CN102000009B - Flaxseed oil-containing cleansing cream and preparation method thereof - Google Patents

Abstract

The invention relates to a facial cleanser containing linseed oil and a preparation method thereof. A facial cleanser containing linseed oil, characterized in that the mass parts of its raw materials are as follows: 21-60 parts of deionized water, 10-30 parts of sodium lauramide glutamate, 0-30 parts of potassium cocoyl glutamate 10 parts, 5-25 parts of betaine, 2-10 parts of refined beeswax, 0.01-1 part of cold-pressed linseed oil, 1-6 parts of camellia seed oil, 0.0001-0.5 parts of antioxidant, 0.1-0.5 parts of Genma BP , 0.01 to 0.1 parts of essence. The facial cleanser prepared by the formula has the characteristics of being natural, non-irritating and non-damaging, and also has a certain nursing and health care effect on facial skin cells.

Description

A kind of facial cleanser containing linseed oil and preparation method thereof

technical field

The invention belongs to the technical field of cleansing cosmetics for human skin, and in particular relates to a facial cleanser and a preparation method thereof.

Background technique

In view of the fact that some facial cleansers on the market have strong degreasing power and strong irritation, long-term use will easily damage the natural water retention barrier of the skin, resulting in an abnormal increase in transepidermal water loss, resulting in dry and rough facial skin, choose a natural, non-irritating surface The active agent system and adding some natural skin care conditioning ingredients have become the main ways to reduce the irritation of facial cleanser (cream) products. For example, the ginseng and aloe facial cleanser (patent application number: CN200510015038.7) invented by Song Guoqiang in my country adds ginseng extract and aloe gel to the surfactant plus weak alkaline soap base cleaning system. A variety of nutrients and moisturizing ingredients are needed, and also have the functions of sterilization, antibacterial, anti-inflammatory, and detoxification; Wu Hongan invented the honey peptide rejuvenating cleansing cream (patent application number: CN200810123277.8) using amino acid surfactants and The soap-based mixed cleansing system plus bee jelly freeze-dried powder claims to have the effect of refreshing, clear and whitening the skin. The active ingredients in facial cleanser/cream contact with the facial skin during the cleaning process, on the one hand, it reduces the irritation of the surfactant and soap base on the facial skin, and some active ingredients are adsorbed on the skin to play the role of nutrition and moisturizing, so as to cleanse the facial skin At the same time realize the nursing function.

At present, due to the poor oxidation stability of linseed oil, there is no relevant report on using linseed oil as a functional ingredient in facial cleansing products to make it have repairing and moisturizing functions.

Contents of the invention

The purpose of the present invention is to provide a facial cleanser containing linseed oil and a preparation method thereof. The facial cleanser prepared by the method has natural and non-irritating characteristics, has no damage to facial skin cells, and has certain repairing and moisturizing effects .

In order to achieve the above object, the technical solution adopted by the present invention is: a facial cleanser containing linseed oil, characterized in that its composition raw materials and mass parts are as follows:

Phase A: 21-60 parts of deionized water,

Sodium lauramide glutamate 10-30 parts,

Potassium cocoyl glutamate 0-10 parts,

5-25 parts of betaine,

                                                                                                   

Phase B: cold-pressed linseed oil 0.01-1 part,

    1 to 6 parts of camellia seed oil,

Phase C: Antioxidant 0.0001～0.5 part,

Genma BP 0.1～0.5 copies,

Essence 0.01-0.1 parts.

The antioxidant is any one of natural vitamin E, ascorbyl palmitate, magnesium ascorbyl phosphate, 2,6-di-tert-butyl-4-methylphenol or a mixture of any two or more (including two) , when any two or more kinds (including two kinds) are mixed, it is an arbitrary proportion.

The best mass fraction of cold-pressed linseed oil is: 0.1-1.

The optimum mass fraction of potassium cocoyl glutamate is 0.1-10 parts.

The optimum proportion by mass of the antioxidant is: 0.001-0.5 parts.

