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CN100409004C - Monofilament capacitive probe measurement system for phase holdup and phase interface in multiphase pipe flow - Google Patents

Monofilament capacitive probe measurement system for phase holdup and phase interface in multiphase pipe flow Download PDF

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CN100409004C
CN100409004C CNB2006100427924A CN200610042792A CN100409004C CN 100409004 C CN100409004 C CN 100409004C CN B2006100427924 A CNB2006100427924 A CN B2006100427924A CN 200610042792 A CN200610042792 A CN 200610042792A CN 100409004 C CN100409004 C CN 100409004C
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monofilament
external
capacitance
phase
capacitance probe
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CN1865966A (en
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郭烈锦
顾汉洋
张晨鸣
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Xian Jiaotong University
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Abstract

多相管流中相含率和相界面的单丝电容探针测量系统,包括单丝电容探针装置以及与单丝电容探针装置相连接的电容电压转换电路和信号处理装置,电容电压转换电路将单丝电容探针装置中的单丝电容探针的电容值转化为直流电压,并将电压值传给信号处理装置,信号处理装置实现对电容电压转换电路的开启和关闭的控制并实现数据处理、显示、存储和打印等功能。本发明采用了单丝电容探针,只要求多相管流中被测相为导电介质,测量结果不受流体温度和杂质成分的影响,从根本上消除了流体电学性质随机变化对测量结果的影响,实现了对多相管流相含率和相界面结构的连续实时在线测量,并且有很高的测量精度。

Figure 200610042792

A monofilament capacitive probe measurement system for phase holdup and phase interface in multiphase pipe flow, including a monofilament capacitive probe device and a capacitive voltage conversion circuit and signal processing device connected to the monofilament capacitive probe device, capacitive voltage conversion The circuit converts the capacitance value of the single-wire capacitance probe in the single-wire capacitance probe device into a DC voltage, and transmits the voltage value to the signal processing device, and the signal processing device controls the opening and closing of the capacitance-voltage conversion circuit and realizes Data processing, display, storage and printing functions. The invention adopts a monofilament capacitive probe, which only requires the measured phase in the multiphase pipe flow to be a conductive medium, and the measurement result is not affected by the fluid temperature and impurity components, and fundamentally eliminates the influence of the random change of the fluid electrical property on the measurement result. The continuous real-time on-line measurement of phase holdup and phase interface structure of multiphase pipe flow has been realized, and the measurement accuracy is very high.

Figure 200610042792

Description

多相管流中相含率和相界面的单丝电容探针测量系统 Monofilament capacitive probe measurement system for phase holdup and phase interface in multiphase pipe flow

技术领域 technical field

本发明涉及一种多相管流中相含率和相界面的连续实时在线测量系统,具体涉及一种多相管流中相含率和相界面的单丝电容探针测量系统。The invention relates to a continuous real-time on-line measurement system for phase holdup and phase interface in multiphase pipe flow, in particular to a single-wire capacitance probe measurement system for phase holdup and phase interface in multiphase pipe flow.

背景技术 Background technique

气-液、液-液、油-气-水多相管流在能源、动力与石油、化工等工业领域广泛应用。实时变化的截面相含率是多相管流中最基本和最重要的特征参数之一。而在分层流、环状流和段塞流中存在着连续的相界面结构,这种相界面结构对多相管流的传热、传质以及阻力特征有着显著的影响。对多相管流的截面相含率和相界面结构的实时准确测量是涉及多相管流的实验研究、技术发展和工业应用中的关键技术之一。Gas-liquid, liquid-liquid, oil-gas-water multiphase pipe flow is widely used in energy, power and petroleum, chemical and other industrial fields. The cross-sectional phase holdup that changes in real time is one of the most basic and important characteristic parameters in multiphase pipe flow. In stratified flow, annular flow and slug flow, there is a continuous phase interface structure, which has a significant impact on the heat transfer, mass transfer and resistance characteristics of multiphase pipe flow. The real-time and accurate measurement of cross-sectional phase holdup and phase interface structure of multiphase pipe flow is one of the key technologies in experimental research, technology development and industrial application involving multiphase pipe flow.

目前测量多相管流截面相含率和相界面结构的方法主要有:快关阀法、射线法、光学法、电学法等。快关阀法是一种机械方法,只适合实验室使用;射线法的准确度较好,但受设备庞大,辐射安全性等因素的影响,光学法受设备昂贵,对测量对象要求苛刻等因素的影响,其使用都受很大的制约。At present, there are mainly methods for measuring phase holdup and phase interface structure of multiphase pipe flow section: quick-closing valve method, ray method, optical method, electrical method, etc. The quick-closing valve method is a mechanical method, which is only suitable for laboratory use; the accuracy of the ray method is better, but it is affected by factors such as huge equipment and radiation safety, and the optical method is affected by factors such as expensive equipment and strict requirements on the measurement object. influence, its use is subject to great constraints.

