CN117224412B - Oil-controlling and anti-dandruff composition and application thereof - Google Patents
Oil-controlling and anti-dandruff composition and application thereof Download PDFInfo
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Abstract
The invention relates to the technical field of cosmetics, in particular to an oil-control and anti-dandruff composition and application thereof. The oil-control anti-dandruff composition comprises zinc salicylate, azelaic acid, avenanthramide, hexamidine bis (isethionate) salt and phenylpropanol. The zinc salicylate, azelaic acid and avenanthramide are compounded to have synergistic effect on controlling oil and removing dandruff, and then compounded with hexamidine di (hydroxyethyl sulfonic acid) salt and phenylpropanol can obviously improve the antibacterial effect, meanwhile, PEG-7 coco glyceride, raffinose and agarose are added as skin conditioning agents to moisten scalp and maintain scalp health.
Description
Technical Field
The invention relates to the technical field of cosmetics, in particular to an oil-control and anti-dandruff composition and application thereof.
Background
At present, more and more people have dandruff trouble, and the people account for about 50% of the total population of the general adults. Several key contributors to dandruff include fungal colonization, sebaceous gland activity, individual sensitivity, and the like. Most of the current commercial anti-dandruff products have single solution scheme, and active ingredients are difficult to leave on the hair roots and have limited anti-dandruff effect.
Disclosure of Invention
The invention aims to overcome the defects of the prior art and provide an oil-control anti-dandruff composition and application thereof. The invention combines zinc salicylate, azelaic acid and avenanthramide powder, has synergistic effect, has the functions of balancing grease secretion and controlling dandruff while maintaining scalp health, and is used for preparing hair products.
In order to achieve the above purpose, the technical scheme adopted by the invention is as follows:
In a first aspect, the present invention provides an oil control anti-dandruff composition comprising the components zinc salicylate, azelaic acid, avenanthramides, hexamidine bis (isethionate) salt and phenylpropanols.
The balance of the scalp's grease is also a guarantee of scalp health, and is susceptible to dandruff either too dry or too greasy. According to the invention, zinc salicylate, azelaic acid and avenanthramide are compounded, salicylic acid can be separated under an acidic condition to have a cutin stripping effect, zinc ions have an anti-inflammatory effect, inflammatory reaction of scalp can be reduced, dandruff generation is reduced, zinc ions can balance the PH value of scalp, excessive oil secretion of scalp is reduced, scalp is kept moist and is not excessively dry, azelaic acid regulates oil secretion of scalp, thereby controlling dandruff generation, avenanthramide helps to relieve itching in the process of removing dandruff, has the effects of relieving telangiectasis and itching caused by inflammation, and the like, and increases scalp comfort level. The experiment of the invention shows that the shampoo added with the oil-control anti-dandruff composition can improve balance grease secretion, and can control dandruff generation while maintaining scalp health. Scalp health is related to the fixation of malassezia on the scalp in addition to the balance of scalp grease. The colonization and proliferation of microorganisms such as malassezia can increase the accumulation of lipid in horny layer, destroy the lipid tissue structure among superficial cells, and cause scalp barrier damage, and cause itching and scalp inflammation. The oil-control anti-dandruff composition provided by the invention has remarkable inhibition effect on candida albicans, aspergillus niger strains and malassezia furfur by adding hexamidine di (isethionate) and phenylpropanol. The hexamidine di (isethionate) (PF-95) is a water-soluble cationic substance with broad-spectrum anti-killing of various gram positive bacteria, gram negative bacteria, various mold and yeast, has good anti-killing effect on various microorganisms, particularly on pityrosporum furfur causing scalp lesions and dandruff, can inhibit growth of microorganisms causing dandruff such as malassezia, and PF-95 can be adsorbed on hair and scalp at the same time, so that the antibacterial effect is more durable, the phenylpropanol has the antibacterial effect, and the hexamidine di (isethionate) and the phenylpropanol are matched to synergistically increase in the antibacterial effect.
