CN102090406A - Application of rotenone to preparation of termite insecticide capable of killing termites effectively - Google Patents
Application of rotenone to preparation of termite insecticide capable of killing termites effectively Download PDFInfo
- Publication number
- CN102090406A CN102090406A CN2009102011461A CN200910201146A CN102090406A CN 102090406 A CN102090406 A CN 102090406A CN 2009102011461 A CN2009102011461 A CN 2009102011461A CN 200910201146 A CN200910201146 A CN 200910201146A CN 102090406 A CN102090406 A CN 102090406A
- Authority
- CN
- China
- Prior art keywords
- rotenone
- termite
- group
- sumicidin
- application
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 229940080817 rotenone Drugs 0.000 title claims abstract description 54
- JUVIOZPCNVVQFO-UHFFFAOYSA-N rotenone Natural products O1C2=C3CC(C(C)=C)OC3=CC=C2C(=O)C2C1COC1=C2C=C(OC)C(OC)=C1 JUVIOZPCNVVQFO-UHFFFAOYSA-N 0.000 title claims abstract description 54
- 241000256602 Isoptera Species 0.000 title claims abstract description 53
- 238000002360 preparation method Methods 0.000 title abstract description 8
- 239000002917 insecticide Substances 0.000 title abstract description 5
- 231100000572 poisoning Toxicity 0.000 claims description 9
- 230000000607 poisoning effect Effects 0.000 claims description 9
- QSHDDOUJBYECFT-UHFFFAOYSA-N mercury Chemical compound [Hg] QSHDDOUJBYECFT-UHFFFAOYSA-N 0.000 claims description 5
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract description 15
- 239000000126 substance Substances 0.000 abstract description 5
- WQGWDDDVZFFDIG-UHFFFAOYSA-N pyrogallol Chemical compound OC1=CC=CC(O)=C1O WQGWDDDVZFFDIG-UHFFFAOYSA-N 0.000 abstract description 3
- 231100000331 toxic Toxicity 0.000 abstract description 3
- 230000002588 toxic effect Effects 0.000 abstract description 3
- 230000000749 insecticidal effect Effects 0.000 abstract description 2
- 239000004094 surface-active agent Substances 0.000 abstract description 2
- 239000000654 additive Substances 0.000 abstract 1
- 230000002349 favourable effect Effects 0.000 abstract 1
- 244000144972 livestock Species 0.000 abstract 1
- NYPJDWWKZLNGGM-UHFFFAOYSA-N fenvalerate Chemical compound C=1C=C(Cl)C=CC=1C(C(C)C)C(=O)OC(C#N)C(C=1)=CC=CC=1OC1=CC=CC=C1 NYPJDWWKZLNGGM-UHFFFAOYSA-N 0.000 description 26
- 239000003814 drug Substances 0.000 description 24
- 239000000575 pesticide Substances 0.000 description 9
- 241000238631 Hexapoda Species 0.000 description 8
- 230000037396 body weight Effects 0.000 description 8
- 241000699666 Mus <mouse, genus> Species 0.000 description 6
- 239000003795 chemical substances by application Substances 0.000 description 6
- 230000000694 effects Effects 0.000 description 6
- 239000000839 emulsion Substances 0.000 description 6
- 238000000034 method Methods 0.000 description 6
- 241001509962 Coptotermes formosanus Species 0.000 description 5
- 241000196324 Embryophyta Species 0.000 description 5
- 241001509967 Reticulitermes flavipes Species 0.000 description 5
- 230000000857 drug effect Effects 0.000 description 5
- 238000012360 testing method Methods 0.000 description 5
- 231100000419 toxicity Toxicity 0.000 description 5
- 230000001988 toxicity Effects 0.000 description 5
- 241000723353 Chrysanthemum Species 0.000 description 4
- 235000007516 Chrysanthemum Nutrition 0.000 description 4
- 235000014347 soups Nutrition 0.000 description 4
- 230000001018 virulence Effects 0.000 description 4
- 239000003905 agrochemical Substances 0.000 description 3
- 238000009395 breeding Methods 0.000 description 3
- 230000001488 breeding effect Effects 0.000 description 3
- 230000006378 damage Effects 0.000 description 3