电学法具有结构简单、反应快速灵敏、运行稳定可靠的特点,成为近20年来多相流测量领域研究的热点技术。电学法可以分为电导法和电容法两类。如中国专利申请文本《地面电导含水分析仪》(公开日2005年3月30日,公开号CN1601265,申请日2004年10月26日)中公开的一种用于测量油田外输液中含水率的地面电导含水分析仪,该专利即采用电导法测量多相管流中的含液率,但是电导法的测量结果随液相电导系数变化而变化,而液相温度、液相中的杂质成分等因素都显著影响液相的电导系数,为了保证测量的精度必须不断对测量结果进行修正,从而无法实现连续的在线测量。如中国专利申请文本《采用内置12极电容传感器的气液两流空泡份额测量仪》(公开日2005年8月17日,公开号CN1654940A,申请日2004年12月29日)中公开的一种气液两相流中空泡份额的测量仪器,该专利即采用电容法测量气液两相流中空泡份额。这类电容法的原理是,布置于两相流动管道上的电极对视为一个电容器,电容值的大小与两相混合物的介电常数ε有关,而ε是气相介电常数εG、液相介电常数εL和空泡份额α的函数。通过测量电极间的电容值得到混合物的空泡份额。但这类电容法的测量结果同样随着液相介电常数的变化而变化,而液相温度、液相中的杂质成分等因素都显著影响液相的介电常数,为了测量的准确也必须不断对测量结果进行修正。在实验研究或者实际工业多相管流中的流体导电系数和介电常数往往是不断变化的,所以目前这些电导法和电容法并不能实现对多相管流相含率以及相界面结构进行连续的实时在线测量。The electrical method has the characteristics of simple structure, fast and sensitive response, stable and reliable operation, and has become a hot technology in the field of multiphase flow measurement in the past 20 years. Electrical methods can be divided into conductometric and capacitive methods. A kind of instrument that is used to measure the water content in the transfusion outside the oilfield as disclosed in the Chinese patent application text "ground conductance water content analyzer" (disclosure date March 30, 2005, publication number CN1601265, application date October 26, 2004) The ground conductivity water content analyzer, the patent uses the conductivity method to measure the liquid content in the multiphase pipe flow, but the measurement result of the conductivity method changes with the change of the liquid phase conductivity, and the liquid phase temperature, the impurity composition in the liquid phase, etc. All factors significantly affect the conductivity of the liquid phase. In order to ensure the accuracy of the measurement, the measurement results must be continuously corrected, so that continuous on-line measurement cannot be realized. As disclosed in the Chinese patent application text "Adopting a Gas-Liquid Two-Flow Cavitation Fraction Measuring Instrument with a Built-in 12-pole Capacitance Sensor" (disclosure date August 17, 2005, publication number CN1654940A, application date December 29, 2004) A measuring instrument for the proportion of voids in gas-liquid two-phase flow, the patent uses the capacitance method to measure the proportion of voids in gas-liquid two-phase flow. The principle of this type of capacitance method is that the electrode pair arranged on the two-phase flow pipeline is regarded as a capacitor, and the capacitance value is related to the dielectric constant ε of the two-phase mixture, and ε is the gas phase dielectric constant ε G , the liquid phase Function of permittivity ε L and void fraction α. The void fraction of the mixture is obtained by measuring the capacitance value between the electrodes. However, the measurement results of this type of capacitance method also change with the change of the dielectric constant of the liquid phase, and factors such as the temperature of the liquid phase and the impurity components in the liquid phase significantly affect the dielectric constant of the liquid phase. In order to measure accurately, it must be The measurement results are constantly corrected. In experimental research or actual industrial multiphase pipe flow, the fluid conductivity and permittivity are often changing, so the current conductivity and capacitance methods cannot achieve continuous analysis of the phase holdup and phase interface structure of multiphase pipe flow. real-time online measurement.

发明内容 Contents of the invention

本发明的目的在于克服上述现有技术的缺点,提供了一种测量结果不受流体温度和杂质成分的影响且测量精度高,能够从根本上消除流体电学性质随机变化对测量结果的影响,实现连续实时在线测量的多相管流中相含率和相界面的单丝电容探针测量系统。The purpose of the present invention is to overcome the shortcomings of the prior art above, to provide a measurement result that is not affected by fluid temperature and impurity components and has high measurement accuracy, which can fundamentally eliminate the influence of random changes in fluid electrical properties on measurement results, and realize A single-wire capacitive probe measurement system for continuous real-time online measurement of phase holdup and phase interface in multiphase pipe flow.

