CN114259051A - A kind of method for rapidly preparing lycopene - Google Patents
A kind of method for rapidly preparing lycopene Download PDFInfo
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- CN114259051A CN114259051A CN202111683001.7A CN202111683001A CN114259051A CN 114259051 A CN114259051 A CN 114259051A CN 202111683001 A CN202111683001 A CN 202111683001A CN 114259051 A CN114259051 A CN 114259051A
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- CN
- China
- Prior art keywords
- lycopene
- solution
- ethanol
- rapidly preparing
- preparing lycopene
- Prior art date
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- UPYKUZBSLRQECL-UKMVMLAPSA-N Lycopene Natural products CC(=C/C=C/C=C(C)/C=C/C=C(C)/C=C/C1C(=C)CCCC1(C)C)C=CC=C(/C)C=CC2C(=C)CCCC2(C)C UPYKUZBSLRQECL-UKMVMLAPSA-N 0.000 title claims abstract description 36
- JEVVKJMRZMXFBT-XWDZUXABSA-N Lycophyll Natural products OC/C(=C/CC/C(=C\C=C\C(=C/C=C/C(=C\C=C\C=C(/C=C/C=C(\C=C\C=C(/CC/C=C(/CO)\C)\C)/C)\C)/C)\C)/C)/C JEVVKJMRZMXFBT-XWDZUXABSA-N 0.000 title claims abstract description 35
- 235000012661 lycopene Nutrition 0.000 title claims abstract description 35
- OAIJSZIZWZSQBC-GYZMGTAESA-N lycopene Chemical compound CC(C)=CCC\C(C)=C\C=C\C(\C)=C\C=C\C(\C)=C\C=C\C=C(/C)\C=C\C=C(/C)\C=C\C=C(/C)CCC=C(C)C OAIJSZIZWZSQBC-GYZMGTAESA-N 0.000 title claims abstract description 35
- 229960004999 lycopene Drugs 0.000 title claims abstract description 35
- 239000001751 lycopene Substances 0.000 title claims abstract description 35
- ZCIHMQAPACOQHT-ZGMPDRQDSA-N trans-isorenieratene Natural products CC(=C/C=C/C=C(C)/C=C/C=C(C)/C=C/c1c(C)ccc(C)c1C)C=CC=C(/C)C=Cc2c(C)ccc(C)c2C ZCIHMQAPACOQHT-ZGMPDRQDSA-N 0.000 title claims abstract description 35
- 238000000034 method Methods 0.000 title claims abstract description 23
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 42
- 238000003756 stirring Methods 0.000 claims abstract description 13
- 235000015113 tomato pastes and purées Nutrition 0.000 claims abstract description 8
- 238000013517 stratification Methods 0.000 claims 1
- 235000007688 Lycopersicon esculentum Nutrition 0.000 abstract description 5
- 235000015067 sauces Nutrition 0.000 abstract description 5
- 229940079593 drug Drugs 0.000 abstract description 3
- 239000003814 drug Substances 0.000 abstract description 3
- 235000013305 food Nutrition 0.000 abstract description 3
- 241000227653 Lycopersicon Species 0.000 abstract 1
- 239000000243 solution Substances 0.000 description 18
- 240000003768 Solanum lycopersicum Species 0.000 description 4
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 3
- 210000002421 cell wall Anatomy 0.000 description 3
- GVJHHUAWPYXKBD-UHFFFAOYSA-N (±)-α-Tocopherol Chemical compound OC1=C(C)C(C)=C2OC(CCCC(C)CCCC(C)CCCC(C)C)(C)CCC2=C1C GVJHHUAWPYXKBD-UHFFFAOYSA-N 0.000 description 2
- HEDRZPFGACZZDS-UHFFFAOYSA-N Chloroform Chemical compound ClC(Cl)Cl HEDRZPFGACZZDS-UHFFFAOYSA-N 0.000 description 2
- 230000003078 antioxidant effect Effects 0.000 description 2
- 235000021466 carotenoid Nutrition 0.000 description 2
- 150000001747 carotenoids Chemical class 0.000 description 2
- 238000000605 extraction Methods 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- 206010028980 Neoplasm Diseases 0.000 description 1
- 229930003427 Vitamin E Natural products 0.000 description 1
- 239000003963 antioxidant agent Substances 0.000 description 1
- 235000006708 antioxidants Nutrition 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 201000011510 cancer Diseases 0.000 description 1
- 150000001746 carotenes Chemical class 0.000 description 1
- 235000005473 carotenes Nutrition 0.000 description 1
- 210000004027 cell Anatomy 0.000 description 1
- 239000002537 cosmetic Substances 0.000 description 1
- 230000006837 decompression Effects 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 230000002708 enhancing effect Effects 0.000 description 1
- 238000001125 extrusion Methods 0.000 description 1
- WIGCFUFOHFEKBI-UHFFFAOYSA-N gamma-tocopherol Natural products CC(C)CCCC(C)CCCC(C)CCCC1CCC2C(C)C(O)C(C)C(C)C2O1 WIGCFUFOHFEKBI-UHFFFAOYSA-N 0.000 description 1
- 239000004519 grease Substances 0.000 description 1
- 230000036039 immunity Effects 0.000 description 1
- 239000011259 mixed solution Substances 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- 230000005855 radiation Effects 0.000 description 1
- 150000003254 radicals Chemical class 0.000 description 1
- 238000000638 solvent extraction Methods 0.000 description 1
