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CN100418203C - Electroluminescence non-destructive testing method for light-emitting diode epitaxial wafers - Google Patents

Electroluminescence non-destructive testing method for light-emitting diode epitaxial wafers Download PDF

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CN100418203C
CN100418203C CNB021236461A CN02123646A CN100418203C CN 100418203 C CN100418203 C CN 100418203C CN B021236461 A CNB021236461 A CN B021236461A CN 02123646 A CN02123646 A CN 02123646A CN 100418203 C CN100418203 C CN 100418203C
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emitting diode
light
epitaxial wafer
type layer
light emitting
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CN1395305A (en
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韩立
董占民
苏哲
陈皓明
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Tsinghua University
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Abstract

The present invention relates to a detection method for epitaxial wafers of light emitting diodes, which belongs to the technical field of detecting instruments. In the present invention, a positive electrode and a negative electrode are arranged on the surface of an epitaxial wafer of a light emitting diode, and a high-voltage constant current source is connected to the positive electrode and the negative electrode to break down a reverse diode composed of a p-shaped layer and an n-shaped layer in the epitaxial wafer of the light emitting diode. The whole circuit is switched on to trigger a luminous layer of the epitaxial wafer of the light emitting diode to emit light for achieving the aim of detection. The measurement method has the advantages of directness, no destruction and convenience, and in respect to photo-fluorescence, the present invention can also obtain electricity parameters of positive switching-on voltage, reverse-leakage current, etc., which are very important to LED (light emitting diode) epitaxial wafers.

Description

发光二极管外延片电致发光无损检测方法 Electroluminescence non-destructive testing method for light-emitting diode epitaxial wafers

技术领域 technical field

本发明涉及发光二极管(LED)外延片的检测方法,属检测仪器领域。The invention relates to a detection method of a light-emitting diode (LED) epitaxial wafer, belonging to the field of detection instruments.

背景技术 Background technique

在白炽灯发明了100多年之后,利用红、绿、蓝三色的LED制成廉价的、高效的白光源早晚有一天会替代这种由爱迪生发明的光源。由于LED具有非常高的经济效益,其发展前景非常广阔,具有极大的市场容量。由于照明消耗占整个电力消耗的20%,因此大力发展LED技术将是节省能源的一个有效途径。LED必将是未来的照明设备。After the incandescent lamp was invented more than 100 years ago, the cheap and efficient white light source made of red, green and blue LEDs will replace the light source invented by Edison sooner or later. Because LED has very high economic benefits, its development prospect is very broad, and it has a huge market capacity. Since lighting consumption accounts for 20% of the total power consumption, vigorously developing LED technology will be an effective way to save energy. LED will definitely be the lighting equipment of the future.

当前LED的主要工作是降低生产成本,提高效率和扩展有用颜色范围。从生产而言,由于LED的市场竞争十分激烈,其生产过程必须十分重视成品率和质量,所以在生产过程中LED半导体外延片的在线检测和质量控制十分重要。目前我国各企业缺乏必要的检测设备,尤其是生产过程中的高速、无损在线检测。The main work for current LEDs is to reduce production costs, increase efficiency and expand the range of useful colors. In terms of production, due to the fierce competition in the LED market, the production process must attach great importance to yield and quality, so the on-line detection and quality control of LED semiconductor epitaxial wafers are very important in the production process. At present, various enterprises in our country lack the necessary testing equipment, especially the high-speed, non-destructive online testing in the production process.

目前LED外延片的发光检测有光致荧光和电致发光两种方法。光致荧光检测方法是用一个短波长的激光照射LED外延片检测其发光效果。但是这是一种间接的检测方法,不能直接反映LED外延片的电致发光效果,同时由于短波长激光器价格昂贵,蓝绿LED外延片检测成本很高。电致发光检测是在LED外延片的p、n结上施加正向偏压,使其发光来检测发光效果,常用的方法是在外延片表面打孔,将一个电极接在p型层上。所以这种检测方法是破坏性的而且也不是连续的。At present, there are two methods for luminescence detection of LED epitaxial wafers: photoluminescence and electroluminescence. The photoluminescent detection method is to use a short-wavelength laser to irradiate the LED epitaxial wafer to detect its luminous effect. However, this is an indirect detection method that cannot directly reflect the electroluminescent effect of LED epitaxial wafers. At the same time, due to the high price of short-wavelength lasers, the detection cost of blue-green LED epitaxial wafers is very high. Electroluminescence detection is to apply a forward bias voltage on the p and n junctions of the LED epitaxial wafer to make it emit light to detect the luminous effect. The common method is to punch holes on the surface of the epitaxial wafer and connect an electrode to the p-type layer. So this detection method is destructive and not continuous.

