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CN109596243B - Fabrication method of sapphire fiber Fa-Per sensor based on femtosecond laser etching - Google Patents

Fabrication method of sapphire fiber Fa-Per sensor based on femtosecond laser etching Download PDF

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CN109596243B
CN109596243B CN201811315399.7A CN201811315399A CN109596243B CN 109596243 B CN109596243 B CN 109596243B CN 201811315399 A CN201811315399 A CN 201811315399A CN 109596243 B CN109596243 B CN 109596243B
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optical fiber
femtosecond laser
sapphire
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CN109596243A (en
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刘铁根
王双
江俊峰
于迅
刘琨
张学智
吴志洋
王润东
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Tianjin University
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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01KMEASURING TEMPERATURE; MEASURING QUANTITY OF HEAT; THERMALLY-SENSITIVE ELEMENTS NOT OTHERWISE PROVIDED FOR
    • G01K11/00Measuring temperature based upon physical or chemical changes not covered by groups G01K3/00, G01K5/00, G01K7/00 or G01K9/00
    • G01K11/32Measuring temperature based upon physical or chemical changes not covered by groups G01K3/00, G01K5/00, G01K7/00 or G01K9/00 using changes in transmittance, scattering or luminescence in optical fibres
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B23MACHINE TOOLS; METAL-WORKING NOT OTHERWISE PROVIDED FOR
    • B23KSOLDERING OR UNSOLDERING; WELDING; CLADDING OR PLATING BY SOLDERING OR WELDING; CUTTING BY APPLYING HEAT LOCALLY, e.g. FLAME CUTTING; WORKING BY LASER BEAM
    • B23K26/00Working by laser beam, e.g. welding, cutting or boring
    • B23K26/36Removing material
    • B23K26/362Laser etching

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Abstract

本发明公开了一种基于飞秒激光刻蚀的蓝宝石光纤法珀传感器及其制作方法,该传感器结构包括蓝宝石光纤(1)、石英光纤(5)及连接这两种光纤的异质光纤熔接点(6),所述蓝宝石光纤(1)尾端具有通过飞秒激光刻蚀加工的法珀微腔(2),法珀微腔(2)所具有的第一反射面(3)和第二反射面(4)产生的两束反射光发生干涉且产生干涉信号(11);当所处的环境温度发生变化时,所述法珀微腔(2)的腔长和材料折射率发生变化,两束反射光之间的光程差随之发生变化,从而导致干涉信号(11)的变化;通过解调干涉信号得到法珀光程差,进而得到被测温度。本发明具有理论创新性,尺寸小、环境适应力强的特点,可用于狭窄测量环境下的高温精确传感。

Figure 201811315399

The invention discloses a sapphire optical fiber Faber sensor based on femtosecond laser etching and a manufacturing method thereof. The sensor structure comprises a sapphire optical fiber (1), a quartz optical fiber (5) and a heterogeneous optical fiber fusion point connecting the two optical fibers (6), the tail end of the sapphire fiber (1) has a Fa-Pere microcavity (2) processed by femtosecond laser etching, and the Fa-Pert microcavity (2) has a first reflection surface (3) and a second reflection surface (3) and a second The two beams of reflected light generated by the reflection surface (4) interfere and generate an interference signal (11); when the ambient temperature changes, the cavity length and the refractive index of the material of the Fa-Per microcavity (2) change, and the two The optical path difference between the beams of reflected light changes accordingly, resulting in the change of the interference signal (11); the Fa-Per optical path difference is obtained by demodulating the interference signal, and then the measured temperature is obtained. The invention has the characteristics of theoretical innovation, small size and strong environmental adaptability, and can be used for high-temperature accurate sensing in a narrow measurement environment.

