CN1031858C - Preparation method of herba Humuli Scandentis extract - Google Patents
Preparation method of herba Humuli Scandentis extract Download PDFInfo
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- CN1031858C CN1031858C CN93111003A CN93111003A CN1031858C CN 1031858 C CN1031858 C CN 1031858C CN 93111003 A CN93111003 A CN 93111003A CN 93111003 A CN93111003 A CN 93111003A CN 1031858 C CN1031858 C CN 1031858C
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- extract
- humulus grass
- leaf
- humuli scandentis
- herba humuli
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- 239000000284 extract Substances 0.000 title claims abstract description 33
- 238000002360 preparation method Methods 0.000 title claims description 11
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims abstract description 20
- 238000000605 extraction Methods 0.000 claims abstract description 8
- 238000002156 mixing Methods 0.000 claims abstract description 5
- 239000007864 aqueous solution Substances 0.000 claims abstract description 3
- 238000004945 emulsification Methods 0.000 claims abstract description 3
- 238000001914 filtration Methods 0.000 claims abstract 2
- 244000025254 Cannabis sativa Species 0.000 claims description 15
- 241000218228 Humulus Species 0.000 claims description 15
- 229920000742 Cotton Polymers 0.000 claims description 6
- 238000005516 engineering process Methods 0.000 claims description 5
- 238000010438 heat treatment Methods 0.000 claims description 5
- 239000000843 powder Substances 0.000 claims description 5
- 238000010298 pulverizing process Methods 0.000 claims description 5
- 238000011109 contamination Methods 0.000 claims description 3
- 239000008367 deionised water Substances 0.000 claims description 3
- 229910021641 deionized water Inorganic materials 0.000 claims description 3
- 239000000839 emulsion Substances 0.000 claims description 3
- 238000001704 evaporation Methods 0.000 claims description 3
- 230000008020 evaporation Effects 0.000 claims description 3
- 239000004744 fabric Substances 0.000 claims description 3
- 229910001220 stainless steel Inorganic materials 0.000 claims description 3
- 239000010935 stainless steel Substances 0.000 claims description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 3
- 238000009941 weaving Methods 0.000 claims description 3
- 238000004140 cleaning Methods 0.000 claims description 2
- 239000003995 emulsifying agent Substances 0.000 claims description 2
- 238000012856 packing Methods 0.000 claims description 2
- 239000002245 particle Substances 0.000 claims description 2
- 238000003756 stirring Methods 0.000 claims description 2
- 238000010257 thawing Methods 0.000 claims description 2
- 235000013305 food Nutrition 0.000 abstract description 7
- 230000036541 health Effects 0.000 abstract description 6
- 238000000034 method Methods 0.000 abstract description 5
- 235000013361 beverage Nutrition 0.000 abstract description 4
- 235000016709 nutrition Nutrition 0.000 abstract description 4
- 241000196324 Embryophyta Species 0.000 abstract description 3
- 230000035764 nutrition Effects 0.000 abstract description 3
- 230000008569 process Effects 0.000 abstract description 3
- 241000218229 Humulus japonicus Species 0.000 abstract description 2
- 239000002994 raw material Substances 0.000 abstract description 2
- 239000000419 plant extract Substances 0.000 abstract 1
- 235000001014 amino acid Nutrition 0.000 description 7
- 229940024606 amino acid Drugs 0.000 description 7
- 150000001413 amino acids Chemical class 0.000 description 7
- 239000003814 drug Substances 0.000 description 4
- GAMYVSCDDLXAQW-AOIWZFSPSA-N Thermopsosid Natural products O(C)c1c(O)ccc(C=2Oc3c(c(O)cc(O[C@H]4[C@H](O)[C@@H](O)[C@H](O)[C@H](CO)O4)c3)C(=O)C=2)c1 GAMYVSCDDLXAQW-AOIWZFSPSA-N 0.000 description 3
- 229930003944 flavone Natural products 0.000 description 3
- 235000011949 flavones Nutrition 0.000 description 3
- VHBFFQKBGNRLFZ-UHFFFAOYSA-N vitamin p Natural products O1C2=CC=CC=C2C(=O)C=C1C1=CC=CC=C1 VHBFFQKBGNRLFZ-UHFFFAOYSA-N 0.000 description 3
- 239000000341 volatile oil Substances 0.000 description 3
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 2
- DHMQDGOQFOQNFH-UHFFFAOYSA-N Glycine Chemical compound NCC(O)=O DHMQDGOQFOQNFH-UHFFFAOYSA-N 0.000 description 2