发明内容 Contents of the invention

本发明的目的是提供一种非破坏性的LED外延片电致发光检测方法。LED外延片的结构(见图1)是其表面层为均匀覆盖的p型层,其下为LED发光层,再下面为高导电的N型层,最后为不导电的衬底。为了进行电致发光检测,需要在外延片表面安置两个电极,其一为固定的负电极(接电源负极);其二为正电极,将一高压恒流源加在两个电极之间。由于LED外延片表面p型层很薄,电阻很大,因此电流将大部分从p-n结组成的二极管上流过。按照二极管的特性,正向二极管相当于导通,高压将主要加在反向连接的二极管上,使其被高压击穿而导通。由于使用了高压恒流源可以控制流经二极管的电流大小保证了反向击穿的二极管在被击穿的条件下不被破坏。为了完成整个外延片发光质量的检测,将正电极在表面上移动就可以得到外延片整片的电致发光质量。The purpose of the present invention is to provide a non-destructive LED epitaxial wafer electroluminescent detection method. The structure of the LED epitaxial wafer (see Figure 1) is that the surface layer is a uniformly covered p-type layer, the LED light-emitting layer is underneath, and the highly conductive N-type layer is underneath, and finally a non-conductive substrate. In order to perform electroluminescent detection, two electrodes need to be placed on the surface of the epitaxial wafer, one of which is a fixed negative electrode (connected to the negative pole of the power supply); the other is a positive electrode, and a high-voltage constant current source is added between the two electrodes. Since the p-type layer on the surface of the LED epitaxial wafer is very thin and has a large resistance, most of the current will flow through the diode formed by the p-n junction. According to the characteristics of the diode, the forward diode is equivalent to conduction, and the high voltage will be mainly applied to the reversely connected diode, causing it to be broken down by the high voltage and conduct. Due to the use of a high-voltage constant current source, the current flowing through the diode can be controlled to ensure that the reverse breakdown diode will not be destroyed under the condition of being broken down. In order to complete the detection of the luminescence quality of the whole epitaxial wafer, the electroluminescence quality of the whole epitaxial wafer can be obtained by moving the positive electrode on the surface.

因此本发明的内容可表达如下:Therefore content of the present invention can be expressed as follows:

在发光二极管外延片的p型层的表面上同时安置正负两个电极,将一个高压恒流源接在正负两极,使发光二极管外延片中的p型层、n型层组成的二极管被击穿导通,使整个电路导通,引发发光二极管外延片的发光层发光,从而达到检测的目的,所述发光层位于p型层和n型层中间,所述负电极固定于p型层表面,正电极可在p型层表面移动。这种测量方法直接、无损、便捷,相对于光致荧光而言还可以得到正向导通电压、反向漏电流等对于LED外延片而言非常重要的电学参数。On the surface of the p-type layer of the light-emitting diode epitaxial wafer, two positive and negative electrodes are placed at the same time, and a high-voltage constant current source is connected to the positive and negative poles, so that the diode composed of the p-type layer and n-type layer in the light-emitting diode epitaxial wafer is Breakdown conduction, the whole circuit is turned on, and the light-emitting layer of the light-emitting diode epitaxial wafer is triggered to emit light, so as to achieve the purpose of detection. The light-emitting layer is located between the p-type layer and the n-type layer, and the negative electrode is fixed on the p-type layer. On the surface, the positive electrode can move on the surface of the p-type layer. This measurement method is direct, non-destructive, and convenient. Compared with photoluminescence, it can also obtain electrical parameters that are very important for LED epitaxial wafers, such as forward conduction voltage and reverse leakage current.

附图说明 Description of drawings

图1为LED外延片结构及检测状态示意图。Figure 1 is a schematic diagram of the LED epitaxial wafer structure and detection state.

