CN109925205A - Natural botanical hair dye and its application method of the compound common Chinese medicine effective component as dyestuff - Google Patents

Abstract

The invention discloses a natural plant hair dye which is compounded with common traditional Chinese medicine active ingredients as a dye and a use method thereof, and belongs to the technical field of hair dyeing. The natural hair dye of the present invention contains agent A of hair finishing agent and agent B which is composed of several active ingredients of traditional Chinese medicines as dyes, and also includes agent C based on trivalent aluminum salt and agent D based on ferric ion salt. Either the agent or the agent E based on ferrous ion salt. The natural plant hair dye of the present invention uses a variety of effective components of traditional Chinese medicine mixed as the dye of the hair dye, and can overcome the defects of the existing plant hair dye such as narrow dyeing range, long dyeing time, high dyeing temperature and poor fastness. At the same time, the active ingredients in common traditional Chinese medicines are also selected as pigments. In addition to being safe and inexpensive, they also have a variety of pharmacological activities, which are beneficial to control scalp itching, dandruff, and even head sores. In addition, the present invention does not use oil-soluble organic solvent, which further improves the green safety of the product.

Description

Natural plant hair dye with compound common traditional Chinese medicine active ingredients as dye and its use method

technical field

The invention belongs to the technical field of hair dyeing, in particular to a natural plant hair dye compounded with common traditional Chinese medicine active ingredients as dyes, and also relates to a method for using the natural plant hair dye compounded with common traditional Chinese medicine active ingredients as dyes.

Background technique

Hair dye is a cosmetic that dyes hair. With the improvement of people's living standards, hair coloring has become a fashion choice for more and more people, including people of all ages. However, traditional hair dyes contain benzene-like substances such as phenylenediamine, p-aminophenol, and hydroquinone. These substances have certain toxicity, and long-term use can lead to various diseases, such as hair loss, skin allergies and even cancer. Therefore, safe and efficient natural plant hair dyes are more attractive to consumers, and it is also the development direction of high-safety hair dyes in the future. In addition to the dyeing function, many natural plant pigments are also effective ingredients such as antibacterial, antioxidant, anti-allergic, and nourishing hair.

Natural plant pigments generally have defects such as narrow dyeing range, long dyeing time, high dyeing temperature and poor fastness. Most natural plant pigments have poor ability to use mordant. Due to the few types of mordants that can be used, the natural plant hair dyes have a single color tone, few types, and the problem of poor dyeing fastness, which greatly limits the application of natural plant hair dyes.

Theoretically, the combination of a variety of plant pigments and appropriate mordant is expected to overcome the deficiencies of the existing natural plant hair dyes. The Chinese patent "natural plant hair dye or dye" (application number: 201110410212.3) involves a hair dye in which red plants, yellow plants and blue plant pigments are mixed as compound dyes. The red plants are Salvia miltiorrhiza or red dragon fruit, and the yellow plants For Phellinus and Turmeric, the blue plants are Banlangen and Daqingye. The patent only focuses on the compounding of multiple vegetable dyes, ignoring the role of dye formulations and mordants. The patent "natural plant hair dye" (application number: 200510029176.0) discloses a plant hair dye consisting of two solutions of A and B, wherein agent A is essentially a mordant composed of an auxiliary agent and a metal ion chelating agent, B The agent is a dye consisting of pomegranate peel extract. The patent "a mordant for curcumin hair dye" (application number: 201210562703.4) discloses methylcyclopentadiene manganese tricarbonyl as a mordant for curcumin hair dye. Although these two patents consider the effect of mordant, the vegetable dye is a single vegetable pigment. It can be seen that using a variety of plant pigments mixed as a hair dye, supplemented by different mordants, can overcome the defects of the existing plant hair dyes. Since most plant pigments are not water-soluble, adding an appropriate amount of surfactant to the water-based matrix can avoid the use of oil-soluble solvents that are unfavorable to health, and can make various pigments highly dispersed, which is conducive to full contact with the hair and improves the dyeing rate.

