CN102962006A - Granulating process of isomaltulose - Google Patents
Granulating process of isomaltulose Download PDFInfo
- Publication number
- CN102962006A CN102962006A CN201210517018XA CN201210517018A CN102962006A CN 102962006 A CN102962006 A CN 102962006A CN 201210517018X A CN201210517018X A CN 201210517018XA CN 201210517018 A CN201210517018 A CN 201210517018A CN 102962006 A CN102962006 A CN 102962006A
- Authority
- CN
- China
- Prior art keywords
- isomalt
- granules
- isomaltulose
- powder
- concentrated solution
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 238000000034 method Methods 0.000 title abstract description 7
- PVXPPJIGRGXGCY-TZLCEDOOSA-N 6-O-alpha-D-glucopyranosyl-D-fructofuranose Chemical compound O[C@@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@@H]1OC[C@@H]1[C@@H](O)[C@H](O)C(O)(CO)O1 PVXPPJIGRGXGCY-TZLCEDOOSA-N 0.000 title abstract 6
- 239000008187 granular material Substances 0.000 claims abstract description 10
- 239000000843 powder Substances 0.000 claims abstract description 10
- 238000002156 mixing Methods 0.000 claims abstract description 8
- 238000003756 stirring Methods 0.000 claims abstract description 8
- 230000032683 aging Effects 0.000 claims abstract description 7
- 239000000463 material Substances 0.000 claims abstract description 6
- SERLAGPUMNYUCK-DCUALPFSSA-N 1-O-alpha-D-glucopyranosyl-D-mannitol Chemical compound OC[C@@H](O)[C@@H](O)[C@H](O)[C@H](O)CO[C@H]1O[C@H](CO)[C@@H](O)[C@H](O)[C@H]1O SERLAGPUMNYUCK-DCUALPFSSA-N 0.000 claims description 20
- 235000010439 isomalt Nutrition 0.000 claims description 20
- 239000000905 isomalt Substances 0.000 claims description 20
- HPIGCVXMBGOWTF-UHFFFAOYSA-N isomaltol Natural products CC(=O)C=1OC=CC=1O HPIGCVXMBGOWTF-UHFFFAOYSA-N 0.000 claims description 20
- 239000002245 particle Substances 0.000 claims description 10
- 238000005469 granulation Methods 0.000 claims description 6
- 230000003179 granulation Effects 0.000 claims description 6
- 238000007599 discharging Methods 0.000 claims description 3
- 239000007787 solid Substances 0.000 claims description 3
- 235000020985 whole grains Nutrition 0.000 claims description 3
- 238000001816 cooling Methods 0.000 abstract 1
- 238000010008 shearing Methods 0.000 abstract 1
- 238000009736 wetting Methods 0.000 abstract 1
- 238000002425 crystallisation Methods 0.000 description 3
- 230000008025 crystallization Effects 0.000 description 3
- 235000011868 grain product Nutrition 0.000 description 2
- 238000010521 absorption reaction Methods 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 235000013379 molasses Nutrition 0.000 description 1
- 239000012452 mother liquor Substances 0.000 description 1
- 238000012216 screening Methods 0.000 description 1
- 239000012798 spherical particle Substances 0.000 description 1
- 239000007921 spray Substances 0.000 description 1
Landscapes
- Glanulating (AREA)
Abstract
The invention relates to a granulating process of isomaltulose. The process comprises the following steps of: A. mixing: adding a concentrated solution of the isomaltulose slowly into dispersed isomaltulose powder, mixing the powder and the solution fully, and controlling the temperature of the concentrated solution of the isomaltulose to be 100 DEG C-120 DEG C; B. granulating and straightening granules: wetting mixed powder-shaped materials gradually, smashing the materials fully into granules through stirring and shearing effects, so that wet granules with fixed sizes and stable spherical shapes are formed, and meanwhile eddy current generated in high-speed rotation enables the granules to be collided, extruded and abraded mutually, and the granules are much uniform and fine; and C. aging: guiding wet granules into another device with stirring, introducing hot air, controlling the temperature to be 60 DEG C-90 DEG C, aging for 2-4 hours, and cooling down to 30 DEG C below. According to the invention, hard isomaltulose granules with compact structures can be obtained, have good mobility, are low hygroscopicity and high in storage stability, and have much good economical value.
Description
Technical field
The present invention relates to a kind of prilling of isomalt.
Background technology
At present, the curing process of isomalt, the one, obtain crystal product by decrease temperature crystalline, but crystallization processes can produce a large amount of mother liquor (molasses), these mother liquors are difficult to carry out crystallization again, so be disadvantageous economically; The 2nd, obtain powder product by drying process with atomizing, and the powder product flowability is relatively poor, is unfavorable for the processing of some process; The 3rd, the method for molten atomizing granulation is not then utilized the crystallization of grain products, and what often obtain is the glassy state material, easily moisture absorption, and fusing point is low.
Summary of the invention
The objective of the invention is the deficiency for prior art, provide to have good fluidity, hygroscopicity is little, the prilling of a kind of isomalt that storage stability is high.