- NCYCYZXNIZJOKI-UHFFFAOYSA-N vitamin A aldehyde Natural products O=CC=C(C)C=CC=C(C)C=CC1=C(C)CCCC1(C)C NCYCYZXNIZJOKI-UHFFFAOYSA-N 0.000 description 1
- 235000019165 vitamin E Nutrition 0.000 description 1
- 229940046009 vitamin E Drugs 0.000 description 1
- 239000011709 vitamin E Substances 0.000 description 1
Landscapes
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
The invention relates to a method for rapidly preparing lycopene, which belongs to the technical field of food processing and medicines and comprises the following steps of 1: adding tomato sauce and ethanol with purity of more than 95% into a stirring tank, and stirring; step 2: breaking the wall of the stirred solution under high pressure; and step 3: then adding ethanol with purity of more than 90 percent into the solution; and 4, step 4: standing for layering, and separating the upper solution to obtain a product containing 15-18% of lycopene. The method only needs about 5 hours for extracting the lycopene, can quickly extract the lycopene in the tomato paste, and has simple process and low cost.
Description
Technical Field
The invention belongs to the technical field of food processing and medicines, and particularly relates to a method for quickly preparing lycopene.
Background
Lycopene is an important carotenoid substance, has a unique long-chain molecular structure and has more unsaturated double bonds than other carotenoids. Because of its special structure, it has the ability of eliminating free radical and antioxidant capacity, and its antioxidant effect is 2 times that of carotene and 100 times that of vitamin E. The health-care function of lycopene covers multiple aspects of delaying senility, preventing cancer, enhancing immunity of organisms, beautifying, resisting ultraviolet radiation and the like, and gradually becomes a new hotspot of research in the fields of health-care food, cosmetics and medicines in international marketing cities. Because lycopene is dissolved in chloroform, benzene and grease and is not dissolved in water, an organic solvent extraction method is generally adopted in the existing industrial extraction process of lycopene, but the method has complex process, high cost and long extraction period, and generally needs about ten days.
Disclosure of Invention
In order to solve the technical problems, the invention provides a method for quickly preparing lycopene.
The technical scheme adopted by the invention is as follows: a method for rapidly preparing lycopene comprises the following steps:
step 1: adding tomato sauce and ethanol with purity of more than 95% into a stirring tank, and stirring;
step 2: breaking the wall of the stirred solution under high pressure;
and step 3: then adding ethanol with purity of more than 90 percent into the solution;
and 4, step 4: standing for layering, and separating the upper solution to obtain a product containing 15-18% of lycopene.
Preferably, the ratio of the tomato paste to the ethanol in the step 1 is 1: 3.5-5.
Preferably, in a method for rapidly preparing lycopene, the stirring time in step 1 is 0.5-1 hour.
Preferably, in the method for rapidly preparing lycopene, the wall of the solution is broken by high pressure using a homogenizer in step 2.
Preferably, the pressure of the homogenizer is 200MPa-300 MPa.
Preferably, the ratio of the solution to the ethanol in the step 3 is 1: 1-1.3.
Preferably, the standing temperature in the step 4 is 30-35 ℃.
Preferably, the standing time in the step 4 is 1-2 hours.
Compared with the prior art, the invention has the beneficial effects that: according to the invention, the tomato sauce and ethanol with purity of more than 95% are added into a stirring tank and stirred; carrying out high-pressure wall breaking on the stirred solution in a homogenizer; then adding ethanol with purity of more than 90 percent into the solution; standing for layering, and separating out the upper solution to obtain a product containing 15-18% of lycopene; the method only needs about 5 hours for extracting the lycopene, can quickly extract the lycopene in the tomato paste, and has simple process and low cost.
Detailed Description
The technical solutions of the present invention will be described in detail below in order to clearly understand the technical features, objects, and advantages of the present invention, but the present invention is not limited to the practical scope of the present invention.