The preparation method of above-mentioned a kind of facial cleanser containing linseed oil is characterized in that following steps are carried out successively:

1) Selection of raw materials: according to the mass parts of each raw material: 21-60 parts of deionized water, 10-30 parts of sodium lauramide glutamate, 0-10 parts of potassium cocoyl glutamate, 5 parts of betaine ~25 parts, refined beeswax 2~10 parts, cold pressed linseed oil 0.01~1 part, camellia seed oil 1~6 parts, antioxidant 0.0001~0.5 parts, Genma BP 0.1~0.5 parts, essence 0.01~0.1 parts ;Choose deionized water, sodium lauramide glutamate, potassium cocoyl glutamate, betaine, refined beeswax, cold-pressed linseed oil, camellia seed oil, antioxidants, Genma BP and essence, and set aside;

2) Add deionized water into the emulsification tank, then put sodium lauramide glutamate into the emulsification tank, stir after soaking; then put refined beeswax and betaine into the emulsification tank, stir; continue stirring and heating to 70-85°C , heat preservation and stirring for 15-60 minutes; add potassium cocoyl glutamate and stir evenly, stop heating and stirring, let stand for 10-60 minutes, until the upper layer has a small amount of foam, and the lower layer is transparent; stir, cool down to 45-58°C, add cold-pressed Flaxseed oil, camellia seed oil and antioxidants; continue to stir, cool down to 35-45°C, add essence and Genma BP, stir well, turn off the power, let it stand overnight, and you can get a facial cleanser containing linseed oil .

The cold-pressed linseed oil used in the present invention is rich in essential fatty acids α-linolenic acid and linoleic acid, and also contains trace amounts of vitamin E, vitamin A, phytosterols, polypeptides and other natural skin care ingredients, especially α-linolenic acid The content is as high as 60wt%, and it has special nourishing and repairing effects on damaged skin lacking in α-linolenic acid. Studies have shown that cold-pressed linseed oil has relatively high vitamin E content and low phospholipid content, which maintains the natural quality of linseed oil and has good skin permeability and repairing effects. Topical application can easily penetrate into the epidermis and dermis. It can enhance and maintain the normal structure and function of skin cell membrane, repair the natural barrier function of skin cells, reduce transepidermal water loss, increase the hydration and moisturizing effect of epidermal cells, etc.

The purpose of adding cold-pressed linseed oil in the present invention is mainly to promote the gradual repair of the natural water-retaining barrier of damaged neutral to dry skin, restore health and moisten; for normal skin, the natural water-retaining barrier function of the skin is enhanced to deeply moisturize. Due to the poor oxidation stability of linseed oil, the cold-pressed linseed oil used in the present invention is mixed with camellia seed oil and antioxidants with good stability and emollient effect in a certain proportion, and its oxidation is measured by RANCIMAT accelerated oxidation instrument. The stability is 5-10 times higher than that of cold-pressed linseed oil alone.

The present invention selects a non-irritating, natural pure amino acid surfactant system, adds functional components rich in nutrients required by facial skin cells and deep moisturizing and repairing factors, cold-pressed linseed oil as functional components, and camellia seed oil and antioxidant composition as functional components The stabilizer and synergist of linseed oil, a facial cleanser containing linseed oil produced through the characteristic formula and specific process of the present invention, can deeply clean the facial skin, avoid excessive degreasing, and minimize skin irritation. The active ingredients in the seed oil damage the defects of skin cells, and provide a new natural cleansing product that integrates facial skin cleansing, repairing and moisturizing. It meets the current requirements of modern people who advocate nature for facial cleansing products, and has a broad market Application prospects.

The pH value of the facial cleanser of the present invention is weakly acidic, close to the pH value of the skin, has beautiful pearl luster, and has excellent cleaning effect. The added various plant essences penetrate deeply, supplementing the nutrition required by the facial skin, repairing and Strengthen the skin's natural barrier function, deeply moisturize and moisturize while cleansing.

The beneficial effects of the present invention are: the prepared facial cleanser is a natural product rich in natural plant essence (containing plant emollient ingredients such as cold-pressed linseed oil and camellia seed oil), which is natural, non-irritating, and environmentally friendly. The pH value (pH value is weakly acidic) is close to that of the skin, and the decontamination effect is good. After washing, the skin is smooth and not tight, moist and shiny, and the facial skin cells are not damaged. It has certain repairing and moisturizing functions for skin cells (with certain Nursing and health care), suitable for all skin types, especially suitable for dry and dry skin. After trial, the test population has no side effects such as skin irritation, allergic reaction or other discomfort.

Detailed ways

In order to better understand the present invention, the content of the present invention is further illustrated below in conjunction with the examples, but the content of the present invention is not limited to the following examples.