- 238000001035 drying Methods 0.000 description 3
- 238000003197 gene knockdown Methods 0.000 description 3
- 230000029058 respiratory gaseous exchange Effects 0.000 description 3
- 241001124076 Aphididae Species 0.000 description 2
- 241001465754 Metazoa Species 0.000 description 2
- 241000699670 Mus sp. Species 0.000 description 2
- 241000255969 Pieris brassicae Species 0.000 description 2
- 241000500437 Plutella xylostella Species 0.000 description 2
- 230000005540 biological transmission Effects 0.000 description 2
- 230000000853 biopesticidal effect Effects 0.000 description 2
- 238000004140 cleaning Methods 0.000 description 2
- 230000007423 decrease Effects 0.000 description 2
- 229940079593 drug Drugs 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- GVYLCNUFSHDAAW-UHFFFAOYSA-N mirex Chemical compound ClC12C(Cl)(Cl)C3(Cl)C4(Cl)C1(Cl)C1(Cl)C2(Cl)C3(Cl)C4(Cl)C1(Cl)Cl GVYLCNUFSHDAAW-UHFFFAOYSA-N 0.000 description 2
- LCCNCVORNKJIRZ-UHFFFAOYSA-N parathion Chemical compound CCOP(=S)(OCC)OC1=CC=C([N+]([O-])=O)C=C1 LCCNCVORNKJIRZ-UHFFFAOYSA-N 0.000 description 2
- 238000003756 stirring Methods 0.000 description 2
- CQOZJDNCADWEKH-UHFFFAOYSA-N 2-[3,3-bis(2-hydroxyphenyl)propyl]phenol Chemical compound OC1=CC=CC=C1CCC(C=1C(=CC=CC=1)O)C1=CC=CC=C1O CQOZJDNCADWEKH-UHFFFAOYSA-N 0.000 description 1
- ACTIUHUUMQJHFO-UHFFFAOYSA-N Coenzym Q10 Natural products COC1=C(OC)C(=O)C(CC=C(C)CCC=C(C)CCC=C(C)CCC=C(C)CCC=C(C)CCC=C(C)CCC=C(C)CCC=C(C)CCC=C(C)CCC=C(C)C)=C(C)C1=O ACTIUHUUMQJHFO-UHFFFAOYSA-N 0.000 description 1
- 241000892865 Heros Species 0.000 description 1
- ZSBXGIUJOOQZMP-UHFFFAOYSA-N Isomatrine Natural products C1CCC2CN3C(=O)CCCC3C3C2N1CCC3 ZSBXGIUJOOQZMP-UHFFFAOYSA-N 0.000 description 1
- ZSBXGIUJOOQZMP-JLNYLFASSA-N Matrine Chemical compound C1CC[C@H]2CN3C(=O)CCC[C@@H]3[C@@H]3[C@H]2N1CCC3 ZSBXGIUJOOQZMP-JLNYLFASSA-N 0.000 description 1
- 102000006746 NADH Dehydrogenase Human genes 0.000 description 1
- 108010086428 NADH Dehydrogenase Proteins 0.000 description 1
- 206010033799 Paralysis Diseases 0.000 description 1
- 241000269799 Perca fluviatilis Species 0.000 description 1
- 235000008331 Pinus X rigitaeda Nutrition 0.000 description 1
- 235000011613 Pinus brutia Nutrition 0.000 description 1
- 241000018646 Pinus brutia Species 0.000 description 1
- VQXSOUPNOZTNAI-UHFFFAOYSA-N Pyrethrin I Natural products CC(=CC1CC1C(=O)OC2CC(=O)C(=C2C)CC=C/C=C)C VQXSOUPNOZTNAI-UHFFFAOYSA-N 0.000 description 1
- 241000607479 Yersinia pestis Species 0.000 description 1
- 210000001015 abdomen Anatomy 0.000 description 1
- 230000009471 action Effects 0.000 description 1
- 230000008901 benefit Effects 0.000 description 1
- 230000001684 chronic effect Effects 0.000 description 1
- ACTIUHUUMQJHFO-UPTCCGCDSA-N coenzyme Q10 Chemical compound COC1=C(OC)C(=O)C(C\C=C(/C)CC\C=C(/C)CC\C=C(/C)CC\C=C(/C)CC\C=C(/C)CC\C=C(/C)CC\C=C(/C)CC\C=C(/C)CC\C=C(/C)CCC=C(C)C)=C(C)C1=O ACTIUHUUMQJHFO-UPTCCGCDSA-N 0.000 description 1
- 235000017471 coenzyme Q10 Nutrition 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 239000000470 constituent Substances 0.000 description 1
- 239000006071 cream Substances 0.000 description 1
- 238000000354 decomposition reaction Methods 0.000 description 1
- FPAFDBFIGPHWGO-UHFFFAOYSA-N dioxosilane;oxomagnesium;hydrate Chemical compound O.[Mg]=O.[Mg]=O.[Mg]=O.O=[Si]=O.O=[Si]=O.O=[Si]=O.O=[Si]=O FPAFDBFIGPHWGO-UHFFFAOYSA-N 0.000 description 1
- 230000027721 electron transport chain Effects 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 230000003203 everyday effect Effects 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 238000003304 gavage Methods 0.000 description 1
- 230000036541 health Effects 0.000 description 1
