同步在上述分搅杆22和边侧调节反应杆20的转动调节下,使得内部所反应物温度,可以有效进行均匀受热,避免温度变量影响整体反应速率。As shown in Figure 5, the side end of the waterproof electric telescopic rod 26 is connected to a temperature-controlled heating conductive block 27, and the temperature-controlled heating conductive block 27 is in contact with the graphene conductive layer 28. The bottom periphery of the reaction tank body 1 is sleeved with a support leg frame 2. If the temperature environment variable is small, a waterproof electric telescopic rod 26 is extended to make the temperature-controlled heating conductive block 27 contact with the graphene conductive layer 28, and utilize the contact reaction with the graphene conductive layer 28 to increase the overall reaction environment temperature. Synchronously, under the rotation adjustment of the above-mentioned sub-stirring rod 22 and the side adjustment reaction rod 20, the temperature of the internal reactants can be effectively and evenly heated to avoid the temperature variable affecting the overall reaction rate.

本发明中的反应罐体1、微处理控制器6、微型泵8、活性传感器9、控制电机16、控制调节电机17、驱动无刷电机180、定向转速调节器181、优化酶箱1891、运动控制器1897、检测仪24、温控发热导电块27和石墨烯导性层28的接线图属于本领域的公知常识,其工作原理是已经公知的技术,其型号根据实际使用选择合适的型号,所以对反应罐体1、微处理控制器6、微型泵8、活性传感器9、控制电机16、控制调节电机17、驱动无刷电机180、定向转速调节器181、优化酶箱1891、运动控制器1897、检测仪24、温控发热导电块27和石墨烯导性层28不再详细解释控制方式和接线布置。The wiring diagram of the reaction tank body 1, microprocessor controller 6, micro pump 8, activity sensor 9, control motor 16, control and adjustment motor 17, drive brushless motor 180, directional speed regulator 181, optimized enzyme box 1891, motion controller 1897, detector 24, temperature-controlled heating conductive block 27 and graphene conductive layer 28 in the present invention belongs to the common knowledge in the field, and its working principle is a well-known technology. The model is selected according to the actual use. Therefore, the control method and wiring arrangement of the reaction tank body 1, microprocessor controller 6, micro pump 8, activity sensor 9, control motor 16, control and adjustment motor 17, drive brushless motor 180, directional speed regulator 181, optimized enzyme box 1891, motion controller 1897, detector 24, temperature-controlled heating conductive block 27 and graphene conductive layer 28 will no longer be explained in detail.

本装置的使用方法及工作原理:首先当进行生物酶催化反应时,将物料从进料控制阀端10中进行投放,便于对进料量和进料速率进行有效控制,当物料置于反应罐体1的内部时,利用所启动的控制电机16带动行星控制齿轮组21进行转动,进而使得行星控制齿轮组21内部三组行星齿轮轴心端通过连接柱所紧固连接的上位转盘在反应罐体1的顶部进行顺时针转动控制,同步带动分搅杆22在反应罐体1进行促进反应速率的转动,并通过分搅杆22表面的离子控制调节器在检测仪24配合下实时对反应罐体1内部的反应速率进行控制,同时在控制调节电机17作用下,根据检测仪24所检测反馈信号,带动齿轮驱动组25进行转动调节,进而带动底轴轨19在反应罐体1的底部内壁表面进行贴合转动,且边侧调节反应杆20同步进行转动,并实时通过杆体表面所安装的ph控制器对整体的反应催化速率进行调节,当边侧调节反应杆20转动时,防水电动伸缩杆26同步跟随转动,并同步在检测仪24的内部实时检测反馈数据作用下,当检测到整体的内部催化速率受环境变量影响时,防水电动伸缩杆26根据所产生的温度环境变量的大小进行控制调节延伸,如温度环境变量小时,一根防水电动伸缩杆26进行延伸,使得温控发热导电块27和石墨烯导性层28进行接触,并利用和石墨烯导性层28的接触反应,来提高整体的反应环境温度量,同步在上述分搅杆22和边侧调节反应杆20的转动调节下,使得内部所反应物温度,可以有效进行均匀受热,避免温度变量影响整体反应速率,接着出液控制阀端15的配合下,便于使得采样管11可以根据需求对出液控制阀端15所控制排出的液体样本进行采样抽取,且使得不同时间段进行多次采样控制,有效对整体的催化反应速率进行实时调节,避免整体的反应速率在温度或者ph的环境变量下,使得整体的反应造成影响,即形成在反馈线路架7配合下,便于将采样管11中所抽取的排出检测样本等量并按照预设时效在微型泵8的配合下进行抽取,并在活性传感器9的作用下,对所抽取样本液进行检测,之后利用反馈线路架7进行反馈至驱动无刷电机180中进行调节控制作业,当驱动无刷电机180受到控制信号时,进行启动,进而在定向转速调节器181配合下带动棘爪轮182进行转动,但此时的转动驱动前提为运动控制器1897接收到驱动无刷电机180所需转动的驱动信号,使得电动控制推杆1898进行前伸,使得第一钴磁石1899和第二钴磁石磁性连接,便于在电动控制推杆1898的推动力作用下,使得受力点触杆1896受力进行转动,进一步使得受力转齿卡杆184带动锥爪183在定向连接轴销189的外部进行转动,即锥爪183和棘爪轮182进行分离,使得棘爪轮182脱落限制,接着导信接触簧片186和受力转齿卡杆184的表面进行接触,便于对受力转齿卡杆184的受力情况信号进行传导至运动控制器1897中,之后棘爪轮182带动定向转盘187进行转动,便于当进行生物酶催化反应内部底物转化率受到影响时,发送电信号至接触伸缩触杆1802,使得接触伸缩触杆1802在定向转盘187的转向带动下,进行周向调节运转,并根据所反馈的信号,进行向下延伸,便于接触伸缩触杆1802的底部和接触滑槽1894的内部接触滑动,当滑动一周圈后,接触伸缩触杆1802的底部和接触簧片1895进行接触,并利用所接触的导电始发信号输送至受压投加端1801中,使得其中一组在接触簧片1895所控制的受压投加端1801进行辅助优化酶投加作业,且当接触伸缩触杆1802形成第一周圈与接触簧片1895接触后,接触伸缩触杆1802回位,根据所反馈的底物转化率来进行后续第二周圈、第三周圈和第四周圈等接触控制操作,有效提高底物浓度,便于底物转化率提高,且所提高的底物浓度根据整体的生物酶催化反应速率进行相适宜平衡控制,避免过高的底物浓度导致整体的催化反应受到抑制,整体装置有效对生物酶的催化反应速率在整体温度、ph、离子、底物转化率的调节下,达到催化平衡,提高整体的催化精准性,降低反应中残存有杂质对整体生物酶催化产生影响。