SUMMARY OF THE INVENTION

In view of this, one of the objects of the present invention is to provide a natural plant hair dye that is compounded with common traditional Chinese medicine active ingredients as dyes; the second object of the present invention is to provide a method of using natural plant hair dyes that compound common traditional Chinese medicine active ingredients as dyes.

To achieve the above-mentioned purpose of the invention, the present invention provides the following technical solutions:

1, the natural plant hair dye of compound common traditional Chinese medicine active ingredient as dyestuff, described natural plant hair dye comprises A agent and B agent, also includes any one in C agent, D agent and E agent, wherein A agent is hair finishing Agent B, according to mass percentage, contains 1-5% of surfactant, and the balance is water; the B agent is a dye, and according to mass percentage, contains 5-15% of several traditional Chinese medicine active ingredient complexes, 5-10% The surfactant, 10-15% of the moisturizing agent, and the balance is water; the C agent contains 6-10% trivalent aluminum salt by mass percentage, and the balance is water; the D agent is based on the mass percentage It contains 6-10% of ferric salt, and the balance is water; the E agent contains 6-10% of ferrous salt according to mass percentage, and the balance is water.

Further, the A agent and the B agent respectively also contain a thickener with a mass percentage of 2-5%.

Further, the compound of several active ingredients of traditional Chinese medicines includes any one or more of coptisine, berberine, curcumin, rutin and baicalin.

Further, the surfactant includes any one or more of sodium lauryl alcohol polyoxyethylene ether sulfate, cocoic acid diethanolamide or lauryl trimethyl ammonium chloride.

Further, the C agent, the D agent and the E agent respectively comprise a thickener in a mass percentage of 1-2%.

Further, agent A, agent B, agent C, agent D and agent E also respectively comprise 0.1-0.5% by mass of plant essence, and the plant essence comprises any one of rose essence, jasmine essence or lavender essence or several.

Further, the thickener comprises any one or more of methyl cellulose, hydroxymethyl cellulose, hydroxyethyl cellulose, carboxymethyl cellulose, guar gum, gum arabic, gelatin or seaweed gum .

Further, the trivalent aluminum salt is potassium aluminum sulfate or aluminum trichloride.

Further, the ferric salt is ferric sulfate or ferric chloride; the divalent ferric salt is ferrous sulfate or ferrous chloride.

2. The use method of the above-mentioned compound common traditional Chinese medicine active ingredient as the natural plant hair dye of dye, the use method is as follows:

(1) First, apply agent A evenly on the hair, put on a shower cap or a special hair dyeing cap, keep it at 30-50°C for 10-30 minutes, and rinse with warm water;

(2) Apply agent B evenly on the hair, put on a shower cap or a special hair dyeing cap, and keep it at 30-50°C for 20-40 minutes;

(3) Apply any one of Agent C, Agent D or Agent E to the hair evenly, keep at 30-50°C for 30-60 minutes, rinse with warm water, and blow dry.

The beneficial effects of the present invention are:

1, the compound common traditional Chinese medicine active ingredient provided by the present invention is used as the natural plant hair dye of dyestuff, use multiple plant pigments to mix as the dyestuff of hair dye, the auxiliary with different compound plant dyes can overcome the narrow dyeing range that existing plant hair dyes have, Defects such as long dyeing time, high dyeing temperature, and poor fastness;

2. The compound common traditional Chinese medicine active ingredients provided by the present invention are used as natural plant hair dyes for dyes. Adding an appropriate amount of surfactant to the water-based matrix can avoid the use of oil-soluble solvents that are unfavorable to health, and can make various pigments highly dispersed, which is beneficial to Fully contact with the hair to improve the dyeing rate;

3. The compound common traditional Chinese medicine active ingredient provided by the present invention is used as the natural plant hair dye of dyestuff, and the selected pigment is the active ingredient in common traditional Chinese medicine, in addition to being safe and inexpensive, it also has a variety of pharmacological activities, which is conducive to controlling scalp pruritus, Dandruff and even head sores. At the same time, the present invention does not use oil-soluble organic solvent, which further improves the green safety of the product.