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 2
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- 229930195729 fatty acid Natural products 0.000 description 2
- 239000000194 fatty acid Substances 0.000 description 2
- -1 flavone compound Chemical class 0.000 description 2
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- 235000019634 flavors Nutrition 0.000 description 2
- 235000013312 flour Nutrition 0.000 description 2
- 239000003205 fragrance Substances 0.000 description 2
- 235000015243 ice cream Nutrition 0.000 description 2
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- 239000011573 trace mineral Substances 0.000 description 2
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- 238000005303 weighing Methods 0.000 description 2
- BMGWZHWESYHXHC-UHFFFAOYSA-N 2-amino-3-methylpentanoic acid;2-amino-4-methylpentanoic acid Chemical compound CCC(C)C(N)C(O)=O.CC(C)CC(N)C(O)=O BMGWZHWESYHXHC-UHFFFAOYSA-N 0.000 description 1
- LQJAALCCPOTJGB-YUMQZZPRSA-N Arg-Pro Chemical compound NC(N)=NCCC[C@H](N)C(=O)N1CCC[C@H]1C(O)=O LQJAALCCPOTJGB-YUMQZZPRSA-N 0.000 description 1
- VYZAMTAEIAYCRO-UHFFFAOYSA-N Chromium Chemical compound [Cr] VYZAMTAEIAYCRO-UHFFFAOYSA-N 0.000 description 1
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 1
- WHUUTDBJXJRKMK-UHFFFAOYSA-N Glutamic acid Natural products OC(=O)C(N)CCC(O)=O WHUUTDBJXJRKMK-UHFFFAOYSA-N 0.000 description 1
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerol Natural products OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 1
- 239000004471 Glycine Substances 0.000 description 1
- QNAYBMKLOCPYGJ-REOHCLBHSA-N L-alanine Chemical compound C[C@H](N)C(O)=O QNAYBMKLOCPYGJ-REOHCLBHSA-N 0.000 description 1
- CKLJMWTZIZZHCS-REOHCLBHSA-N L-aspartic acid Chemical compound OC(=O)[C@@H](N)CC(O)=O CKLJMWTZIZZHCS-REOHCLBHSA-N 0.000 description 1
- LEVWYRKDKASIDU-IMJSIDKUSA-N L-cystine Chemical compound [O-]C(=O)[C@@H]([NH3+])CSSC[C@H]([NH3+])C([O-])=O LEVWYRKDKASIDU-IMJSIDKUSA-N 0.000 description 1
- FFEARJCKVFRZRR-BYPYZUCNSA-N L-methionine Chemical compound CSCC[C@H](N)C(O)=O FFEARJCKVFRZRR-BYPYZUCNSA-N 0.000 description 1
- COLNVLDHVKWLRT-QMMMGPOBSA-N L-phenylalanine Chemical compound OC(=O)[C@@H](N)CC1=CC=CC=C1 COLNVLDHVKWLRT-QMMMGPOBSA-N 0.000 description 1
- OUYCCCASQSFEME-QMMMGPOBSA-N L-tyrosine Chemical compound OC(=O)[C@@H](N)CC1=CC=C(O)C=C1 OUYCCCASQSFEME-QMMMGPOBSA-N 0.000 description 1
- KZSNJWFQEVHDMF-BYPYZUCNSA-N L-valine Chemical compound CC(C)[C@H](N)C(O)=O KZSNJWFQEVHDMF-BYPYZUCNSA-N 0.000 description 1
- KDXKERNSBIXSRK-UHFFFAOYSA-N Lysine Natural products NCCCCC(N)C(O)=O KDXKERNSBIXSRK-UHFFFAOYSA-N 0.000 description 1
- 239000004472 Lysine Substances 0.000 description 1
- PWHULOQIROXLJO-UHFFFAOYSA-N Manganese Chemical compound [Mn] PWHULOQIROXLJO-UHFFFAOYSA-N 0.000 description 1
- 241000218231 Moraceae Species 0.000 description 1
- MTCFGRXMJLQNBG-UHFFFAOYSA-N Serine Natural products OCC(N)C(O)=O MTCFGRXMJLQNBG-UHFFFAOYSA-N 0.000 description 1
- 244000228451 Stevia rebaudiana Species 0.000 description 1
- 235000006092 Stevia rebaudiana Nutrition 0.000 description 1
- AYFVYJQAPQTCCC-UHFFFAOYSA-N Threonine Natural products CC(O)C(N)C(O)=O AYFVYJQAPQTCCC-UHFFFAOYSA-N 0.000 description 1
- 239000004473 Threonine Substances 0.000 description 1
- 241000209140 Triticum Species 0.000 description 1
- 235000021307 Triticum Nutrition 0.000 description 1
- KZSNJWFQEVHDMF-UHFFFAOYSA-N Valine Natural products CC(C)C(N)C(O)=O KZSNJWFQEVHDMF-UHFFFAOYSA-N 0.000 description 1
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 description 1
- 239000004480 active ingredient Substances 0.000 description 1
- 235000004279 alanine Nutrition 0.000 description 1
- 229910021529 ammonia Inorganic materials 0.000 description 1
- 230000003026 anti-oxygenic effect Effects 0.000 description 1
- 235000019789 appetite Nutrition 0.000 description 1
- 230000036528 appetite Effects 0.000 description 1
- 230000003833 cell viability Effects 0.000 description 1
- 229910052804 chromium Inorganic materials 0.000 description 1
- 239000011651 chromium Substances 0.000 description 1
- 239000000470 constituent Substances 0.000 description 1
- 229910052802 copper Inorganic materials 0.000 description 1
- 239000010949 copper Substances 0.000 description 1