Preferably, the oil-control anti-dandruff composition comprises, by weight, 1-10% of zinc salicylate, 5-20% of azelaic acid, 3-10% of avenanthramide, 0.2-4% of hexamidine bis (isethionate) and 5-30% of phenylpropanol.
The components are within the scope of the invention, and the scalp grease content of the subject is reduced after the use, so that the dandruff condition is greatly improved. The MIC of the hexamidine di (isethionate) salt and the phenylpropanol for inhibiting malassezia by compounding is very low, and the malassezia is obviously reduced after the shampoo added with the oil control and anti-dandruff composition is used for 28 days, so that the shampoo has a strong antibacterial effect. Malassezia is a key bacterium causing abnormal growth of dandruff, and can well inhibit the growth of the malassezia within the scope of the invention, thereby reducing the generation of the dandruff.
Preferably, the oil-control anti-dandruff composition comprises, by weight, 5-10% of zinc salicylate, 5-15% of azelaic acid, 5-10% of avenanthramide, 2-4% of hexamidine bis (isethionate) and 5-20% of phenylpropanol.
Preferably, the oil-control anti-dandruff composition further comprises a skin conditioner, wherein the skin conditioner comprises at least three of PEG-7 cocoyl glyceride, sodium gluconate, raffinose and agarose.
After PEG-7 cocoyl glyceride, sodium gluconate, raffinose and agarose are added into the oil-control and anti-dandruff composition, the moisture content of scalp cuticle can be improved, and the oil-control and anti-dandruff composition has a remarkable improvement effect on moisturizing scalp. PEG-7 cocoyl glyceride can supplement lipid lost by hair after washing, has a conditioning effect, sodium gluconate can further amplify the original surface active micelle, reduce the number of penetrating into a stratum corneum and reduce degreasing, raffinose is used as a humectant, a skin conditioner and a softener, and agarose has good moisturizing and softening effects, can increase the texture and thickness of a product, and can enable skin to feel moist and comfortable.
Preferably, in the oil-control anti-dandruff composition, the skin conditioning agent comprises PEG-7 cocoyl glyceride, sodium gluconate, raffinose and agarose, wherein the weight ratio of the PEG-7 cocoyl glyceride to the sodium gluconate to the raffinose to the agarose is PEG-7 cocoyl glyceride to sodium gluconate to raffinose to agarose= (1-10) to (10-30) to (5-35) to (2-20).
Preferably, in the oil-control anti-dandruff composition, the weight ratio of the PEG-7 cocoglyceride, the sodium gluconate, the raffinose and the agarose is PEG-7 cocoglyceride, sodium gluconate, raffinose and agarose= (1-5), 18-30, 15-20 and 10-20.
More preferably, the oil-control anti-dandruff composition comprises the following components, by weight, 5% of zinc salicylate, 15% of azelaic acid, 5% of avenanthramide, 2% of hexamidine di (isethionic acid), 20% of phenylpropanol, 5% of PEG-7 cocoyl glyceride, 18% of sodium gluconate, 20% of raffinose and 10% of agarose.
Under the specific weight percentage, the prepared oil-control anti-dandruff composition has strong antibacterial capacity on candida albicans, aspergillus niger and malassezia furfur, wherein the minimum antibacterial concentration of the oil-control anti-dandruff composition on malassezia furfur reaches 0.0002wt%, and the water content of the horny layer, the scalp fat content, the malassezia furfur number and the condition of dandruff at the top of the head are greatly improved by using the oil-control anti-dandruff composition prepared by the specific weight percentage, and the oil-control anti-dandruff composition has remarkable improvement on the aspects of oil control, anti-dandruff, antibacterial and the like, and can comprehensively solve the scalp problem.
The preparation method of the oil-control anti-dandruff composition comprises the step of uniformly mixing the components in percentage by weight to obtain the oil-control anti-dandruff composition.
In a second aspect, the present invention provides the use of the above oil control anti-dandruff composition in hair products.
In a third aspect, the present invention provides a hair product comprising the oil control anti-dandruff composition described above.
Preferably, in the hair product, the oil control and anti-dandruff composition accounts for 0.2-2% of the weight of the hair product.
