CN102161899A - Efficient internal thermal type oil extraction device for powder oil shale and extraction method thereof - Google Patents
Efficient internal thermal type oil extraction device for powder oil shale and extraction method thereof Download PDFInfo
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- CN102161899A CN102161899A CN2011100676557A CN201110067655A CN102161899A CN 102161899 A CN102161899 A CN 102161899A CN 2011100676557 A CN2011100676557 A CN 2011100676557A CN 201110067655 A CN201110067655 A CN 201110067655A CN 102161899 A CN102161899 A CN 102161899A
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- 239000000843 powder Substances 0.000 title claims abstract description 40
- 239000004058 oil shale Substances 0.000 title claims abstract description 22
- 238000000605 extraction Methods 0.000 title claims abstract description 11
- 239000002184 metal Substances 0.000 claims abstract description 34
- 238000000197 pyrolysis Methods 0.000 claims abstract description 34
- 239000000571 coke Substances 0.000 claims abstract description 17
- 238000003860 storage Methods 0.000 claims abstract description 14
- 238000000034 method Methods 0.000 claims abstract description 9
- 238000010438 heat treatment Methods 0.000 claims abstract description 6
- 239000000463 material Substances 0.000 claims abstract 2
- 239000007789 gas Substances 0.000 claims description 124
- 238000001816 cooling Methods 0.000 claims description 21
- 239000002994 raw material Substances 0.000 claims description 15
- 239000003079 shale oil Substances 0.000 claims description 12
- 238000002485 combustion reaction Methods 0.000 claims description 9
- 239000007788 liquid Substances 0.000 claims description 7
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 claims description 6
- 238000009833 condensation Methods 0.000 claims description 6
- 230000005494 condensation Effects 0.000 claims description 6
- 239000003546 flue gas Substances 0.000 claims description 6
- 238000003763 carbonization Methods 0.000 claims 9
- 238000001035 drying Methods 0.000 claims 4
- 229910000831 Steel Inorganic materials 0.000 claims 1
- 230000005484 gravity Effects 0.000 claims 1
- 239000010959 steel Substances 0.000 claims 1
- 239000003921 oil Substances 0.000 abstract description 31
- 238000009826 distribution Methods 0.000 abstract description 11
- 238000005516 engineering process Methods 0.000 abstract description 8
- 239000010779 crude oil Substances 0.000 abstract description 2
- 238000004519 manufacturing process Methods 0.000 abstract description 2
- 230000015572 biosynthetic process Effects 0.000 description 5
- 230000000694 effects Effects 0.000 description 5
- 238000011084 recovery Methods 0.000 description 5
- 230000008901 benefit Effects 0.000 description 2
- 238000000354 decomposition reaction Methods 0.000 description 2
- 238000009792 diffusion process Methods 0.000 description 2
- 238000004821 distillation Methods 0.000 description 2
- 238000007789 sealing Methods 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000003245 coal Substances 0.000 description 1
- 238000010276 construction Methods 0.000 description 1
- 230000002950 deficient Effects 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 239000002803 fossil fuel Substances 0.000 description 1
- 239000000446 fuel Substances 0.000 description 1
- 238000010248 power generation Methods 0.000 description 1
- 239000011435 rock Substances 0.000 description 1
- 238000009423 ventilation Methods 0.000 description 1
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- Production Of Liquid Hydrocarbon Mixture For Refining Petroleum (AREA)
Abstract
本发明涉及一种高效内热式粉末油页岩提油装置及工艺，该装置由气体均布器、干馏炉、旋风夹套、水冷电捕焦器、储油罐、燃烧器和金属蜂巢换热器组成，干馏炉内的干馏段设置了气体均布器实现了粉料和气体热载体的直接换热，大幅度提高了热效率；采用多层均匀布风技术，保证油页岩干馏完全；整个系统不需要额外能源供给，实现能量的自己自足。这种高效内热式粉末油页岩提油新工艺采用内热法，即气体与粉末油页岩直接加热的方式加热油页岩，油页岩受热分解产生干馏油气，然后冷凝收集得到高质量原油及气体瓦斯。此新工艺具有热效率高，稳定安全，简单可靠等特点，大幅度降低粉末油页岩提油的生产成本，显著提高出油率，从而提高油页岩的综合利用率。
The invention relates to a high-efficiency internal heating powder oil shale oil extraction device and its technology. The device consists of a gas uniform distributor, a dry distillation furnace, a cyclone jacket, a water-cooled electric coke catcher, an oil storage tank, a burner and a metal honeycomb for heat exchange The dry distillation section in the dry distillation furnace is equipped with a gas uniform distributor to realize the direct heat exchange between the powder material and the gas heat carrier, which greatly improves the thermal efficiency; the multi-layer uniform air distribution technology is adopted to ensure the complete dry distillation of oil shale; the whole The system does not require additional energy supply and realizes energy self-sufficiency. This new high-efficiency internal heating powder oil shale oil extraction process adopts the internal heat method, that is, the gas and powder oil shale are directly heated to heat the oil shale, and the oil shale is thermally decomposed to produce carbonized oil gas, which is then condensed and collected to obtain high-quality crude oil and gas gas. This new process has the characteristics of high thermal efficiency, stability, safety, simplicity and reliability, etc. It greatly reduces the production cost of powder oil shale oil extraction, significantly improves the oil yield, and thus improves the comprehensive utilization rate of oil shale.