The use method and working principle of the device are as follows: first, when the bio-enzyme catalytic reaction is carried out, the material is fed from the feed control valve end 10, so as to effectively control the feed amount and feed rate. When the material is placed inside the reaction tank body 1, the activated control motor 16 is used to drive the planetary control gear set 21 to rotate, so that the upper turntable to which the shaft ends of the three sets of planetary gears inside the planetary control gear set 21 are fastened through the connecting column and is controlled to rotate clockwise on the top of the reaction tank body 1, and the sub-stirring rod 22 is synchronously driven to rotate in the reaction tank body 1 to promote the reaction rate, and the ion control on the surface of the sub-stirring rod 22 is The regulator controls the reaction rate inside the reaction tank body 1 in real time with the cooperation of the detector 24. At the same time, under the action of the control and adjustment motor 17, according to the feedback signal detected by the detector 24, the gear drive group 25 is driven to rotate and adjust, thereby driving the bottom shaft rail 19 to rotate in contact with the bottom inner wall surface of the reaction tank body 1, and the side adjustment reaction rod 20 rotates synchronously, and the overall reaction catalytic rate is adjusted in real time through the ph controller installed on the surface of the rod body. When the side adjustment reaction rod 20 rotates, the waterproof electric telescopic rod 26 rotates synchronously, and synchronously detects the feedback data in real time inside the detector 24 Under the action, when it is detected that the overall internal catalytic rate is affected by the environmental variables, the waterproof electric telescopic rod 26 is controlled and adjusted to extend according to the size of the temperature environmental variables generated. For example, when the temperature environmental variables are small, a waterproof electric telescopic rod 26 is extended to make the temperature-controlled heating conductive block 27 contact the graphene conductive layer 28, and utilize the contact reaction with the graphene conductive layer 28 to increase the overall reaction environment temperature. Synchronously, under the rotation adjustment of the above-mentioned sub-stirring rod 22 and the side adjustment reaction rod 20, the temperature of the internal reactants can be effectively and evenly heated to avoid the temperature variables affecting the overall reaction rate. With the cooperation of the liquid outlet control valve end 15, it is convenient for the sampling tube 11 to sample and extract the liquid sample discharged by the liquid outlet control valve end 15 according to the demand, and to perform multiple sampling controls in different time periods, so as to effectively adjust the overall catalytic reaction rate in real time, and avoid the overall reaction rate being affected by the environmental variables of temperature or pH, that is, under the cooperation of the feedback