CN103819940A - Fire-retardant black iron oxide pigment - Google Patents
Fire-retardant black iron oxide pigment Download PDFInfo
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- CN103819940A CN103819940A CN201410049092.2A CN201410049092A CN103819940A CN 103819940 A CN103819940 A CN 103819940A CN 201410049092 A CN201410049092 A CN 201410049092A CN 103819940 A CN103819940 A CN 103819940A
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- Prior art keywords
- iron oxide
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- pigment
- fire
- black iron
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- SZVJSHCCFOBDDC-UHFFFAOYSA-N iron(II,III) oxide Inorganic materials O=[Fe]O[Fe]O[Fe]=O SZVJSHCCFOBDDC-UHFFFAOYSA-N 0.000 title claims abstract description 23
- 239000001034 iron oxide pigment Substances 0.000 title claims abstract description 17
- WTFXARWRTYJXII-UHFFFAOYSA-N iron(2+);iron(3+);oxygen(2-) Chemical compound [O-2].[O-2].[O-2].[O-2].[Fe+2].[Fe+3].[Fe+3] WTFXARWRTYJXII-UHFFFAOYSA-N 0.000 title claims abstract description 15
- 239000003063 flame retardant Substances 0.000 title claims abstract description 12
- ADCOVFLJGNWWNZ-UHFFFAOYSA-N antimony trioxide Chemical compound O=[Sb]O[Sb]=O ADCOVFLJGNWWNZ-UHFFFAOYSA-N 0.000 claims abstract description 12
- 239000002994 raw material Substances 0.000 claims abstract description 11
- 239000004698 Polyethylene Substances 0.000 claims abstract description 9
- -1 polyethylene Polymers 0.000 claims abstract description 9
- 229920000573 polyethylene Polymers 0.000 claims abstract description 9
- 239000000049 pigment Substances 0.000 claims abstract description 8
- 229910052901 montmorillonite Inorganic materials 0.000 claims abstract description 6
- 239000000463 material Substances 0.000 claims abstract description 5
- CJZGTCYPCWQAJB-UHFFFAOYSA-L calcium stearate Chemical compound [Ca+2].CCCCCCCCCCCCCCCCCC([O-])=O.CCCCCCCCCCCCCCCCCC([O-])=O CJZGTCYPCWQAJB-UHFFFAOYSA-L 0.000 claims abstract description 4
- 235000013539 calcium stearate Nutrition 0.000 claims abstract description 4
- 239000008116 calcium stearate Substances 0.000 claims abstract description 4
- 239000000203 mixture Substances 0.000 claims description 15
- 239000000843 powder Substances 0.000 claims description 8
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 7
- 241000596504 Tamarindus Species 0.000 claims description 6
- 235000004298 Tamarindus indica Nutrition 0.000 claims description 6
- 239000012752 auxiliary agent Substances 0.000 claims description 6
- 238000001035 drying Methods 0.000 claims description 6
- 238000002360 preparation method Methods 0.000 claims description 6
- DAJSVUQLFFJUSX-UHFFFAOYSA-M sodium;dodecane-1-sulfonate Chemical compound [Na+].CCCCCCCCCCCCS([O-])(=O)=O DAJSVUQLFFJUSX-UHFFFAOYSA-M 0.000 claims description 6
- 238000003756 stirring Methods 0.000 claims description 6
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims description 4
- GUJOJGAPFQRJSV-UHFFFAOYSA-N dialuminum;dioxosilane;oxygen(2-);hydrate Chemical compound O.[O-2].[O-2].[O-2].[Al+3].[Al+3].O=[Si]=O.O=[Si]=O.O=[Si]=O.O=[Si]=O GUJOJGAPFQRJSV-UHFFFAOYSA-N 0.000 claims description 4
- 239000000047 product Substances 0.000 claims description 4
- 229910052903 pyrophyllite Inorganic materials 0.000 claims description 4
- 239000011734 sodium Substances 0.000 claims description 4