Example 1:

A preparation method of a facial cleanser containing linseed oil, which comprises the steps of:

1) Selection of raw materials: The parts by weight of each raw material are: 31.80 parts of deionized water, 15.5 parts of sodium lauramide glutamate, 2.8 parts of potassium cocoyl glutamate, 12 parts of betaine, and 4.3 parts of refined beeswax , 0.35 parts of cold-pressed linseed oil, 3 parts of camellia seed oil, 0.0005 parts of antioxidants (specifically 0.00001 ascorbyl palmitate and 0.00049 parts of natural vitamin E), 0.25 parts of Genma BP (Beijing Samp Genma BP, preservative ), essence 0.01 part; select deionized water, sodium lauramide glutamate, potassium cocoyl glutamate, betaine, refined beeswax, cold-pressed linseed oil, camellia seed oil, antioxidants, Gemma BP and Essence, spare;

2) Add deionized water into the emulsification tank, then put sodium lauramide glutamate into the emulsification tank, stir after soaking; then put refined beestaine and betaine into the emulsification tank, stir; continue to stir and heat to 85°C, keep warm Stir for 15 minutes; add potassium cocoyl glutamate and stir well, stop heating and stirring, and let it stand for 25 minutes until the upper layer has a little foam and the lower layer is transparent; stir, cool down to 45°C, add cold-pressed linseed oil, camellia seed oil and Antioxidant; continue to stir, cool down to 35°C, add essence and Genma BP, stir evenly, turn off the power, and let it stand overnight to obtain a facial cleanser containing linseed oil.

After testing, the cold-pressed linseed oil meets the national GB/T 8253-2008 standard for pressing first-grade linseed oil, the pH value of the facial cleanser containing linseed oil is 5.8, and the heat-resistant, cold-resistant stability, and hygienic indicators all meet the national standard QB/T1645-2004 standard.

The facial cleanser containing linseed oil obtained in this embodiment, after trial use, the test population has no side reactions such as skin irritation, allergic reaction or other discomfort, no damage to facial skin cells, good decontamination effect, and the skin is smooth and smooth after washing. Tight, moist and shiny, it has a certain repairing and moisturizing function for skin cells.

Example 2:

A preparation method of a facial cleanser containing linseed oil, which comprises the steps of:

1) Selection of raw materials: The parts by weight of each raw material are: 48.15 parts of deionized water, 24 parts of sodium lauramide glutamate, 6 parts of potassium cocoyl glutamate, 18 parts of betaine, and 6.5 parts of refined beeswax , 0.5 parts of cold-pressed linseed oil, 2.5 parts of camellia seed oil, 0.001 parts of antioxidants (specifically 0.0001 parts of ascorbyl palmitate, 0.0001 parts of 2,6-di-tert-butyl-4-methylphenol and 0.0008 parts of natural vitamin E), 0.5 parts of Genma BP (Beijing Samp Genma BP, preservative), 0.05 parts of essence; choose deionized water, sodium lauramide glutamate, potassium cocoyl glutamate, betaine, refined beeswax , cold-pressed linseed oil, camellia seed oil, antioxidants, Gemma BP and essence, spare;

2) Add deionized water into the emulsification tank, then put sodium lauramide glutamate into the emulsification tank, stir after soaking; then put refined beeswax and betaine into the emulsification tank, stir; continue to stir and heat to 75°C, keep warm Stir for 45 minutes; add potassium cocoyl glutamate and stir well, stop heating and stirring, and let it stand for 35 minutes until the upper layer has a little foam and the lower layer is transparent; stir, cool down to 50°C, add cold-pressed linseed oil, camellia seed oil and Antioxidant; continue to stir, cool down to 45°C, add essence and Genma BP, stir evenly, turn off the power, and let it stand overnight to obtain a facial cleanser containing linseed oil.

After testing, the cold-pressed linseed oil meets the national GB/T 8253-2008 standard for pressing first-grade linseed oil, the pH value of the facial cleanser containing linseed oil is 5.8, and the heat-resistant, cold-resistant stability, and hygiene indicators all meet the national QB /T1645-2004 standard.

The facial cleanser containing linseed oil obtained in this embodiment, after trial use, the test population has no side reactions such as skin irritation, allergic reaction or other discomfort, no damage to facial skin cells, good decontamination effect, and the skin is smooth and smooth after washing. Tight, moist and shiny, it has a certain repairing and moisturizing function for skin cells.