Description
Technical field
The present invention relates to a kind of efficient internal heat type powder resinous shale and carry oily novel process and device, be characterized in designing a kind of particular structure, solve gas not good problem of ventilation property in powder, realized the direct heat exchange of powder and gaseous heat-carrier, increased substantially thermo-efficiency; Adopt multilayer even distributing wind technology, guarantee that oil shale distillation is complete; Total system does not need additional energy source to supply with, and realizes the own self-sustaining of energy.
Background technology
World's oil shale resources are abundant, and its reserves are converted to shale oil up to more than 4,000 hundred million t, verify crude oil reserve more than 1,700 hundred million t for big far beyond the world, are big than world's crude resources 3,000 hundred million t also.In the epoch of current soaring oil prices, the exploitation of many national oil shale reserves and destructive distillation are produced and are become necessary and feasible, and in some only about 20～40 dollars/barrel of its oil prices of country of having ready conditions and producing rock page or leaf oil, so resinous shale can become the additional energy of oil.Owing to have an economic benefit and to the growing demand of liquid fuel, the development of oil shale industry has good prospect.
Resinous shale is that important oil gas substitutes fossil fuel resource, in some areas of China, makes full use of the direct combustion power generation of resinous shale on the one hand, has solved China's partial area electric power and has supplied with problem; Utilize the oil shale distillation technology to produce shale oil on the other hand, also alleviated the China's oil problem of shortage to a certain extent.But domestic powder resinous shale was carried oil and was produced and not form scale as yet present stage, and because indirect heating is adopted in the heating of powder resinous shale more, therefore in actual production, there are defectives such as heat transfer efficiency is low, oil yield is not high, treatment capacity is less, seriously restricted resinous shale and carried oily industrial expansion.Therefore inventing a kind of powder of internal heat type efficiently resinous shale oil extraction plant has huge economic potential.
Summary of the invention
In order to solve the problems of the technologies described above, the purpose of this invention is to provide a kind of simple in structurely, safe and reliable, heat exchange is abundant, and the thermo-efficiency height improves dry distillation efficiency, and the hot type powder resinous shale of the sensible heat of refiltered oil shale semicockes is carried the devices and methods therefor of oil.
Technical scheme of the present invention is: plant efficient internal heat type powder resinous shale oil extraction plant, this device is made up of even gas distribution device, gas retort, whirlwind chuck, water-cooled electric coke catcher, storage tank, burner and honeycomb metal interchanger; Described gas retort comprises dryer section, retort section and cooling section; The destructive distillation gas outlet of the retort section upper end of described gas retort connects by pipeline and described whirlwind chuck one end pipe, and cooling section is by pipeline and described honeycomb metal heat exchange
Device connects; The other end of described whirlwind chuck connects by pipeline and described water-cooled electric coke catcher pipe, described water-cooled electric coke catcher by pipeline with connect respectively at the cooling section pipe of described storage tank, burner and described gas retort, described burner and honeycomb metal interchanger join, and described honeycomb metal interchanger is connected with dryer section with the retort section of described gas retort respectively by pipeline; Wherein, described even gas distribution device is welded on the sidewall of retort section of described gas retort, and an end is provided with inlet mouth and described gas retort UNICOM, the other end sealing; The both sides of described even gas distribution device are welded with metal column and are used to prevent stream in the powder; Connect with steelframe between the described metal column, be used to guarantee the intensity of described metal column.