为达到上述目的,本发明采用的技术方案是:包括单丝电容探针装置以及与单丝电容探针装置相连接的电容电压转换电路和信号处理装置,其特点是,所说的单丝电容探针装置包括设置在测量管道内的单丝电容探针,在测量管道的外侧对称设置有上支架和下支架,上支架和下支架内均设置密封套,上支架上设置有套管和上端盖,上端盖通过螺栓与上支架相连接,且在上端盖上还设置有与单丝电容探针的一端相连接的电极接线柱,下支架上设置有锁紧螺栓和与单丝电容探针的另一端相连接的下端盖;所说的电容电压转换电路采用CAV424芯片,CAV424芯片的外接第一、第二和第三管角分别与参考振荡电路电阻Rosc、第一积分器电流调整电阻Rcx1、第二积分器电流调整电阻Rcx2相连接,且参考振荡电路电阻Rosc、第一积分器电流调整电阻Rcx1、第二积分器电流调整电阻Rcx2连同CAV424芯片的外接第十管角接地;CAV424芯片的外接第四管角与输出电压放大电阻RL1连接,该输出电压放大电阻RL1的另一端引到外接电压输出端V0,同时从CAV424芯片的外接第四管角引出导线与另外一个输出电压放大电阻RL2连接,输出电压放大电阻RL2的另外一端与CAV424芯片的外接第六管角连接;CAV424芯片的外接第六管角与载荷电容CVM连接,该载荷电容CVM的另外一端接地;同时CAV424芯片的外接第六管角直接与另外一个电压输出端V1连接;CAV424芯片的外接第十一管角引出导线与直流电压电源外接端Vcc连接;CAV424芯片的外接第十二、十三、十五和十六管角分别与振荡电路电容COSC、低通电路电容CL2、另一低通电路电容CL1及参考电容CX1连接,这些电容的另外一端均接地;从CAV424芯片的外接第十四管角引出导线到外接单丝电容探针装置的一端C0,同时从接地线引出到外接单丝电容探针装置的另一端C1,从直流电压电源外接端Vcc接入5伏的直流电源;在外接单丝电容探针装置的两个外接端C0、C1分别与单丝电容探针的两端相连接,信号处理装置采用C8051F000单片机,信号处理装置的输入端与电容电压转换电路的电压输出端V1和电压输出端V0连接。In order to achieve the above object, the technical solution adopted in the present invention is: comprising a monofilament capacitance probe device and a capacitance voltage conversion circuit and a signal processing device connected with the monofilament capacitance probe device, it is characterized in that said monofilament capacitance The probe device includes a monofilament capacitive probe arranged in the measuring pipeline, an upper bracket and a lower bracket are arranged symmetrically on the outside of the measuring pipeline, sealing sleeves are arranged in the upper bracket and the lower bracket, and a casing and an upper end are arranged on the upper bracket. The upper end cover is connected with the upper bracket by bolts, and an electrode terminal connected with one end of the single-wire capacitance probe is also arranged on the upper end cover, and a locking bolt is arranged on the lower bracket and connected with the single-wire capacitance probe. The other end connected to the lower end cover; said capacitance voltage conversion circuit adopts CAV424 chip, and the external first, second and third tube angles of CAV424 chip are respectively connected with the reference oscillation circuit resistance Rosc, the first integrator current adjustment resistance Rcx 1. The second integrator current adjustment resistor Rcx 2 is connected, and the reference oscillator circuit resistance Rosc, the first integrator current adjustment resistor Rcx 1 , the second integrator current adjustment resistor Rcx 2 and the external tenth tube angle of the CAV424 chip are grounded ; The external fourth tube angle of the CAV424 chip is connected to the output voltage amplifying resistor R L1 , the other end of the output voltage amplifying resistor R L1 is led to the external voltage output terminal V 0 , and the wire is drawn from the external fourth tube angle of the CAV424 chip to connect with Another output voltage amplifying resistor R L2 is connected, and the other end of the output voltage amplifying resistor R L2 is connected to the sixth external tube angle of the CAV424 chip; the external sixth tube angle of the CAV424 chip is connected to the load capacitor C VM , and the load capacitor C VM The other end of the CAV424 chip is connected to the ground; at the same time, the sixth tube corner of the CAV424 chip is directly connected to another voltage output terminal V 1 ; the lead wire of the eleventh tube corner of the CAV424 chip is connected to the external terminal V cc of the DC voltage power supply; The twelfth, thirteenth, fifteenth and sixteenth tube corners are respectively connected to the oscillation circuit capacitor C OSC , the low-pass circuit capacitor C L2 , another low-pass circuit capacitor C L1 and the reference capacitor C X1 , and the other ends of these capacitors are Grounding; Lead wires from the fourteenth tube corner of the CAV424 chip to one end C 0 of the external single-wire capacitance probe device, and at the same time lead from the ground wire to the other end C 1 of the external single-wire capacitance probe device, from DC The external terminal V cc of the voltage power supply is connected to a 5 volt DC power supply; the two external terminals C 0 and C 1 of the external monofilament capacitance probe device are respectively connected to the two ends of the monofilament capacitance probe, and the signal processing device adopts C8051F000 The single-chip microcomputer and the input terminal of the signal processing device are connected with the voltage output terminal V 1 and the voltage output terminal V 0 of the capacitor-voltage conversion circuit.

本发明的单丝电容探针包括不锈钢丝和涂敷在不锈钢丝外侧的聚四氟乙烯层;测量管道与上支架及下支架之间还设置有第一绝缘垫片和第二绝缘垫片;锁紧螺栓和下端盖之间还设置有弹簧。The monofilament capacitive probe of the present invention comprises a stainless steel wire and a polytetrafluoroethylene layer coated on the outside of the stainless steel wire; a first insulating gasket and a second insulating gasket are also arranged between the measuring pipeline, the upper bracket and the lower bracket; A spring is also arranged between the locking bolt and the lower end cover.

由于本发明采用了单丝电容探针,只要求多相管流中被测相为导电介质,测量结果不受流体温度和杂质成分的影响,从根本上消除了流体电学性质随机变化对测量结果的影响,实现了对多相管流相含率和相界面结构的连续实时在线测量,并且有很高的测量精度。Since the present invention adopts the monofilament capacitive probe, only the phase to be measured in the multiphase pipe flow is required to be a conductive medium, and the measurement results are not affected by the fluid temperature and impurity components, which fundamentally eliminates the influence of random changes in the electrical properties of the fluid on the measurement results. The continuous real-time on-line measurement of phase holdup and phase interface structure of multiphase pipe flow is realized, and the measurement accuracy is very high.