Example 3:

A preparation method of a facial cleanser containing linseed oil, which comprises the steps of:

2) Selection of raw materials: The parts by weight of each raw material are: 60 parts of deionized water, 30 parts of sodium lauramide glutamate, 1 part of potassium cocoyl glutamate, 25 parts of betaine, and 8.5 parts of refined beeswax , 0.8 parts of cold-pressed linseed oil, 4 parts of camellia seed oil, 0.4 parts of antioxidants (specifically 0.389 parts of magnesium ascorbyl phosphate, 0.001 parts of natural vitamin E and 0.0001 parts of 2,6-di-tert-butyl-4-methyl phenol); Genma BP (preservative) 0.4 parts, essence 0.1 parts; select deionized water, sodium lauramide glutamate, potassium cocoyl glutamate, betaine, refined beeswax, cold-pressed linseed oil, Camellia seed oil, antioxidants, preservatives and flavors, set aside;

2) Add deionized water into the emulsification tank, then put sodium lauramide glutamate into the emulsification tank, stir after soaking; then put refined beeswax and betaine into the emulsification tank, stir; continue to stir and heat to 70°C, keep warm Stir for 60 minutes; add potassium cocoyl glutamate and stir well, stop heating and stirring, and let it stand for 10 minutes until the upper layer is slightly foamy and the lower layer is transparent; stir, cool down to 55°C, add cold-pressed linseed oil, camellia seed oil and Antioxidant: Continue to stir, cool down to 40°C, add essence and Genma BP, stir evenly, turn off the power, and let it stand overnight to obtain a facial cleanser containing linseed oil.

After testing, the cold-pressed linseed oil meets the national GB/T 8253-2008 standard for pressing first-grade linseed oil, the pH value of the facial cleanser containing linseed oil is 5.8, and the heat-resistant, cold-resistant stability, and hygienic indicators all meet the national standard QB/T1645-2004 standard.

The facial cleanser containing linseed oil obtained in this embodiment, after trial use, the test population has no side reactions such as skin irritation, allergic reaction or other discomfort, no damage to facial skin cells, good decontamination effect, and the skin is smooth and smooth after washing. Tight, moist and shiny, it has a certain repairing and moisturizing function for skin cells.

Example 4:

A preparation method of a facial cleanser containing linseed oil, which comprises the steps of:

2) Selection of raw materials: The parts by weight of each raw material are: 53.6 parts of deionized water, 30 parts of sodium lauramide glutamate, 0.1 part of potassium cocoyl glutamate, 23 parts of betaine, and 10 parts of refined beeswax , 1 part of cold-pressed linseed oil, 6 parts of camellia seed oil, 0.5 part of antioxidant (specifically 0.0001 part of ascorbyl palmitate, 0.0002 part of 2,6-di-tert-butyl-4-methylphenol, 0.0003 part of natural vitamin E and 0.4994 parts of magnesium ascorbyl phosphate), 0.5 parts of Genma BP, 0.1 part of essence; select deionized water, sodium lauramide glutamate, potassium cocoyl glutamate, betaine, refined beeswax, cold-pressed flax Seed oil, camellia seed oil, antioxidants, preservatives and essence, spare;

2) Add deionized water into the emulsification tank, then put sodium lauramide glutamate into the emulsification tank, stir after soaking; then put refined beestaine and betaine into the emulsification tank, stir; continue to stir and heat to 85°C, keep warm Stir for 25 minutes; add potassium cocoyl glutamate and stir well, stop heating and stirring, and let it stand for 60 minutes until the upper layer has a small amount of foam and the lower layer is transparent; stir, cool down to 58°C, add cold-pressed linseed oil, camellia seed oil and Antioxidant; continue to stir, cool down to 38°C, add essence and Genma BP, stir evenly, turn off the power, let it stand overnight, and you can get a facial cleanser containing linseed oil.

After testing, the cold-pressed linseed oil meets the national GB/T 8253-2008 standard for pressing first-grade linseed oil, the pH value of the facial cleanser containing linseed oil is 5.8, and the heat-resistant, cold-resistant stability, and hygienic indicators all meet the national standard QB/T1645-2004 standard.

The facial cleanser containing linseed oil obtained in this embodiment, after trial use, the test population has no side reactions such as skin irritation, allergic reaction or other discomfort, no damage to facial skin cells, good decontamination effect, and the skin is smooth and smooth after washing. Tight, moist and shiny, it has a certain repairing and moisturizing function for skin cells.

Example 5:

A preparation method of a facial cleanser containing linseed oil, which comprises the steps of:

1) Selection of raw materials: according to the mass parts of each raw material: 21 parts of deionized water, 10 parts of sodium lauramide glutamate, 5 parts of potassium cocoyl glutamate, 5 parts of betaine, 2 parts of refined beeswax 0.01 part of cold-pressed linseed oil, 1 part of camellia seed oil, 0.0001 part of antioxidant (specifically 0.00001 part of ascorbyl palmitate, 0.00001 part of natural vitamin E and 0.00008 part of magnesium ascorbyl phosphate), 0.1 part of Genma BP, essence 0.01 part; select deionized water, sodium lauramide glutamate, potassium cocoyl glutamate, betaine, refined beeswax, cold-pressed linseed oil, camellia seed oil, antioxidants, Gemma BP and essence, spare ;