More preferably, the oil control and anti-dandruff composition comprises 0.8% by mass of the hair product.
Preferably, the hair product further comprises a cosmetically acceptable adjuvant.
The invention has the advantages that:
The zinc salicylate, azelaic acid and oat alkaloid powder have synergistic effect on controlling oil and removing dandruff, and the synergistic effect of the compounded hexamidine di (hydroxyethyl sulfonate) and phenylpropanol can be obviously improved, and the bactericidal agent with different mechanisms has synergistic effect, unlike the products such as ZPT, selenium disulfide and the like, dry itching is easy to cause, and the oil is moderately controlled. Meanwhile, the PEG-7 cocoyl glyceride, raffinose and agarose are added as skin conditioning agents, so that scalp can be moistened, scalp health is maintained, and the oil-control and dandruff-removing composition prepared by the invention can simultaneously control dandruff production from multiple angles, has obvious dandruff-removing effect, comprehensively solves the scalp problem, and can be used for preparing hair products.
Detailed Description
For a better description of the objects, technical solutions and advantages of the present invention, the present invention will be further described with reference to the following specific examples.
Example 1:
An embodiment of the oil control and anti-dandruff composition comprises the following components in percentage by weight: 5% of zinc salicylate, 15% of azelaic acid, 5% of avenanthramide, 2% of hexamidine bis (hydroxyethyl sulfonic acid), 20% of phenylpropanol, 5% of PEG-7 coco glyceride, 18% of sodium gluconate, 20% of raffinose and 10% of agarose.
Example 2:
An embodiment of the oil control and anti-dandruff composition comprises the following components in percentage by weight: 1% of zinc salicylate, 20% of azelaic acid, 3% of avenanthramide, 0.2% of hexamidine bis (hydroxyethyl sulfonic acid), 30% of phenylpropanol, 10% of PEG-7 coco glyceride, 10% of sodium gluconate, 15% of raffinose and 10.8% of agarose.
Example 3:
An embodiment of the oil control and anti-dandruff composition comprises the following components in percentage by weight: 10% of zinc salicylate, 5% of azelaic acid, 10% of avenanthramide, 4% of hexamidine bis (hydroxyethyl sulfonic acid), 5% of phenylpropanol, 1% of PEG-7 coco glyceride, 30% of sodium gluconate, 15% of raffinose and 20% of agarose.
Example 4:
An embodiment of the oil control and anti-dandruff composition comprises the following components in percentage by weight: 5% of zinc salicylate, 15% of azelaic acid, 5% of avenanthramide, 2% of hexamidine bis (hydroxyethyl sulfonic acid), 25% of phenylpropanol, 5% of PEG-7 coco glyceride, 18% of sodium gluconate, 5% of raffinose and 20% of agarose.
Example 5:
An embodiment of the oil control and anti-dandruff composition comprises the following components, by weight, 5% of zinc salicylate, 15% of azelaic acid, 5% of avenanthramide, 2% of hexamidine di (isethionic acid) salt, 13% of phenylpropanol, 5% of PEG-7 cocoyl glyceride, 18% of sodium gluconate, 35% of raffinose and 2% of agarose.
Example 6:
An embodiment of the oil control and anti-dandruff composition comprises the following components, by weight, 5% of zinc salicylate, 15% of azelaic acid, 5% of avenanthramide, 2% of hexamidine di (isethionic acid) salt, 20% of phenylpropanol, 18% of sodium gluconate, 20% of raffinose, 10% of agarose and the balance of water to 100%.
Example 7:
An embodiment of the oil control and anti-dandruff composition comprises the following components, by weight, 5% of zinc salicylate, 15% of azelaic acid, 5% of avenanthramide, 2% of hexamidine di (isethionic acid) salt, 20% of phenylpropanol, 5% of PEG-7 cocoyl glyceride, 20% of raffinose, 10% of agarose and the balance of water to 100%.