Detailed ways

The preferred embodiments of the present invention will be described in detail below. The experimental methods for which specific conditions are not indicated in the examples are usually in accordance with conventional conditions or in accordance with the conditions suggested by the manufacturer.

Example 1

Preparation of Agent A: Weigh 25 g of sodium dodecyl alcohol polyoxyacetate sulfate, 10 g of diethanolamine cocoate, and 15 g of dodecyl trimethoxy ammonium chloride in a 1000 ml beaker; measure the remaining amount of water 950 g and add it to the beaker medium; stir and dissolve at room temperature to make the mixture uniform to obtain agent A.

Preparation of agent B: weigh coptisine 25g, curcumin 25g, rutin 50g, baicalin 50g, add lauryl alcohol polyoxyethylene ether sodium sulfate 30g, coconut oleic acid diethanolamide 30g, dodecyltrimethyl Add 40 g of ammonium chloride, 50 g of glycerol, 50 g of propylene glycol, and 650 g of distilled water into a 1000-ml beaker, stir and dissolve in a 75°C water bath, and mix evenly to obtain agent B.

Preparation of agent C: Weigh 30 g of aluminum trichloride and 30 g of potassium aluminum sulfate, add 940 g of distilled water to dissolve, and mix them evenly to obtain agent C.

Preparation of agent D: Weigh 30 g of ferric sulfate and 30 g of ferric chloride, add 940 g of distilled water to dissolve, and mix them evenly to obtain agent D.

Preparation of agent E: Weigh 30 g of ferrous sulfate and 30 g of ferrous chloride, add 940 g of distilled water to dissolve, and mix them evenly to obtain agent E.

Example 2

Preparation of Agent A: Weigh 5g of sodium dodecyl alcohol polyoxyacetate sulfate, 5g of dodecyl trimethoxyammonium chloride and 1g of rose essence in a 1000ml beaker; weigh 10g of methylcellulose, carboxymethyl cellulose 2 g of base cellulose, 5 g of guar gum, 1 g of gum arabic, and 2 g of gelatin are placed in another beaker; 969 g of remaining water is measured, and half of each is added to the above two beakers; the beaker containing surfactant is stirred at room temperature. For dissolution, the beaker containing the thickener is stirred and dissolved in a water bath at 90°C; the two solutions are combined, stirred and mixed evenly to obtain agent A.

Preparation of agent B: weigh 30 g of berberine, 10 g of rutin, and 10 g of baicalin, add 50 ml of glycerol, 50 ml of propylene glycol, and 500 g of distilled water into a 1000 ml beaker, stir and dissolve in a water bath at 75°C for later use; weigh 10 g of methylcellulose, 10 g of guar Add 5g of glue, 2g of gum arabic, and 3g of gelatin in another beaker, add 380g of distilled water, stir and dissolve in a 95°C water bath; combine the above two cups of solutions, stir and mix evenly to obtain agent B

Preparation of agent C: Weigh 70 g of aluminum trichloride, add 500 g of distilled water to dissolve it for later use; also call 10 g of methyl cellulose, 5 g of guar gum, 2 g of gum arabic, and 3 g of gelatin in another container, add 410 g of water, and place in a water bath at 95°C Under stirring and dissolving for subsequent use; the above two solutions are combined and mixed evenly to obtain agent C.

Preparation of agent D: Weigh 70g of ferric sulfate, add 500g of distilled water to dissolve it for later use; also call 10g of methylcellulose, 5g of guar gum, 2g of gum arabic, and 3g of gelatin in another container, add 410g of water, and stir in a 90°C water bath. Dissolve for later use; combine the above two solutions and mix evenly to obtain agent D.

Preparation of agent E: Weigh 70 g of ferrous sulfate, add 500 g of distilled water to dissolve it for later use; also call 10 g of methyl cellulose, 5 g of guar gum, 2 g of gum arabic, and 3 g of gelatin in another container, add 410 g of water, and place in a water bath at 90°C. Stir and dissolve for later use; combine the above two solutions and mix evenly to obtain agent E.

