CN101263217A - Process of plant oil, crude protein and fiber by water extraction - Google Patents
Process of plant oil, crude protein and fiber by water extraction Download PDFInfo
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- CN101263217A CN101263217A CNA2005800500196A CN200580050019A CN101263217A CN 101263217 A CN101263217 A CN 101263217A CN A2005800500196 A CNA2005800500196 A CN A2005800500196A CN 200580050019 A CN200580050019 A CN 200580050019A CN 101263217 A CN101263217 A CN 101263217A
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- 235000019750 Crude protein Nutrition 0.000 title claims abstract description 28
- 239000000835 fiber Substances 0.000 title claims abstract description 22
- 238000000034 method Methods 0.000 title claims description 37
- 230000008569 process Effects 0.000 title claims description 19
- 239000010773 plant oil Substances 0.000 title abstract 3
- 238000003809 water extraction Methods 0.000 title abstract 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 24
- 239000003921 oil Substances 0.000 claims abstract description 23
- 235000015112 vegetable and seed oil Nutrition 0.000 claims description 26
- 239000008158 vegetable oil Substances 0.000 claims description 26
- 102000004895 Lipoproteins Human genes 0.000 claims description 25
- 108090001030 Lipoproteins Proteins 0.000 claims description 25
- 235000019198 oils Nutrition 0.000 claims description 22
- 239000000284 extract Substances 0.000 claims description 17
- 235000013311 vegetables Nutrition 0.000 claims description 16
- 238000005516 engineering process Methods 0.000 claims description 15
- 238000007654 immersion Methods 0.000 claims description 15
- 238000002386 leaching Methods 0.000 claims description 12
- 238000003672 processing method Methods 0.000 claims description 11
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- 238000001223 reverse osmosis Methods 0.000 claims description 5
- 238000000108 ultra-filtration Methods 0.000 claims description 5
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- 239000001648 tannin Substances 0.000 claims description 4
- 230000001351 cycling effect Effects 0.000 claims description 3
- 239000012141 concentrate Substances 0.000 claims description 2
- 238000001035 drying Methods 0.000 claims description 2
- 238000013467 fragmentation Methods 0.000 claims description 2
- 238000006062 fragmentation reaction Methods 0.000 claims description 2
- 238000001816 cooling Methods 0.000 claims 1
- 238000012545 processing Methods 0.000 abstract description 9
- 238000004140 cleaning Methods 0.000 abstract 1
- 238000007598 dipping method Methods 0.000 abstract 1
- 239000000463 material Substances 0.000 abstract 1
- 238000002360 preparation method Methods 0.000 abstract 1
- 238000005086 pumping Methods 0.000 abstract 1
- 241000196324 Embryophyta Species 0.000 description 43
- 238000004519 manufacturing process Methods 0.000 description 18
- 244000068988 Glycine max Species 0.000 description 15
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- 239000002904 solvent Substances 0.000 description 14
- 235000017060 Arachis glabrata Nutrition 0.000 description 13
- 244000105624 Arachis hypogaea Species 0.000 description 13
- 235000010777 Arachis hypogaea Nutrition 0.000 description 13
- 235000018262 Arachis monticola Nutrition 0.000 description 13
- 235000020232 peanut Nutrition 0.000 description 13
- 239000004519 grease Substances 0.000 description 9
- 239000000126 substance Substances 0.000 description 8
- 239000000047 product Substances 0.000 description 6
- 235000018102 proteins Nutrition 0.000 description 6
- 102000004169 proteins and genes Human genes 0.000 description 6
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- 210000004027 cell Anatomy 0.000 description 3
- 238000011109 contamination Methods 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- 230000036541 health Effects 0.000 description 3
- 238000003801 milling Methods 0.000 description 3
- 240000007594 Oryza sativa Species 0.000 description 2
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- 244000046052 Phaseolus vulgaris Species 0.000 description 2
- 235000010627 Phaseolus vulgaris Nutrition 0.000 description 2
- 244000000231 Sesamum indicum Species 0.000 description 2
- 235000003434 Sesamum indicum Nutrition 0.000 description 2
- 108010073771 Soybean Proteins Proteins 0.000 description 2
- 244000269722 Thea sinensis Species 0.000 description 2
- 235000001667 Vitex agnus castus Nutrition 0.000 description 2
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- 235000013305 food Nutrition 0.000 description 2