Another object of the present invention provides the method for above-mentioned efficient powder resinous shale oil extraction plant,, specifically may further comprise the steps:
At first, the raw material powder resinous shale enters in the gas retort from feeding unit, through after the dryer section, enter in the retort section, temperature be 550 ~ 650 ℃ the inlet mouth of hot gas gas by the even gas distribution device enter in the retort section evenly to around diffusion, carry out direct heat exchange with the raw material powder resinous shale that falls, the raw material powder resinous shale is heated to 450 ~ 500 ℃, generation oil gas is decomposed in destructive distillation;
Then, the oil gas that decomposition is come out enters the water-cooled electric coke catcher from the outlet of destructive distillation gas through the whirlwind chuck and carries out condensation, is cooled to liquid shale oil and enters storage tank; Not by destructive distillation resinous shale formation completely semicoke, enter under the self gravitation effect in the cooling section of gas retort bottom in the gas retort, cooled shale semicockes are discharged from the gas retort bottom;
At last, a gas gas part that is not condensed feeds burner and burns, and another part enters the sensible heat of the cooling section recovery semicoke of gas retort, enters in the honeycomb metal interchanger; Through the hot flue gas of burner combustion and the gas gas heat exchange in the honeycomb metal interchanger, dryer section and retort section that heated gas gas feeds gas retort realize circulation with this.
The invention has the beneficial effects as follows: owing to adopt technique scheme, the major advantage of technology of the present invention have following some:
1. powder resinous shale and coal mine gas direct heat exchange, heat exchange is abundant, the thermo-efficiency height.
2. adopt the even gas distribution technology of multilayer, realize the constant temperature destructive distillation on the short transverse, the constant temperature destructive distillation can effectively reduce resinous shale at residing time in furnace, improves dry distillation efficiency; Arranging multiplayer circulation uniform device feeds in the stove destructive distillation gas uniformly on short transverse on short transverse.
3. the sensible heat of refiltered oil shale semicockes, total system does not need extra energy resource supply, can realize the self-sufficient of energy.
4. simple in structure, safe and reliable, can steady running.
Description of drawings
Fig. 1 carries the structural representation of the interior retort section of gas retort of oily device for the efficient internal heat type powder of the present invention resinous shale.
Fig. 2 is the even gas distribution device structural representation of retort section of the present invention.
The efficient internal heat type powder of Fig. 3 the present invention resinous shale is carried the device one-piece construction synoptic diagram of oil.
Among the figure:
| 1. even | 7. belong to the honeycomb interchanger |
| 2. gas retort | 8. |
| 3. whirlwind chuck | 9. steelframe |
| 4. water-cooled | 10. inlet mouth |
| 5. | 11. destructive |
| 6. burner | ? |
Embodiment:
Below in conjunction with the accompanying drawing specific embodiment technical scheme of the present invention is described further.