- 229910052708 sodium Inorganic materials 0.000 claims description 4
- WYTZZXDRDKSJID-UHFFFAOYSA-N (3-aminopropyl)triethoxysilane Chemical compound CCO[Si](OCC)(OCC)CCCN WYTZZXDRDKSJID-UHFFFAOYSA-N 0.000 claims description 3
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 3
- BLRPTPMANUNPDV-UHFFFAOYSA-N Silane Chemical compound [SiH4] BLRPTPMANUNPDV-UHFFFAOYSA-N 0.000 claims description 3
- WNROFYMDJYEPJX-UHFFFAOYSA-K aluminium hydroxide Chemical compound [OH-].[OH-].[OH-].[Al+3] WNROFYMDJYEPJX-UHFFFAOYSA-K 0.000 claims description 3
- 229910021502 aluminium hydroxide Inorganic materials 0.000 claims description 3
- 238000000498 ball milling Methods 0.000 claims description 3
- 239000006185 dispersion Substances 0.000 claims description 3
- 239000012467 final product Substances 0.000 claims description 3
- 239000010881 fly ash Substances 0.000 claims description 3
- 229910021389 graphene Inorganic materials 0.000 claims description 3
- 238000000227 grinding Methods 0.000 claims description 3
- 239000000395 magnesium oxide Substances 0.000 claims description 3
- CPLXHLVBOLITMK-UHFFFAOYSA-N magnesium oxide Inorganic materials [Mg]=O CPLXHLVBOLITMK-UHFFFAOYSA-N 0.000 claims description 3
- AXZKOIWUVFPNLO-UHFFFAOYSA-N magnesium;oxygen(2-) Chemical compound [O-2].[Mg+2] AXZKOIWUVFPNLO-UHFFFAOYSA-N 0.000 claims description 3
- 229940045641 monobasic sodium phosphate Drugs 0.000 claims description 3
- 229940059574 pentaerithrityl Drugs 0.000 claims description 3
- WXZMFSXDPGVJKK-UHFFFAOYSA-N pentaerythritol Chemical compound OCC(CO)(CO)CO WXZMFSXDPGVJKK-UHFFFAOYSA-N 0.000 claims description 3
- 239000011347 resin Substances 0.000 claims description 3
- 229920005989 resin Polymers 0.000 claims description 3
- 229910000077 silane Inorganic materials 0.000 claims description 3
- AJPJDKMHJJGVTQ-UHFFFAOYSA-M sodium dihydrogen phosphate Chemical compound [Na+].OP(O)([O-])=O AJPJDKMHJJGVTQ-UHFFFAOYSA-M 0.000 claims description 3
- 238000004519 manufacturing process Methods 0.000 claims description 2
- DBMJMQXJHONAFJ-UHFFFAOYSA-M Sodium laurylsulphate Chemical compound [Na+].CCCCCCCCCCCCOS([O-])(=O)=O DBMJMQXJHONAFJ-UHFFFAOYSA-M 0.000 abstract 2
- 239000006087 Silane Coupling Agent Substances 0.000 abstract 1
- 238000005299 abrasion Methods 0.000 abstract 1
- 239000010883 coal ash Substances 0.000 abstract 1
- 239000013049 sediment Substances 0.000 abstract 1
- UQSXHKLRYXJYBZ-UHFFFAOYSA-N Iron oxide Chemical compound [Fe]=O UQSXHKLRYXJYBZ-UHFFFAOYSA-N 0.000 description 2
- RNFJDJUURJAICM-UHFFFAOYSA-N 2,2,4,4,6,6-hexaphenoxy-1,3,5-triaza-2$l^{5},4$l^{5},6$l^{5}-triphosphacyclohexa-1,3,5-triene Chemical compound N=1P(OC=2C=CC=CC=2)(OC=2C=CC=CC=2)=NP(OC=2C=CC=CC=2)(OC=2C=CC=CC=2)=NP=1(OC=1C=CC=CC=1)OC1=CC=CC=C1 RNFJDJUURJAICM-UHFFFAOYSA-N 0.000 description 1
- 206010037660 Pyrexia Diseases 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000011248 coating agent Substances 0.000 description 1
- 238000000576 coating method Methods 0.000 description 1
- 239000000835 fiber Substances 0.000 description 1
- 230000009970 fire resistant effect Effects 0.000 description 1
- 239000011174 green composite Substances 0.000 description 1
- 229910052500 inorganic mineral Inorganic materials 0.000 description 1
- JEIPFZHSYJVQDO-UHFFFAOYSA-N iron(III) oxide Inorganic materials O=[Fe]O[Fe]=O JEIPFZHSYJVQDO-UHFFFAOYSA-N 0.000 description 1