- 235000009566 rice Nutrition 0.000 description 2
- 238000000926 separation method Methods 0.000 description 2
- 235000012424 soybean oil Nutrition 0.000 description 2
- 239000003549 soybean oil Substances 0.000 description 2
- 235000019710 soybean protein Nutrition 0.000 description 2
- 239000010729 system oil Substances 0.000 description 2
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- 108010082495 Dietary Plant Proteins Proteins 0.000 description 1
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- 235000011868 grain product Nutrition 0.000 description 1
- 238000012423 maintenance Methods 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- 239000003208 petroleum Substances 0.000 description 1
- 238000003825 pressing Methods 0.000 description 1
- 230000009257 reactivity Effects 0.000 description 1
- 238000011084 recovery Methods 0.000 description 1
- 238000007670 refining Methods 0.000 description 1
- 230000002787 reinforcement Effects 0.000 description 1
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- -1 under cold condition Substances 0.000 description 1
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- Coloring Foods And Improving Nutritive Qualities (AREA)
- Medicines Containing Plant Substances (AREA)
Abstract
Preparation of plant oil, crude protein and fiber by water extraction, which includings: selecting an oil plant, cleaning, shelling, crushing and dipping in water with ultrasonic processing, pumping the material into a centrifugal machine, separating the plant oil, crude protein and plant fiber.
Description
Technical field
The invention relates to the comprehensive development and utilization of oilseed plant, particularly at soybean, can be raw material also, use water leaching method therefrom to extract the processing method of Vegetable oil lipoprotein, plant crude protein and vegetable fibre fine oilseed plants such as peanut, sesame, tea seed, perillaseed, Sha chaste tree, Semen Flos Carthamis.
Background technology
For a long time, China comprises that the farming industry of grain is in a backward condition.Since the reform and opening-up, China's grain department is introduced some advanced foodstuff processing technology equipment, and the grain processing industry level has raising.But national cereal product processing industry is also relatively backward on the whole, and processing enterprise's small scale is divided spreading, and equipment is poor, and majority is in the preliminary working stage.This backward situation not only makes agricultural resource can not get rationally, fully develop, and makes the quality of agricultural product amount not high, a little less than the market competitiveness.
China has abundant oilseed plant resource, soybean, peanut equal yield line are all at the forefront in the world, therefore we will make full use of this advantageous condition, the road of walking to develop agriculture through science and technology, deeply excavate the grain oil product potentiality, carry out precision work, the deep processing of product, to strengthen homemade grain oil product competitive power.
With the soybean is example, and it is not only important high-quality oil sources, but also is epochmaking quality protein source.Have only the modern novel technique of employing, could both fully extract soybean oil, do not destroy soybean protein again.In other words, be exactly both to have improved oil yield, the intact again soybean protein that utilizes.Same soybean " whole body is precious " is the same, and other all oilseed plants such as peanut all can be used modern technology, by essence, deep processing reasonable development, the wherein various main components of utilization.
Though China has numerous oil man factories now, because the restriction of production technique is not fully up to expectations to utilizing of oilseed plant, the especially proteic aspect that utilizes.
Domestic be grease production producer " milling process " system oil that adopt of raw material with the peanut more, so-called " milling process " is by physical pressure grease directly to be separated from oil plant, whole process does not relate to any chemical additive, and safety, health, free of contamination advantage are arranged.Not only oil yield is low, oil is not high but use oil extraction by pressing, also makes the protein denaturation in the peanut, and the grouts after the oil expression have lost the reprocessing meaning, can only do feed, fertilizer processing, causes the huge waste of protein resource.
