CN102879316A - Device and method for testing feedback ions of low-light-level image intensifier component - Google Patents
Device and method for testing feedback ions of low-light-level image intensifier component Download PDFInfo
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Abstract
微光像增强器组件反馈离子测试装置及方法,属于光电成像器件领域,包括聚焦紫外光源、真空室、无阴极微光像增强器组件、离子导管、离子探测器、屏蔽盒;方法是:聚焦紫外光源通过紫外窗口入射到微通道板表面,激发出的电子使微光像增强器组件工作,微光像增强器组件中产生的反馈离子经加速后,经离子导管、隔离栅网进入离子探测器,输出信号经电荷放大器放大后输入到多道脉冲幅度分析器,通过脉冲幅度分析将离子脉冲信号与噪声信号进行分离,得到反馈离子脉冲信号幅度值,然后将信号幅值做为阈值输入到单道谱仪中,实现离子脉冲计数。该装置能够实现复杂电磁环境下的极微弱离子流检测,用于微光像增强器中防离子反馈膜离子阻透特性的测量。
A low-light image intensifier component feedback ion test device and method belong to the field of photoelectric imaging devices, including a focused ultraviolet light source, a vacuum chamber, a cathode-less low-light image intensifier component, an ion guide, an ion detector, and a shielding box; the method is: focusing The ultraviolet light source is incident on the surface of the microchannel plate through the ultraviolet window, and the excited electrons make the low-light image intensifier component work, and the feedback ions generated in the low-light image intensifier component are accelerated and enter the ion detection through the ion guide and the isolation grid. The output signal is amplified by the charge amplifier and then input to the multi-channel pulse amplitude analyzer. The ion pulse signal and the noise signal are separated through the pulse amplitude analysis, and the feedback ion pulse signal amplitude value is obtained, and then the signal amplitude is input as the threshold value to the In a single-channel spectrometer, ion pulse counting is realized. The device can realize the detection of extremely weak ion current in a complex electromagnetic environment, and is used for the measurement of the ion barrier characteristics of the anti-ion feedback membrane in the low-light image intensifier.
Description
技术领域 technical field
本发明涉及一种微光像增强器组件反馈离子测试装置及其方法,是一种能够实现复杂电磁环境下的极微弱离子流检测装置,能够用于微光器件中的防离子反馈膜离子阻透特性测量。The invention relates to a low-light image intensifier component feedback ion testing device and a method thereof, which is a device capable of realizing extremely weak ion current detection in a complex electromagnetic environment, and can be used for anti-ion feedback membrane ion resistance in low-light devices. Permeability measurement.
背景技术 Background technique
像管工作时,管内残余气体分子在微通道板输出端被高密度电子云电离形成气体离子,并沿微通道反馈至微通道板输入端,在输入端近贴区电场加速作用下,高速轰击光阴极,使光阴极发射电子,造成信噪比降低,在荧光屏上形成离子斑;高速离子的轰击还会使GaAs光阴极表面Cs-O层受到损伤,灵敏度急剧下降,使阴极寿命大幅度缩短。为解决这一问题,在微通道板输入面上均覆盖一层介质薄膜,用以阻止气体离子由通道内射出,达到保护光阴极的目的,这层薄膜称之为防离子反馈膜。据报道,MCP覆防离子反馈膜后可使像管工作寿命达到10000小时以上。When working like a tube, the residual gas molecules in the tube are ionized by the high-density electron cloud at the output end of the microchannel plate to form gas ions, and feed back to the input end of the microchannel plate along the microchannel. The photocathode makes the photocathode emit electrons, which reduces the signal-to-noise ratio and forms ion spots on the fluorescent screen; the bombardment of high-speed ions will also damage the Cs-O layer on the surface of the GaAs photocathode, and the sensitivity will drop sharply, which will greatly shorten the life of the cathode. . In order to solve this problem, a layer of dielectric film is covered on the input surface of the microchannel plate to prevent gas ions from ejecting from the channel and achieve the purpose of protecting the photocathode. This film is called anti-ion feedback film. According to reports, after MCP covers the ion feedback film, the working life of the image tube can reach more than 10,000 hours.