Example 3

Preparation of agent A: weigh 15g of sodium lauryl alcohol polyoxyethylene ether sulfate and 15g of dodecyltrimethylammonium chloride in a 1000ml beaker for later use; weigh 10g of hydroxymethyl cellulose, 10g of guar gum, and alginate 5g is stored in another beaker for later use; Measure 945g of distilled water, add half to each of the above two beakers; stir and dissolve the beaker containing the surfactant at room temperature, stir and dissolve the beaker of the thickener at 75 ℃, and combine the above two beakers. The solution in a beaker is mixed evenly to obtain agent A

Preparation of agent B: 10g of coptisine or berberine, 20g of curcumin, 20g of rutin, 20g of baicalin, 30g of sodium lauryl alcohol polyoxyethylene ether sulfate, 40g of lauryl trimethyl ammonium chloride, Add 150g of propylene glycol and 2g of jasmine essence to a suitable container, add 400g of distilled water, keep warm in a 65°C water bath, and stir until completely dissolved for later use; take another weighing 20g of hydroxyethyl cellulose, 5g of guar gum, 2g of gum arabic, 5g of gelatin, and alginate 3 g, add 408 g of water, keep warm in a water bath at 85°C, stir and dissolve for later use; combine the above two solutions and mix them evenly.

Preparation of agent C: Weigh 80g of potassium aluminum sulfate, add 500g of distilled water to dissolve for later use; also call 5g of hydroxymethyl cellulose and 10g of gum arabic, in another container, add 390g of water, stir and dissolve in a 95°C water bath for later use; The two solutions are combined and mixed evenly to obtain agent C.

Preparation of agent D: Weigh 80 g of ferric chloride, add 500 g of distilled water to dissolve for later use; also call 5 g of hydroxymethyl cellulose and 10 g of gum arabic in another container, add 405 g of water, and stir and dissolve in a water bath at 80 °C for later use; The solutions are combined and mixed evenly to obtain agent D.

Preparation of agent E: weigh 80 g of ferrous chloride, add 500 g of distilled water to dissolve for later use; also call 20 g of hydroxymethyl cellulose, put 10 g of gum arabic in another container, add 390 g of water, stir and dissolve in a water bath at 80 °C for later use; mix the above two The solutions are combined and mixed evenly to obtain agent E.

Example 4

Preparation of agent A: weigh 20 g of sodium lauryl polyoxyethylene ether sulfate, 10 g of diethanolamine cocoate, and 10 g of dodecyl trimethyl ammonium chloride in a 1000 ml beaker, add 500 g of distilled water to stir and dissolve for later use; 20 g of hydroxyethyl cellulose, 5 g of guar gum, and 10 g of gum arabic, add 410 g of distilled water, keep warm in a 90°C water bath, and stir until completely dissolved for later use; combine the above two solutions, and mix well to obtain agent A.

Preparation of agent B: weigh coptisine or berberine 25g, curcumin 25g, rutin 25g, baicalin 25g, lauryl alcohol polyoxyethylene ether sodium sulfate 30g, coconut oleic acid diethanolamide 40g, glycerin 150g at appropriate Add 400g of distilled water to the container, keep warm in a water bath at 80°C, stir until completely dissolved for later use; take 10g of carboxymethyl cellulose, 5g of guar gum, 2g of gum arabic, 5g of gelatin, add 390g of water, keep warm in a 95°C water bath, stir and dissolve For subsequent use; combine the above two solutions and mix evenly to obtain agent B.

Preparation of agent C: Weigh 90g of aluminum chloride and 5g of lavender essence, add 500g of distilled water to dissolve for later use; also call 5g of hydroxyethyl cellulose, 5g of guar gum, and 3g of gelatin in another container, add 370g of water, and place in a water bath at 85°C Under stirring and dissolving for subsequent use; the above two solutions are combined and mixed evenly to obtain agent C.

Preparation of agent D: weigh 90g of ferric sulfate, add 500g of distilled water, dissolve for later use: also call 5g of hydroxyethyl cellulose, 5g of guar gum, 2g of gelatin, add 398g of distilled water, keep at 80°C, stir and dissolve completely for later use; The solutions are combined and mixed evenly to obtain agent D.