- 235000008216 herbs Nutrition 0.000 description 1
- 230000036039 immunity Effects 0.000 description 1
- 230000009545 invasion Effects 0.000 description 1
- -1 kuh-seng Substances 0.000 description 1
- 231100000518 lethal Toxicity 0.000 description 1
- 230000001665 lethal effect Effects 0.000 description 1
- 231100000225 lethality Toxicity 0.000 description 1
- 231100000053 low toxicity Toxicity 0.000 description 1
- 229930014456 matrine Natural products 0.000 description 1
- 230000010534 mechanism of action Effects 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 231100000252 nontoxic Toxicity 0.000 description 1
- 230000003000 nontoxic effect Effects 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 238000006303 photolysis reaction Methods 0.000 description 1
- 239000002574 poison Substances 0.000 description 1
- 231100000614 poison Toxicity 0.000 description 1
- 244000144977 poultry Species 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- HYJYGLGUBUDSLJ-UHFFFAOYSA-N pyrethrin Natural products CCC(=O)OC1CC(=C)C2CC3OC3(C)C2C2OC(=O)C(=C)C12 HYJYGLGUBUDSLJ-UHFFFAOYSA-N 0.000 description 1
- VJFUPGQZSXIULQ-XIGJTORUSA-N pyrethrin II Chemical compound CC1(C)[C@H](/C=C(\C)C(=O)OC)[C@H]1C(=O)O[C@@H]1C(C)=C(C\C=C/C=C)C(=O)C1 VJFUPGQZSXIULQ-XIGJTORUSA-N 0.000 description 1
- NPCOQXAVBJJZBQ-UHFFFAOYSA-N reduced coenzyme Q9 Natural products COC1=C(O)C(C)=C(CC=C(C)CCC=C(C)CCC=C(C)CCC=C(C)CCC=C(C)CCC=C(C)CCC=C(C)CCC=C(C)CCC=C(C)C)C(O)=C1OC NPCOQXAVBJJZBQ-UHFFFAOYSA-N 0.000 description 1
- 230000011514 reflex Effects 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 239000007921 spray Substances 0.000 description 1
- 210000002784 stomach Anatomy 0.000 description 1
- 231100000027 toxicology Toxicity 0.000 description 1
- 229940035936 ubiquinone Drugs 0.000 description 1
- 210000002700 urine Anatomy 0.000 description 1
Landscapes
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The invention relates to novel application of a substance, in particular to application of rotenone to preparation of a termite insecticide capable of killing termites effectively, wherein the weight of the rotenone in the termite insecticide is 1-20mg/L. Additives are surfactants, pyrogallic acid, water and the like. The termite insecticide provided in the invention is environment-friendly and safe for people and livestock and has favorable toxic effect and remarkable contact insecticidal action.
Description
Technical field:
The present invention relates to a kind of new purposes of material, be specifically related to the application of rotenone in preparing the termite poisoning agent that effectively to kill termite.
Background technology:
Termite is as one of worldwide five major pests, seriously invading and harassing the eating of people, wears, lives, OK.As everyone knows, termite is the building insect, and they are startling especially to the harm that urban architecture causes.The economic loss of being brought and the destruction of cultural assets also allow the people shake.Along with reconstruction of the old city town, a large amount of old houses are split, destroyed the institute of termite perch, and large quantities of termites seek new habitat and the gesture that causes private residence, street tree to be subjected to the invasion and attack harm of termite again and again and have wildness day by day to spread.But hypertoxic chemical pesticide is mostly used in domestic control to termite at present.And " mirex " of domestic main control termites and " Niran " have now been forbidden by the world, and it is extremely urgent to seek the novel environment friendly agricultural chemicals.