Figure 201811315399

Description

Method for manufacturing sapphire optical fiber Fabry-Perot sensor based on femtosecond laser etching
Technical Field
The invention relates to the technical field of optical fiber sensing, in particular to a manufacturing method of a miniaturized sapphire optical fiber high-temperature sensor manufactured based on a femtosecond laser precision etching process.
Background
The high-temperature sensing technology based on the sapphire optical fiber plays an important role in the field of high-temperature monitoring due to the characteristics of oxidation resistance, high precision, electromagnetic interference resistance, miniaturization and the like.
In recent years, various types of sapphire optical fiber sensors have been proposed to achieve extremely high temperature (1000 ℃ or higher) measurement, such as a fiber grating type, a black body radiation type, and a fiber fabry-perot type. Wherein: (1) the sapphire fiber grating sensor is limited by the larger numerical aperture of the sapphire fiber, the mode interference is serious, and the measurement precision is lower than that of other methods. (2) The blackbody radiation type sapphire optical fiber sensor has good temperature measurement precision in a high-temperature region (600 plus 1600 ℃) based on the Planck blackbody radiation law, but the temperature measurement range is limited because the radiation power of a low-temperature section is obviously reduced, the signal-to-noise ratio is attenuated at the maximum speed below 600 ℃, and the temperature measurement range is only used for monitoring the temperature of the high-temperature section. (3) The sapphire optical fiber Fabry-Perot sensor has an extremely wide measuring range, can be flexibly designed according to requirements, is manufactured by adopting a traditional grinding process and a laser etching technology, can be produced in batches, and is low in cost, so that the sapphire optical fiber Fabry-Perot sensor has a wide application range.
Because the sapphire optical fiber is manufactured in a crystal growth mode and is limited in length, remote sensing is generally realized internationally in a mode of welding the sapphire optical fiber and the quartz optical fiber, namely the sapphire optical fiber is used in a high-temperature area, and the quartz optical fiber is used in a normal-temperature area to lengthen the transmission distance. In the heterogeneous optical fiber coupling process, in order to achieve the coupling efficiency as high as possible, the sapphire optical fiber and the quartz optical fiber end face need to be polished to reduce the scattering loss of the fusion point.
Disclosure of Invention
Aiming at the defects of large size and low response speed of the traditional sapphire optical fiber sensor, the invention provides a manufacturing method of a sapphire optical fiber Fabry-Perot sensor based on femtosecond laser etching.
The invention relates to a method for manufacturing a sapphire optical fiber Fabry-Perot sensor based on femtosecond laser etching, which comprises a sapphire optical fiber 1, a quartz optical fiber 5 and a heterogeneous optical fiber fusion point 6 for connecting the two optical fibers, wherein the tail end of the sapphire optical fiber 1 is provided with a Fabry-Perot microcavity 2 processed by femtosecond laser etching, and two beams of reflected light generated by a first reflecting surface 3 and a second reflecting surface 4 of the Fabry-Perot microcavity 2 interfere with each other to generate an interference signal 11; when the ambient temperature changes, the cavity length and the material refractive index of the Fabry-Perot microcavity 2 change, and the optical path difference between the two beams of reflected light changes, so that the interference signal 11 changes; obtaining a Fabry-Perot optical path difference by demodulating the interference signal, and further obtaining the measured temperature; the manufacturing method specifically comprises the following steps:
step one, preparing a sapphire optical fiber with polished double end faces as a sensor material, and specifically operating the steps of:
cutting a sapphire optical fiber with the diameter of 100 micrometers into a section with the length of 15 centimeters, fixing the section through an optical fiber grinding machine spindle, exposing one end of the section out of the end face of the fixed ceramic ferrule by 0.2-0.5 millimeter, and adjusting the angle between the central shaft of the optical fiber grinding machine spindle and a grinding disc to be vertical to each other by 90 degrees; before polishing, selecting 10um fineness diamond grinding paper to shape and process the end face of the optical fiber: firstly, wetting a grinding disc by using water, and rotationally adsorbing grinding paper onto the grinding disc; checking the attaching degree between the grinding paper and the grinding disc, and processing after flattening and no bubble; controlling the spindle of the grinding machine to lift and fall through a five-dimensional displacement angle adjusting frame until the end face of the optical fiber is attached to grinding paper, enabling the ceramic ferrule to be in no contact with the grinding paper, turning on a rotary disc switch of the grinding machine, adjusting the rotating speed to be 50 revolutions per