The technical scheme that the present invention takes is: a kind of prilling of isomalt, it is characterized in that it comprises the following steps: A, mix: with purity the isomalt powder more than 98% and solid content be more than 90% and purity in the isomalt concentrated solution more than 98%, 1～3 ︰ 1 is fed in the Granulation Equipments in mass ratio, wherein the isomalt concentrated solution is slowly to join in the isomalt powder that has disperseed, powder and solution are fully mixed, and the temperature of isomalt concentrated solution is controlled at 100 ℃～120 ℃; B, granulation and whole grain: after the mixing, granular material is moistening gradually, through stirring and shear action, make material fully be broken into particle, form the wet granular of a certain size stable ball-type, the eddy current that produces in high speed rotating simultaneously produces mutually collision, extruding and friction in the middle of making particle, makes particle more even, careful; C, aging: the wet granular that obtains is imported in the equipment of another band stirring, pass into hot blast, the control temperature wore out 2～4 hours at 60 ℃～90 ℃, was cooled to below 30 ℃, and discharging namely obtains finished product.
Adopt the present invention, can obtain the hard isomalt particle of compact structure, its good fluidity, hygroscopicity is little, and storage stability is high, has good economic worth.
The specific embodiment,
The invention will be further described below in conjunction with embodiment.It comprises the following steps:
One, in mixing and blending machine, adds purity at 98% above 5kg powdery isomalt, stirring
Effect is lower disperse fully after, slowly spray into temperature at 100 ℃～120 ℃, solid content be more than 90%, purity is at the isomalt fused solution 4kg more than 98%;
Two, granulation and whole grain: after the mixing, granular material is moistening gradually, through stirring and shear action, makes
Material fully is broken into particle, forms the wet granular of a certain size stable spherical particles, and the eddy current that produces in high speed rotating simultaneously produces mutually collision, extruding and friction in the middle of making particle, obtains even, careful wet granular;
Three, will obtain the isomalt wet granular and be transported in the aging equipment, logical hot blast control aging temperature is 60 ℃～90 ℃, ageing time 2～4 hours, and then logical cold wind is down to below 30 ℃, discharging, screening obtains the grain products that particle size range is 1～6mm.
Claims (1)
1. the prilling of an isomalt, it is characterized in that it comprises the following steps: A, mixing: with purity the isomalt powder more than 98% and solid content be more than 90% and purity in the isomalt concentrated solution more than 98%, 1～3 ︰ 1 is fed in the Granulation Equipments in mass ratio, wherein the isomalt concentrated solution is slowly to join in the isomalt powder that has disperseed, powder and solution are fully mixed, and the temperature of isomalt concentrated solution is controlled at 100 ℃～120 ℃; B, granulation and whole grain: after the mixing, granular material is moistening gradually, through stirring and shear action, make material fully be broken into particle, form the wet granular of a certain size stable ball-type, the eddy current that produces in high speed rotating simultaneously produces mutually collision, extruding and friction in the middle of making particle, makes particle more even, careful; C, aging: the wet granular that obtains is imported in the equipment of another band stirring, pass into hot blast, the control temperature wore out 2～4 hours at 60 ℃～90 ℃, was cooled to below 30 ℃, and discharging namely obtains finished product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201210517018XA CN102962006A (en) | 2012-12-06 | 2012-12-06 | Granulating process of isomaltulose |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201210517018XA CN102962006A (en) | 2012-12-06 | 2012-12-06 | Granulating process of isomaltulose |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN102962006A true CN102962006A (en) | 2013-03-13 |
Family
ID=47792610
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201210517018XA Pending CN102962006A (en) | 2012-12-06 | 2012-12-06 | Granulating process of isomaltulose |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN102962006A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109608509A (en) * | 2018-12-10 | 2019-04-12 | 浙江华康药业股份有限公司 | A kind of continuous preparation method of graininess isomalt |
| CN119344438A (en) * | 2024-12-23 | 2025-01-24 | 山东百龙创园生物科技股份有限公司 | Isomalt granules and preparation method thereof |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20080050605A1 (en) * | 2004-10-15 | 2008-02-28 | Rapp Knut M | Pan Coating Process |
| CN101747389A (en) * | 2008-12-03 | 2010-06-23 | 山东福田投资有限公司 | Method for preparing powder crystal maltitol |
| CN101869236A (en) * | 2010-06-09 | 2010-10-27 | 山东福田药业有限公司 | Xylitol particles capable of being directly pressed into tablets and preparation method thereof |
-
2012
- 2012-12-06 CN CN201210517018XA patent/CN102962006A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20080050605A1 (en) * | 2004-10-15 | 2008-02-28 | Rapp Knut M | Pan Coating Process |
| CN101747389A (en) * | 2008-12-03 | 2010-06-23 | 山东福田投资有限公司 | Method for preparing powder crystal maltitol |
| CN101869236A (en) * | 2010-06-09 | 2010-10-27 | 山东福田药业有限公司 | Xylitol particles capable of being directly pressed into tablets and preparation method thereof |
Non-Patent Citations (2)
| Title |
|---|
| CHRISTELLE TURCHIULI等: "Fluidised bed agglomeration: Agglomerates shape and end-use properties", 《POWDER TECHNOLOGY》, vol. 157, 23 June 2005 (2005-06-23) * |
| 苏雪梅: "异麦芽酮糖醇的生产工艺及其设备选型", 《中国调味品》, vol. 36, no. 11, 30 November 2011 (2011-11-30) * |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109608509A (en) * | 2018-12-10 | 2019-04-12 | 浙江华康药业股份有限公司 | A kind of continuous preparation method of graininess isomalt |
| CN119344438A (en) * | 2024-12-23 | 2025-01-24 | 山东百龙创园生物科技股份有限公司 | Isomalt granules and preparation method thereof |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C02 | Deemed withdrawal of patent application after publication (patent law 2001) | ||
| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20130313 |