Preparation of agent E: weigh 90g of ferrous sulfate, add 500g of distilled water, dissolve for later use: also call it 20g of hydroxyethyl cellulose, 5g of guar gum, 10g of gelatin, add 375g of distilled water, keep at 70°C, stir and dissolve completely for later use; Combine the above two solutions and mix them evenly to obtain agent E.

Example 5

Preparation of agent A: 15g sodium lauryl alcohol polyoxyethylene ether sulfate, 15g lauryl trimethyl ammonium chloride, 15g coconut oleic acid diethanolamide, add 500g distilled water to dissolve for later use; also known as carboxymethyl fiber 15g of cellulose, 5g of hydroxyethyl cellulose, and 15g of guar gum, add 410g of distilled water, keep at 70°C, stir and dissolve for later use: combine the above two solutions and mix them evenly to obtain agent A.

Preparation of agent B: 10g of coptisine or berberine, 20g of curcumin, 50g of rutin, 50g of baicalin, 30g of sodium lauryl alcohol polyoxyethylene ether sulfate, 30g of coconut oleic acid diethanolamide, and lauryl 30g of trimethylammonium chloride, 100g of glycerol, and 50g of propylene glycol, add 400g of distilled water to a suitable container, keep warm in a water bath at 70°C, and stir until completely dissolved for later use; in addition, weigh 10g of methylcellulose, 30g of hydroxymethylcellulose, 5 g of guar gum, 3 g of gum arabic, and 2 g of seaweed gum, add 210 g of water, keep warm in a 90° C. water bath, stir and dissolve for later use; combine the above two solutions and mix well to obtain agent B.

Preparation of agent C: Weigh 100g of potassium aluminum sulfate, add 500g of distilled water to dissolve it for later use; 5g of carboxymethyl cellulose and 5g of alginate are added to another container, add 355g of water, and stir and dissolve in a 95°C water bath for later use; The two solutions are combined and mixed evenly to obtain agent C.

Preparation of agent D: weigh 100g of ferric chloride, add 500g of distilled water and 3g of lavender essence, and dissolve for later use: also called 5g of carboxymethyl cellulose and 5g of alginate, add 352g of distilled water, keep the temperature at 75°C, and stir and dissolve completely for later use; The two solutions are combined and mixed evenly to obtain agent D.

Preparation of agent E: weigh 100g of ferrous chloride, add 500g of distilled water, dissolve for later use: also called 20g of hydroxyethyl cellulose and 5g of seaweed glue, add 355g of distilled water, keep at 90°C, stir and dissolve completely for later use; The solutions are combined and mixed evenly to obtain agent E.

Embodiment 6 using method

Volunteer 1, a college teacher, male, 53 years old, with white hair accounting for about 30-40%, wants to dye the white hair dark, dislikes yellow and red, and says that he has never used any hair dye. Accordingly, the product of Example 2 of the present invention is used to dye hair, and I am very satisfied with the result. The specific process is: apply about 20g of agent A to the hair evenly, put on a shower cap, cover with a towel, put on an electric heating cap, control the temperature at 40°C for 20 minutes, rinse with warm water, and dry with a towel; take agent B Apply about 50g of agent A evenly to the hair, follow the operation of agent A, keep warm for 30 minutes, then take about 50g of agent E and apply it evenly to the hair, continue to keep at 40 ℃ for 40 minutes, rinse with warm water, and blow dry with a hair dryer; the result is all gray hair Dyeing, the overall color is dark brown.

Volunteer 2, female, college student, with short hair, has a history of using hair dye, and dyed his hair using the product of Example 2 of the present invention, and the result was yellow as a whole. The use process is: apply about 50g of agent A to the hair evenly, cover with a towel, put on an electric heating cap, control the temperature at 50°C for 10 minutes, feel unbearable, cut off the power immediately, keep it for 10 minutes, rinse with warm water , towel dry; take 50g of agent B and apply it to the hair evenly, operate according to agent A, after 20 minutes at 50 ℃, apply 50g of agent C evenly on the hair, continue to keep at 50 ℃ for 30 minutes, rinse with warm water, blow dry .