- 229960003067 cystine Drugs 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000000151 deposition Methods 0.000 description 1
- 238000001514 detection method Methods 0.000 description 1
- 235000005911 diet Nutrition 0.000 description 1
- 230000037213 diet Effects 0.000 description 1
- 201000010099 disease Diseases 0.000 description 1
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 150000004665 fatty acids Chemical class 0.000 description 1
- 235000012041 food component Nutrition 0.000 description 1
- 235000011389 fruit/vegetable juice Nutrition 0.000 description 1
- 235000013922 glutamic acid Nutrition 0.000 description 1
- 239000004220 glutamic acid Substances 0.000 description 1
- 150000004676 glycans Chemical class 0.000 description 1
- 235000011187 glycerol Nutrition 0.000 description 1
- 239000004519 grease Substances 0.000 description 1
- 230000008821 health effect Effects 0.000 description 1
- HNDVDQJCIGZPNO-UHFFFAOYSA-N histidine Natural products OC(=O)C(N)CC1=CN=CN1 HNDVDQJCIGZPNO-UHFFFAOYSA-N 0.000 description 1
- 230000036737 immune function Effects 0.000 description 1
- 229910052742 iron Inorganic materials 0.000 description 1
- 229910052748 manganese Inorganic materials 0.000 description 1
- 239000011572 manganese Substances 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000002398 materia medica Substances 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 230000004060 metabolic process Effects 0.000 description 1
- 229930182817 methionine Natural products 0.000 description 1
- 235000013336 milk Nutrition 0.000 description 1
- 239000008267 milk Substances 0.000 description 1
- 210000004080 milk Anatomy 0.000 description 1
- 231100000957 no side effect Toxicity 0.000 description 1
- 235000003170 nutritional factors Nutrition 0.000 description 1
- COLNVLDHVKWLRT-UHFFFAOYSA-N phenylalanine Natural products OC(=O)C(N)CC1=CC=CC=C1 COLNVLDHVKWLRT-UHFFFAOYSA-N 0.000 description 1
- 230000035790 physiological processes and functions Effects 0.000 description 1
- 229920001282 polysaccharide Polymers 0.000 description 1
- 239000005017 polysaccharide Substances 0.000 description 1
- 229930188195 rebaudioside Natural products 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 238000000638 solvent extraction Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 235000019605 sweet taste sensations Nutrition 0.000 description 1
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- 239000011701 zinc Substances 0.000 description 1
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- Coloring Foods And Improving Nutritive Qualities (AREA)
- Medicines Containing Plant Substances (AREA)
- Non-Alcoholic Beverages (AREA)
Abstract
The invention relates to a method for preparing extracts of herbaceous plants, which takes natural herbaceous plant humulus scandens as raw materials, and the extracts are prepared by the processes of crushing, aqueous solution extraction, ether extraction, emulsification, mixing, filtration to finished products and the like, and are mixed according to a certain proportion and added into various foods and beverages to increase nutrition, treat and protect health, thereby providing a low-cost, delicious, and easily digested and absorbed nutritional health natural plant extract for the life of people.
Description
The invention belongs to herbal method for preparing extractive, particularly a kind of grass is got the thing preparation method.
Humulus grass [Humulus Scandens (lour) Merr] (seeing version " Chinese medicine voluminous dictionary " in 1986 the volume two P2313 of Shanghai science tech publishing house page or leaf) belongs to moraceae plants, is annual or perennial climing property draft wild plant.It is vegetables with the humulus grass that the people is often arranged in the rural area, or be used for preventing and treating some disease, have the effect that medicine food has both, all put down in writing to some extent in medical literature in ancient times " not record ", the Compendium of Material Medica, can promote metabolism into body, health care is good for one's health.Traditional usage, it is back broken that the humulus grass is dried in the shade, and decoction is taken, and destroys its nutrition and active ingredient, influences medicine, edibility, makes human nutrition out of proportion.