Example 1:
adding 100L tomato sauce and 350L 95% ethanol into a stirring tank, stirring for 0.5 hr, the purpose of adding ethanol at this moment is mainly to destroy cell walls in the tomato paste, the stirred solution is subjected to high-pressure wall breaking in a homogenizer, the pressure of the homogenizer is set to be 200MPa, the homogenizer enables the tomato paste and the ethanol to further destroy the cell walls under the triple effects of extrusion, strong impact and decompression expansion, the cell surfaces and the lycopene contained in the tomato paste are effectively separated, substances in the mixed solution are finely mixed, then 450L of ethanol with the purity of 90 percent is added into the solution, standing at 30 deg.C for 1 hr, because lycopene is insoluble in water and ethanol, and lycopene and ethanol solution are layered, since the density of lycopene is less than that of ethanol solution, lycopene is in the upper layer of the solution, and the upper layer solution is separated to obtain the product containing 15.2% of lycopene.
Example 2:
adding 100L tomato sauce and 500L ethanol with purity of 96% into a stirring tank, stirring for 1 hr, breaking cell wall of the stirred solution at high pressure in a homogenizer with pressure of 300MPa, adding 780L ethanol with purity of 95% into the solution, standing at 35 deg.C for 2 hr, and separating the upper layer solution to obtain product containing lycopene 17.6%.
It is to be understood that the above-described embodiments are only a few, and not all, embodiments of the present invention. All other embodiments, which can be derived by a person skilled in the art from the embodiments of the present invention without making any creative effort, shall fall within the protection scope of the present invention.
Claims (8)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202111683001.7A CN114259051A (en) | 2021-12-31 | 2021-12-31 | A kind of method for rapidly preparing lycopene |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202111683001.7A CN114259051A (en) | 2021-12-31 | 2021-12-31 | A kind of method for rapidly preparing lycopene |
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| Publication Number | Publication Date |
|---|---|
| CN114259051A true CN114259051A (en) | 2022-04-01 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202111683001.7A Pending CN114259051A (en) | 2021-12-31 | 2021-12-31 | A kind of method for rapidly preparing lycopene |
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| Country | Link |
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| CN (1) | CN114259051A (en) |
Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4781936A (en) * | 1986-07-09 | 1988-11-01 | Del Monte Corporation | Coloring compositions |
| CN1176577A (en) * | 1994-10-31 | 1998-03-18 | 马克特辛姆化学工厂有限公司 | Stable lycopene concentrate and its preparation method |
| WO2001038443A1 (en) * | 1999-11-23 | 2001-05-31 | Societe Des Produits Nestle S.A. | A process for the extraction of lycopene |
| CN1405235A (en) * | 2002-10-22 | 2003-03-26 | 赵京城 | Method for preparing high-purity lycopene |
| WO2003028481A1 (en) * | 2001-09-28 | 2003-04-10 | Xinjiang Jinqi Industry Limited | Method of preparing lycopene |
| CN1493622A (en) * | 2003-09-15 | 2004-05-05 | 广州优宝工业有限公司 | Preparation method of lycopene |
| WO2006036125A1 (en) * | 2004-09-28 | 2006-04-06 | Gao Shen Sdn Bhd | A process for producing lycopene extract |
-
2021
- 2021-12-31 CN CN202111683001.7A patent/CN114259051A/en active Pending
Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4781936A (en) * | 1986-07-09 | 1988-11-01 | Del Monte Corporation | Coloring compositions |
| CN1176577A (en) * | 1994-10-31 | 1998-03-18 | 马克特辛姆化学工厂有限公司 | Stable lycopene concentrate and its preparation method |
| WO2001038443A1 (en) * | 1999-11-23 | 2001-05-31 | Societe Des Produits Nestle S.A. | A process for the extraction of lycopene |
| WO2003028481A1 (en) * | 2001-09-28 | 2003-04-10 | Xinjiang Jinqi Industry Limited | Method of preparing lycopene |
| CN1405235A (en) * | 2002-10-22 | 2003-03-26 | 赵京城 | Method for preparing high-purity lycopene |
| CN1493622A (en) * | 2003-09-15 | 2004-05-05 | 广州优宝工业有限公司 | Preparation method of lycopene |
| WO2006036125A1 (en) * | 2004-09-28 | 2006-04-06 | Gao Shen Sdn Bhd | A process for producing lycopene extract |
Non-Patent Citations (2)
| Title |
|---|
| 孙培冬，刘云秋，孙燕鼎: "高压法提取天然色素", 《中国食品添加剂》, no. 5 * |
| 林泽华，任娇艳: "天然番茄红素提取工艺研究进展", 《食品科学技术学报》, vol. 32, no. 5, pages 50 - 55 * |
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