- 239000002932 luster Substances 0.000 description 1
- 239000011707 mineral Substances 0.000 description 1
- 231100000252 nontoxic Toxicity 0.000 description 1
- 230000003000 nontoxic effect Effects 0.000 description 1
- NDLPOXTZKUMGOV-UHFFFAOYSA-N oxo(oxoferriooxy)iron hydrate Chemical class O.O=[Fe]O[Fe]=O NDLPOXTZKUMGOV-UHFFFAOYSA-N 0.000 description 1
- 238000011056 performance test Methods 0.000 description 1
- PVGBHEUCHKGFQP-UHFFFAOYSA-N sodium;n-[5-amino-2-(4-aminophenyl)sulfonylphenyl]sulfonylacetamide Chemical compound [Na+].CC(=O)NS(=O)(=O)C1=CC(N)=CC=C1S(=O)(=O)C1=CC=C(N)C=C1 PVGBHEUCHKGFQP-UHFFFAOYSA-N 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000004381 surface treatment Methods 0.000 description 1
Landscapes
- Pigments, Carbon Blacks, Or Wood Stains (AREA)
- Compositions Of Macromolecular Compounds (AREA)
Abstract
The invention relates to an iron oxide pigment, in particular to a fire-retardant black iron oxide pigment. The pigment provided by the invention is prepared from the following raw materials in parts by weight: 280 to 300 parts of black iron oxide, 5 to 8 parts of Na-montmorillonite, 1 to 2 parts of a silane coupling agent KH-5501-2, 3 to 5 parts of antimonous oxide, 4 to 6 parts of pyrophillite, 1 to 2 parts of calcium stearate, 3 to 5 parts of polyethylene wax, 1 to 2 parts of sodium dodecyl sulfate, 10 to 12 parts of coal ash, and 4 to 5 parts of an assistant. According to the pigment provided by the invention, the raw materials such as the polyethylene wax and the sodium dodecyl sulfate are used for improving the surface activity of a black iron oxide power; thus the distributing in a base material is more uniform, and the probability of sediment is low. The added raw materials such as Na-montmorillonite, antimonous oxide and pyrophillite ensure the black iron oxide pigment has the characteristics of fire resistance, flexibility, abrasion resistance, watertightness and damp resistance, and the like; during actual use, the fire-retardant black iron oxide pigment is safe and reliable, the covering power is large, and the application value is extremely high.
Description
Technical field
The present invention relates to a kind of iron oxide pigment, be specifically related to a kind of fire-retardant black iron oxide pigment and preparation method thereof.
Background technology
Iron oxide pigment is the widely used mineral dye of a class, in building, coating, ink, pottery, in the industries such as makeup, widely apply, it is stable chemical performance not only, acid-fast alkali-proof, fast light heat-resisting, to dry wet, the tolerance level of the weathers such as fever and chills is high, also there is chromatogram wide, tinting strength is stronger, the nontoxic advantage such as inexpensive, the ferric oxide series pigment that existing market is used mainly contains red iron oxide, iron oxide black, iron oxide yellow and orange, palm fibre, the green composite pigment that waits, apply very extensive, but exist easily and reunite in actual use, difficult dispersed in medium, the problems such as color and luster is bright not, in order to obtain better use properties, often need iron oxide pigment to carry out surface treatment and improvement in performance, to improve production application performance, improve added value of product.