对于高性能的防离子反馈膜,需要具有高的电子透过率和离子阻挡率,膜层的性能与膜层的制作工艺、膜层组份等因素相关,为此需要一种能够直接测量防离子反馈膜离子阻透特性的装置,对膜层性能进行定量检测,为制备优质膜层提供依据。防离子反馈膜的厚度只有几个纳米,制作的时候必须有衬底的存在,所以不能将膜层独立出来进行离子阻透特性测量;从理论分析和软件模拟仿真所得结果可知微光像管中反馈离子流小于10-15A,现有技术条件下无法获得如此低离子流的离子源,采用离子源进行测量是不可行的。目前国内外没有相关测试设备的报道及产品出现。For a high-performance anti-ion feedback film, it is necessary to have a high electron transmission rate and ion barrier rate. The performance of the film layer is related to factors such as the production process of the film layer and the film composition. Therefore, a method that can directly measure the anti-ion feedback film is required. The device for ion feedback membrane ion barrier properties can quantitatively detect the performance of the membrane layer and provide a basis for the preparation of high-quality membrane layers. The thickness of the anti-ion feedback film is only a few nanometers, and there must be a substrate when it is fabricated, so the film layer cannot be isolated to measure the ion barrier characteristics; from the results obtained from theoretical analysis and software simulation, it can be known that the low-light image tube Feedback ion current is less than 10 -15 A, the ion source with such a low ion current cannot be obtained under the current technical conditions, and it is not feasible to use ion source for measurement. At present, there are no reports and products of relevant testing equipment at home and abroad.
发明内容: Invention content:
本发明所要解决的技术问题是提供一种微光像增强器组件反馈离子测试装置及其方法,它能够模拟真实像管工作状态,实现防离子反馈膜离子阻透特性的测量。The technical problem to be solved by the present invention is to provide a low-light image intensifier component feedback ion test device and its method, which can simulate the working state of the real image tube and realize the measurement of ion barrier characteristics of the anti-ion feedback membrane.
本发明的技术方案是设计一种微光像增强器组件反馈离子测试装置,包括聚焦紫外光源、真空室、无阴极微光像增强器组件、离子导管、离子探测器、屏蔽盒;所述的真空室设置有紫外窗口,真空室内部的无阴极微光像增强器组件斜上方对准离子导管;所述的屏蔽盒内置有电场隔离栅网、光阑和离子探测器,所述离子探测器与电荷放大器连接;所述的电荷放大器分别与多道脉冲幅度分析器、单道谱仪连接;所述无阴极微光像增强器组件和离子探测器中间设置离子导管、电场隔离网和光阑。其中聚焦紫外光源光斑尺寸可调;所述的离子导管与屏蔽盒无缝连接;离子导管出口沿轴线方向投影完全覆盖在光阑上。The technical solution of the present invention is to design a low-light image intensifier assembly feedback ion test device, including a focused ultraviolet light source, a vacuum chamber, a cathode-free low-light image intensifier assembly, an ion guide, an ion detector, and a shielding box; The vacuum chamber is provided with an ultraviolet window, and the cathode-free low-light image intensifier assembly inside the vacuum chamber is aligned with the ion guide obliquely; the shielding box is equipped with an electric field isolation grid, a diaphragm and an ion detector. It is connected with a charge amplifier; the charge amplifier is respectively connected with a multi-channel pulse amplitude analyzer and a single-channel spectrometer; an ion guide, an electric field isolation net and an aperture are arranged between the cathode-free micro-light image intensifier assembly and the ion detector. The spot size of the focused ultraviolet light source is adjustable; the ion guide is seamlessly connected with the shielding box; the projection of the ion guide outlet along the axial direction completely covers the diaphragm.
发明一种微光像增强器组件反馈离子测试方法,聚焦后的紫外光线,也就是聚焦紫外光源通过紫外窗口入射到无阴极微光像增强器组件中的微通道板表面,激发出的电子使无阴极微光像增强器组件工作,无阴极微光像增强器组件中产生的反馈离子经加速后,经离子导管、电场隔离栅网进入离子探测器,输出信号经电荷放大器放大后输入到多道脉冲幅度分析器,通过脉冲幅度分析将离子脉冲信号与噪声信号进行分离,得到反馈离子脉冲信号幅度值区间,然后将信号幅值下限做为阈值输入到单道谱仪中实现离子脉冲计数;其中,激发光源采用光斑尺寸可调的聚焦紫外光源。Invented a low-light image intensifier component feedback ion test method, the focused ultraviolet light, that is, the focused ultraviolet light source is incident on the surface of the microchannel plate in the cathode-free low-light image intensifier component through the ultraviolet window, and the excited electrons make The non-cathode low-light image intensifier component works, and the feedback ions generated in the non-cathode low-light image intensifier component are accelerated, then enter the ion detector through the ion guide and the electric field isolation grid, and the output signal is amplified by the charge amplifier and then input to the multiple The channel pulse amplitude analyzer separates the ion pulse signal from the noise signal through pulse amplitude analysis to obtain the feedback ion pulse signal amplitude value interval, and then inputs the lower limit of the signal amplitude as a threshold value into the single channel spectrometer to realize ion pulse counting; Wherein, the excitation light source adopts a focused ultraviolet light source with adjustable spot size.