circuit frame 7, it is convenient to extract the discharge test sample extracted from the sampling tube 11 in equal amounts and according to the preset time under the cooperation of the micro pump 8, and detect the extracted sample liquid under the action of the activity sensor 9, Afterwards, the feedback circuit frame 7 is used to feed back to the brushless motor 180 for adjustment and control. When the brushless motor 180 receives the control signal, it is started, and then the ratchet wheel 182 is driven to rotate with the cooperation of the directional speed regulator 181. However, the rotation drive at this time is premised on the motion controller 1897 receiving the driving signal required for the brushless motor 180 to rotate, so that the electric control push rod 1898 extends forward, so that the first cobalt magnet 1899 and the second cobalt magnet are magnetically connected, so that under the driving force of the electric control push rod 1898, the force point contact rod 1896 is forced to rotate, and the rotation is carried out. In one step, the stressed rotating gear clamp rod 184 drives the cone claw 183 to rotate outside the directional connecting shaft pin 189, that is, the cone claw 183 and the ratchet wheel 182 are separated, so that the ratchet wheel 182 is restricted from falling off, and then the fuse contact spring 186 contacts the surface of the stressed rotating gear clamp rod 184, so that the force condition signal of the stressed rotating gear clamp rod 184 is transmitted to the motion controller 1897, and then the ratchet wheel 182 drives the directional rotating disk 187 to rotate, so that when the internal substrate conversion rate of the biological enzyme catalytic reaction is affected, an electrical signal is sent to the contact telescopic contact rod 1802, so that the contact telescopic contact rod 1802 is 02 Under the steering drive of the directional turntable 187, it performs circumferential adjustment operation, and according to the feedback signal, it extends downward to facilitate the bottom of the contact telescopic feeler rod 1802 and the internal contact sliding of the contact chute 1894. After sliding a circle, the bottom of the contact telescopic feeler rod 1802 contacts the contact spring 1895, and the conductive initial signal is transmitted to the pressurized dosing end 1801 by the contact, so that one group of the pressurized dosing end 1801 controlled by the contact spring 1895 performs auxiliary optimization enzyme dosing operation, and when the contact telescopic feeler rod 1802 forms the first circle and contacts the contact spring 1895, , the contact telescopic feeler rod 1802 returns to its original position, and the subsequent second, third and fourth contact control operations are performed according to the feedback substrate conversion rate, which effectively increases the substrate concentration and facilitates the improvement of the substrate conversion rate. The increased substrate concentration is appropriately balanced and controlled according to the overall bio-enzyme catalytic reaction rate to avoid the inhibition of the overall catalytic reaction due to excessive substrate concentration. The overall device effectively adjusts the catalytic reaction rate of the bio-enzyme under the overall temperature, pH, ions, and substrate conversion rate to achieve catalytic balance, improve the overall catalytic accuracy, and reduce the influence of residual impurities in the reaction on the overall bio-enzyme catalysis.

