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CN114812196B - A method for drying packages using waste heat from smelting brown corundum - Google Patents

A method for drying packages using waste heat from smelting brown corundum Download PDF

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Publication number
CN114812196B
CN114812196B CN202210506475.2A CN202210506475A CN114812196B CN 114812196 B CN114812196 B CN 114812196B CN 202210506475 A CN202210506475 A CN 202210506475A CN 114812196 B CN114812196 B CN 114812196B
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Prior art keywords
electrode paste
silicon carbide
layer
material layer
bag
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CN114812196A (en
Inventor
赵魁胜
魏显平
刘兴民
刘敏
李彦涛
郭晓乐
任晓军
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Shanxi Luliangshan Mineral Products Co ltd
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Shanxi Luliangshan Mineral Products Co ltd
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    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F27FURNACES; KILNS; OVENS; RETORTS
    • F27DDETAILS OR ACCESSORIES OF FURNACES, KILNS, OVENS OR RETORTS, IN SO FAR AS THEY ARE OF KINDS OCCURRING IN MORE THAN ONE KIND OF FURNACE
    • F27D5/00Supports, screens or the like for the charge within the furnace
    • F27D5/0068Containers
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B35/00Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/66Monolithic refractories or refractory mortars, including those whether or not containing clay
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/70Aspects relating to sintered or melt-casted ceramic products
    • C04B2235/74Physical characteristics
    • C04B2235/77Density
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/70Aspects relating to sintered or melt-casted ceramic products
    • C04B2235/96Properties of ceramic products, e.g. mechanical properties such as strength, toughness, wear resistance

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  • Engineering & Computer Science (AREA)
  • Chemical & Material Sciences (AREA)
  • Ceramic Engineering (AREA)
  • Manufacturing & Machinery (AREA)
  • Materials Engineering (AREA)
  • Structural Engineering (AREA)
  • Organic Chemistry (AREA)
  • Mechanical Engineering (AREA)
  • General Engineering & Computer Science (AREA)
  • Ceramic Products (AREA)
  • Electrolytic Production Of Metals (AREA)

Abstract

The invention discloses a method for baking bags by utilizing waste heat of smelting brown fused alumina, which comprises the following steps: firstly, preparing electrode paste, preparing two manufactured bags and a bag body to be manufactured, preheating the bag body, pouring the electrode paste from an opening, and gradually filling and lining the electrode paste at the bottom of an inner cavity of the bag body; a knotting material layer is circularly built on the cavity wall of the inner cavity, and a silicon carbide brick layer is circularly built on the outer side of the knotting material layer by utilizing a plurality of silicon carbide bricks; the method comprises the steps of clamping a bag body between two bags filled with brown fused alumina, baking electrode paste slurry to form an electrode paste graphitization layer serving as a bag bottom of the bag body, forming a bag wall of the bag body by an inner knotting material layer and an outer silicon carbide brick layer, and finally cooling. The invention utilizes the waste heat of the upper and lower bags filled with brown fused alumina to bake and manufacture the bag body, fully utilizes energy and equipment conditions, and implements the green and environment-friendly production concept.