所述离子导管与被测表面有30度~40度的倾角。该装置用于探测微光像增强器组件中的反馈离子流。The ion guide has an inclination angle of 30-40 degrees to the measured surface. The setup is used to detect feedback ion currents in low-light image intensifier assemblies.
本发明的工作原理及有益效果如下:本发明的无阴极微光像增强器组件和离子探测组件安装在真空室中,在真空室顶端设置了紫外入射窗口;采用紫外光源直接激发微光像增强器组件中微通道板表面发出二次电子形成微通道板输入电流,替代了光电阴极,为反馈离子提供了运行通道,使之能够入射到离子探测器上。The working principle and beneficial effects of the present invention are as follows: the non-cathode low-light image intensifier assembly and the ion detection assembly of the present invention are installed in a vacuum chamber, and an ultraviolet incident window is set on the top of the vacuum chamber; an ultraviolet light source is used to directly excite the low-light image intensifier Secondary electrons are emitted from the surface of the microchannel plate in the detector assembly to form the input current of the microchannel plate, which replaces the photocathode and provides a running channel for the feedback ions to be incident on the ion detector.
离子探测器装置在屏蔽盒中,屏蔽盒采用金属材料制作,既能实现电磁屏蔽,又能有效地屏蔽紫外光,避免直接入射紫外光和真空室内多次反射紫外光入射到离子探测器上;屏蔽盒下端连接离子导管,离子导管的入口以30度~40度的倾角对准无阴极微光像增强器组件上表面并保证不覆盖上表面,避免遮挡紫外光束,离子导管采用吸收紫外的介质材料制作,能够将微光像增强器表面反射的紫外光强降低,同时为离子提供一条运行通道;在离子导管和离子探测器间设置了电场隔离网,用以消除离子加速电场对离子探测器正常工作状态的影响;在电场隔离网和离子探测器之间设置了光阑,使通过离子导管入射的紫外光强进一步降低,从而最大限度地减小了紫外光激发离子探测器产生光电流。The ion detector is installed in a shielding box, which is made of metal materials, which can not only realize electromagnetic shielding, but also effectively shield ultraviolet light, avoiding direct incident ultraviolet light and multiple reflections of ultraviolet light in the vacuum chamber incident on the ion detector; The lower end of the shielding box is connected to the ion guide, and the entrance of the ion guide is aligned with the upper surface of the non-cathode low-light image intensifier component at an inclination angle of 30 degrees to 40 degrees and ensures that the upper surface is not covered to avoid blocking the ultraviolet beam. The ion guide adopts a medium that absorbs ultraviolet rays Made of materials, it can reduce the intensity of ultraviolet light reflected by the surface of the low-light image intensifier, and at the same time provide a running channel for ions; an electric field isolation net is set between the ion guide and the ion detector to eliminate the impact of the ion acceleration electric field on the ion detector The impact of normal working conditions; a diaphragm is set between the electric field isolation net and the ion detector to further reduce the intensity of ultraviolet light incident through the ion guide, thereby minimizing the photocurrent generated by the ion detector excited by ultraviolet light.