Rotenone is present in the root skin zone of plant widely, is the very strong material of a kind of specificity on toxicology, and insect especially cabbage caterpillar, diamond-back moth and aphid are had strong tagging and two kinds of effects of stomach toxicity.The early stage mechanism of action that studies show that rotenone mainly is the respiration that influences insect, mainly be and nadh dehydrogenase and ubiquinone between a certain composition have an effect.Rotenone is suppressed the electron transport chain of insect cell, thereby the ATP level that reduces in the organism finally makes insect can not get the energy supply, then drumble, paralysis and slowly dead.Though rotenone is known to the toxic action of cabbage caterpillar, diamond-back moth and aphid, up to the present, also be not used to control termites.
Summary of the invention:
Technical problem to be solved by this invention provides the application of rotenone in preparing the termite poisoning agent that can effectively kill termite, to solve " mirex " and " Niran " problem of environment pollution caused of existing control termites.
Described application, the weight of rotenone is 1-20mg in wherein every hydrargyrum oxydatum crudum agent.Be preferably 1-10mg.1-5mg more preferably.Further be preferably 1-2.5mg.
Termite poisoning agent of the present invention is better than the chemical pesticide sumicidin, has good toxic effect, action of contace poison is remarkable, and toxicity is little, safe, to the person poultry safety.The medicine source plant resource of termite poisoning agent of the present invention is widely distributed, and growth rapidly.And because the easy photodissociation of rotenone, easily oxidation Decomposition is the compound of nontoxic or low toxicity in air, residence time weak point in environment, environmentally safe.Simultaneously, the time that insect contacts with it is short, has also reduced the chance that insect develops immunity to drugs.
Embodiment
For technological means, creation characteristic that the present invention is realized, reach purpose and effect is easy to understand, below in conjunction with concrete example, further set forth the present invention.
The preparation of embodiment 1 medicament of the present invention
Adopt surfactant (technical grade) (MP-10P), rotenone (white crystalline powder), pyrogallic acid (triphenol) and water prepares rotenone water emulsion, each constituent mass such as following table 1:
Table 1 rotenone water emulsion prepares required medicine and each mass distribution table
| Nomenclature of drug | MP-10P | Rotenone | Pyrogallic acid | Water |
| Required quality | 2.5766g | 2.5611g | 2.1742g | 65g |
Get required medicine on electronic balance, claim required quality, put into the beaker medicine that is dissolved in water.Beaker is put into the time constant-temperature magnetic stirrer stir, about 20min.At last medicament is placed on high shear and disperses emulsion to carry out last stirring, about 45min finishes the preparation of medicament.The pH value of the rotenone water emulsion of being prepared is 4.5.
Get the aqueous emulsion that contains 3.5% rotenone that configures in right amount, add entry, make that soup (rotenone) concentration is 1mg/L.
The preparation of embodiment 2 cloud chrysanthemum medicaments
With cloud chrysanthemum (5% natural pyrethrin cream), the Shanghai biopesticide detects institute and provides, and adds an amount of water and is mixed with that to measure liquor strength be 1mg/L.
The preparation of embodiment 3 kuh-seng medicaments
With aqueous matrine solution (0.5%) (claiming green space again), the Shanghai biopesticide detects institute and provides, and adds an amount of water and is mixed with that to measure concentration be 1mg/L.
Embodiment 4 compares the desinsection drug effect with medicine based on herbs
The test termite is from insect museum (raising 2 years), and the feeding environment temperature is controlled at 24～27 ℃, and relative moisture is controlled at 75%～80%.Termite is fed with pine, and the water source is provided, lucifuge.
Get each 120 of Shanghai coptotermes formosanus and eastern subterranean termites, be divided into control group, rotenone group, kuh-seng group, Yun Ju group.According to medicine embrane method, with pipette the medicament 0.5ml for preparing among the embodiment 1-3 is dripped on filter paper, form even medicine film, put into clean culture dish after drying naturally, drip the 1ml redistilled water on the filter paper, each drops into 30 termites; Termite is stayed breeding observing in the culture dish.
Time recording termite rate of knockdown and death toll are until whole death.Calculate termite killing time of 50(KT50) and half death time.With the soup of isoconcentration to the termite effect after, killing time of 50(KT50) and killing time of 50(KT50) are short more, this pesticide efficacy is good more.