Summary of the invention
The object of the invention is to, a kind of fire-retardant black iron oxide pigment is provided, make it have good use properties, to achieve these goals, the technical solution used in the present invention is as follows:
A kind of fire-retardant black iron oxide pigment, it is characterized in that, pigment of the present invention is made up of the raw material of following weight part: iron oxide black 280-300, sodium-based montmorillonite 5-8, silane resin acceptor kh-550 1-2, antimonous oxide 3-5, pyrophyllite powder 4-6, calcium stearate 1-2, polyethylene wax 3-5, sodium laurylsulfonate 1-2, flyash 10-12, auxiliary agent 4-5.
Described auxiliary agent is made up of the raw material of following weight part: aluminium hydroxide 2-4, aminopropyl triethoxysilane 1-2, tamarind seed gum 0.5-1, pearlstone 10-12, Graphene 6-8, tetramethylolmethane 2-3, magnesium oxide 1-3, SODIUM PHOSPHATE, MONOBASIC 1-2, Starso 1-2; Preparation method first mixes tamarind seed gum, Starso, add appropriate water, be stirred to mixture and dissolve dispersion completely, add again subsequently other remaining component, after stirring, freeze-day with constant temperature 3-4h at 50-60 ℃, grinds to form 250-300 order powder by mixture after being dried, and to obtain final product.
The fire-retardant black iron oxide pigment of described one, its preparation technology is:
(1) first iron oxide black is mixed with polyethylene wax, be heated to 90-95 ℃, after stirring, send into grinding in ball grinder 20-30min, cross 100-150 mesh sieve;
(2) appropriate 40-60 ℃ hot water will be added in sodium laurylsulfonate, being stirred to mixture dissolves completely, add subsequently step (1) gained material and other remaining component, after mix and blend 25-30min, drying and processing under 50-60 ℃ of condition, ball milling 20-25min after drying, crosses 250-300 mesh sieve, gets product.
Beneficial effect of the present invention is: utilize the raw material such as polyethylene wax, sodium laurylsulfonate to improve the surfactivity of iron oxide black powder, it is disperseed in body material more even, there is good anti-settling function, the raw materials such as the sodium-based montmorillonite, antimonous oxide, pyrophyllite powder adding make black iron oxide pigment have the characteristic such as fire resistant flame retardant, pliable and tough wear-resisting, anti-water resistance tide, safe and reliable when actual use, strong covering power, has using value.
Embodiment
Embodiment
The present embodiment pigment is made up of following weight part raw material: iron oxide black 300, sodium-based montmorillonite 8, silane resin acceptor kh-550 1, antimonous oxide 5, pyrophyllite powder 6, calcium stearate 1, polyethylene wax 4, sodium laurylsulfonate 1, flyash 12, auxiliary agent 5.
Described auxiliary agent is made up of the raw material of following weight part: aluminium hydroxide 4, aminopropyl triethoxysilane 1, tamarind seed gum 1, pearlstone 12, Graphene 8, tetramethylolmethane 2, magnesium oxide 3, SODIUM PHOSPHATE, MONOBASIC 2, Starso 1; Preparation method first mixes tamarind seed gum, Starso, adds appropriate water, is stirred to mixture and dissolves dispersion completely, add again subsequently other remaining component, after stirring, freeze-day with constant temperature 4h at 50-60 ℃, after dry, mixture is ground to form to 300 order powders, to obtain final product.
The fire-retardant black iron oxide pigment of described one, its preparation technology is:
(1) first iron oxide black is mixed with polyethylene wax, be heated to 95 ℃, after stirring, send into grinding in ball grinder 30min, cross 150 mesh sieves;
(2) 60 ℃ of appropriate hot water will be added in sodium laurylsulfonate, being stirred to mixture dissolves completely, add subsequently step (1) gained material and other remaining component, after mix and blend 30min, drying and processing under 60 ℃ of conditions, ball milling 25min after drying, crosses 300 mesh sieves, gets product.
