CN103668948A - Three-proofing finishing agent for fabric - Google Patents
Three-proofing finishing agent for fabric Download PDFInfo
- Publication number
- CN103668948A CN103668948A CN201310615646.6A CN201310615646A CN103668948A CN 103668948 A CN103668948 A CN 103668948A CN 201310615646 A CN201310615646 A CN 201310615646A CN 103668948 A CN103668948 A CN 103668948A
- Authority
- CN
- China
- Prior art keywords
- parts
- fabric
- finishing agent
- raw material
- proof finishing
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn
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- 239000004744 fabric Substances 0.000 title claims abstract description 29
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 26
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims abstract description 23
- 239000002994 raw material Substances 0.000 claims abstract description 18
- 239000003921 oil Substances 0.000 claims abstract description 12
- -1 polysiloxane Polymers 0.000 claims abstract description 9
- WCRKLZYTQVZTMM-UHFFFAOYSA-N 2-octadecylphenol Chemical compound CCCCCCCCCCCCCCCCCCC1=CC=CC=C1O WCRKLZYTQVZTMM-UHFFFAOYSA-N 0.000 claims abstract description 8
- 229920002134 Carboxymethyl cellulose Polymers 0.000 claims abstract description 8
- 235000010948 carboxy methyl cellulose Nutrition 0.000 claims abstract description 8
- 235000011187 glycerol Nutrition 0.000 claims abstract description 8
- SNGREZUHAYWORS-UHFFFAOYSA-N perfluorooctanoic acid Chemical compound OC(=O)C(F)(F)C(F)(F)C(F)(F)C(F)(F)C(F)(F)C(F)(F)C(F)(F)F SNGREZUHAYWORS-UHFFFAOYSA-N 0.000 claims abstract description 8
- 235000005979 Citrus limon Nutrition 0.000 claims abstract description 5
- 244000131522 Citrus pyriformis Species 0.000 claims abstract description 5
- 239000000341 volatile oil Substances 0.000 claims abstract description 5
- 244000178870 Lavandula angustifolia Species 0.000 claims abstract description 4
- 235000010663 Lavandula angustifolia Nutrition 0.000 claims abstract description 4
- 239000001102 lavandula vera Substances 0.000 claims abstract description 4
- 235000018219 lavender Nutrition 0.000 claims abstract description 4
- 239000001768 carboxy methyl cellulose Substances 0.000 claims abstract description 3
- 239000008112 carboxymethyl-cellulose Substances 0.000 claims abstract description 3
- 229910052710 silicon Inorganic materials 0.000 claims description 7
- 239000010703 silicon Substances 0.000 claims description 7
- 235000013599 spices Nutrition 0.000 claims description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract description 11
- 238000002360 preparation method Methods 0.000 abstract description 2
- 125000003709 fluoroalkyl group Chemical group 0.000 abstract 2
- 239000002304 perfume Substances 0.000 abstract 2
- 229920001296 polysiloxane Polymers 0.000 abstract 2
- 229920001807 Urea-formaldehyde Polymers 0.000 abstract 1
- GZCGUPFRVQAUEE-SLPGGIOYSA-N aldehydo-D-glucose Chemical compound OC[C@@H](O)[C@@H](O)[C@H](O)[C@@H](O)C=O GZCGUPFRVQAUEE-SLPGGIOYSA-N 0.000 abstract 1
- OBFQBDOLCADBTP-UHFFFAOYSA-N aminosilicon Chemical compound [Si]N OBFQBDOLCADBTP-UHFFFAOYSA-N 0.000 abstract 1
- 238000010186 staining Methods 0.000 abstract 1
- 239000004753 textile Substances 0.000 description 3
- 230000003373 anti-fouling effect Effects 0.000 description 2
- 239000000835 fiber Substances 0.000 description 2
- 239000012467 final product Substances 0.000 description 2
- 238000011056 performance test Methods 0.000 description 2
- 238000003756 stirring Methods 0.000 description 2
- 238000005406 washing Methods 0.000 description 2
- 229920000742 Cotton Polymers 0.000 description 1
- 230000004888 barrier function Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 230000002265 prevention Effects 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
Landscapes
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
Abstract
The invention discloses a three-proofing finishing agent for a fabric which comprises the following raw materials in parts by weight: 10-18 parts of octadecyl phenol, 8-13 parts of fluoroalkyl polysiloxane, 5-8 parts of carboxymethylcellulose, 2-8 parts of urea formaldehyde resin, 30-40 parts of glycerin and 0.5-1 part of perfume, wherein fluoroalkyl polysiloxane is synthesized by perfluoro caprylic acid and amino silicon oil as raw materials; the perfume is lemon essential oil or lavender essential oil. According to the three-proofing finishing agent, the fabric is good in water repellency, oil repellency and staining resistance, and the water repellency rate of the fabric still can be kept more than 90% after the fabric is washed by water 30 times; a preparation method of the three-proofing finishing agent is simple and easy to operate and can be widely popularized and applied.