Description

Method for baking ladle by using waste heat of smelting brown corundum
Technical Field
The invention belongs to the technical field of brown fused alumina ladle receiving, and particularly relates to a method for drying a ladle by utilizing waste heat of smelting brown fused alumina.
Background
Brown fused block is crystallized by mixing three raw materials of high bauxite chamotte, carbon material and scrap iron, adding the raw materials into an electric arc furnace, and cooling after high-temperature melting and impurity reduction, and the smelting process is to reduce main impurities in bauxite by utilizing the basic principle that the affinity of aluminum to oxygen is greater than that of iron, silicon, titanium and the like, and the reduced impurities generate ferrosilicon alloy and are separated from corundum melt, so that brown fused block products are obtained.
The ladle is a key device in the intermittent production process of brown corundum, is a container (similar to a ladle), the smelted brown corundum melt is poured into the ladle and is subjected to processes such as precipitation, cooling and the like in the ladle, the ladle is required to bear strong impact of the high-temperature brown corundum melt, corrosion of ferrosilicon alloy and other chemical elements to a packing material at the temperature is prevented, the working condition is extremely severe, and along with the progress of scientific technology, the growing of the brown corundum smelting equipment is improved increasingly, the automation, pollution-free, low-consumption, long-service life and the like, at present, most of the ladle bottom and the ladle wall of the ladle for brown corundum production are paved by a block of semi-graphite carbon bricks, brick joints are difficult to exist between two adjacent bricks, the brick joints are seriously oxidized, the brick joints are easy to damage, larger cracks are formed over time, the bonding slag is serious, the service life cannot meet the requirements of customers, and particularly the risk of penetrating the brown corundum melt after the ladle bottom and the ladle wall are oxidized.
Disclosure of Invention
The invention aims to provide a method for baking bags by utilizing the waste heat of smelting brown fused alumina, which is environment-friendly, integrates the bag bottom and the bag wall, has no seam, improves the oxidation resistance, avoids the damage of the connected bags, thoroughly solves the problem of serious slag adhesion of the bag bottom and the bag wall, and improves the production quality.
To achieve the above object, the solution of the present invention is: a method for baking ladle by using waste heat of smelting brown alumina comprises the following steps:
S1: firstly, preparing electrode paste, preparing two manufactured bags and a bag body to be manufactured, preheating the bag body to be manufactured, wherein an inner cavity is formed in the bag body, an opening is formed in the top of the inner cavity, and an inner flange is horizontally arranged around the opening;
S2: then pouring electrode paste into the bottom of the inner cavity of the bag body from the opening, and gradually filling and lining the electrode paste on the bottom of the inner cavity of the bag body;
S3: then a knotting material layer is circularly built on the cavity wall of the inner cavity, a silicon carbide brick layer is circularly built on the outer side of the knotting material layer by utilizing a plurality of silicon carbide bricks, and the knotting material layer and the lower part of the silicon carbide brick layer are inserted into the edge part of the electrode paste slurry, so that the edge part of the electrode paste slurry is inwards sunk to form an annular groove;
S4: then pouring the smelted brown fused alumina into two manufactured bags for precipitation, gradually semi-graphitizing the brown fused alumina with waste heat along with the temperature reduction, stacking the bag body to be manufactured above one of the manufactured bags, stacking the other manufactured bag above the bag body to be manufactured, clamping the bag body to be manufactured in the middle by the two manufactured bags, baking the bag body in the middle by the waste heat of the upper bag and the lower bag, baking the electrode paste slurry to form an electrode paste graphitization layer serving as the bag bottom of the bag body, and simultaneously, heating and expanding the inner layer of the