附图说明 Description of drawings

图1是本发明的整体示意图;Fig. 1 is the overall schematic diagram of the present invention;

图2是本发明单丝电容探针装置18的装配图;Fig. 2 is the assembly diagram of monofilament capacitive probe device 18 of the present invention;

图3是本发明单丝电容探针9的结构示意图;Fig. 3 is the structural representation of monofilament capacitive probe 9 of the present invention;

图4是本发明电容电压转换电路19的原理图;FIG. 4 is a schematic diagram of the capacitive voltage conversion circuit 19 of the present invention;

图5是本发明对分层界面的测量图,其中横坐标为无量钢液位高度,纵坐标为本发明的测量值;Fig. 5 is the measuring figure of the present invention to layered interface, and wherein abscissa is the liquid level height of measureless steel, and ordinate is the measured value of the present invention;

图6是本发明对泡状流液相相含率的测量图,其中横坐标为液相相含率,纵坐标为测量值。Fig. 6 is a measurement diagram of the liquid phase holdup of bubbly flow according to the present invention, wherein the abscissa is the liquid phase holdup, and the ordinate is the measured value.

具体实施方式 Detailed ways

下面结合附图对本发明的结构原理和工作原理作进一步详细说明。The structural principle and working principle of the present invention will be further described in detail below in conjunction with the accompanying drawings.

参见图1,本发明包括单丝电容探针装置18以及与单丝电容探针装置18相连接的电容电压转换电路19和信号处理装置20,电容电压转换电路19将单丝电容探针装置18中的单丝电容探针的电容值转化为直流电压,并将电压值传给信号处理装置20,信号处理装置20实现对电容电压转换电路19的开启和关闭的控制并实现数据处理、显示、存储和打印等功能。Referring to Fig. 1, the present invention comprises monofilament capacitive probe device 18 and the capacitive voltage conversion circuit 19 and the signal processing device 20 that are connected with monofilament capacitive probe device 18, capacitive voltage conversion circuit 19 converts monofilament capacitive probe device 18 The capacitance value of the monofilament capacitive probe in the circuit is converted into a DC voltage, and the voltage value is passed to the signal processing device 20, and the signal processing device 20 realizes the control of opening and closing of the capacitance voltage conversion circuit 19 and realizes data processing, display, functions such as storage and printing.

参见图2,本发明的单丝电容探针装置18包括设置在测量管道8内的单丝电容探针9,在测量管道8的外壁面径向对称方向上铣出两个对称的圆锥形槽口,外径为0.3mm的圆柱形单丝电容探针9穿过两个圆锥形槽口,参见图3,圆柱形单丝电容探针9采用中心为直径0.1厘米的不锈钢丝16,不锈钢丝外涂厚度为0.1mm聚四氟乙烯层17的漆包线,单丝电容探针9的一端穿过硅树脂密封套5,密封套5制作成圆锥形与圆锥形槽口吻合,除去单丝电容探针9末端的聚四氟乙烯层17后固定在电极接线柱1上,并将电极接线柱1固定在上端盖3上,通过上端盖3上的螺栓2将上端盖3固定在铜质上支架6上固定,在上端盖3往下运动过程中,通过套管4将硅树脂密封套5往测量管道8的壁上的圆锥形槽口挤压起到密封作用。如果测量管道8为非导电材质时,上支架6用固定胶直接固定在测量管道8的外壁上,如果测量管道8为导电材质时,上支架6和测量管道8外壁之间加入绝缘垫片7并用固定胶固定。通过锁紧螺栓13往铜质下支架11上锁紧的过程中挤压硅树脂密封套12对单丝电容探针9的另一端进行密封,下支架11与测量管道8的固定方式与上支架6相同,调节单丝电容探针9的长度并将单丝电容探针9的末端固定在下端盖15上,下端盖15压缩设置在锁紧螺栓13凹槽内的弹簧14,使单丝电容探针9保持一定的张力从而消除流体流动冲击探针产生的振动。单丝电容探针装置18中的单丝电容探针9沿着管道径向垂直穿过测试管道,探针两端分别与端盖和电极接线螺栓连接,利用两端的支架、端盖、螺栓和紧锁螺栓结构对探针进行固定,并利用弹簧将探针张紧消除流动冲击引起的振动,采用硅树脂密封套对探针穿出管道的位置实现良好的密封。Referring to Fig. 2, the monofilament capacitive probe device 18 of the present invention comprises the monofilament capacitive probe 9 that is arranged in the measuring pipe 8, mills out two symmetrical conical grooves on the radially symmetrical direction of the outer wall surface of the measuring pipe 8 A cylindrical monofilament capacitance probe 9 with an outer diameter of 0.3 mm passes through two conical notches, see Fig. 3, the cylindrical monofilament capacitance probe 9 adopts a stainless steel wire 16 with a diameter of 0.1 cm in the center, and the stainless steel wire An enameled wire coated with a polytetrafluoroethylene layer 17 with a thickness of 0.1 mm, one end of the monofilament capacitance probe 9 passes through the silicone resin sealing sleeve 5, and the sealing sleeve 5 is made into a conical shape to match the conical notch, and the monofilament capacitance probe is removed. The polytetrafluoroethylene layer 17 at the end of the needle 9 is finally fixed on the electrode terminal 1, and the electrode terminal 1 is fixed on the upper end cover 3, and the upper end cover 3 is fixed on the copper upper bracket through the bolt 2 on the upper end cover 3 6, and during the downward movement of the upper end cover 3, the sleeve 4 squeezes the silicone resin sealing sleeve 5 to the conical notch on the wall of the measuring pipe 8 to play a sealing role. If the measuring pipe 8 is made of a non-conductive material, the upper bracket 6 is directly fixed on the outer wall of the measuring pipe 8 with fixing glue; if the measuring pipe 8 is made of a conductive material, an insulating gasket 7 is added between the upper bracket 6 and the outer wall of the measuring pipe 8 And fix it with glue. In the process of locking the copper lower bracket 11 through the locking bolt 13, the silicone resin sealing sleeve 12 is squeezed to seal the other end of the monofilament capacitive probe 9, and the fixing method of the lower bracket 11 and the measuring pipe 8 is the same as that of the upper bracket. 6 is the same, adjust the length of the monofilament capacitor probe 9 and fix the end of the monofilament capacitor probe 9 on the lower end cover 15, and the lower end cover 15 compresses the spring 14 arranged in the groove of the locking bolt 13, so that the monofilament capacitor The probe 9 maintains a certain tension so as to eliminate the vibration generated by the fluid flow impacting the probe. The single-wire capacitance probe 9 in the single-wire capacitance probe device 18 passes through the testing pipeline vertically along the radial direction of the pipeline, and the two ends of the probe are respectively connected with the end caps and the electrode wiring bolts. The locking bolt structure fixes the probe, and the spring is used to tension the probe to eliminate the vibration caused by the flow impact, and the silicone resin sealing sleeve is used to achieve a good seal at the position where the probe passes out of the pipeline.

