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CN102913135A - Polycrystalline diamond compound sheet and manufacturing process thereof - Google Patents

Polycrystalline diamond compound sheet and manufacturing process thereof Download PDF

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Publication number
CN102913135A
CN102913135A CN201210462514XA CN201210462514A CN102913135A CN 102913135 A CN102913135 A CN 102913135A CN 201210462514X A CN201210462514X A CN 201210462514XA CN 201210462514 A CN201210462514 A CN 201210462514A CN 102913135 A CN102913135 A CN 102913135A
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CN
China
Prior art keywords
polycrystalline diamond
hard alloy
alloy substrate
cobalt
parts
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Pending
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CN201210462514XA
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Chinese (zh)
Inventor
王宏志
黄莹祥
黄毅
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WANLONG DIAMOND TOOLS CO Ltd
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WANLONG DIAMOND TOOLS CO Ltd
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Priority to CN201210462514XA priority Critical patent/CN102913135A/en
Publication of CN102913135A publication Critical patent/CN102913135A/en
Pending legal-status Critical Current

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Abstract

The invention discloses a polycrystalline diamond compound sheet and a manufacturing process thereof. The polycrystalline diamond compound sheet comprises a hard alloy base body, wherein a high-density polycrystalline diamond layer is compounded on the hard alloy base body; 90 to 95 parts by weight of diamond, 0.5 to 3 parts by weight of rare earth, 2 to 10 pars by weight of cobalt and 1 to 2 parts by weight of nickel are mixed; the mixed material is subjected to ultra-high-pressure high-temperature treatment; under the condition that the pressure intensity of the ultra-high-pressure high-temperature treatment is 5.6 to 7.5 Gpa, and the temperature is not less than 1,300 DEG C, the mixed material is manufactured into a semi-finished product; and the semi-finished product is compounded with the hard alloy base body to form a finished product. The polycrystalline diamond compound sheet is high in hardness, high in abrasion resistance, high in thermal stability, high in flexibility and high in cutting efficiency; the service life can be greatly prolonged; and the production cost of an enterprise is reduced.