尽管参照前述实施例对本发明进行了详细的说明,对于本领域的技术人员来说,其依然可以对前述各实施例所记载的技术方案进行修改,或者对其中部分技术特征进行等同替换,凡在本发明的精神和原则之内,所作的任何修改、等同替换、改进等,均应包含在本发明的保护范围之内。Although the present invention has been described in detail with reference to the aforementioned embodiments, it is still possible for those skilled in the art to modify the technical solutions described in the aforementioned embodiments, or to make equivalent substitutions for some of the technical features therein. Any modifications, equivalent substitutions, improvements, etc. made within the spirit and principles of the present invention should be included in the protection scope of the present invention.

Claims (10)

1.一种生物酶催化化学反应罐装置,其特征在于:包括反应罐体(1),所述反应罐体(1)的侧端顶部连通有优化酶输送通道(4),所述优化酶输送通道(4)的内部安装设置定量平衡组件(18),所述优化酶输送通道(4)的顶部侧端连通有投加口(5);1. A bio-enzyme catalytic chemical reaction tank device, characterized in that it comprises a reaction tank body (1), the top of the side end of the reaction tank body (1) is connected to an optimized enzyme delivery channel (4), a quantitative balance component (18) is installed inside the optimized enzyme delivery channel (4), and the top side end of the optimized enzyme delivery channel (4) is connected to a dosing port (5); 所述定量平衡组件(18)包括驱动无刷电机(180),所述驱动无刷电机(180)的底部安装设置定向转速调节器(181),所述定向转速调节器(181)的底部轴心端安装设置棘爪轮(182),所述棘爪轮(182)的底部轴心端安装设置定向转盘(187),所述棘爪轮(182)的侧角边卡合连接有锥爪(183),所述锥爪(183)的侧端一体成型有受力转齿卡杆(184),所述受力转齿卡杆(184)的侧端表面贯穿设置中心轴柱(185),所述定向转盘(187)的表面上安装设置导信接触簧片(186),所述受力转齿卡杆(184)的侧端接触连接有接触杆(188),所述接触杆(188)的侧端通过连接杆柱安装设置定向连接轴销(189),所述接触杆(188)的侧端紧固连接有受力点触杆(1896),所述受力点触杆(1896)的侧壁表面安装设置第一钴磁石(1899),所述定向连接轴销(189)的底部安装设置连接架构(1890),所述连接架构(1890)的侧端架设安装优化酶箱(1891),所述优化酶箱(1891)的侧壁表面紧固连接有运动控制器(1897),所述运动控制器(1897)的侧端安装设置电动控制推杆(1898),所述电动控制推杆(1898)的顶部安装设置第二钴磁石,所述第一钴磁石(1899)和第二钴磁石磁性连接,所述定向转盘(187)的轴心端底部连接设置有轴向转柱,所述轴向转柱的底部周侧安装设置进料盘(1893),所述进料盘(1893)的侧端连通有柔性伸缩轴向管(1892),所述柔性伸缩轴向管(1892)的侧端和优化酶箱(1891)的表面连通。The quantitative balancing component (18) comprises a brushless driving motor (180), a directional speed regulator (181) is mounted on the bottom of the brushless driving motor (180), a ratchet wheel (182) is mounted on the bottom axial end of the directional speed regulator (181), a directional rotating disk (187) is mounted on the bottom axial end of the ratchet wheel (182), a cone claw (183) is snap-connected to the side corner edge of the ratchet wheel (182), and the side end of the cone claw (183) is integrally formed with a A force-bearing rotating gear clamp rod (184), a central shaft column (185) is provided through the side end surface of the force-bearing rotating gear clamp rod (184), a guide contact spring (186) is installed on the surface of the directional rotating disk (187), the side end of the force-bearing rotating gear clamp rod (184) is in contact with a contact rod (188), a directional connecting shaft pin (189) is installed on the side end of the contact rod (188) through a connecting rod column, and the side end of the contact rod (188) is fastened and connected to a force-bearing point contact rod (189). 