Example 8:
An embodiment of the oil control and anti-dandruff composition comprises the following components, by weight, 5% of zinc salicylate, 15% of azelaic acid, 5% of avenanthramide, 2% of hexamidine di (isethionic acid) salt, 20% of phenylpropanol, 5% of PEG-7 coco glyceride, 18% of sodium gluconate, 20% of agarose and the balance of water to 100%.
Example 9:
An embodiment of the oil control and anti-dandruff composition comprises the following components, by weight, 5% of zinc salicylate, 15% of azelaic acid, 5% of avenanthramide, 2% of hexamidine di (isethionic acid) salt, 20% of phenylpropanol, 5% of PEG-7 cocoyl glyceride, 18% of sodium gluconate, 20% of raffinose and the balance of water to 100%.
Comparative example 1:
A comparative example of the oil control and anti-dandruff composition comprises the following components, by weight, 15% of azelaic acid, 5% of avenanthramide, 2% of hexamidine di (isethionic acid) salt, 20% of phenylpropanol, 5% of PEG-7 cocoyl glyceride, 18% of sodium gluconate, 20% of raffinose, 10% of agarose and the balance of water to 100%.
Comparative example 2:
a comparative example of the oil-control and anti-dandruff composition comprises, by weight, 5% of zinc salicylate, 5% of avenanthramide, 2% of hexamidine di (isethionic acid) salt, 20% of phenylpropanol, 5% of PEG-7 cocoyl glyceride, 18% of sodium gluconate, 20% of raffinose, 10% of agarose and water to 100%.
Comparative example 3:
A comparative example of the oil-control and anti-dandruff composition comprises, by weight, 5% of zinc salicylate, 15% of azelaic acid, 2% of hexamidine bis (isethionic acid) salt, 20% of phenylpropanol, 5% of PEG-7 cocoyl glyceride, 18% of sodium gluconate, 20% of raffinose, 10% of agarose and water to 100%.
Comparative example 4:
A comparative example of the oil-control and anti-dandruff composition comprises the following components in percentage by weight, 5% of zinc salicylate, 15% of azelaic acid, 5% of avenanthramide, 20% of phenylpropanol, 5% of PEG-7 cocoyl glyceride, 18% of sodium gluconate, 20% of raffinose, 10% of agarose and the balance of water to 100%.
Comparative example 5:
A comparative example of the oil-control and anti-dandruff composition comprises, by weight, 5% of zinc salicylate, 15% of azelaic acid, 5% of avenanthramide, 2% of hexamidine di (isethionic acid) salt, 5% of PEG-7 coco glyceride, 18% of sodium gluconate, 20% of raffinose, 10% of agarose and water to 100%.
Comparative example 6:
A comparative example of the oil-control and anti-dandruff composition comprises the following components, by weight, 5% of zinc salicylate, 15% of azelaic acid, 5% of avenanthramide, 5% of PEG-7 cocoyl glyceride, 18% of sodium gluconate, 20% of raffinose, 10% of agarose and water which are added to 100%.
Comparative example 7:
A comparative example of the oil-control and anti-dandruff composition comprises, by weight, 14% of zinc salicylate, 25% of azelaic acid, 1% of avenanthramide, 0.1% of hexamidine di (isethionic acid) salt, 10% of phenylpropanol, 5% of PEG-7 coco glyceride, 22.9% of sodium gluconate, 3% of raffinose and 25% of agarose. Application example 1:
The invention relates to an application example of an oil-control anti-dandruff composition, in particular to shampoo, which comprises the oil-control anti-dandruff composition.
The weight percentage of the oil control and anti-dandruff composition in the shampoo is 0.8 percent.
Application example 2:
The invention relates to an application example of an oil-control anti-dandruff composition, in particular to shampoo, which comprises the oil-control anti-dandruff composition.
The weight percentage of the oil control and anti-dandruff composition in the shampoo is 0.2 percent.
Application example 3:
The invention relates to an application example of an oil-control anti-dandruff composition, in particular to shampoo, which comprises the oil-control anti-dandruff composition.
The weight percentage of the oil control and anti-dandruff composition in the shampoo is 2%.