Description

A kind of composite polycrystal-diamond and manufacture craft thereof
Technical field
The present invention relates to diamond cutting tool, refer to specifically a kind of composite polycrystal-diamond and manufacture craft thereof.
Background technology
The drill bit of making cutting edge is called diamond bit.This drill bit belongs to the integral type drill bit, and whole drill bit does not have movable component, and is relatively simple for structure, has high strength, high abrasion and shock proof ability, is one of world's drilling well eighties in 20th century three large new technologies.Find in long-term putting into practice in the manufacturing process, the existing drill bit that is made by diamond, regular because of it, touch hard material for a long time, cause its degree of wear higher, abrasion resistance is low, and operation will affect the efficient of cutting for a long time, increases cost of production.
Summary of the invention
The present invention is to provide a kind of composite polycrystal-diamond and manufacture craft thereof, its main purpose is to solve the problems referred to above that prior art exists.
Technical scheme of the present invention is as follows:
A kind of composite polycrystal-diamond includes hard alloy substrate, is compounded with one deck high density polycrystalline diamond layer on the described hard alloy substrate.
As improvement of the present invention, the contact surface of described hard alloy substrate and high density polycrystalline diamond layer is provided with the jog that cooperatively interacts.
As a further improvement on the present invention, the component of described high density polycrystalline diamond layer and mass fraction are diadust 90-95 part, rare earth 0.5-3 part, cobalt 2-10 part, nickel 1-2 part.
Further improve as of the present invention, the composition of described rare earth is a kind of or two kinds or more of in lanthanum, cerium, praseodymium, neodymium, promethium, samarium, europium, gadolinium, terbium, dysprosium, holmium, erbium, thulium, ytterbium, lutetium, scandium and the yttrium again.
A kind of manufacture craft of composite polycrystal-diamond, be diadust 90-95 part with mass fraction, rare earth 0.5-3 part, cobalt 2-10 part after nickel 1-2 part is mixed, is carried out high pressure high temperature to mixed material and is processed, the pressure that described high pressure high temperature is processed is 5.6-7.5Gpa, temperature is made semiproduct for being not less than 1300 ℃, again these semiproduct and hard alloy substrate is combined into product.
By the above-mentioned description of this invention as can be known, be compared with existing technology, the invention has the advantages that:
One, the present invention forms by high pressure high temperature take diadust as main material, and its existing adamantine abrasion resistance has again the resistance to impact of carbide alloy.
Two, the present invention has added rare earth can improve the physical and chemical performance of alloy, and improves Alloy At Room Temperature and high-temperature mechanical property, increases the toughness of product.
Three, the present invention has added cobalt, and cobalt is mainly used in producing alloy.The shear steel that contains a certain amount of cobalt can improve abrasion resistance and the cutting ability of steel significantly.Be heated to 1000 ℃ and also can not lose its original hardness even contain the stellite of cobalt more than 50%, nowadays this carbide alloy has become and has contained the most important material of using between golden cutting element and aluminium.In this material, cobalt combines other metal carbides crystal grain in the alloy composition, makes the higher toughness of alloy tool, and reduces the sensitive property of impact, the advantage of cobalt on magnetic material clearly, the cobalt metal also is widely used at aspects such as plating, glass, dyeing, medicine medical treatment.The cobalt acid lithium made from lithium carbonate and cobalt oxide is the most general high-energy battery positive electrode of modern Application.
Four, the present invention has added nickel, nickel: matter is hard, has magnetic and good plasticity.Good corrosion resistance is arranged, not oxidized in air, anti-highly basic again.Ductility and can high polish and anticorrosive is arranged; Be plated in and prevent from other metals getting rusty.
Five, the contact surface of hard alloy substrate of the present invention and high density polycrystalline diamond layer is provided with the jog that cooperatively interacts, and makes both in conjunction with tightr, not easily separated.
Six, hardness of the present invention is high, and abrasion resistance is strong, Heat stability is good, and stock-removing efficiency is high, can significantly increase the service life, and reduces the cost of production of enterprise.
The specific embodiment
A kind of composite polycrystal-diamond includes hard alloy substrate, is compounded with one deck high density polycrystalline diamond layer on the hard alloy substrate.The contact surface of hard alloy substrate and high density polycrystalline diamond layer is provided with the jog that cooperatively interacts.The component of high density polycrystalline diamond layer and mass fraction are diadust 90-95 part, rare earth 0.5-3 part, cobalt 2-10 part, nickel 1-2 part.The composition of rare earth is a kind of or two kinds or more of in lanthanum, cerium, praseodymium, neodymium, promethium, samarium, europium, gadolinium, terbium, dysprosium, holmium, erbium, thulium, ytterbium, lutetium, scandium and the yttrium.
A kind of manufacture craft of composite polycrystal-diamond, be diadust 90-95 part with mass fraction, rare earth 0.5-3 part, cobalt 2-10 part after nickel 1-2 part is mixed, is carried out high pressure high temperature to mixed material and is processed, the pressure that described high pressure high temperature is processed is 5.6-7.5Gpa, temperature is made semiproduct for being not less than 1300 ℃, again these semiproduct and hard alloy substrate is combined into product.
Embodiment one