参见图3,单丝电容探针9采用中心为直径0.1厘米的不锈钢丝16,不锈钢丝外涂厚度为0.1mm聚四氟乙烯层17的漆包线,本发明采用外径为0.3mm的圆柱形单丝电容探针,单丝电容探针的测量原理如下:探针的中心为直径为0.1mm的不锈钢丝,不锈钢丝16具有较好的强度和良好的导电性,该不锈钢丝16即作为单丝电容探针9的一个电极。不锈钢丝16外均匀地喷涂厚度为0.1mm的聚四氟乙烯层17,该环状聚四氟乙烯层17即成为单丝电容探针9的电解质。聚四氟乙烯有稳定的电学性质,其电绝缘性和介电常数在很宽的范围内不受环境温度和激励频率的影响。当导电流体接触单丝电容探针9时,导电流体构成单丝电容探针9的另外一个电极。此时内部的不锈钢丝16、聚四氟乙烯层17和与聚四氟乙烯层17接触的导电流体共同组成了柱状电容。聚四氟乙烯具有固体材料中最小的表面张力,被测流体不会粘附其上,所以测量过程中信号响应滞后现象十分微弱。当导电流体与单丝电容探针9在某处接触的长度为h,那么该处形成的柱状电容值C1为:Referring to Fig. 3, the monofilament capacitive probe 9 adopts the stainless steel wire 16 of diameter 0.1 centimeter in the center, and the enamelled wire of 0.1mm polytetrafluoroethylene layer 17 is coated with thickness outside the stainless steel wire, and the present invention adopts the cylindrical monolithic wire that outer diameter is 0.3mm The measurement principle of the wire capacitance probe and the single wire capacitance probe is as follows: the center of the probe is a stainless steel wire with a diameter of 0.1mm, and the stainless steel wire 16 has good strength and good conductivity, and the stainless steel wire 16 is used as a single wire One electrode of the capacitive probe 9. The stainless steel wire 16 is evenly sprayed with a polytetrafluoroethylene layer 17 with a thickness of 0.1 mm, and the annular polytetrafluoroethylene layer 17 becomes the electrolyte of the monofilament capacitive probe 9 . PTFE has stable electrical properties, and its electrical insulation and dielectric constant are not affected by ambient temperature and excitation frequency in a wide range. When the conductive fluid contacts the monofilament capacitive probe 9 , the conductive fluid constitutes another electrode of the monofilament capacitive probe 9 . At this time, the internal stainless steel wire 16, the polytetrafluoroethylene layer 17 and the conductive fluid in contact with the polytetrafluoroethylene layer 17 together form a columnar capacitor. PTFE has the smallest surface tension among solid materials, and the measured fluid will not adhere to it, so the signal response hysteresis is very weak during the measurement. When the length of the contact between the conductive fluid and the monofilament capacitance probe 9 is h at a certain place, the columnar capacitance C1 formed at this place is:

CC 11 == 22 πϵhπϵh lnln (( DD. dd )) -- -- -- (( 11 ))

其中ε为聚四氟乙烯的介电常数,D,d分别为单丝电容探针的外径和中心位置不锈钢丝的直径。当单丝电容探针9置于多相管流中时,导电流体与之接触形成了一个或者一系列并联的电容,根据并联电容的计算公式可知,单丝电容探针上的总电容C为:Where ε is the dielectric constant of polytetrafluoroethylene, D and d are the outer diameter of the single-wire capacitive probe and the diameter of the stainless steel wire at the center, respectively. When the monofilament capacitance probe 9 is placed in the multiphase pipe flow, the conductive fluid contacts it to form one or a series of parallel capacitors. According to the calculation formula of parallel capacitance, the total capacitance C on the monofilament capacitance probe is :

CC == ΣΣ ii == 11 nno CC ii == 22 πϵπϵ lnln (( DD. dd )) ΣΣ ii == 11 nno hh ii == == 22 πϵπϵ lnln (( DD. dd )) hh ll -- -- -- (( 22 ))