As shown in Figure 1-Figure 3, a kind of efficient internal heat type powder resinous shale is carried the device of oil, and this device is made up of even gas distribution device 1, gas retort 2, whirlwind chuck 3, water-cooled electric coke catcher 4, storage tank 5, burner 6 and honeycomb metal interchanger 7;
Wherein, gas retort 2 comprises dryer section, retort section and cooling section; Even gas distribution device 1 is welded on the sidewall of retort section of gas retort 2, and an end is provided with inlet mouth 10 and described gas retort 1 UNICOM, the other end sealing; Both sides are welded with and are used to prevent stream metal column 8 in the powder, in order to increase the intensity between the metal column 8, will be between the metal column 8 connect with steelframe 9, the destructive distillation gas outlet of retort section upper end 11 connects by pipeline and whirlwind chuck 3 one end pipes, and cooling section is connected with honeycomb metal interchanger 7 by pipeline; The other end of whirlwind chuck 3 connects by pipeline and described water-cooled electric coke catcher 4 pipes, described water-cooled electric coke catcher 4 by pipeline with connect respectively at the cooling section pipe of described storage tank 5, burner 6 and furnace 2, burner 6 and honeycomb metal interchanger 7 join, and belong to honeycomb interchanger 7 and are connected with dryer section with the retort section of described gas retort 2 respectively by pipeline;
Above-mentioned efficient powder resinous shale is put forward the method for the device of oil, specifically may further comprise the steps:
At first, the raw material powder resinous shale enters in the gas retort 2 from feeding unit, through after the dryer section, enters in the retort section, and temperature is that 550 ~ 650 ℃ the inlet mouth 10 of hot gas gas by even gas distribution device 1 enters dried
Evenly to diffusion all around, carry out direct heat exchange with the raw material powder resinous shale that falls in the section of heating up in a steamer, the raw material powder resinous shale is heated to 450 ~ 500 ℃, generation oil gas is decomposed in destructive distillation;
Then, the oil gas that decomposition is come out enters water-cooled electric coke catcher 4 from destructive distillation gas outlet 11 through whirlwind chucks 3 and carries out condensation, is cooled to liquid shale oil and enters storage tank 5; Not by destructive distillation resinous shale formation completely semicoke, enter under the self gravitation effect in the cooling section of gas retort 2 bottoms in the gas retort 2, cooled shale semicockes are discharged from gas retort 2 bottoms;
At last, a gas gas part that is not condensed feeds burner 4 and burns, and another part enters the sensible heat of the cooling section recovery semicoke of gas retort 2, enters in the honeycomb metal interchanger 7; Dryer section and retort section that gas gas heat exchange in hot flue gas of burner 6 incendiary and honeycomb metal interchanger, heated gas gas feed gas retort 2 realize circulation with this.
The raw material powder resinous shale is entered in the gas retort from feeding unit, through after the dryer section with the constant temperature retort section in 550 ℃ hot gas gas carry out direct heat exchange, the raw material powder resinous shale is heated to 450 ℃, destructive distillation is decomposed and is produced oil gas; Decompose the oil gas that comes out and enter the condenser system condensation, be cooled to liquid shale oil and enter storage tank from the body of heater top through oil gas collecting device.By destructive distillation resinous shale formation completely semicoke, enter the cooling section of gas retort bottom under the self gravitation effect in the gas retort, cooled shale semicockes are discharged from the bottom.A gas gas part that is not condensed feeds burner combustion, and another part enters the sensible heat of the cooling section recovery semicoke of gas retort, enters efficient metal honeycomb interchanger subsequently; Through the hot flue gas and the gas heat exchange that feeds efficient metal honeycomb interchanger of burner combustion, heated gas feeds the gas retort retort section and realizes circulation with this.
Embodiment 2:
The raw material powder resinous shale is entered in the gas retort from feeding unit, through after the dryer section with the constant temperature retort section in 600 ℃ hot gas gas carry out direct heat exchange, the raw material powder resinous shale is heated to 475 ℃, destructive distillation is decomposed and is produced oil gas; Decompose the oil gas that comes out and enter the condenser system condensation, be cooled to liquid shale oil and enter storage tank from the body of heater top through oil gas collecting device.By destructive distillation resinous shale formation completely semicoke, enter the cooling section of gas retort bottom under the self gravitation effect in the gas retort, cooled shale semicockes are discharged from the bottom.A gas gas part that is not condensed feeds burner combustion, and another part enters the sensible heat of the cooling section recovery semicoke of gas retort, enters the honeycomb metal interchanger subsequently; Through the hot flue gas and the gas heat exchange that feeds the honeycomb metal interchanger of burner combustion, heated gas feeds the gas retort retort section and realizes circulation with this.