electrode paste graphitization layer, wherein the upper part of the silicon carbide brick layer is gradually folded towards the middle and tightly closing the brick joints under the condition that the upper part of the expanded knotting layer is limited by an inner flange and the lower part of the silicon carbide brick layer is supported by the electrode paste graphitization layer; the expanded knotting material layer extrudes the silicon carbide brick layer outwards to continuously push the gap between the silicon carbide brick layer and the ring groove to be tightly closed, so that the knotting material layer on the inner side and the silicon carbide brick layer on the outer side form a bag wall of the bag body together;
S5: and finally unloading the upper and lower packets, and integrally cooling the middle packet body to obtain the seamless packet.
Further, the knotting layer is made of brown corundum fine materials.
Further, the bag receiving body is of a basin-shaped structure with a wide upper part and a narrow lower part, and the bag wall is obliquely arranged along the cavity wall of the inner cavity.
Further, the electrode paste is made of a heat-resistant material.
Further, the heat-resistant material is composed of the following components in percentage by weight: 13-15% of ash, 9-12.0% of volatile matters, 70.5-72.5% of fixed carbon and the balance of water, wherein the water content is at least 0.5%.
After the scheme is adopted, the gain effect of the invention is as follows:
The invention utilizes the waste heat of the upper and lower bags filled with brown fused alumina to bake the bag body to be manufactured, does not need to additionally purchase baking equipment, fully utilizes energy and equipment conditions, implements the environment-friendly production concept, and in addition, the bag bottom is specially designed into a whole electrode paste graphitization layer, so that the bag bottom is integrated and seamless, i.e. the bag bottom has no gap, the package wall is specially designed into a layered structure with an inner layer and an outer layer, and the knotting material layer on the inner side is thermally expanded to extrude the silicon carbide brick layer on the outer side to eliminate brick joints, so that the package wall is more compact, slag can not be adhered to the package, package damage caused by oxidization and oxidation is fundamentally avoided, the service life of the package is prolonged, the production quality of brown fused alumina is higher, overturning is easy, and the production efficiency is faster.
Drawings
FIG. 1 is a schematic diagram of the structure of the present invention;
FIG. 2 is an enlarged schematic view at A in FIG. 1 (schematic view of top variation of the wall covering elimination brick joint);
Fig. 3 is a schematic diagram of the method for baking a bread according to the present invention.
Description of the reference numerals: 1. a bag receiving body; 11. an inner cavity; 12. an inner flange; 2. a bag bottom; 21. a ring groove; 3.a wall wrapping; 31. a knotting material layer; 32. a silicon carbide brick layer; 321. brick joints; 4. the finished bag is connected.
Detailed Description
In order to more clearly illustrate the embodiments of the invention or the technical solutions of the prior art, the drawings which are used in the description of the embodiments or the prior art will be briefly described, it being obvious that the drawings in the description below are only some embodiments of the invention, and that other drawings can be obtained according to these drawings without inventive faculty for a person skilled in the art.
The invention provides a method for baking bags by utilizing waste heat of smelting brown fused alumina, which is shown in figure 1 and comprises the following steps:
s1: firstly, preparing electrode paste, preparing two manufactured bags 4 and a bag body 1 to be manufactured, preheating the bag body 1 to be manufactured, wherein the bag body 1 is provided with an inner cavity 11, an opening is formed in the top of the inner cavity 11, and an inner flange 12 is horizontally arranged around the opening in a surrounding manner in combination with fig. 2;
s2: then pouring electrode paste into the bottom of the inner cavity 11 of the bag body 1 from the opening, and gradually filling and lining the electrode paste on the bottom of the inner cavity 11 of the bag body 1;