The objective of the invention is to overcome above technical deficiency, and a kind of flavone compound that contains is provided, the Herba humuli scandentis extract preparation method of multiple nutritional components such as trace element, amino acid replenishes the necessary nutritional factors of human body.
The present invention is achieved in that getting flower humulus grass blade, leaf in earlier stage dries in the shade removal of contamination; After the cleaning, crusher in crushing, length 1-2cm, the cotton of packing into the bag of weaving cotton cloth is tightened sack, drop in the deionized water of pH=7-8, bath raio 1: 50, heating is extracted in the stainless steel jacketed pan, in 20 minutes temperature rise 90-95 ℃, time 0.5-1 hour, water-soluble extract; With humulus grass blade, the leaf 40 order powder after pulverizing, soak ether in airtight container in 1: 2 ratio, stirred 1 time in 0.5 hour at interval, the heating evaporation ether gets the oily extract after 10 hours; Water-soluble extract and oily extract are put into container, add while stirring, emulsifying agent HLB=3-9, addition is 0.1%, heats 80 ℃ of thawings, time 3-5 minute, get emulsion, add the extract mixing, be filtered to finished product.
Prove after testing, use in the Herba humuli scandentis extract of the present invention's preparation, general flavone content is 0.14% (gram/gram), and polyoses content is 4.86%, volatile oil content is 0.088%, contain 17 seed amino acids and various trace elements, have no side effect, can add in every way in food, the beverage meals and enjoy for human body, regulate human physiological functions, strengthen immunologic function and cell viability, absorb the human body meals effectively and reasonably, reach therapeuticing and health effect.
Specify with by way of example below in conjunction with accompanying drawing.
Fig. 1 shows careless extract preparation technology flow chart.
This preparation technology flow process, earlier with humulus grass blade, leaf collection, through wash, dry in the shade, pulverizing, extraction with aqueous solution, extracted with diethyl ether, emulsification then mixes, and is filtered to finished product.
Embodiment
Getting flower humulus grass blade, leaf in earlier stage dries in the shade, removal of contamination, clean, two kinds in breaking length 1-2cm particle diameter, 40 order powder, the broken cauline leaf of weighing 10kgl-2cm are put into the cotton bag of weaving cotton cloth, tighten in the deionized water that sack drops into pH=7-8; bath raio 1: 50, heating is extracted in the stainless steel jacketed pan, in 20 minutes temperature rise 90-95 ℃; time 0.5-1 hour, the water-soluble extract of 400kg; Take by weighing humulus grass 40 order powder 10kg, extraction in the airtight container during the 20kg ether soaks was stirred 1 time at interval in 0.5 hour, and the evaporation ether is carried the oily extract after 10 hours; With the multitudinous sugar fatty acid of 1ml glycerine fatty acid and 1ml, HLB=3-9, addition is 0.1%, add in the grease of extraction 80 ℃ of temperature, time 3-5 minute, vibration evenly adds the water-soluble extract of 400kg, mixing, adopt the G4 pan to filter, is standard with pure, manufactured goods 400kg, the pH value is 8.0-8.5, is pale brown look, translucent Herba humuli scandentis extract.
Detection through college of traditional Chinese medicine institute of Chinese materia medica, Liaoning Province
Table 1 humulus grass active constituent content measuring
General flavone content 0.14% (gram/gram)
Polysaccharide 4.86%
Volatile oil 0.088%
The first rope mg/kg of trace
Zinc 16.9
Copper 178.0
Iron 28.0
Manganese 43.5
Chromium 82.5
Table 2 humulus grass amino acid content is measured 17 seed amino acids
| The amino acid name | Asparatate | Threonine | Serine | Glutamic acid | Glycine | Alanine |
| Content % | ????1.54 | ??0.49 | ??0.53 | ??1.30 | ??0.58 | ??0.66 |
| The amino acid name | Valine | Methionine | Isoleucine | Leucine | Tyrosine | Phenylalanine |
| Content % | ?0.68 | ??0.10 | ??0.59 | ??0.90 | ??0.24 | ??0.58 |
| The amino acid name | Lysine | Ammonia | Histidine | Arginine | Proline | Cystine |
| Content % | ?0.69 | ?0.39 | ??0.18 | ??0.57 | ??0.39 | Do not detect |
Process characteristic of the present invention:
1, extract does not add chemical substance;
2, the water-soluble extraction of extract, the volatile oil solvent extraction;
3, antioxygenic property is good.