A kind of composite polycrystal-diamond includes hard alloy substrate, is compounded with one deck high density polycrystalline diamond layer on the hard alloy substrate.The contact surface of hard alloy substrate and high density polycrystalline diamond layer is provided with the jog that cooperatively interacts.The component of high density polycrystalline diamond layer and mass fraction are 90 parts of diadusts, 0.5 part of rare earth, 2 parts of cobalts, 1 part in nickel.The composition of rare earth is a kind of or two kinds or more of in lanthanum, cerium, praseodymium, neodymium, promethium, samarium, europium, gadolinium, terbium, dysprosium, holmium, erbium, thulium, ytterbium, lutetium, scandium and the yttrium.
A kind of manufacture craft of composite polycrystal-diamond, be 90 parts of diadusts with mass fraction, 0.5 part of rare earth, 2 parts of cobalts after 1 part of mixing of nickel, carry out high pressure high temperature to mixed material and process, the pressure that described high pressure high temperature is processed is 5.6Gpa, temperature is made semiproduct for being not less than 1300 ℃, again these semiproduct and hard alloy substrate is combined into product.
The present invention forms by high pressure high temperature take diadust as main material, and its existing adamantine abrasion resistance has again the resistance to impact of carbide alloy.
The present invention has added rare earth can improve the physical and chemical performance of alloy, and improves Alloy At Room Temperature and high-temperature mechanical property, increases the toughness of product.
The present invention has added cobalt, and cobalt is mainly used in producing alloy.The shear steel that contains a certain amount of cobalt can improve abrasion resistance and the cutting ability of steel significantly.Be heated to 1000 ℃ and also can not lose its original hardness even contain the stellite of cobalt more than 50%, nowadays this carbide alloy has become and has contained the most important material of using between golden cutting element and aluminium.In this material, cobalt combines other metal carbides crystal grain in the alloy composition, makes the higher toughness of alloy tool, and reduces the sensitive property of impact, the advantage of cobalt on magnetic material clearly, the cobalt metal also is widely used at aspects such as plating, glass, dyeing, medicine medical treatment.The cobalt acid lithium made from lithium carbonate and cobalt oxide is the most general high-energy battery positive electrode of modern Application.
The present invention has added nickel, nickel: matter is hard, has magnetic and good plasticity.Good corrosion resistance is arranged, not oxidized in air, anti-highly basic again.Ductility and can high polish and anticorrosive is arranged; Be plated in and prevent from other metals getting rusty.
Hardness of the present invention is high, and abrasion resistance is strong, Heat stability is good, and stock-removing efficiency is high, can significantly increase the service life, and reduces the cost of production of enterprise.
The contact surface of hard alloy substrate of the present invention and high density polycrystalline diamond layer is provided with the jog that cooperatively interacts, and makes both in conjunction with tightr, not easily separated.
Embodiment two
Present embodiment and embodiment one are roughly the same, and a kind of composite polycrystal-diamond includes hard alloy substrate, are compounded with one deck high density polycrystalline diamond layer on the hard alloy substrate.The contact surface of hard alloy substrate and high density polycrystalline diamond layer is provided with the jog that cooperatively interacts.The component of high density polycrystalline diamond layer and mass fraction are 95 parts of diadusts, 3 parts of rare earths, 10 parts of cobalts, 2 parts in nickel.The composition of rare earth is a kind of or two kinds or more of in lanthanum, cerium, praseodymium, neodymium, promethium, samarium, europium, gadolinium, terbium, dysprosium, holmium, erbium, thulium, ytterbium, lutetium, scandium and the yttrium.
A kind of manufacture craft of composite polycrystal-diamond, be diadust 90-95 part with mass fraction, 3 parts of rare earths, 10 parts of cobalts after 2 parts of mixing of nickel, carry out high pressure high temperature to mixed material and process, the pressure that described high pressure high temperature is processed is 7.5Gpa, temperature is made semiproduct for being not less than 1300 ℃, again these semiproduct and hard alloy substrate is combined into product.
Embodiment three
Present embodiment and embodiment one and embodiment two are roughly the same, are preferred version of the present invention, and a kind of composite polycrystal-diamond includes hard alloy substrate, are compounded with one deck high density polycrystalline diamond layer on the hard alloy substrate.The contact surface of hard alloy substrate and high density polycrystalline diamond layer is provided with the jog that cooperatively interacts.The component of high density polycrystalline diamond layer and mass fraction are 92 parts of diadusts, 1.5 parts of rare earths, 6 parts of cobalts, 1.5 parts in nickel.The composition of rare earth is a kind of or two kinds or more of in lanthanum, cerium, praseodymium, neodymium, promethium, samarium, europium, gadolinium, terbium, dysprosium, holmium, erbium, thulium, ytterbium, lutetium, scandium and the yttrium.
A kind of manufacture craft of composite polycrystal-diamond, be 92 parts of diadusts with mass fraction, 1.5 parts of rare earths, 6 parts of cobalts after 1.5 parts of mixing of nickel, carry out high pressure high temperature to mixed material and process, the pressure that described high pressure high temperature is processed is 6.5Gpa, temperature is made semiproduct for being not less than 1300 ℃, again these semiproduct and hard alloy substrate is combined into product.
Above-mentioned only is the specific embodiment of the present invention, but design concept of the present invention is not limited to this, allly utilizes this design that the present invention is carried out the change of unsubstantiality, all should belong to the behavior of invading protection domain of the present invention.