Plant source pesticide rotenone, Yun Ju, kuh-seng the results are shown in following table 2 to the insecticidal action of Shanghai coptotermes formosanus and eastern subterranean termite:
The comparing result that table 2 rotenone, Yun Ju, kuh-seng are imitated the termite insecticide
From last table as seen, plant source pesticide rotenone, kuh-seng, cloud chrysanthemum can both kill termite.But relatively behind killing time of 50(KT50) and the LD50 time, we find: the desinsection drug effect of rotenone is obviously good than cloud chrysanthemum and kuh-seng.
Embodiment 4 compares the desinsection drug effect with organic agricultural chemicals
Preparation rotenone and sumicidin (chemical pesticide, 5% missible oil) medicament make liquor strength be respectively high concentration 20mg/L, 10mg/L, 5mg/L, 2.5mg/L, 1mg/L.
Get each 1250 of Shanghai coptotermes formosanus and Huang Xiong reticulitermes flavipes, be divided in control group (0mg/L), rotenone high dose group (20mg/L), rotenone high dose group (10mg/L), the rotenone dosage group (2.5mg/L), rotenone low dose group (1mg/L) in dosage group (5mg/L), the rotenone.Sumicidin high dose group (20mg/L), sumicidin high dose group (10mg/L), dosage group (2.5mg/L) in dosage group (5mg/L), the sumicidin in the sumicidin, sumicidin low dose group (1mg/L).
Every group is dropped into 30 termites, termite is continued to stay breeding observing in the former culture dish.If 3 repetitions.
According to medicine embrane method, pipette soup 0.5ml with pipette, drip on filter paper, form even medicine film, put into clean culture dish after drying naturally, drip the 1ml redistilled water on the filter paper, drop into 30 termites; Termite is continued to stay breeding observing in the former culture dish.Time recording termite rate of knockdown and death toll the results are shown in following table 3 and table 4:
Table 3 rotenone and sumicidin are to the influence of Shanghai coptotermes formosanus
Table 4 rotenone and sumicidin are to the influence of eastern subterranean termite
From table 3 and table 4 as seen, rotenone and sumicidin to the termite effect after, the half lethal time and the time of partly knocking down shorten along with the increase gradually of pesticide concentration.Integrate and see, relatively rotenone and sumicidin are to the drug effect of coptotermes formosanus and eastern subterranean termite, both drug effect there was no significant differences (p＞0.05).
Embodiment 5 termites are to the indoor virulence transmission of rotenone medicament
Transmit the method for testing of medicament according to contact, rotenone (2% aqueous emulsion) adds an amount of water, and to be mixed with concentration be behind 1% the medicament, to pipette the 1ml soup with pipette, evenly drips on filter paper, puts into culture dish after drying naturally, 50 of input termites.
Be mixed with the pulvis of experimental concentration with talcum powder after, get 15mg, in culture dish, evenly spray, drop into 50 of termites in the culture dish in advance, make and be stained with pulvis on the termite health uniformly.The termite that will occupy pulvis then moves in the culture dish of a cleaning, and the culture dish bottom is covered with filter paper.With dripping the 1ml redistilled water on the filter paper after the said method processing, observe.When the termite that is moved into another termite culture dish knock down and dead individual sum also reach drop into the termite sum 20% the time, shift out 8 termites alive again, drop into the culture dish that another is placed with 50 termites in advance.So repeatable operation until being moved into termite lethality＜90%, finishes test.
If blank is established 3 repetitions.The record termite is knocked down number or death toll, the results are shown in Table 5:
Table 5 termite is transmitted test result to the agricultural chemicals indoor virulence
| Group | Killing time of 50(KT50) (min) | LD50 time (min) | Dead quantity (head) |
| Control group (0%) | Do not have | Do not have | Do not have |
| First group (dropping in advance) | 7.21±0.16 | 15.22±0.48 | 8 |
| Second group | 15.01±0.44 | 20.12±0.49 | 8 |
The result shows: effective virulence degree of transitivity 〉=1 time proves to have the virulence transmission effect.
Embodiment 6 rotenone are to the mensuration of animal poisoning
Reference example 4 preparation rotenone and sumicidin medicaments.