Test results
1. Minimum Inhibitory Concentration (MIC) determination-agar dilution method
The minimum inhibitory concentration (minimum inhibitory concentration, MIC) is the minimum drug concentration which can inhibit the obvious increase of a certain microorganism when incubated under a specific environment, namely the minimum inhibitory concentration, and is used for quantitatively measuring the in-vitro antibacterial activity.
Preparing fungus bacterial liquid, inoculating the strain onto a slant of a culture medium before the experiment, washing the cultured active strain into a sterilizing conical flask with sterilized normal saline, shaking the sterilized conical flask fully and uniformly, sucking the bacterial liquid from the conical flask by a pipetting gun, sequentially diluting the bacterial liquid by 10 times, counting the total number of fungi in 5 medium grids by using a blood cell counting plate for each dilution, wherein the fungus suspension in the range is 1 multiplied by 10 7 cfu/mL needed by people.
The MIC is tested by adopting an agar dilution method, and the method comprises the steps of adding 2.5mL of bacteriostatic composition with different concentrations into 50 ℃ C17.5mL of agar culture medium, uniformly mixing, solidifying, dividing the culture medium into 2 areas, dripping one fungus into each area, dripping each fungus into different positions of the corresponding area for 5 times, dripping 1 mu L of fungus solution each time, and culturing for 48 hours at 28 ℃. The antibacterial capacity is mainly achieved by detecting the minimum antibacterial concentration of antibacterial drugs on candida albicans, aspergillus niger strains and malassezia furfur. The minimum concentration of sterile growth, the MIC of the antimicrobial agent tested, results are shown in table 1.
TABLE 1
It can be seen that the oil control and anti-dandruff compositions of examples 1-5, which are included in the present invention, provide significant inhibition of fungal growth, wherein malassezia is a critical bacterium responsible for abnormal growth of dandruff, thereby greatly reducing dandruff formation.
Comparative example 6 is inferior to example 1 in bacteriostasis due to the absence of hexamidine bis (isethionate) and phenylpropanol.
Compared with comparative examples 4 and 5, the minimum inhibitory concentration of the example 1 on candida albicans, aspergillus niger strains and malassezia furfur is obviously reduced, the malassezia furfur inhibition only needs 0.0002wt%, and the minimum inhibitory concentration of the comparative examples 4 and 5 on malassezia furfur is 0.015-0.04 wt%, which indicates that the compound antibacterial effect of hexamidine bis (hydroxyethyl sulfonic acid) salt and phenylpropanol is better.
2. Evaluation of anti-dandruff oil control
Study screening 31 subjects meeting the test conditions an open double blind self-control study was used to replace the original shampoo of the subjects, and shampoo containing 0.8% of the oil control anti-dandruff composition of the invention (i.e. application example 1) was used periodically to clean hair for 28 days according to personal shampoo habits. The shampoo formulations are shown in table 2.
TABLE 2
And heating, dissolving and cooling the mixture A to 40 ℃, uniformly mixing the mixture B at normal temperature, adding the mixture A, and then adding the mixture C to obtain the shampoo. Before and after using T0d (Test 0day, T0D) and T28d (Test 28day, T28D), measuring the moisture content of the stratum corneum at the top of the head and the data of the scalp grease content by using Moisture Meter SC, sebumScale and other instruments, calculating the average value, collecting a scalp malassezia sample by using a detection card, and calculating the average value by dyeing and counting the number of malassezia.
Dandruff evaluation the dandruff evaluation was adjusted according to the "ASFS score" (ADHERENT SCALP FLAKING score, adhesive scalp scale score) for clinical evaluation. The number of invisible desquamation is 0, the number of even small desquamation of hairy roots is 1, the number of visible small desquamation of hairy roots is 2, the number of small large desquamation or large small desquamation is 3, and the number of large desquamation is 4. And evaluating the oil control and anti-dandruff effects of the shampoo by analyzing the correlation of the indexes. The results are shown in Table 3.