Volunteer 3, male, graduate student, had itchy scalp and dandruff. After using the product of Example 2 of the present invention once, the hair was dyed brown, and the itching disappeared. The specific use process is as follows: take 20g of agent A and apply it to the hair evenly, put on a shower cap, then put on an electric heating cap, keep it at 30°C for 30 minutes, rinse with warm water, and dry it with a towel; take 50g of agent B and apply it all over the hair, wear Put on the shower cap and keep the electric heating mantle at 30°C for 40 minutes. Apply 50g of Agent D to the hair evenly, continue to keep at 30°C for 60 minutes, rinse with warm water and blow dry.

Finally, it should be noted that the above preferred embodiments are only used to illustrate the technical solutions of the present invention and not to limit them. Although the present invention has been described in detail through the above preferred embodiments, those skilled in the art should Various changes may be made in details without departing from the scope of the invention as defined by the claims.

Claims (10)

1. compound common traditional Chinese medicine active ingredient as the natural plant hair dye of dyestuff, it is characterized in that, described natural plant hair dye comprises A agent and B agent, also comprises any one in C agent, D agent and E agent, wherein A The agent is a hair finishing agent, which contains 1-5% of surfactants by mass percentage, and the balance is water; the B agent is a dye, and contains 5-15% by mass of several active ingredient complexes of traditional Chinese medicine, 5-10% of surfactant, 10-15% of humectant, and the balance is water; the C agent contains 6-10% trivalent aluminum salt by mass percentage, and the balance is water; the D agent According to mass percentage, it contains 6-10% of ferric salt, and the balance is water; the E agent contains 6-10% of divalent iron salt according to mass percentage, and the balance is water. 2 . The natural plant hair dye according to claim 1 , wherein the A agent and the B agent further comprise a thickener with a mass percentage of 2-5%, respectively. 3 . 3. according to the natural plant hair dye of claim 1, it is characterized in that, described several kinds of Chinese medicine active ingredient complex comprise any one or several in coptisine, berberine, curcumin, rutin and baicalin. kind. 4. The natural plant hair dye according to claim 1, wherein the surfactant comprises sodium lauryl alcohol polyoxyethylene ether sulfate, cocoic acid diethanolamide or lauryl trimethyl Any one or more of ammonium chloride. 5 . The natural plant hair dye according to claim 1 , wherein the C agent, the D agent and the E agent further comprise 1-2% by mass of a thickener respectively. 6 . 6. The natural plant hair dye according to any one of claims 1 to 5, wherein agent A, agent B, agent C, agent D and agent E also contain 0.1 to 0.5% of plant essence by mass percentage respectively. , the plant essence comprises any one or more of rose essence, jasmine essence or lavender essence. 7. The natural plant hair dye according to claim 6, wherein the thickener comprises methyl cellulose, hydroxymethyl cellulose, hydroxyethyl cellulose, carboxymethyl cellulose, guar gum , any one or more of gum arabic, gelatin or seaweed. 8. The natural plant hair dye according to claim 7, wherein the trivalent aluminum salt is potassium aluminum sulfate or aluminum trichloride. 9. a kind of natural plant hair dye according to claim 8, is characterized in that, described ferric salt is ferric sulfate or ferric chloride; Described divalent ferric salt is ferrous sulfate or ferrous chloride. 10. The method of using a natural plant hair dye according to any one of claims 1 to 9, wherein the method of using is as follows: (1) First, apply agent A evenly on the hair, put on a shower cap or a special hair dyeing cap, keep it at 30-50 ℃ for 10-30 minutes, and rinse with warm water; (2) Apply agent B evenly on the hair, put on a shower cap or a special hair dyeing cap, and keep it at 30-50°C for 20-40min; (3) Apply any one of Agent C, Agent D or Agent E to the hair evenly, keep at 30-50°C for 30-60 minutes, rinse with warm water, and blow dry.