6), a first cobalt magnet (1899) is installed on the side wall surface of the force-bearing point contact rod (1896), a connecting frame (1890) is installed on the bottom of the directional connecting shaft pin (189), an optimized enzyme box (1891) is installed on the side end of the connecting frame (1890), a motion controller (1897) is fastened to the side wall surface of the optimized enzyme box (1891), an electric control push rod (1898) is installed on the side end of the motion controller (1897), and the A second cobalt magnet is installed on the top of the electric control push rod (1898), the first cobalt magnet (1899) and the second cobalt magnet are magnetically connected, an axial rotating column is connected to the bottom of the axial end of the directional turntable (187), a feed disc (1893) is installed on the bottom circumference of the axial rotating column, the side end of the feed disc (1893) is connected to a flexible telescopic axial tube (1892), and the side end of the flexible telescopic axial tube (1892) is connected to the surface of the optimized enzyme box (1891). 2.根据权利要求1所述的生物酶催化化学反应罐装置,其特征在于:所述进料盘(1893)的顶壁周侧表面开设有接触滑槽(1894),所述进料盘(1893)的表面上等距安装设置四组受压投加端(1801),四组所述受压投加端(1801)的边侧连接设置接触簧片(1895),所述接触簧片(1895)在接触滑槽(1894)的内部贴合安装,所述定向转盘(187)的底部边侧紧固连接有接触伸缩触杆(1802),所述接触伸缩触杆(1802)呈线性在接触滑槽(1894)的顶部安装设置。2. The bio-enzyme catalytic chemical reaction tank device according to claim 1 is characterized in that: a contact chute (1894) is provided on the peripheral surface of the top wall of the feed disc (1893), four groups of pressurized feeding ends (1801) are equidistantly installed on the surface of the feed disc (1893), and contact springs (1895) are connected to the sides of the four groups of pressurized feeding ends (1801), and the contact springs (1895) are fitted inside the contact chute (1894), and a contact telescopic contact rod (1802) is fastened to the bottom side of the directional turntable (187), and the contact telescopic contact rod (1802) is linearly installed on the top of the contact chute (1894). 3.根据权利要求1所述的生物酶催化化学反应罐装置,其特征在于:所述优化酶输送通道(4)的侧壁表面安装设置微处理控制器(6),所述优化酶输送通道(4)的顶部安装设置反馈线路架(7),所述反馈线路架(7)的侧端连接有微型泵(8),所述微型泵(8)的底侧端安装设置活性传感器(9),所述微型泵(8)的底部连通有采样管(11)。3. The bio-enzyme catalytic chemical reaction tank device according to claim 1 is characterized in that: a microprocessor controller (6) is installed on the side wall surface of the optimized enzyme delivery channel (4), a feedback circuit frame (7) is installed on the top of the optimized enzyme delivery channel (4), a micro pump (8) is connected to the side end of the feedback circuit frame (7), an activity sensor (9) is installed on the bottom side end of the micro pump (8), and a sampling tube (11) is connected to the bottom of the micro pump (8). 4.根据权利要求1所述的生物酶催化化学反应罐装置,其特征在于:所述反应罐体(1)的另一侧端连通有进料控制阀端(10),所述反应罐体(1)的底端表面上连通有出液控制阀端(15),所述出液控制阀端(15)的侧端和采样管(11)的底端连通,所述反应罐体(1)的底部另一侧表面连通有废液处理阀端(12),所述反应罐体(1)的顶部另一侧表面上分别对称连通有第一液体控制阀端(13)和第二液体控制阀端。4. The bio-enzyme catalytic chemical reaction tank device according to claim 1 is characterized in that: the other side end of the reaction tank body (1) is connected to a feed control valve end (10), the bottom surface of the reaction tank body (1) is connected to a liquid outlet control valve end (15), the side end of the liquid outlet control valve end (15) is connected to the bottom end of a sampling tube (11), the other side surface of the bottom of the reaction tank body (1) is connected to a waste liquid treatment valve end (12), and the other side surface of the top of the reaction tank body (1) is symmetrically connected to a first liquid control valve end (13) and a second liquid control valve end. 5.根据权利要求1所述的生物酶催化化学反应罐装置,其特征在于:所述反应罐体(1)的顶部安装设置行星控制齿轮组(21),所述行星控制齿轮组(21)的轴心端顶部连接设置控制电机(16),所述行星控制齿轮组(21)的内部三组行星齿轮轴心端通过连接柱紧固连接有上位转盘,所述上位转盘的顶部安装设置防护盖板(14)。