The performance test results of pigment of the present invention is:
Claims (2)
1. a fire-retardant black iron oxide pigment, it is characterized in that, this pigment is made up of the raw material of following weight part: iron oxide black 280-300, sodium-based montmorillonite 5-8, silane resin acceptor kh-550 1-2, antimonous oxide 3-5, pyrophyllite powder 4-6, calcium stearate 1-2, polyethylene wax 3-5, sodium laurylsulfonate 1-2, flyash 10-12, auxiliary agent 4-5;
Described auxiliary agent is made up of the raw material of following weight part: aluminium hydroxide 2-4, aminopropyl triethoxysilane 1-2, tamarind seed gum 0.5-1, pearlstone 10-12, Graphene 6-8, tetramethylolmethane 2-3, magnesium oxide 1-3, SODIUM PHOSPHATE, MONOBASIC 1-2, Starso 1-2; Preparation method first mixes tamarind seed gum, Starso, add appropriate water, be stirred to mixture and dissolve dispersion completely, add again subsequently other remaining component, after stirring, freeze-day with constant temperature 3-4h at 50-60 ℃, grinds to form 250-300 order powder by mixture after being dried, and to obtain final product.
2. the fire-retardant black iron oxide pigment of one as claimed in claim 1, its production stage is as follows:
(1) first iron oxide black is mixed with polyethylene wax, be heated to 90-95 ℃, after stirring, send into grinding in ball grinder 20-30min, cross 100-150 mesh sieve;
(2) appropriate 40-60 ℃ hot water will be added in sodium laurylsulfonate, being stirred to mixture dissolves completely, add subsequently step (1) gained material and other remaining component, after mix and blend 25-30min, drying and processing under 50-60 ℃ of condition, ball milling 20-25min after drying, crosses 250-300 mesh sieve, gets product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410049092.2A CN103819940A (en) | 2014-02-12 | 2014-02-12 | Fire-retardant black iron oxide pigment |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410049092.2A CN103819940A (en) | 2014-02-12 | 2014-02-12 | Fire-retardant black iron oxide pigment |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN103819940A true CN103819940A (en) | 2014-05-28 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
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| CN201410049092.2A Pending CN103819940A (en) | 2014-02-12 | 2014-02-12 | Fire-retardant black iron oxide pigment |
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| CN (1) | CN103819940A (en) |
Cited By (15)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105038324A (en) * | 2015-07-27 | 2015-11-11 | 安徽明珠颜料科技有限公司 | Iron oxide black paint for purifying air and preparation method of iron oxide black paint |
| CN105038323A (en) * | 2015-07-27 | 2015-11-11 | 安徽明珠颜料科技有限公司 | Parasite-dispelling iron oxide black pigment and preparation method thereof |
| CN105038325A (en) * | 2015-07-27 | 2015-11-11 | 安徽明珠颜料科技有限公司 | Deodorant iron oxide black pigment and preparation method thereof |
| CN105062143A (en) * | 2015-07-25 | 2015-11-18 | 铜陵瑞莱科技有限公司 | Flame-retardant iron oxide black pigment and preparation method therefor |
| CN105086517A (en) * | 2015-07-27 | 2015-11-25 | 安徽明珠颜料科技有限公司 | Ferric oxide black pigment with refreshing and consciousness-restoring functions and preparation method thereof |
| CN105131653A (en) * | 2015-07-25 | 2015-12-09 | 铜陵瑞莱科技有限公司 | Iron oxide black pigment used for printing ink and preparation method thereof |
| CN105131654A (en) * | 2015-07-25 | 2015-12-09 | 铜陵瑞莱科技有限公司 | Antibacterial black iron oxide pigment and preparation method thereof |