And be grease production producer " chemical solvents lixiviation process " system oil that adopt of raw material with the soybean more, its principle is exactly to utilize chemical solvents different substances to be had the character of different solubilities in fact, with the separating process in addition of relevant composition in the solid materials, also claim " extraction ".Use " No. six solvent for extraction " (being commonly called as petroleum naphtha No. six) organic solvent in the production, with pulverize after oilseed plant carry out thorough mixing after, carry out greasy extracting again.Solvent is gone in the cell by Xi Bao Bi Seepage, and oil then enters solvent in cell, is sending constantly under the situation of fresh solvent, and the oil in the oilseed plant almost all comes out from the cell internal diffusion, makes oil and albumen sepn.The soybean oil that this explained hereafter goes out has residual oil content low (oil yield height) in the dregs of rice, and labour intensity is low, and Working environment is good, the measured advantage of the matter of the dregs of rice.
Though " chemical solvents lixiviation process " is than " milling process ", improved oil yield, reduce protein thermal denaturation, but, most of solvent can't be removed in the production process because there is drawback in himself technology, and operation is many, technical process is long, and energy consumption height (will carry out " five take off ") can cause in the grease residual solvent too high, influence food sanitation safe, and production cost increases.Can't have dissolvent residual in grease and dregs of beans with avoiding, will inevitably influence the quality of grease and dregs of beans, cause food safety and sanitation, environmental pollution and production safety problem to be difficult to solve simultaneously.
Summary of the invention
Technical problem to be solved by this invention is to overcome the technological process of production complexity that traditional technology exists, and the shortcoming of solvent contamination provides a kind of new production process that uses the aqua lixiviation process to extract Vegetable oil lipoprotein, plant crude protein and vegetable fibre.
The present invention solves the problems of the technologies described above by the following technical programs, and water leaching method extracts the processing method of Vegetable oil lipoprotein, plant crude protein and vegetable fibre, may further comprise the steps:
(1) prepares raw material: select the branded oil tannin plant as the raw material that extracts Vegetable oil lipoprotein;
(2) clean selection: craft or machine clean and select oilseed plant to be used;
(3) decortication is broken: will clean the oilseed plant decortication fragmentation of selecting with specialized apparatus;
(4) soak: the broken oilseed plant that crosses of will peeling is soaked fully, uses ultrasonic wave in the time of immersion, and the control temperature of charge is between 30 ℃～55.5 ℃ in the immersion process;
(5) separate: the oilseed plant after the immersion beats to a whizzer with water pump, utilizes whizzer to separate, and isolates Vegetable oil lipoprotein, plant crude protein and three kinds of products of fiber simultaneously.
The time of soaking in step (4) immersion process is controlled between 2 hours～8 hours.
The processing method that this water leaching method extracts Vegetable oil lipoprotein, plant crude protein and vegetable fibre comprises that also the isolated plant crude protein of step (6) carries out drying by the technology of reverse osmosis and ultrafiltration, and the water of generation directly refills in the steeping tank in the immersion process and carries out cycling and reutilization.
The processing method advantage that water leaching method of the present invention extracts Vegetable oil lipoprotein, plant crude protein and vegetable fibre is: avoided the chemical solvents pollution from production technique, hazardness problems such as chemical solvents safety have ensured people's diet health.Water is cooked solvent and has also been simplified production technique, has reduced Production Flow Chart, has reduced production energy consumption, thereby can realize that industrialization has guaranteed production safety when producing.In order to keep Sustainable development; reinforcement is to the protection of environment, and the present invention has given prominence to the making full use of of raw material, and finishes the recovery fully of albumen, sugar, fiber by the technology that adopts existing reverse osmosis and ultrafiltration; so guaranteed cleaner production finally to realize non-pollution discharge.
Description of drawings
The invention will be further described in conjunction with the embodiments with reference to the accompanying drawings.
Fig. 1 is the processing method process step figure that water leaching method of the present invention extracts Vegetable oil lipoprotein, plant crude protein and vegetable fibre.