The raw material powder resinous shale is entered in the gas retort from feeding unit, through after the dryer section with the constant temperature retort section in 650 ℃ hot gas gas carry out direct heat exchange, the raw material powder resinous shale is heated to 500 ℃, destructive distillation is decomposed and is produced oil gas; Decompose the oil gas that comes out and enter the condenser system condensation, be cooled to liquid shale oil and enter storage tank from the body of heater top through oil gas collecting device.By destructive distillation resinous shale formation completely semicoke, enter the cooling section of gas retort bottom under the self gravitation effect in the gas retort, cooled shale semicockes are discharged from the bottom.A gas gas part that is not condensed feeds burner combustion, and another part enters the sensible heat of the cooling section recovery semicoke of gas retort, enters the honeycomb metal interchanger subsequently; Through the hot flue gas and the gas heat exchange that feeds the honeycomb metal interchanger of burner combustion, heated gas feeds the gas retort retort section and realizes circulation with this.
Claims (2)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 201110067655 CN102161899B (en) | 2011-03-21 | 2011-03-21 | Efficient internal thermal type oil extraction device for powder oil shale and extraction method thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 201110067655 CN102161899B (en) | 2011-03-21 | 2011-03-21 | Efficient internal thermal type oil extraction device for powder oil shale and extraction method thereof |
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| CN102161899A true CN102161899A (en) | 2011-08-24 |
| CN102161899B CN102161899B (en) | 2013-05-08 |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104498069A (en) * | 2014-12-30 | 2015-04-08 | 汪清县龙腾能源开发有限公司 | Oil shale distillation process employing dry coke exhaust gas heat carrier |
| CN107513396A (en) * | 2017-08-31 | 2017-12-26 | 榆林煤化工产业促进中心 | A kind of fine coal drying oven dried based on packed bed and drying device and technique based on the drying oven |
| CN112708430A (en) * | 2021-01-04 | 2021-04-27 | 山东省科学院能源研究所 | Continuous solid organic matter pyrolysis poly-generation system and use method thereof |
| CN114440227A (en) * | 2022-03-11 | 2022-05-06 | 江苏碳峰蓝节能科技有限公司 | Belt type in-situ oxidation device |
| CN116333771A (en) * | 2023-05-10 | 2023-06-27 | 中国矿业大学 | A device and method for increasing the yield of oil shale light oil |
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2011
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Patent Citations (6)
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| GB785863A (en) * | 1955-02-14 | 1957-11-06 | Kellogg M W Co | Improvements in or relating to carbonization of carbonaceous materials |
| US3887453A (en) * | 1971-09-06 | 1975-06-03 | Petroleo Brasileiro Sa | Process for obtaining oil, gas and byproducts from pyrobituminous shale or other solid materials impregnated with hydrocarbons |
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Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104498069A (en) * | 2014-12-30 | 2015-04-08 | 汪清县龙腾能源开发有限公司 | Oil shale distillation process employing dry coke exhaust gas heat carrier |
| CN107513396A (en) * | 2017-08-31 | 2017-12-26 | 榆林煤化工产业促进中心 | A kind of fine coal drying oven dried based on packed bed and drying device and technique based on the drying oven |
| CN107513396B (en) * | 2017-08-31 | 2024-05-07 | 榆林煤化工产业促进中心 | Pulverized coal drying furnace based on packed bed drying and drying device and process based on drying furnace |
| CN112708430A (en) * | 2021-01-04 | 2021-04-27 | 山东省科学院能源研究所 | Continuous solid organic matter pyrolysis poly-generation system and use method thereof |
| CN112708430B (en) * | 2021-01-04 | 2022-03-04 | 山东省科学院能源研究所 | A kind of continuous solid organic matter pyrolysis polygeneration system and using method thereof |
| CN114440227A (en) * | 2022-03-11 | 2022-05-06 | 江苏碳峰蓝节能科技有限公司 | Belt type in-situ oxidation device |
| CN116333771A (en) * | 2023-05-10 | 2023-06-27 | 中国矿业大学 | A device and method for increasing the yield of oil shale light oil |
| CN116333771B (en) * | 2023-05-10 | 2023-10-20 | 中国矿业大学 | A device and method for improving light oil yield in oil shale |
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| CN102161899B (en) | 2013-05-08 |
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