| CN105153757A (en) * | 2015-07-25 | 2015-12-16 | 铜陵瑞莱科技有限公司 | Highly water-resistant iron oxide black pigment and preparation method therefor |
| CN105153756A (en) * | 2015-07-25 | 2015-12-16 | 铜陵瑞莱科技有限公司 | Highly wear-resistant iron oxide black pigment and preparation method therefor |
| CN105968880A (en) * | 2016-04-06 | 2016-09-28 | 安徽明珠颜料科技有限公司 | Black iron oxide pigment with high water resistance and preparation method thereof |
| CN109486241A (en) * | 2018-11-19 | 2019-03-19 | 岳西县邦玉铁系颜料有限公司 | A kind of iron oxide pigment that tinting strength, tinting power is well easily dispersed |
| CN109504153A (en) * | 2018-11-19 | 2019-03-22 | 岳西县邦玉铁系颜料有限公司 | A kind of iron oxide pigment that wearability is good |
| CN109535774A (en) * | 2018-11-19 | 2019-03-29 | 岳西县邦玉铁系颜料有限公司 | A kind of high temperature resistant mica-iron oxide pigment |
| CN112111179A (en) * | 2020-08-18 | 2020-12-22 | 江苏宇星工贸有限公司 | Production process of heat-resistant iron oxide black |
| CN115232487A (en) * | 2022-06-30 | 2022-10-25 | 宇虹颜料股份有限公司 | Preparation method of superfine pigment preparation for coloring polyolefin |
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| CN105131653A (en) * | 2015-07-25 | 2015-12-09 | 铜陵瑞莱科技有限公司 | Iron oxide black pigment used for printing ink and preparation method thereof |
| CN105153756A (en) * | 2015-07-25 | 2015-12-16 | 铜陵瑞莱科技有限公司 | Highly wear-resistant iron oxide black pigment and preparation method therefor |
| CN105153757A (en) * | 2015-07-25 | 2015-12-16 | 铜陵瑞莱科技有限公司 | Highly water-resistant iron oxide black pigment and preparation method therefor |
| CN105062143A (en) * | 2015-07-25 | 2015-11-18 | 铜陵瑞莱科技有限公司 | Flame-retardant iron oxide black pigment and preparation method therefor |
| CN105131654A (en) * | 2015-07-25 | 2015-12-09 | 铜陵瑞莱科技有限公司 | Antibacterial black iron oxide pigment and preparation method thereof |
| CN105086517A (en) * | 2015-07-27 | 2015-11-25 | 安徽明珠颜料科技有限公司 | Ferric oxide black pigment with refreshing and consciousness-restoring functions and preparation method thereof |
| CN105038324A (en) * | 2015-07-27 | 2015-11-11 | 安徽明珠颜料科技有限公司 | Iron oxide black paint for purifying air and preparation method of iron oxide black paint |
| CN105038325A (en) * | 2015-07-27 | 2015-11-11 | 安徽明珠颜料科技有限公司 | Deodorant iron oxide black pigment and preparation method thereof |
| CN105038323A (en) * | 2015-07-27 | 2015-11-11 | 安徽明珠颜料科技有限公司 | Parasite-dispelling iron oxide black pigment and preparation method thereof |
| CN105968880A (en) * | 2016-04-06 | 2016-09-28 | 安徽明珠颜料科技有限公司 | Black iron oxide pigment with high water resistance and preparation method thereof |
| CN109486241A (en) * | 2018-11-19 | 2019-03-19 | 岳西县邦玉铁系颜料有限公司 | A kind of iron oxide pigment that tinting strength, tinting power is well easily dispersed |
| CN109504153A (en) * | 2018-11-19 | 2019-03-22 | 岳西县邦玉铁系颜料有限公司 | A kind of iron oxide pigment that wearability is good |
| CN109535774A (en) * | 2018-11-19 | 2019-03-29 | 岳西县邦玉铁系颜料有限公司 | A kind of high temperature resistant mica-iron oxide pigment |
| CN112111179A (en) * | 2020-08-18 | 2020-12-22 | 江苏宇星工贸有限公司 | Production process of heat-resistant iron oxide black |
| CN112111179B (en) * | 2020-08-18 | 2021-08-27 | 江苏宇星科技有限公司 | Production process of heat-resistant iron oxide black |
| CN115232487A (en) * | 2022-06-30 | 2022-10-25 | 宇虹颜料股份有限公司 | Preparation method of superfine pigment preparation for coloring polyolefin |
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