测量方法是离子入射到离子探测器上产生电流脉冲,并送入电荷放大器进行放大;测量装置中存在着多组高压电源,测试时涡轮分子泵也保持工作状态,残余的紫外光会激发离子探测器产生二次电子,离子探测器本身存在固有的暗计数率,上述的多种干扰因素都会影响极微弱离子流的检测,为此在电荷放大器后端连接了多道脉冲幅度分析器,用以对电荷放大器输出信号进行脉冲幅度分析,找到离子信号脉冲和噪声脉冲的临界点,从而判定离子信号脉冲的幅度特征;在大量脉冲信号输入的情况下,相对数量较少的离子信号脉冲会因多道脉冲幅度分析器工作速度的影响而产生信号丢失的情况,从而影响离子信号脉冲的测量精度,在电荷放大器后端同时连接一台单道谱仪,根据脉冲幅度分析结果得到离子脉冲的阈值电压,从而在单道谱仪上实现离子信号脉冲的无丢失计数测量,大大提高了测量精度。The measurement method is that ions are incident on the ion detector to generate a current pulse, and sent to the charge amplifier for amplification; there are multiple sets of high-voltage power supplies in the measurement device, and the turbomolecular pump also keeps working during the test, and the residual ultraviolet light will excite the ion detector. The secondary electrons are generated by the ion detector, and the ion detector itself has an inherent dark count rate. The above-mentioned various interference factors will affect the detection of the extremely weak ion current. Therefore, a multi-channel pulse amplitude analyzer is connected to the rear end of the charge amplifier to Analyze the pulse amplitude of the output signal of the charge amplifier to find the critical point of the ion signal pulse and the noise pulse, so as to determine the amplitude characteristics of the ion signal pulse; Due to the influence of the working speed of the channel pulse amplitude analyzer, signal loss occurs, which affects the measurement accuracy of the ion signal pulse. A single channel spectrometer is connected to the back end of the charge amplifier at the same time, and the threshold voltage of the ion pulse is obtained according to the pulse amplitude analysis results. , so that the non-missing counting measurement of ion signal pulses is realized on a single-channel spectrometer, and the measurement accuracy is greatly improved.
本发明提供的测试装置和方法,能够实现有膜和无膜微通道板反馈离子流的测量,从而实现防离子反馈膜离子阻透特性的测量。The test device and method provided by the invention can realize the measurement of the feedback ion flow of the microchannel plate with and without the membrane, so as to realize the measurement of the ion barrier property of the anti-ion feedback membrane.
附图说明 Description of drawings
下面结合附图及具体实施方式对本发明作进一步说明Below in conjunction with accompanying drawing and specific embodiment the present invention will be further described
图1为本发明的微光像增强器组件反馈离子测试装置示意图Fig. 1 is the sketch map of feedback ion testing device of micro-light image intensifier assembly of the present invention
图2为本发明的信号脉冲幅度分析结果Fig. 2 is the signal pulse amplitude analysis result of the present invention
图3为沿y轴放大后的信号脉冲幅度分析结果Figure 3 shows the analysis results of the signal pulse amplitude enlarged along the y-axis
图中1-聚焦紫外光源,2-紫外窗口,3-真空室,4-无阴极微光像增强器组件,5-电场隔离栅网,6-光阑,7-离子导管,8-离子探测器,9-屏蔽盒,10-电荷放大器,11-多道脉冲幅度分析器,12-单道谱仪。In the figure 1-focused ultraviolet light source, 2-ultraviolet window, 3-vacuum chamber, 4-non-cathode low-light image intensifier assembly, 5-electric field isolation grid, 6-diaphragm, 7-ion guide, 8-ion detection Device, 9-shielding box, 10-charge amplifier, 11-multi-channel pulse amplitude analyzer, 12-single-channel spectrometer.
具体实施方式 Detailed ways
图1为本发明的微光像增强器组件反馈离子测试装置示意图,下面对本发明装置做进一步描述。Fig. 1 is a schematic diagram of the low-light image intensifier component feedback ion test device of the present invention, and the device of the present invention will be further described below.
本发明装置包括聚焦紫外光源1、顶端设置紫外窗口2的真空室3、无阴极微光像增强器组件4、与离子入射口处有无缝连接的离子导管7及内置电场隔离栅网5、光阑6和离子探测器8的屏蔽盒9、电荷放大器10、多道脉冲幅度分析器11、单道谱仪12;离子导管的入口以30度~40度的倾角一定倾角对准无阴极微光像增强器组件上表面并保证不覆盖上表面;离子探测器与电荷放大器连接;单道谱仪和多道脉冲幅度分析器分别与电荷放大器连接;微光像增强器组件、离子探测组件都放置在真空室中,其中离子导管出口沿轴线方向投影完全覆盖在光阑上。The device of the present invention includes a focused
测量时,紫外光斑聚焦在无阴极微光像增强器组件上表面,紫外光激发微通道板产生二次电子作为微通道板的入射电子,这些电子经微通道板倍增后,在其输出端及微光像增强器组件后近贴空间形成高密度电子云,并轰击组件内残余的气体分子形成离子,离子经微通道板工作电压加速后,反馈至微通道板输入端形成反馈离子,反馈离子在离子加速电场的作用下,入射至离子探测器,从而形成离子激发形成的电流脉冲,对这个电流脉冲计数即可测得极微弱离子流。During measurement, the ultraviolet light spot is focused on the upper surface of the non-cathode low-light image intensifier component, and the ultraviolet light excites the micro-channel plate to generate secondary electrons as the incident electrons of the micro-channel plate. After the low-light image intensifier component is close to the space, a high-density electron cloud is formed, and the residual gas molecules in the component are bombarded to form ions. After the ions are accelerated by the working voltage of the micro-channel plate, they are fed back to the input end of the micro-channel plate to form feedback ions. Under the action of the ion accelerating electric field, it is incident to the ion detector, thereby forming a current pulse formed by ion excitation, and the extremely weak ion current can be measured by counting the current pulse.