Employing is available from totally 70 of cleaning level 20 age in days ICR heros, the female mices (each 35) of Shanghai Slac Experimental Animal Co., Ltd. (credit number SCXX (Shanghai) 2003-0003), average weight 18 grams.Adapt to after 5 days and be divided into dosage group (1g/ml), sumicidin low dose group (0.1g/mg), sumicidin low dose group (0.01g/ml), sumicidin skin contact group (0.1mg/L) in normal group (0g/ml), rotenone low dose group (0.1g/ml), rotenone low dose group (0.01g/ml), rotenone skin contact group (0.1g/ml), the sumicidin at random by body weight.Every group 8, each organizes initial body weight there was no significant difference.Each organizes equal ad lib, water inlet.Except that normal group, all the other each groups all experimentize by the following method:
A) administration by gavage
Be decided to be rotenone (0.1g/ml, 0.01g/ml) group, sumicidin (1g/ml, 0.1g/ml, 0.01g/ml) group according to experiment test concentration, establish blank.Behind every day every mice lavage 1ml medicament, observed result after 24 hours.As the mensuration of chronic murder by poisoning, observed continuously 14 days, observe its body weight and have or not decline, get the food situation, and other physiological reactions (breathing, heartbeat, stool and urine etc.).
B) skin contact toxicity determination method
Embrocate the solvent (concentration is 0.1g/ml) of medicament on skin of abdomen, embrocate area and be generally 1 square inch, observe its poisoning sign (breathing, heartbeat etc.), skin is embrocated the reflection at position and is caused the dead time, the results are shown in Table 6:
Table 6 rotenone and sumicidin are to the influence of small white mouse body weight
| Group | 1d(g) | 7d(g) | 14d(g) | Dead quantity (head) |
| Normal group (0g/ml) | 18.41±0.16 | 29.31±0.31 | 34.63±0.28 | Do not have |
| Rotenone group (0.1g/ml) | 18.31±0.23 | 24.25±0.18 | 28.06±0.15 | Do not have |
| Rotenone group (0.01g/ml) | 18.35±0.18 | 27.39±0.35 | 31.02±0.45 | Do not have |
| Rotenone skin group (0.1g/ml) | 19.16±0.52 | 29.23±0.49 | 34.08±0.51 | Do not have |
| Sumicidin group (1g/ml) | 18.57±0.21 | Do not have | ||
| Sumicidin group (0.1g/ml) | 19.07±0.31 | 22.82±0.22 | 26.85±0.24 | Do not have |
| Sumicidin group (0.01g/ml) | 19.06±0.16 | 23.07±0.21 | 27.31±0.02 | Do not have |
| Sumicidin skin group (0.1g/ml) | 19.13±0.11 | 24.01±0.11 | 28.72±0.21 | Do not have |
As seen from Table 1, sumicidin group mouse body weight obviously descends (p＜0.05) than normal group mouse body weight really, and sumicidin is respectively organized mouse weight ratio rotenone and respectively organized the mouse body weight significant difference (p＜0.05) is arranged.Wherein rotenone skin group (0.1g/ml) does not have significant difference (p＞0.05) though the mouse body weight also has decline scope with normal group.
Experimental result shows that plant source pesticide rotenone is better than the chemical pesticide sumicidin, environmental protection and safety.Sumicidin toxicity is big, to animal and even the bigger toxicity of human body.
More than show and described basic principle of the present invention, principal character and advantage of the present invention.The technical staff of the industry should understand; the present invention is not restricted to the described embodiments; that describes in the foregoing description and the specification just illustrates principle of the present invention; the present invention also has various changes and modifications without departing from the spirit and scope of the present invention, and these changes and improvements all fall in the claimed scope of the invention.The claimed scope of the present invention is defined by appending claims and equivalent thereof.
Claims (5)
1. the application of rotenone in preparing the termite poisoning agent that effectively to kill termite.
2. application as claimed in claim 1 is characterized in that: the weight of rotenone is 1-20mg in every hydrargyrum oxydatum crudum agent.
3. application according to claim 2 is characterized in that: the weight of rotenone is 1-10mg in every hydrargyrum oxydatum crudum agent.
4. application according to claim 3 is characterized in that: the weight of rotenone is 1-5mg in every hydrargyrum oxydatum crudum agent.