具体实施方式 Detailed ways

图1中1为p型层,2为n型层,3为发光层,4为基底。检测时在LED外延片表面放置正、负两个电极并加上高压恒流源。由于反向二极管击穿,即可测得被测点的发光状况。测完一点后移动正电极,同上法可继续检测,不断移动正电极即可测得整个LED外延片的发光状况。In FIG. 1, 1 is a p-type layer, 2 is an n-type layer, 3 is a light-emitting layer, and 4 is a substrate. When testing, place positive and negative electrodes on the surface of the LED epitaxial wafer and add a high-voltage constant current source. Due to the breakdown of the reverse diode, the luminous condition of the measured point can be measured. After measuring a point, move the positive electrode, and the same method as above can continue to detect, and continuously move the positive electrode to measure the luminescence status of the entire LED epitaxial wafer.

Claims (1)

1. 一种发光二极管外延片的检测方法,其特征是在发光二极管外延片的p型层的表面上同时安置正负两个电极,将一个高压恒流源接在正负两极,使发光二极管外延片中的p型层、n型层组成的二极管被击穿导通,使整个电路导通,引发发光二极管外延片的发光层发光,从而达到检测的目的,所述发光层位于p型层和n型层中间,所述负电极固定于p型层表面,正电极可在p型层表面移动。1. A detection method for a light-emitting diode epitaxial wafer, which is characterized in that two positive and negative electrodes are placed on the surface of the p-type layer of the light-emitting diode epitaxial wafer, and a high-voltage constant current source is connected to the positive and negative poles, so that the light-emitting diode The diode composed of p-type layer and n-type layer in the epitaxial wafer is broken down and turned on, so that the entire circuit is turned on, causing the light-emitting layer of the light-emitting diode epitaxial wafer to emit light, so as to achieve the purpose of detection. The light-emitting layer is located in the p-type layer Between the n-type layer, the negative electrode is fixed on the surface of the p-type layer, and the positive electrode can move on the surface of the p-type layer.
CNB021236461A 2002-07-05 2002-07-05 Electroluminescence non-destructive testing method for light-emitting diode epitaxial wafers Expired - Fee Related CN100418203C (en)

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JP3882773B2 (en) * 2003-04-03 2007-02-21 ソニー株式会社 Image display device, drive circuit device, and light-emitting diode defect detection method
CN1330970C (en) * 2003-11-14 2007-08-08 佛山市国星光电科技有限公司 Method for testing power type LED thermal resistance and special purpose chip thereof
CN100573173C (en) * 2007-06-27 2009-12-23 重庆大学 A kind of detection method of led chip
CN102866143A (en) * 2011-07-08 2013-01-09 光达光电设备科技(嘉兴)有限公司 Characteristic test device for epitaxial material layer
US9057757B2 (en) * 2011-08-21 2015-06-16 Bruker Nano, Inc. Testing of electroluminescent semiconductor wafers
CN102520221B (en) * 2011-12-21 2014-02-19 中微光电子(潍坊)有限公司 Manufacturing method of electroluminescence test electrode
CN102841281B (en) * 2012-09-18 2015-07-22 苏州纳方科技发展有限公司 Detection method and device for LED epitaxial wafer
CN105203305A (en) * 2015-11-03 2015-12-30 山东华光光电子有限公司 Nondestructive wavelength classifying and screening method for semiconductor laser
CN109444701A (en) * 2017-08-31 2019-03-08 山东浪潮华光光电子股份有限公司 A kind of nondestructive test device and test method of LED epitaxial wafer
CN109119524B (en) * 2018-08-13 2019-09-13 广东晶科电子股份有限公司 A LED lamp bead marking device and marking method
CN113436983B (en) * 2020-03-19 2024-08-13 京东方科技集团股份有限公司 Mu LED substrate, preparation method, EL detection method and EL detection device
CN111537858A (en) * 2020-04-22 2020-08-14 深圳市华星光电半导体显示技术有限公司 Detection device and detection method

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JPH09330849A (en) * 1996-06-11 1997-12-22 Toshiba Corp Polarized capacitor polarity determination device
CN2452031Y (en) * 2000-11-02 2001-10-03 顺德市顺达电脑厂有限公司 Touch type detecting apparatus for luminous diode

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