S3: then a knotting material layer 31 is circularly built on the wall of the inner cavity 11, a silicon carbide brick layer 32 is circularly built on the outer side of the knotting material layer 31 by utilizing a plurality of silicon carbide bricks, the knotting material layer 31 and the lower parts of the silicon carbide brick layer 32 are inserted into the edge parts of the electrode paste, the edge parts of the electrode paste are inwards sunk to form annular grooves 21, and the inner flange 12 is correspondingly arranged on the tops of the knotting material layer 31 and the silicon carbide brick layer 32;
S4: then pouring the smelted brown fused alumina into the two manufactured bags 4 for precipitation, gradually semi-graphitizing the brown fused alumina with waste heat along with the temperature reduction, stacking the bag body 1 to be manufactured above one of the manufactured bags 4, stacking the other bag 4 above the bag body 1 to be manufactured, clamping the bag body 1 to be manufactured in the middle by the two manufactured bags 4, baking the bag body 1 in the middle by the waste heat of the upper bag 4 and the lower bag 4, forming an electrode paste graphitization layer as a bag bottom 2 of the bag body by baking the electrode paste slurry, simultaneously heating and expanding the inner knotting layer 31, extruding the silicon carbide brick layer 32 outwards by the expanded knotting layer 31, gradually closing the brick joints towards the middle under the conditions that the upper part of the silicon carbide brick layer 32 is limited by the inner flange 12 and the lower part is supported by the electrode paste graphitization layer; the expanded knotting material layer 31 presses the silicon carbide brick layer 32 outwards to continuously push the gap between the silicon carbide brick layer 32 and the ring groove 21 to be tightly closed, so that the knotting material layer 31 on the inner side and the silicon carbide brick layer 32 on the outer side jointly form the wrapping wall of the ladle body 1;
s5: and finally unloading the upper and lower manufactured bags 4, and integrally cooling the middle bag body 1 to obtain the seamless bag.
The brown corundum receiving bag manufactured by the method comprises a receiving bag body 1, a bag bottom 2 and a bag wall 3.
The bag body 1 is of a basin-shaped structure with a wide upper part and a narrow lower part, the bag bottom 2 is an electrode paste graphitized layer which is formed by filling and lining the bottom of the inner cavity 11 with electrode paste and baking, the electrode paste graphitized layer is equivalent to a graphite electrode, has certain conductivity, and the whole layer of electrode paste is simpler in manufacturing process than a half graphite carbon brick paved with a block, and does not have a brick joint 321, so that the problem of slag sticking does not exist at all, damage caused by oxidation of the brick joint 321 is avoided, and the service life of the bag is prolonged.
Furthermore, the covering wall 3 is connected above the edge of the covering bottom 2. The lower part of the wrapping wall 3 is matched with an annular groove 21 embedded in the edge of the wrapping bottom 2, and the wrapping wall 3 is annularly arranged on the inner wall of the inner cavity 11 and is obliquely arranged along the cavity wall of the inner cavity 11.
The bag wall 3 comprises a knotting material layer 31 on the inner side and a silicon carbide brick layer 32 arranged on the outer side of the knotting material layer 31, the knotting material layer 31 is made of brown alumina fine materials, the knotting material layer 31 is clung to the inner wall of the bag body 1, the silicon carbide brick layer 32 is formed by stacking a block of silicon carbide bricks, and the silicon carbide brick layer 32 is clung to the outer side of the knotting material layer 31.
The electrode paste is made of a heat-resistant material, and the heat-resistant material comprises the following components in percentage by weight: 13-15% of ash, 9-12.0% of volatile matter, 70.5-72.5% of fixed carbon, the balance of water, at least 0.5% of water, and the volume density of the electrode paste prepared according to the components is about 1.38t/m 3 and the compressive strength is about 17 Mpa.
The above embodiments are only preferred embodiments of the present invention, and are not limited to the present invention, and all equivalent changes made according to the design key of the present invention fall within the protection scope of the present invention.