Description
Technical field
The invention belongs to textile auxiliary field, be specifically related to a kind of fabric three-proof finishing agent.
Background technology
Fabric three-proof finishing agent is a kind of finishing agent that is widely used in the fabric panels such as cotton, hair, silk, chemical fibre and blend fibre, it can give the super water and oil repellant of fabric and anti-pollution function, the surface property of the fabric of processing with three-proof finishing agent improves, be difficult for by water and glossy wet or stain, three prevention fabrics have consequence in textile industry, and the existing performance of China preferably three-proof finishing agent mostly be imported product, China still needs further raising to the research of three-proof finishing agent.
Therefore, developing a kind of well behaved three-proof finishing agent is existing textile auxiliary field technical barrier urgently to be resolved hurrily.
Summary of the invention
The oil of refusing that the object of the invention is to overcome the deficiencies in the prior art and provide a kind of fabric three-proof finishing agent, fabric three-proof finishing agent of the present invention to have excellence is refused water and antifouling property.
Technical scheme of the present invention:
Fabric three-proof finishing agent, comprise the following raw material according to mass fraction meter: octadecyl phenol 10-18 part, fluoroalkylpolysiloxane 8-13 part, carboxymethyl cellulose 5-8 part, pollopas 2-8 part, glycerol 30-40 part, spices 0.5-1 part, wherein, fluoroalkylpolysiloxane is that raw material is synthetic by perfluoro caprylic acid and amido silicon oil.
Described fabric three-proof finishing agent, comprise the following raw material according to mass fraction meter: 13 parts, octadecyl phenol, 10 parts of fluoroalkylpolysiloxanes, 6 parts of carboxymethyl celluloses, 6 parts of pollopass, 35 parts of glycerol, 0.66 part of spices, wherein, fluoroalkylpolysiloxane is that raw material is synthetic by perfluoro caprylic acid and amido silicon oil.
Described spices is lemon or lavender essential oil.
Each raw material mixing and stirring is got final product to obtain to fabric three-proof finishing agent of the present invention.
Beneficial effect: fabric three-proof finishing agent of the present invention can make fabric have good water and oil repellant and antifouling property, washes 30 times, and fabric water repellency still can keep more than 90%; Preparation method of the present invention is simple, can wide popularization and application.
the specific embodiment
Below in conjunction with embodiment, the present invention is described in further detail.
Embodiment 1
Fabric three-proof finishing agent, comprise the following raw material according to mass fraction meter: 10 parts, octadecyl phenol, 8 parts of fluoroalkylpolysiloxanes, 5 parts of carboxymethyl celluloses, 2 parts of pollopass, 30 parts of glycerol, 0.5 part of lemon, wherein, fluoroalkylpolysiloxane is that raw material is synthetic by perfluoro caprylic acid and amido silicon oil.
Embodiment 2
Fabric three-proof finishing agent, comprise the following raw material according to mass fraction meter: 18 parts, octadecyl phenol, 13 parts of fluoroalkylpolysiloxanes, 8 parts of carboxymethyl celluloses, 8 parts of pollopass, 40 parts of glycerol, 1 part of lavender essential oil, wherein, fluoroalkylpolysiloxane is that raw material is synthetic by perfluoro caprylic acid and amido silicon oil.
Embodiment 3
Fabric three-proof finishing agent, comprise the following raw material according to mass fraction meter: 13 parts, octadecyl phenol, 10 parts of fluoroalkylpolysiloxanes, 6 parts of carboxymethyl celluloses, 6 parts of pollopass, 35 parts of glycerol, 0.66 part of lemon, wherein, fluoroalkylpolysiloxane is that raw material is synthetic by perfluoro caprylic acid and amido silicon oil.
Each raw material mixing and stirring is got final product to obtain to fabric three-proof finishing agent of the present invention.
Fabric three-proof finishing agent of the present invention is carried out to performance test, and WATER REPELLENCY is carried out according to GB/T14577-93 standard, the results are shown in Table 1:
Table 1 performance test data
| Washing times | Embodiment 1 | Embodiment 2 | Embodiment 3 |
| 10 | 98 | 98 | 97 |
| 20 | 90 | 93 | 90 |
| 30 | 91 | 93 | 92 |
As seen from the above table, finishing agent of the present invention is given the waterproof WATER REPELLENCY of fabric excellence, while washing 30 times, still has good WATER REPELLENCY.