上式中hl为与置于管道内单丝电容探针接触的导电流体的总长度。式(2)中的ε,D,d都是确定的常数,所以任何时刻从单丝电容探针9检测到的电容值只跟与单丝电容探针9接触的导电流体的长度有关并成正比。所以通过检测单丝电容探针9的电容即可得到多相管流中管道界面相含率和界面结构。In the above formula, h l is the total length of the conductive fluid in contact with the single-wire capacitive probe placed in the pipeline. In formula (2), ε, D, d are all definite constants, so the capacitance value detected from the monofilament capacitive probe 9 at any moment is only related to the length of the conductive fluid contacted with the monofilament capacitive probe 9 and becomes Proportional. Therefore, by detecting the capacitance of the monofilament capacitive probe 9, the phase holdup and interface structure of the pipeline interface in the multiphase pipeline flow can be obtained.

参见图4,本发明的电容电压转换电路19采用CAV424芯片,该芯片具有电容的高检测灵敏度并可以克服寄生电容和环境变化的影响,实现对单丝电容探针9电容值的检测并将电容信号转变为直流的电压信号。CAV424芯片的第一、第二和第三管角分别与参考振荡电路电阻Rosc、第一积分器电流调整电阻Rcx1、第二积分器电流调整电阻Rcx2相连接,且参考振荡电路电阻Rosc、第一积分器电流调整电阻Rcx1、第二积分器电流调整电阻Rcx2连同CAV424芯片的外接第十管角接地;CAV424芯片的外接第四管角与输出电压放大电阻RL1连接,该电压放大电阻RL1的另一端引到外接电压输出端V0,同时从CAV424芯片外接第四管角引出导线与另外一个输出电压放大电阻RL2连接,该电阻RL2的另外一端与CAV424芯片的外接第六管角连接;CAV424芯片的外接第六管角与载荷电容CVM连接,该载荷电容CVM的另外一端接地;同时CAV424芯片的外接第六管角直接与另外一个电压输出端V1连接;CAV424芯片的外接第十一管角引出导线与直流电压电源外接端Vcc连接;CAV424芯片的外接第十二、十三、十五和十六管角分别与振荡电路电容COSC、低通电路电容CL2、另一低通电路电容CL1及参考电容CX1连接,这些电容的另外一端均接地;从CAV424芯片的外接第十四管角引出导线到外接单丝电容探针装置的一端C0,同时从接地线引出到外接单丝电容探针装置的另一端C1,从直流电压电源外接端Vcc接入5伏的直流电源;在外接单丝电容探针装置的两个外接端C0、C1分别与单丝电容探针9的两端相连接,当管道材质导电时C1直接与管道外壁连接,当单管道材质非导电时,从单丝电容探针的下游10mm处的管壁打孔从管内引出一电极与C1连接(该电极与被测流体连接);从V0,V1外接端输出经该电路转化得到直流电压。在测试管道内的被测液相相含率为零时通过调节电阻Rcx1、Rcx2对该C-V电路进行调零;通过调节电阻RL1、RL2调节输出差变电压的大小,使得处在管道内的单丝电容探针都浸没在导电流体时输出的最大电压小于最大量程。Referring to Fig. 4, capacitance-to-voltage conversion circuit 19 of the present invention adopts CAV424 chip, and this chip has the high detection sensitivity of capacitance and can overcome the influence of parasitic capacitance and environment change, realizes the detection to the capacitance value of monofilament capacitance probe 9 and changes capacitance The signal is converted to a DC voltage signal. The first, second and third tube corners of the CAV424 chip are respectively connected to the reference oscillating circuit resistance Rosc, the first integrator current adjusting resistor Rcx 1 , and the second integrator current adjusting resistor Rcx 2 , and the reference oscillating circuit resistance Rosc, The first integrator current adjustment resistor Rcx 1 , the second integrator current adjustment resistor Rcx 2 and the external tenth tube corner of the CAV424 chip are grounded; the external fourth tube corner of the CAV424 chip is connected to the output voltage amplification resistor RL1 , and the voltage amplifies The other end of the resistor R L1 is connected to the external voltage output terminal V 0 , and at the same time, the wire connected to the fourth tube corner of the CAV424 chip is connected to another output voltage amplifying resistor R L2 , and the other end of the resistor R L2 is connected to the external fourth tube corner of the CAV424 chip. The six tube corners are connected; the external sixth tube corner of the CAV424 chip is connected to the load capacitor C VM , and the other end of the load capacitor C VM is grounded; at the same time, the external sixth tube corner of the CAV424 chip is directly connected to another voltage output terminal V1 ; The lead wire of the eleventh tube corner of the CAV424 chip is connected to the external terminal V cc of the DC voltage power supply; the twelfth, thirteenth, fifteenth and sixteenth tube corners of the CAV424 chip are respectively connected to the oscillation circuit capacitor C OSC and the low-pass circuit Capacitor C L2 , another low-pass circuit capacitor C L1 and reference capacitor C X1 are connected, and the other ends of these capacitors are all grounded; lead wires from the fourteenth tube corner of the CAV424 chip to one end of the external monofilament capacitance probe device C 0 , lead out from the ground wire to the other end C 1 of the external single-wire capacitance probe device, and connect a 5-volt DC power supply from the external terminal V cc of the DC voltage power supply; The external terminals C 0 and C 1 are respectively connected to the two ends of the monofilament capacitance probe 9. When the pipe material is conductive, C 1 is directly connected to the outer wall of the pipe. When the single pipe material is non-conductive, the downstream end of the monofilament capacitance probe The pipe wall at 10mm is drilled and an electrode is drawn from the pipe to connect with C1 (the electrode is connected with the measured fluid); the output from the V0 and V1 external terminals is transformed by the circuit to obtain a DC voltage. When the measured liquid holdup in the test pipeline is zero, the CV circuit is zeroed by adjusting the resistors Rcx 1 and Rcx 2 ; the output differential voltage is adjusted by adjusting the resistors R L1 and R L2 , so that it is at When the monofilament capacitive probes in the pipeline are immersed in the conductive fluid, the maximum output voltage is less than the maximum range.