Embodiment
See also Fig. 1, water leaching method of the present invention extracts Vegetable oil lipoprotein, plant crude protein and vegetable fibre and is divided into following steps:
(1) prepares raw material: can select branded oil tannin plants such as soybean or peanut as the raw material that extracts Vegetable oil lipoprotein, use oilseed plant can guarantee that the Vegetable oil lipoprotein that extracts is harmless fully to human body, guarantee people's diet health;
(2) clean selection: craft or machine clean and select oilseed plants such as soybean to be used or peanut, can use existing various wash machine;
(3) decortication is broken: will clean the oilseed plant of selecting with special-purpose decortication disintegrating apparatus and peel broken;
(4) soak: the oilseed plants such as broken soybean that crosses or peanut of will peeling are soaked fully, use ultrasonic wave in the time of immersion, open plant cell wall, grease is released, and isolates the former activated albumen of maintenance.Should guarantee constant temperature in the process that this soybean or peanut soak, through the test of many times analysis, draw that to soak effect better when temperature remains between 30 ℃～55.5 ℃, when temperature during at 50 ℃ effect best, temperature is too high, the easy sex change of the albumen in soybean or the peanut, cause the huge waste of protein resource, temperature is too low, and then the oil yield of soybean or peanut is low, adopts a temperature control unit to reach this homothermic control in this immersion process.The time of soaking be controlled between 2 hours～8 hours, and the time is oversize, inefficiency then, and the time is too short, and then oil yield is low, and the time is that to soak effect in 6 hours best;
(5) separate: oilseed plants such as soybean after the immersion or peanut beat to a whizzer with water pump, utilize the centrifugal force of whizzer to separate, thereby isolate Vegetable oil lipoprotein simultaneously, plant crude protein and three kinds of products of vegetable fibre.This isolated vegetable oil and fat refining later on promptly can be as edible oil, and plant crude protein and vegetable fibre can be made other byproduct, as adopting the technology of existing reverse osmosis and ultrafiltration can extract sugar in the plant crude protein, vegetable fibre can be processed into Mierocrystalline cellulose etc.;
(6) recycle of water in the plant crude protein: isolated plant crude protein concentrates by the technology of reverse osmosis and ultrafiltration; the dry water that produces also directly refills and carries out cycling and reutilization in the immersion process; thereby reduced cost in the time of the conserve water resource; and do not have discharging, pollution-free, help environment protection.
The present invention is primarily aimed at soybean, can be raw material also for peanut, sesame, tea seed, perillaseed, Sha chaste tree, Semen Flos Carthami branded oil tannin plant, because the extraction process of soybean is the most complicated, the technology that goes for the soybean extraction can be applied to other oilseed plants usually, in conjunction with the supersonic wave wall breaking technology, is to leach solvent with water, under cold condition, grease in the high efficiency separation oilseed plant and albumen obtain Vegetable oil lipoprotein and plant crude protein, and apply to the technology and the production technique of suitability for industrialized production.Thereby efficiently solve the existing problems such as the chemical solvents that exists in the grease production is residual, by-product value is low of producing, realize that industrialization produces high yield, high-quality Vegetable oil lipoprotein and highly active plant crude protein.
Simultaneously, when extracting Vegetable oil lipoprotein, also taken into full account the problem of utilizing of plant crude protein, make Vegetable oil lipoprotein and albumen cryogenically pollution-free separation in water, obtained the free of contamination vegetable active protein of high-quality, kept proteic high reactivity (being the PSI height), for making full use of the oilseed plant resource, improve the industrial chain that Vegetable oil lipoprotein is produced, new channel has been expanded in the deep processing development of oilseed plant.
Claims (5)
1. a water leaching method extracts the processing method of Vegetable oil lipoprotein, plant crude protein and vegetable fibre, may further comprise the steps:
(1) prepares raw material: select the branded oil tannin plant as the raw material that extracts Vegetable oil lipoprotein;
(2) clean selection: craft or machine clean and select oilseed plant to be used;
(3) decortication is broken: will clean the oilseed plant decortication fragmentation of selecting with specialized apparatus;
(4) soak: the broken oilseed plant that crosses of will peeling is soaked fully, uses ultrasonic wave in the time of immersion;
(5) separate: soak the back oilseed plant and beat to a whizzer, utilize whizzer to separate, isolate Vegetable oil lipoprotein, plant crude protein and three kinds of products of fiber simultaneously with water pump;
It is characterized in that: the control temperature of charge is between 30 ℃～55.5 ℃ in described step (4) immersion process.
2. water leaching method as claimed in claim 1 extracts the processing method of Vegetable oil lipoprotein, plant crude protein and vegetable fibre, it is characterized in that: the control temperature of charge is at 50 ℃ in step (4) immersion process.