5. application according to claim 4 is characterized in that: the weight of rotenone is 1-2.5mg in every hydrargyrum oxydatum crudum agent.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2009102011461A CN102090406A (en) | 2009-12-15 | 2009-12-15 | Application of rotenone to preparation of termite insecticide capable of killing termites effectively |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2009102011461A CN102090406A (en) | 2009-12-15 | 2009-12-15 | Application of rotenone to preparation of termite insecticide capable of killing termites effectively |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN102090406A true CN102090406A (en) | 2011-06-15 |
Family
ID=44123803
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN2009102011461A Pending CN102090406A (en) | 2009-12-15 | 2009-12-15 | Application of rotenone to preparation of termite insecticide capable of killing termites effectively |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN102090406A (en) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103125499A (en) * | 2011-11-30 | 2013-06-05 | 中国人民解放军疾病预防控制所 | Repellent of snakes, scorpions and centipedes |
| CN106942304A (en) * | 2017-04-11 | 2017-07-14 | 安徽省明美矿物化工有限公司 | A kind of concave convex rod ant killing agent and preparation method thereof |
| CN107467081A (en) * | 2017-08-28 | 2017-12-15 | 广西壮族自治区农业科学院植物保护研究所 | A kind of plant source kills ant pulvis and preparation method thereof |
| CN113057180A (en) * | 2021-04-13 | 2021-07-02 | 万一 | Herbal insect-resist agent |
-
2009
- 2009-12-15 CN CN2009102011461A patent/CN102090406A/en active Pending
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103125499A (en) * | 2011-11-30 | 2013-06-05 | 中国人民解放军疾病预防控制所 | Repellent of snakes, scorpions and centipedes |
| CN106942304A (en) * | 2017-04-11 | 2017-07-14 | 安徽省明美矿物化工有限公司 | A kind of concave convex rod ant killing agent and preparation method thereof |
| CN107467081A (en) * | 2017-08-28 | 2017-12-15 | 广西壮族自治区农业科学院植物保护研究所 | A kind of plant source kills ant pulvis and preparation method thereof |
| CN113057180A (en) * | 2021-04-13 | 2021-07-02 | 万一 | Herbal insect-resist agent |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN103004858B (en) | Insecticidal composition containing methylamino abamectin and pyrethroid compound | |
| CN101461364B (en) | Poison bait for killing solenopsis invicta | |
| JPH03505458A (en) | Methods and terrestrial release compositions for controlling insect and habitat-associated pest populations in terrestrial environments | |
| CN112568235B (en) | Film spreading oil solution sanitary pesticide for killing mosquito as dengue fever vector infectious disease transmission vector and preparation method thereof | |
| CN101658169B (en) | Solenopsis invicta and termite touch killing powder containing ethofenprox | |
| CN104938528B (en) | A kind of termite-killing trapping medicament and preparation method | |
| CN103651519A (en) | Compound pesticide composition containing flonicamid and bifenthrin | |
| CN101861876A (en) | Soil termite trapping medicine and soil termite trapping method by using the same | |
| CN102657176A (en) | Tolfenpxrad-containing smoke agent | |
| CN102090406A (en) | Application of rotenone to preparation of termite insecticide capable of killing termites effectively | |
| CN104872216A (en) | Plant-source synergist and insect aerosol prepared by same | |
| CN104522054A (en) | Biological source synergistic compound insecticide, preparation method and application thereof | |
| CN103004854A (en) | Allyl isothiocyanate and nicotine compound insecticide and application thereof | |
| CN103651552B (en) | Ultra-low-volume liquor containing chlorfenapyr | |
| CN102334516A (en) | Attractant synergist at early stage of egg laying of monochamus alternatus hope and preparation method thereof | |
| CN105410013A (en) | Insecticide-pesticide mixture preparation | |
| CN102933082A (en) | Compositions and methods for control of sand flies and other blood sucking insects | |
| CN102246839A (en) | Compounded pesticide for controlling diseases and insects of rice and forest | |
| CN101637181A (en) | Pesticide mixture agent for preventing ostrinia nubilalis and application thereof | |
| CN111296478A (en) | Boric acid-containing insecticidal composition and application thereof | |
| CN101341877B (en) | Pesticide preparation mixed with tubatoxin, pyrethroid and phoxim | |
| CN1433693A (en) | Abamectin and entomogenous fungi composed microbial pesticide | |
| CN1070026C (en) | Hygienic biocide composition | |
| CN107821413A (en) | A kind of cockroach bait formulation and preparation method thereof | |
| CN113180044A (en) | Solenopsis invicta pheromone attractant and killing agent containing the same |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C02 | Deemed withdrawal of patent application after publication (patent law 2001) | ||
| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20110615 |