2) Add deionized water into the emulsification tank, then put sodium lauramide glutamate into the emulsification tank, stir after soaking; then put refined beestaine and betaine into the emulsification tank, stir; continue to stir and heat to 85°C, keep warm Stir for 15 minutes; add potassium cocoyl glutamate and stir well, stop heating and stirring, and let it stand for 30 minutes until the upper layer has a little foam and the lower layer is transparent; stir, cool down to 55°C, add cold-pressed linseed oil, camellia seed oil and Antioxidant; continue to stir, cool down to 35°C, add essence and Genma BP, stir evenly, turn off the power, and let it stand overnight to obtain a facial cleanser containing linseed oil.

After testing, the cold-pressed linseed oil meets the national GB/T 8253-2008 standard for pressing first-grade linseed oil, the pH value of the facial cleanser containing linseed oil is 5.8, and the heat-resistant, cold-resistant stability, and hygienic indicators all meet the national standard QB/T1645-2004 standard.

The facial cleanser containing linseed oil obtained in this embodiment, after trial use, the test population has no side reactions such as skin irritation, allergic reaction or other discomfort, no damage to facial skin cells, good decontamination effect, and the skin is smooth and smooth after washing. Tight, moist and shiny, it has a certain repairing and moisturizing function for skin cells.

Each raw material enumerated in the present invention, and the upper and lower limits of each raw material of the present invention, the interval value, and the upper and lower limits of process parameters (such as temperature, time, etc.), the interval value can realize the present invention, do not enumerate one by one here Example.

Claims (4)

1. A facial cleanser containing linseed oil, characterized in that its composition raw materials and mass parts are as follows: Phase A: 21 to 60 parts of deionized water, Sodium lauramide glutamate 10-30 parts, Potassium cocoyl glutamate 0.1-10 parts, Betaine 5-25 parts, Refined beeswax 2-10 parts, Phase B: 0.01 to 1 part of cold-pressed linseed oil, Camellia seed oil 1-6 parts, Phase C: Antioxidant 0.0001～0.5 part, Genma BP 0.1～0.5 copies, Essence 0.01～0.1 parts; The antioxidant is any one of natural vitamin E, ascorbyl palmitate, magnesium ascorbyl phosphate, 2,6-di-tert-butyl-4-methylphenol or a mixture of any two or more, any two or more It can be mixed in any ratio. 2. A facial cleanser containing linseed oil according to claim 1, characterized in that: the mass fraction of cold-pressed linseed oil is: 0.1-1 part. 3 . A facial cleanser containing linseed oil according to claim 1 , characterized in that the antioxidants account for 0.001-0.5 parts by mass. 4. a method for preparing the facial cleanser containing linseed oil as claimed in claim 1, is characterized in that carrying out successively according to the following steps: 1) Selection of raw materials: according to the mass fraction of each raw material: 21-60 parts of deionized water, 10-30 parts of sodium lauramide glutamate, 0.1-10 parts of potassium cocoyl glutamate, 5 parts of betaine ~25 parts, refined beeswax 2~10 parts, cold pressed linseed oil 0.01~1 part, camellia seed oil 1~6 parts, antioxidant 0.0001~0.5 parts, Genma BP 0.1~0.5 parts, essence 0.01~0.1 parts ;Choose deionized water, sodium lauramide glutamate, potassium cocoyl glutamate, betaine, refined beeswax, cold-pressed linseed oil, camellia seed oil, antioxidants, Genma BP and essence, and set aside; The antioxidant is any one of natural vitamin E, ascorbyl palmitate, magnesium ascorbyl phosphate, 2,6-di-tert-butyl-4-methylphenol or a mixture of any two or more, any two or more When mixing, it is in any proportion; 2) Add deionized water into the emulsification tank, then put sodium lauramide glutamate into the emulsification tank, stir after soaking; then put refined beeswax and betaine into the emulsification tank, stir; continue stirring and heating to 70-85°C , heat preservation and stirring for 15-60 minutes; add potassium cocoyl glutamate and stir evenly, stop heating and stirring, let stand for 10-60 minutes, until the upper layer has a small amount of foam, and the lower layer is transparent; stir, cool down to 45-58°C, add cold-pressed Flaxseed oil, camellia seed oil and antioxidants; continue to stir, cool down to 35-45°C, add essence and Genma BP, stir well, turn off the power, let it stand overnight, and you can get a facial cleanser containing linseed oil .