Claims (3)
1. fabric three-proof finishing agent, it is characterized in that, comprise the following raw material according to mass fraction meter: octadecyl phenol 10-18 part, fluoroalkylpolysiloxane 8-13 part, carboxymethyl cellulose 5-8 part, pollopas 2-8 part, glycerol 30-40 part, spices 0.5-1 part, wherein, fluoroalkylpolysiloxane is that raw material is synthetic by perfluoro caprylic acid and amido silicon oil.
2. fabric three-proof finishing agent as claimed in claim 1, it is characterized in that, comprise the following raw material according to mass fraction meter: 13 parts, octadecyl phenol, 10 parts of fluoroalkylpolysiloxanes, 6 parts of carboxymethyl celluloses, 6 parts of pollopass, 35 parts of glycerol, 0.66 part of spices, wherein, fluoroalkylpolysiloxane is that raw material is synthetic by perfluoro caprylic acid and amido silicon oil.
3. fabric three-proof finishing agent as claimed in claim 1, is characterized in that, described spices is lemon or lavender essential oil.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310615646.6A CN103668948A (en) | 2013-11-28 | 2013-11-28 | Three-proofing finishing agent for fabric |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310615646.6A CN103668948A (en) | 2013-11-28 | 2013-11-28 | Three-proofing finishing agent for fabric |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN103668948A true CN103668948A (en) | 2014-03-26 |
Family
ID=50307670
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201310615646.6A Withdrawn CN103668948A (en) | 2013-11-28 | 2013-11-28 | Three-proofing finishing agent for fabric |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN103668948A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104250930A (en) * | 2014-09-25 | 2014-12-31 | 苏州印丝特纺织数码科技有限公司 | Silk fabric acid-resistant finishing agent and preparation method thereof |
| CN112267299A (en) * | 2020-09-23 | 2021-01-26 | 浙江桐星纺织科技发展股份有限公司 | Production process of three-proofing soil-release fabric |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP1088873A1 (en) * | 1999-03-29 | 2001-04-04 | Asahi Glass Company Ltd. | Water-dispersible water-and-oil repellant composition |
| CN101016697A (en) * | 2007-02-15 | 2007-08-15 | 浙江工业大学 | Method of preparing fluorine and silicon containing hydrophobic and oil repellent fabric finishing agent |
| CN101435160A (en) * | 2008-12-18 | 2009-05-20 | 浙江闰土股份有限公司 | A kind of organosilicon-fluorine multifunctional fabric finishing agent and preparation method thereof |
| CN101760967A (en) * | 2008-11-14 | 2010-06-30 | 杨玉生 | Waterproof and oilproof finishing agent for fabric and leather and preparation thereof |
-
2013
- 2013-11-28 CN CN201310615646.6A patent/CN103668948A/en not_active Withdrawn
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP1088873A1 (en) * | 1999-03-29 | 2001-04-04 | Asahi Glass Company Ltd. | Water-dispersible water-and-oil repellant composition |
| CN101016697A (en) * | 2007-02-15 | 2007-08-15 | 浙江工业大学 | Method of preparing fluorine and silicon containing hydrophobic and oil repellent fabric finishing agent |
| CN101760967A (en) * | 2008-11-14 | 2010-06-30 | 杨玉生 | Waterproof and oilproof finishing agent for fabric and leather and preparation thereof |
| CN101435160A (en) * | 2008-12-18 | 2009-05-20 | 浙江闰土股份有限公司 | A kind of organosilicon-fluorine multifunctional fabric finishing agent and preparation method thereof |
Non-Patent Citations (3)
| Title |
|---|
| 商品学教材编写组: "《商品学》", 28 February 1981, article "《商品学》", pages: 176 * |
| 李媛媛等: "氟烷基聚硅氧烷防水防油剂的制备与性能研究", 《化工新型材料》, vol. 34, no. 06, 30 June 2006 (2006-06-30) * |
| 沈一丁: "《轻化工助剂》", 31 July 2004, article "《轻化工助剂》", pages: 326-328 * |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104250930A (en) * | 2014-09-25 | 2014-12-31 | 苏州印丝特纺织数码科技有限公司 | Silk fabric acid-resistant finishing agent and preparation method thereof |
| CN112267299A (en) * | 2020-09-23 | 2021-01-26 | 浙江桐星纺织科技发展股份有限公司 | Production process of three-proofing soil-release fabric |
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| PB01 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C04 | Withdrawal of patent application after publication (patent law 2001) | ||
| WW01 | Invention patent application withdrawn after publication |
Application publication date: 20140326 |