TABLE 3 Table 3
From the evaluation results of the anti-dandruff oil control, it is understood that the anti-dandruff compositions of examples 1 to 5 have reduced scalp fat content and malassezia number after 28 days of use of the shampoo containing the anti-dandruff composition of the invention, the anti-dandruff score is greatly improved, and that comparative examples 1 to 5 lacking any one of zinc salicylate, azelaic acid, avenanthramide, hexamidine bis (hydroxyethylsulfonate) salt, and phenylpropanol have no effect in all aspects as the invention.
Comparative example 7 and examples 1-5 show that the weight percent of the components is outside the scope of the present invention and the oil control and anti-dandruff effects are inferior to the present invention.
Comparative example 6 is inferior to example 1 in bacteriostasis due to the absence of hexamidine bis (isethionate) and phenylpropanol.
Compared with the embodiment 1, the reduction amount of the malassezia is obviously lower than that of the embodiment 1, which shows that the lack of any one of hexamidine di (hydroxyethyl sulfonate) and phenylpropanol can affect the antibacterial effect and the oil control and anti-dandruff effect, and the compound antibacterial effect of the hexamidine di (hydroxyethyl sulfonate) and the phenylpropanol is better, so that the synergistic effect is achieved.
The shampoo has effects of moisturizing scalp and regulating moisture content of scalp horny layer. In addition, the balance of the oil and fat of the scalp is also a guarantee of scalp health, and the scalp is easy to cause dandruff whether the scalp is too dry or too greasy. With proper scalp moisture content, the degree of dandruff production depends on the degree of oil secretion of the scalp. The experiment shows that the shampoo with the oil control and anti-dandruff composition can improve the moisture content of scalp cuticle, balance the secretion of grease and control the generation of dandruff while maintaining the health of scalp.
Scalp health is related to the colonization of the scalp with malassezia, in addition to the balance of scalp moisture and scalp grease. The colonization and proliferation of microorganisms such as malassezia can increase the accumulation of lipid in horny layer, destroy the lipid tissue structure among superficial cells, and cause scalp barrier damage, and cause itching and scalp inflammation. The oil-control anti-dandruff composition provided by the invention has very low MIC for inhibiting malassezia, and malassezia is obviously reduced after the shampoo added with the oil-control anti-dandruff composition is used for 28 days, so that the oil-control anti-dandruff composition provided by the invention has a strong antibacterial effect and can also have the effects of relieving telangiectasis, pruritus and the like caused by inflammation.
In conclusion, the oil-control anti-dandruff composition provided by the invention can simultaneously control the generation of dandruff from multiple angles, and has obvious anti-dandruff effect.
Finally, it should be noted that the above embodiments are only for illustrating the technical solution of the present invention and not for limiting the scope of the present invention, and although the present invention has been described in detail with reference to the preferred embodiments, it should be understood by those skilled in the art that the technical solution of the present invention may be modified or substituted equally without departing from the spirit and scope of the technical solution of the present invention.
Claims (9)
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| CN112754985A (en) * | 2021-01-04 | 2021-05-07 | 珠海伊斯佳科技股份有限公司 | Composition containing bacillus fermentation product and shampoo containing composition |
| CN116327669A (en) * | 2023-03-15 | 2023-06-27 | 广州天翼化妆品有限公司 | Acne-removing composition with skin barrier repairing function and preparation method thereof |
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| EP1923041A1 (en) * | 2006-10-20 | 2008-05-21 | Symrise GmbH & Co. KG | Use of C10-C14 alkane diols for the preparation of a composition for the prophylaxis and/or treatment of Malassezia-induced dandruff, and compositions comprising C10-C14 alkane diols |
| WO2019166089A1 (en) * | 2018-02-28 | 2019-09-06 | Symrise Ag | Dermatological product |
| CN116747159A (en) * | 2023-08-10 | 2023-09-15 | 羽楠(广州)化妆品有限公司 | A kind of plant oil control and anti-dandruff composition, skin care product and preparation method thereof |
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| CN116327669A (en) * | 2023-03-15 | 2023-06-27 | 广州天翼化妆品有限公司 | Acne-removing composition with skin barrier repairing function and preparation method thereof |
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