信号处理装置20以单片机为核心,采用C8051F000单片机,信号处理装置20的输入端与电容电压转换电路的外接端V1和V0连接。采集和处理频率为2000kH。实现对电容-电压(C-V)转换电路的开启和关闭控制,并实现对数据进行实时处理、显示、存储和打印等功能。The signal processing device 20 takes a single-chip microcomputer as the core, and adopts a C8051F000 single-chip microcomputer. The input terminal of the signal processing device 20 is connected with the external terminals V 1 and V 0 of the capacitor voltage conversion circuit. The acquisition and processing frequency is 2000kH. Realize the on and off control of the capacitance-voltage (CV) conversion circuit, and realize the functions of real-time processing, display, storage and printing of data.

使用该系统前首先在单丝电容探针装置无流体时对电容电压转换电路19调零消除装置制作过程中引入的额外电容,再测定单丝电容探针装置18中充满导电流体时单丝电容探针9的最大电容转化得到的最大电压,这样就完成了对该测量系统的初始化设置。因为本发明的测量值不受测量流体介电常数的影响,在测量过程中无需再对测量系统进行设置或者对测量结果进行修正,通过信号处理装置控制该系统,实现对多相管流的相含率和相界面结构、连续的实时在线测量和显示。Before using the system, firstly when the monofilament capacitance probe device has no fluid, the extra capacitance introduced in the process of making the capacitance voltage conversion circuit 19 is zeroed to eliminate the device, and then the monofilament capacitance is measured when the monofilament capacitance probe device 18 is filled with conductive fluid. The maximum capacitance of the probe 9 is transformed into the maximum voltage, thus completing the initial setting of the measurement system. Because the measured value of the present invention is not affected by the dielectric constant of the measured fluid, there is no need to set up the measurement system or correct the measurement results during the measurement process. Holdup and phase interface structure, continuous real-time online measurement and display.

本发明提供的单丝电容探针测量系统结构简单紧凑、成本低廉,实现了对多相管流相含率和相界面的实时在线测量和显示;只要求被测相具有导电性,测量结果不受多相流体的温度以及电学性质随机变化的影响所以有很强适用性,并且测量过程中无需对测量结果进行修正能实现连续的在线测量;检测的电容信号与被测物理量呈良好的线性关系,测量结果的精度很高;本发明的测量系统通过实验表明对分层流界面厚度测量的绝对误差小于1.0%,而对泡状流截面相含率测量的绝对误差小于2.5%。说明本发明能很好地满足实验研究和工业领域对多相管流中相含率和界面结构测量的精度要求。The monofilament capacitive probe measurement system provided by the invention has a simple and compact structure and low cost, and realizes real-time on-line measurement and display of the phase holdup and phase interface of the multiphase pipe flow; only the measured phase is required to have conductivity, and the measurement results are not Affected by the temperature and random changes of the electrical properties of the multiphase fluid, it has strong applicability, and continuous online measurement can be realized without correction of the measurement results during the measurement process; the detected capacitance signal has a good linear relationship with the measured physical quantity , the accuracy of the measurement results is very high; the measurement system of the present invention shows through experiments that the absolute error of the measurement of the thickness of the stratified flow interface is less than 1.0%, while the absolute error of the measurement of the cross-sectional phase holdup of the bubbly flow is less than 2.5%. It shows that the present invention can well meet the accuracy requirements of experimental research and industrial field for phase holdup and interface structure measurement in multiphase pipe flow.

在使用该测量系统前,完成对系统的初始化设置,测量过程中不再对测量系统设置和测量结果进行任何的修改。使用本发明的测量系统对不同含盐量的水在分层情况的相界面结构和对不同温度下的空气-水泡状流的相含率的测量结果如图5,6所示。Before using the measurement system, complete the initial setting of the system, and do not make any changes to the measurement system settings and measurement results during the measurement process. Figures 5 and 6 show the measurement results of the phase interface structure of water with different salinity in stratification and the phase holdup of air-bubble flow at different temperatures using the measurement system of the present invention.

图5给出本发明的测量系统对三组不同含盐量的水在分层情况下的界面特征的测量值和实验值的比较,无量纲高度的实验值通过已知液体体积和几何关系求出。从该图可以看出该测量系统的测量结果与实验结果相比绝对误差和实验的重复性误差均小于1%。Fig. 5 provides the measurement system of the present invention to the comparison of the measured value and the experimental value of the interface characteristics of three groups of water with different salinity in the case of layering, the experimental value of the dimensionless height is obtained by known liquid volume and geometric relationship out. It can be seen from the figure that the measurement result of the measurement system is less than 1% in both the absolute error and the repeatability error of the experiment compared with the experimental result.