Claims (5)

1.一种利用冶炼棕刚玉的余热进行烘包的方法,其特征在于,包括以下步骤:1. A method for drying a bag using the waste heat from smelting brown corundum, characterized in that it comprises the following steps: S1:首先,制备电极糊浆料,以及准备两个已制作好的接包和一个待制作的接包本体,将待制作的接包本体进行预热,所述接包本体设有内腔,内腔顶部开设开口,开口四周水平环设内凸缘;S1: First, prepare electrode paste, and prepare two prepared connecting packages and a connecting package body to be prepared, and preheat the connecting package body to be prepared, wherein the connecting package body is provided with an inner cavity, an opening is provided at the top of the inner cavity, and an inner flange is horizontally arranged around the opening; S2:然后,将电极糊浆料从开口倒入接包本体的内腔底部,电极糊浆料逐渐填充铺衬在接包本体的内腔底部;S2: Then, pour the electrode paste slurry from the opening into the bottom of the inner cavity of the receiving package body, and the electrode paste slurry gradually fills and lines the bottom of the inner cavity of the receiving package body; S3:接着在内腔的腔壁环形修砌一打结料层,再在打结料层外侧利用多个碳化硅砖环形修砌出碳化硅砖层,打结料层和碳化硅砖层的下部插入在电极糊浆料的边部,使电极糊浆料的边部内陷形成环槽;S3: Then, a knotting material layer is built in a circular manner on the cavity wall of the inner cavity, and then a silicon carbide brick layer is built in a circular manner outside the knotting material layer using a plurality of silicon carbide bricks, and the lower parts of the knotting material layer and the silicon carbide brick layer are inserted into the edge of the electrode paste slurry, so that the edge of the electrode paste slurry is sunken to form an annular groove; S4:再然后,将冶炼好的棕刚玉熔液倒入两个已制作好的接包内进行沉淀,随着温度下降,棕刚玉熔液带有余热且逐渐半石墨化,然后将待制作的接包本体叠放在其中一个已制作好的接包上方,再将另一个已制作好的接包叠放在待制作的接包本体上方,从而待制作的接包本体被两个已制作好的接包夹合在中间,通过上下两个接包的余热烘烤中间的接包本体,电极糊浆料经过烘烤形成电极糊石墨化层作为接包本体的包底,同时,内侧的打结料层受热膨胀,膨胀的打结料层向外挤压碳化硅砖层,碳化硅砖层上部受到内凸缘的限制、下部受到电极糊石墨化层提供的支撑力的情况下,碳化硅砖层上下部逐渐向中间收拢,紧闭砖缝;而且膨胀的打结料层向外挤压碳化硅砖层不断推动碳化硅砖层和环槽之间的间隙紧闭,从而,内侧的打结料层和外侧的碳化硅砖层共同构成接包本体的包壁;S4: Then, pour the smelted brown corundum melt into two prepared connection packages for precipitation. As the temperature drops, the brown corundum melt carries residual heat and gradually becomes semi-graphitized. Then, the connection package body to be made is stacked on one of the prepared connection packages, and then the other prepared connection package is stacked on the connection package body to be made, so that the connection package body to be made is sandwiched between the two prepared connection packages. The connection package body in the middle is baked by the residual heat of the upper and lower connection packages, and the electrode paste slurry is baked to form an electrode paste. The graphitized layer serves as the bottom of the package body. At the same time, the inner knotted material layer expands due to heat, and the expanded knotted material layer squeezes the silicon carbide brick layer outward. When the upper part of the silicon carbide brick layer is restricted by the inner flange and the lower part is supported by the graphitized layer of the electrode paste, the upper and lower parts of the silicon carbide brick layer gradually converge toward the middle to close the brick seam. Moreover, the expanded knotted material layer squeezes the silicon carbide brick layer outward to continuously push the gap between the silicon carbide brick layer and the annular groove to close, so that the inner knotted material layer and the outer silicon carbide brick layer together constitute the package wall of the package body. S5:最后卸载上下两个接包,将中间的接包本体整体冷却,得到无缝接包。S5: Finally, the upper and lower connecting packages are unloaded, and the middle connecting package body is cooled as a whole to obtain a seamless connecting package. 2.如权利要求1所述的一种利用冶炼棕刚玉的余热进行烘包的方法,其特征在于:所述打结料层为棕刚玉细料制成。2. A method for drying bags using waste heat from smelting brown corundum as claimed in claim 1, characterized in that the knotted material layer is made of fine brown corundum. 3.如权利要求1所述的一种利用冶炼棕刚玉的余热进行烘包的方法,其特征在于:所述接包本体为上宽下窄的盆状结构,所述包壁沿内腔的腔壁倾斜设置。3. A method for drying a bag using the waste heat of smelting brown corundum as described in claim 1, characterized in that: the bag receiving body is a basin-shaped structure that is wide at the top and narrow at the bottom, and the bag wall is arranged obliquely along the wall of the inner cavity. 4.如权利要求1所述的一种利用冶炼棕刚玉的余热进行烘包的方法,其特征在于:所述电极糊浆料采用耐热材料制作。4. The method for baking the package by utilizing the waste heat of smelting brown corundum as claimed in claim 1, characterized in that the electrode paste is made of heat-resistant material. 5.如权利要求4所述的一种利用冶炼棕刚玉的余热进行烘包的方法,其特征在于:所述耐热材料由以下重量百分比的组分组成:灰分13—15%,挥发分9-12.0%,固定碳70.5-72.5%,余量为水分,水分至少为0.5%。5. A method for drying bags using waste heat from smelting brown corundum as claimed in claim 4, characterized in that the heat-resistant material is composed of the following components in weight percentage: ash 13-15%, volatile matter 9-12.0%, fixed carbon 70.5-72.5%, and the balance is water, which is at least 0.5%.
CN202210506475.2A 2022-05-11 2022-05-11 A method for drying packages using waste heat from smelting brown corundum Active CN114812196B (en)

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Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1236398A (en) * 1997-06-27 1999-11-24 奥地利钢铁联合企业阿尔帕工业设备制造公司 Apparatus and method for producing molten metal

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN211921345U (en) * 2019-12-27 2020-11-13 贵州银星新材料科技有限公司 A kind of bag receiving device for brown corundum production

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1236398A (en) * 1997-06-27 1999-11-24 奥地利钢铁联合企业阿尔帕工业设备制造公司 Apparatus and method for producing molten metal

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