Claims (5)

1. a composite polycrystal-diamond includes hard alloy substrate, it is characterized in that: be compounded with one deck high density polycrystalline diamond layer on the described hard alloy substrate.
2. a kind of composite polycrystal-diamond according to claim 1, it is characterized in that: the contact surface of described hard alloy substrate and high density polycrystalline diamond layer is provided with the jog that cooperatively interacts.
3. a kind of composite polycrystal-diamond according to claim 1, it is characterized in that: the component of described high density polycrystalline diamond layer and mass fraction are diadust 90-95 part, rare earth 0.5-3 part, cobalt 2-10 part, nickel 1-2 part.
4. a kind of composite polycrystal-diamond according to claim 3 is characterized in that: the composition of described rare earth is a kind of or two kinds or more of in lanthanum, cerium, praseodymium, neodymium, promethium, samarium, europium, gadolinium, terbium, dysprosium, holmium, erbium, thulium, ytterbium, lutetium, scandium and the yttrium.
5. the manufacture craft of a composite polycrystal-diamond, it is characterized in that: be diadust 90-95 part with mass fraction, rare earth 0.5-3 part, cobalt 2-10 part after nickel 1-2 part is mixed, is carried out high pressure high temperature to mixed material and is processed, the pressure that described high pressure high temperature is processed is 5.6-7.5Gpa, temperature is made semiproduct for being not less than 1300 ℃, again these semiproduct and hard alloy substrate is combined into product.
CN201210462514XA 2012-11-16 2012-11-16 Polycrystalline diamond compound sheet and manufacturing process thereof Pending CN102913135A (en)

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105817631A (en) * 2016-03-25 2016-08-03 河南四方达超硬材料股份有限公司 Manufacturing method for polycrystalline diamond ultra-thin cutting blade
CN108972922A (en) * 2018-07-10 2018-12-11 山西中聚晶科半导体有限公司 A kind of sapphire crystal ingot draws stick drilling pipe knife
CN117403089A (en) * 2023-10-17 2024-01-16 河南省煤科院耐磨技术有限公司 A method for preparing high toughness and high hardness wear-resistant blocks

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN2403541Y (en) * 2000-02-01 2000-11-01 河南四方超硬材料有限公司 Synneusis diamond hard alloy composite tooth
CN1433862A (en) * 2003-02-27 2003-08-06 武汉理工大学 Method for preparing composition gradient intermediate transition layer on wedge shape or complex shape drill working-surface
CN2881059Y (en) * 2005-11-25 2007-03-21 江汉石油钻头股份有限公司 Impact resistant polycrystal diamond composite sheet
US20080142276A1 (en) * 2006-05-09 2008-06-19 Smith International, Inc. Thermally stable ultra-hard material compact constructions
CN101518822A (en) * 2009-03-30 2009-09-02 上海江信超硬材料有限公司 Boric diamond composite sheet synthesized at high temperature and pressure and method for preparing same
CN202055757U (en) * 2011-04-26 2011-11-30 深圳市海明润实业有限公司 Polycrystalline diamond compact with arc-shaped layer interface

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN2403541Y (en) * 2000-02-01 2000-11-01 河南四方超硬材料有限公司 Synneusis diamond hard alloy composite tooth
CN1433862A (en) * 2003-02-27 2003-08-06 武汉理工大学 Method for preparing composition gradient intermediate transition layer on wedge shape or complex shape drill working-surface
CN2881059Y (en) * 2005-11-25 2007-03-21 江汉石油钻头股份有限公司 Impact resistant polycrystal diamond composite sheet
US20080142276A1 (en) * 2006-05-09 2008-06-19 Smith International, Inc. Thermally stable ultra-hard material compact constructions
CN101518822A (en) * 2009-03-30 2009-09-02 上海江信超硬材料有限公司 Boric diamond composite sheet synthesized at high temperature and pressure and method for preparing same
CN202055757U (en) * 2011-04-26 2011-11-30 深圳市海明润实业有限公司 Polycrystalline diamond compact with arc-shaped layer interface

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105817631A (en) * 2016-03-25 2016-08-03 河南四方达超硬材料股份有限公司 Manufacturing method for polycrystalline diamond ultra-thin cutting blade
CN108972922A (en) * 2018-07-10 2018-12-11 山西中聚晶科半导体有限公司 A kind of sapphire crystal ingot draws stick drilling pipe knife
CN117403089A (en) * 2023-10-17 2024-01-16 河南省煤科院耐磨技术有限公司 A method for preparing high toughness and high hardness wear-resistant blocks

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Application publication date: 20130206