利用本发明的测量系统对垂直管内的不同温度下空气-水泡状流的液相相含率进行测量,水的温度通过泵的运行对工质水自动加热。图6给出本发明的测量系统测量结果和实验结果的比较,实验结果采用快关阀法给出。从该图可以看出该测量系统的测量结果与实验结果相比绝对误差和实验的重复性误差均小于2.5%。The measurement system of the invention is used to measure the liquid phase holdup of the air-bubble flow in the vertical pipe at different temperatures, and the temperature of the water automatically heats the working medium water through the operation of the pump. Fig. 6 shows the comparison of the measurement results of the measurement system of the present invention and the experimental results, and the experimental results are given by the quick-closing valve method. It can be seen from the figure that the measurement result of the measurement system is less than 2.5% in absolute error and experimental repeatability error compared with the experimental result.

从以上两个实验结果可以看出本发明的单丝电容探针测量系统能实现对多相管流中相含率和相界面的连续在线实时测量,无需对测量结果进行修正并且具有很高的测量精度。From the above two experimental results, it can be seen that the monofilament capacitive probe measurement system of the present invention can realize continuous online real-time measurement of phase holdup and phase interface in multiphase pipe flow, without the need to correct the measurement results and has a high measurement accuracy.

Claims (4)

1. the monofilament capacitance Probe Measurement System for Fluid of phase content and phase interface in the multiphase pipe flow, comprise monofilament capacitance probe device (18) and capacitance voltage change-over circuit (19) that is connected with monofilament capacitance probe device (18) and signal processing apparatus (20), it is characterized in that: said monofilament capacitance probe device (18) comprises the monofilament capacitance probe (9) that is arranged in the measuring channel (8), be symmetrically arranged with upper bracket (6) and lower carriage (11) in the outside of measuring channel (8), in upper bracket (6) and the lower carriage (11) sealing shroud (5 is set all, 12), upper bracket (6) is provided with sleeve pipe (4) and upper end cover (3), upper end cover (3) is connected with upper bracket (6) by bolt (2), and also be provided with the electrode terminal (1) that is connected with an end of monofilament capacitance probe (9) on upper end cover (2), lower carriage (11) is provided with the bottom end cover (15) that clamping screw (13) is connected with the other end with monofilament capacitance probe (9);
Said capacitance voltage change-over circuit (19) adopts the CAV424 chip, and external first, second of CAV424 chip adjusted resistance R cx with reference oscillation circuitous resistance Rosc, first integrator electric current respectively with the 3rd limb 1, second integral device electric current adjusts resistance R cx 2Be connected, and reference oscillation circuitous resistance Rosc, first integrator electric current adjustment resistance R cx 1, second integral device electric current adjusts resistance R cx 2External the tenth limb ground connection together with the CAV424 chip; External the 4th limb of CAV424 chip and output voltage amplify resistance R L1Connect, this output voltage amplifies resistance R L1The other end guide to external voltage output terminal V 0, draw lead and another one output voltage amplification resistance R from external the 4th limb of CAV424 chip simultaneously L2Connect, output voltage amplifies resistance R L2An other end be connected with external the 6th limb of CAV424 chip; External the 6th limb and the load capacitance C of CAV424 chip VMConnect this load capacitance C VMAn other end ground connection; Direct and the another one voltage output end V of external the 6th limb of while CAV424 chip 1Connect; External the 11 limb of CAV424 chip is drawn lead and dc voltage power supply external connection end V CcConnect; External the 12,13,15 and 16 limbs of CAV424 chip respectively with the oscillatory circuit capacitor C OSC, the low pass circuit capacitor C L2, another low pass circuit capacitor C L1And reference capacitance C X1Connect the equal ground connection of an other end of these electric capacity; Draw the end C of lead from external the 14 limb of CAV424 chip to external monofilament capacitance probe device 0, be drawn out to the other end C of external monofilament capacitance probe device simultaneously from ground wire 1, from dc voltage power supply external connection end V CcInsert 5 volts direct supply; Two external connection end C of order silk capacitance probe device outside 0, C 1Two ends with monofilament capacitance probe (9) are connected respectively,
Signal processing apparatus (20) adopts C8051F000 single-chip microcomputer, the voltage output end V of the input end of signal processing apparatus (20) and capacitance voltage change-over circuit (19) 1With voltage output end V 0Connect.
2. the monofilament capacitance Probe Measurement System for Fluid of phase content and phase interface in the multiphase pipe flow according to claim 1 is characterized in that: said monofilament capacitance probe (9) comprises stainless steel wire (16) and is coated in the polytetrafluoroethylene floor (17) in stainless steel wire (16) outside.
3. the monofilament capacitance Probe Measurement System for Fluid of phase content and phase interface in the multiphase pipe flow according to claim 1 is characterized in that: also be provided with first insulation spacer (7) and second insulation spacer (10) between said measuring channel (8) and upper bracket (6) and the lower carriage (11).
4. the monofilament capacitance Probe Measurement System for Fluid of phase content and phase interface in the multiphase pipe flow according to claim 1 is characterized in that: also be provided with spring (14) between said clamping screw (13) and the bottom end cover (15).
CNB2006100427924A 2006-05-11 2006-05-11 Monofilament capacitive probe measurement system for phase holdup and phase interface in multiphase pipe flow Expired - Fee Related CN100409004C (en)

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