3. water leaching method as claimed in claim 1 extracts the processing method of Vegetable oil lipoprotein, plant crude protein and vegetable fibre, and it is characterized in that: step (4): the time of soaking in the immersion process is controlled between 2 hours～8 hours.
4. water leaching method as claimed in claim 1 extracts the processing method of Vegetable oil lipoprotein, plant crude protein and vegetable fibre, and it is characterized in that: step (4): the time of soaking in the immersion process was controlled at 6 hours.
5. water leaching method as claimed in claim 1 extracts the processing method of Vegetable oil lipoprotein, plant crude protein and vegetable fibre, it is characterized in that: comprise step (6): isolated plant crude protein by reverse osmosis and ultrafiltration technology concentrate, drying, directly refill after the water cooling of generation and carry out cycling and reutilization in the immersion process.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNA2005800500196A CN101263217A (en) | 2005-12-13 | 2005-12-13 | Process of plant oil, crude protein and fiber by water extraction |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNA2005800500196A CN101263217A (en) | 2005-12-13 | 2005-12-13 | Process of plant oil, crude protein and fiber by water extraction |
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| CN101263217A true CN101263217A (en) | 2008-09-10 |
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| CNA2005800500196A Pending CN101263217A (en) | 2005-12-13 | 2005-12-13 | Process of plant oil, crude protein and fiber by water extraction |
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Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101775334A (en) * | 2010-03-01 | 2010-07-14 | 郑小非 | Method for extracting tea seed oil by using water |
| CN101797038A (en) * | 2010-04-14 | 2010-08-11 | 山东省花生研究所 | Peanut dietary fiber ultrasonic wave or microwave auxiliary extraction and purification method |
| CN101531690B (en) * | 2009-04-28 | 2011-09-14 | 浙江神茗山茶业科技有限公司 | New technology for extracting tea saponin and tea seed oil from tea seeds by using water as solvent |
| CN102433217A (en) * | 2011-10-25 | 2012-05-02 | 江西省粮油科学技术研究所 | Method for extracting edible cornus wilsoniana seed oil from fresh cornus wilsoniana seed fruits at low temperature |
| CN103906436A (en) * | 2011-06-09 | 2014-07-02 | 联邦科学技术研究组织 | Vegetable oil extraction |
| CN108192719A (en) * | 2017-11-30 | 2018-06-22 | 潍坊友容实业有限公司 | A kind of Suaeda salsa seed oil, crude protein and crude fibre synthesis preparation method |
-
2005
- 2005-12-13 CN CNA2005800500196A patent/CN101263217A/en active Pending
Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101531690B (en) * | 2009-04-28 | 2011-09-14 | 浙江神茗山茶业科技有限公司 | New technology for extracting tea saponin and tea seed oil from tea seeds by using water as solvent |
| CN101775334A (en) * | 2010-03-01 | 2010-07-14 | 郑小非 | Method for extracting tea seed oil by using water |
| CN101797038A (en) * | 2010-04-14 | 2010-08-11 | 山东省花生研究所 | Peanut dietary fiber ultrasonic wave or microwave auxiliary extraction and purification method |
| CN101797038B (en) * | 2010-04-14 | 2012-06-13 | 山东省花生研究所 | Peanut dietary fiber ultrasonic wave or microwave auxiliary extraction and purification method |
| CN103906436A (en) * | 2011-06-09 | 2014-07-02 | 联邦科学技术研究组织 | Vegetable oil extraction |
| CN103906436B (en) * | 2011-06-09 | 2016-06-01 | 联邦科学技术研究组织 | The extraction of vegetable oil |
| CN102433217A (en) * | 2011-10-25 | 2012-05-02 | 江西省粮油科学技术研究所 | Method for extracting edible cornus wilsoniana seed oil from fresh cornus wilsoniana seed fruits at low temperature |
| CN108192719A (en) * | 2017-11-30 | 2018-06-22 | 潍坊友容实业有限公司 | A kind of Suaeda salsa seed oil, crude protein and crude fibre synthesis preparation method |
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Open date: 20080910 |