但是在测量装置中存在着高压电源、涡轮分子泵、残余的紫外光激发离子探测器、离子探测器暗计数率等影响因素,从而产生大量的干扰脉冲,影响极微弱离子流的检测,经分析可知,干扰脉冲信号一般幅度较低。图2为电荷放大器输出信号做脉冲幅度分析的结果,在低幅度区间存在着大量的干扰脉冲信号。However, there are high-voltage power supply, turbomolecular pump, residual ultraviolet light excitation ion detector, ion detector dark count rate and other influencing factors in the measuring device, which generate a large number of interference pulses and affect the detection of extremely weak ion current. After analysis It can be seen that the amplitude of the interference pulse signal is generally low. Figure 2 shows the result of the pulse amplitude analysis of the output signal of the charge amplifier. There are a large number of interference pulse signals in the low amplitude range.
在大量脉冲信号输入的情况下,相对数量较少的离子信号脉冲会因多道脉冲幅度分析器工作速度的影响而产生信号丢失的情况,从而影响离子信号脉冲的测量精度。为解决离子信号脉冲丢失问题,在电荷放大器后端连接了多道脉冲幅度分析器,用以对电荷放大器输出信号进行脉冲幅度分析,找到离子信号脉冲和噪声脉冲的临界点,从而判定离子信号脉冲的幅度特征,图3为图2脉冲幅度分析结果的y轴放大结果,从图3可以看出,在本实施例中干扰脉冲和离子信号脉冲在65道有明显的临界点。在电荷放大器后端同时连接一台单道谱仪,将产生临界点的道数折合成电压值作为单道谱仪的阈值电压,滤除了干扰脉冲计数,从而实现了离子信号脉冲的无丢失计数测量,大大提高了测量精度,从而实现了微光像增强器组件反馈离子测试目的,从而能够对微光器件中防离子反馈膜的离子阻透特性进行高精度定量测量,对其性能进行客观评价。In the case of a large number of pulse signal inputs, a relatively small number of ion signal pulses will cause signal loss due to the influence of the working speed of the multi-channel pulse amplitude analyzer, thereby affecting the measurement accuracy of ion signal pulses. In order to solve the problem of ion signal pulse loss, a multi-channel pulse amplitude analyzer is connected to the back end of the charge amplifier to analyze the pulse amplitude of the output signal of the charge amplifier, find the critical point of the ion signal pulse and the noise pulse, and determine the ion signal pulse Fig. 3 is the y-axis enlarged result of the pulse amplitude analysis result in Fig. 2. It can be seen from Fig. 3 that in this embodiment, the interference pulse and the ion signal pulse have an obvious critical point in track 65. A single-channel spectrometer is connected to the back end of the charge amplifier at the same time, and the number of channels that generate the critical point is converted into a voltage value as the threshold voltage of the single-channel spectrometer, which filters out the counting of interference pulses, thereby realizing the lossless counting of ion signal pulses measurement, which greatly improves the measurement accuracy, thereby realizing the purpose of the low-light image intensifier component feedback ion test, so that the ion barrier characteristics of the anti-ion feedback film in the low-light device can be measured quantitatively with high precision, and its performance can be objectively evaluated .
需要指出的是,在不脱离本发明的技术思想的基础上,所进行的任何形式的等效代换所形成的测试装置及方法均属于本发明的保护范围。It should be pointed out that, on the basis of not departing from the technical idea of the present invention, the testing device and method formed by any form of equivalent substitution all belong to the protection scope of the present invention.
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