Use Herba humuli scandentis extract to add various food, have additional nutrients, improve various flavours in food products, and with health role.
1, careless extract ice-cream stick
Prescription: Herba humuli scandentis extract 3.75kg, STEVIA REBAUDIANA 7.15kg, flour 147g, milk 115g is processed into 72 ice-cream sticks.
Food back sugariness is moderate, pure good to eat, and the delicate fragrance pleasant impression is long, tasty and refreshing not puckery tooth, slightly slight Radix Glycyrrhizae flavor.
2, Herba humuli scandentis extract drink formula: Herba humuli scandentis extract 50kg, rebaudioside 25g mixes at 40 ℃, makes beverage.
Sweet taste is pure, and delicate fragrance is good to eat, is even pale brown look, 36 ℃ of following insolation a few hours nondiscolourings, no flocculent deposit in depositing.
3, Herba humuli scandentis extract vermicelli
Prescription: Herba humuli scandentis extract 1kg, superior wheat flour 5kg, edible refined salt 10g makes vermicelli through the oven dry of compressing tablet slitting.
Edible this remedy diet helps digest, and whets the appetite.The present invention is a raw material with the natural herb plant, is equipped with suitable technology preparation, and technology is reasonable, convenient feasible, be easy to realize suitability for industrialized production, the Herba humuli scandentis extract of preparation can add in various food, the beverage, have additional nutrients, treatment and health is for people's life provides a kind of popular edible extract.
Claims (1)
1, Herba humuli scandentis extract preparation method is characterized in that Herba humuli scandentis extract preparation finished by following technology;
A, collection
Get flower humulus grass blade, leaf in earlier stage and dry in the shade removal of contamination;
B, pulverizing
With humulus grass blade, the leaf crusher in crushing after cleaning, long 1-2cm, particle diameter 40 order powder;
C, extraction
(1) extraction with aqueous solution
With the cotton bag of weaving cotton cloth of packing into of the humulus grass after pulverizing, tighten sack, drop in the deionized water of pH=7-8, bath raio 1: 50, heating is extracted in the stainless steel jacketed pan, in 20 minutes temperature rise 90-95 ℃, time 0.5-1 hour, water-soluble extract;
(2) extracted with diethyl ether
With humulus grass blade, the leaf 40 order powder after pulverizing, soak ether in airtight container in 1: 2 ratio, stirred 1 time in 0.5 hour at interval, the heating evaporation ether gets the oily extract after 10 hours;
D, emulsification
Above-mentioned oily extract and water-soluble extract are put into container, add while stirring, emulsifying agent HLB=3-9, addition is 0.1%, heats 80 ℃ of thawings, time 3-5 minute, gets emulsion;
E, mixing
Emulsion is added the extract mixing;
F, be filtered to finished product
Filtering with the G4 pan, is the metric system finished product with pure.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN93111003A CN1031858C (en) | 1993-03-26 | 1993-03-26 | Preparation method of herba Humuli Scandentis extract |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN93111003A CN1031858C (en) | 1993-03-26 | 1993-03-26 | Preparation method of herba Humuli Scandentis extract |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN1079623A CN1079623A (en) | 1993-12-22 |
| CN1031858C true CN1031858C (en) | 1996-05-29 |
Family
ID=4988814
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN93111003A Expired - Fee Related CN1031858C (en) | 1993-03-26 | 1993-03-26 | Preparation method of herba Humuli Scandentis extract |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN1031858C (en) |
Families Citing this family (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101690587B (en) * | 2007-01-16 | 2012-10-03 | 李明 | Humulus scandens (Lour.)Merr health-care pastries |
| CN101904902B (en) * | 2010-07-29 | 2011-11-02 | 郑州牧业工程高等专科学校 | Immunity enhancement taking Japanese hop as main formula |
| CN105918604A (en) * | 2016-05-21 | 2016-09-07 | 徐静 | Humulus scandens ice-cream stick and processing technology thereof |
| CN105994928A (en) * | 2016-05-21 | 2016-10-12 | 徐静 | Humulus ice cream and processing method thereof |
| CN106360226A (en) * | 2016-10-24 | 2017-02-01 | 牛保仁 | Humulus scandens vinegar drink |
| CN107048099A (en) * | 2017-06-23 | 2017-08-18 | 深圳市富炜城投资有限公司 | A kind of prawn feed with immunomodulator and preparation method thereof |
-
1993
- 1993-03-26 CN CN93111003A patent/CN1031858C/en not_active Expired - Fee Related
Also Published As
| Publication number | Publication date |
|---|---|
| CN1079623A (en) | 1993-12-22 |
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