5. The bio-enzyme catalytic chemical reaction tank device according to claim 1 is characterized in that: a planetary control gear set (21) is installed on the top of the reaction tank body (1), and a control motor (16) is connected to the top of the axial end of the planetary control gear set (21), and the axial ends of the three sets of planetary gears inside the planetary control gear set (21) are fastened to an upper turntable through connecting columns, and a protective cover plate (14) is installed on the top of the upper turntable. 6.根据权利要求5所述的生物酶催化化学反应罐装置,其特征在于:所述上位转盘的周侧转动连接有轨道,所述轨道安装设置在反应罐体(1)的顶部,所述防护盖板(14)在反应罐体(1)的顶部进行盖合安装,所述上位转盘的底部轴心端连接设置中心柱体(23),所述上位转盘的底部周侧连接设置分搅杆(22),所述中心柱体(23)的底部周测套设安装检测仪(24)。6. The bio-enzyme catalytic chemical reaction tank device according to claim 5 is characterized in that: the circumferential side of the upper turntable is rotatably connected to a track, the track is installed on the top of the reaction tank body (1), the protective cover plate (14) is installed on the top of the reaction tank body (1), the bottom axial end of the upper turntable is connected to a central column (23), the bottom circumferential side of the upper turntable is connected to a stirring rod (22), and the bottom circumferential sleeve of the central column (23) is equipped with a detector (24). 7.根据权利要求1所述的生物酶催化化学反应罐装置,其特征在于:所述反应罐体(1)的底部安装设置齿轮驱动组(25),所述齿轮驱动组(25)的一侧齿轮轴心端安装设置控制调节电机(17),所述齿轮驱动组(25)的另一侧齿轮顶部轴心端连接安装底轴轨(19)。7. The bio-enzyme catalytic chemical reaction tank device according to claim 1 is characterized in that: a gear drive group (25) is installed at the bottom of the reaction tank body (1), a control and adjustment motor (17) is installed at the shaft center end of the gear on one side of the gear drive group (25), and a bottom shaft rail (19) is connected to the top shaft center end of the gear on the other side of the gear drive group (25). 8.根据权利要求7所述的生物酶催化化学反应罐装置,其特征在于:所述底轴轨(19)安装设置在反应罐体(1)的内部底端,所述底轴轨(19)的顶部转动连接有边侧调节反应杆(20)。8. The bio-enzyme catalytic chemical reaction tank device according to claim 7 is characterized in that: the bottom shaft rail (19) is installed at the bottom end of the interior of the reaction tank body (1), and the top of the bottom shaft rail (19) is rotatably connected to a side adjustment reaction rod (20). 9.根据权利要求8所述的生物酶催化化学反应罐装置,其特征在于:所述反应罐体(1)的外部周测套设有保温防护壳(3),所述保温防护壳(3)的内壁表面设置石墨烯导性层(28),所述边侧调节反应杆(20)的外壁表面安装设置防水电动伸缩杆(26)。9. The bio-enzyme catalytic chemical reaction tank device according to claim 8 is characterized in that: the outer peripheral casing of the reaction tank body (1) is provided with a heat-insulating protective shell (3), the inner wall surface of the heat-insulating protective shell (3) is provided with a graphene conductive layer (28), and the outer wall surface of the side adjustment reaction rod (20) is installed with a waterproof electric telescopic rod (26). 10.根据权利要求9所述的生物酶催化化学反应罐装置,其特征在于:所述防水电动伸缩杆(26)的侧端连接设置温控发热导电块(27),所述温控发热导电块(27)和石墨烯导性层(28)接触设置,所述反应罐体(1)的底部周侧套设安装支撑腿架(2)。10. The bio-enzyme catalytic chemical reaction tank device according to claim 9 is characterized in that: a temperature-controlled heating conductive block (27) is connected to the side end of the waterproof electric telescopic rod (26), the temperature-controlled heating conductive block (27) is in contact with the graphene conductive layer (28), and a support leg frame (2) is sleeved and installed on the bottom circumference of the reaction tank body (1).
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