minute, and processing the end face of the optical fiber for the first time; roughly polishing the end face of the optical fiber to be flat, observing the end face of the optical fiber under a microscope, and finding that the end face is in a nearly circular hexagon and the surface is smooth and free of defects; sequentially changing the polishing paper into 7 microns, 3 microns and 1 micron, and polishing the end face of the optical fiber in the same steps; after finishing grinding and shaping, finally, carrying out high-precision polishing and grinding on the end face of the optical fiber, replacing the grinding paper with diamond polishing paper with the fineness of 0.3 mu m, spraying clean water on the contact part of the optical fiber and the grinding paper in the grinding process, keeping the optical fiber wet, adjusting the rotating speed to 30 revolutions per minute, and grinding for 15 minutes;
step two, utilize heterogeneous optical fiber fusion technique to construct sensor system, namely pass through the optical fiber fusion splicer with the one end of the sapphire optical fiber of bi-polar face polishing and quartz fiber and carry out manual butt fusion, constitute a complete transmission waveguide, concrete operation includes:
the quartz optical fiber is cut flat by an optical fiber cutter, the end face of the quartz optical fiber and the end face of the sapphire optical fiber are adjusted to be coaxial under a microscope of an optical fiber fusion splicer, the distance between the end faces is controlled to be 10-20 mu m, the advancing distance of an optical fiber clamping motor of the fusion splicer is set to be 30-35 mu m, and heterogeneous optical fibers are fused; after welding, one end of the quartz fiber is connected with the fiber coupler through a fiber jumper, the input end of the coupler is connected to the LED light source, and the receiving end of the coupler is connected to the micro spectrometer;
step three, performing femtosecond laser calibration and sapphire fiber Fabry-Perot microcavity etching, and specifically operating the steps of:
fixing a sapphire optical fiber on a clean glass slide, fixing the glass slide on a femtosecond laser processing platform, firstly adjusting the optical path collimation of a femtosecond laser, testing the processing precision of the femtosecond laser, and selecting a processing focal plane; controlling the processing platform to enable the focus of the femtosecond laser focusing objective lens to fall on the outer surface of the glass slide close to the objective lens, observing a clear image on the surface of the glass slide on a visible light microscope with the same optical path, and proving that the focus is aligned; moving the processing platform in the horizontal and vertical directions until the image surface is clear, proving that the processing platform is adjusted vertically, overlapping the outer surface of the glass slide with the focal plane of a focusing objective of a femtosecond laser, starting the femtosecond laser, selecting 500KHz for repetition frequency, 4W for power selection and 100ms for starting time, and performing trial processing on the sample wafer; shutting down, observing the surface of the sample wafer: if a black small hole with the diameter of 10-20 mu m is processed on the outer surface of the glass slide, the processing focus position is correctly selected; if the diameter of the processing hole is too large, or no burnt black hole appears on the sample wafer, the focal plane is found by fine adjustment of the position again; after the focusing is finished, the femtosecond laser focuses on the surface of the glass slide; controlling the electric control displacement table to move, displacing the blank glass slide from the position to the clamped end face of the sapphire optical fiber, and adjusting the position to be placed in a centering way; after moving, the focus of the femtosecond laser still aligns on the outer surface of the glass slide, a sapphire optical fiber to be processed is arranged between the objective lens and the glass slide, the electric control displacement platform is adjusted, the sample wafer is vertically retreated by the distance of the diameter of the sapphire optical fiber, and when the sample wafer under the microscope does not shake any more, the position is finely adjusted until an image presented under the microscope is clear; at the moment, a bright line is arranged at the position, closest to the objective lens, of the sapphire optical fiber, and the processing focal length is aligned to the edge of the outermost edge of the sapphire optical fiber; turning on a femtosecond laser, setting the repetition frequency of the femtosecond laser to be 500kHz, setting the power to be 2W, starting to process the sapphire optical fiber Fabry-Perot sensor, setting a processing platform to vertically displace according to a program, processing the optical fiber into strip edges when the optical fiber passes through a focus, and repeatedly processing the strip edges, wherein the width of each strip edge is determined by the diameter of a light spot; after a strip edge is processed, horizontally moving the processing platform, continuously processing to finish the processing of a shallow groove with the width of 70 mu m, then vertically pushing for 5 mu m, and repeating the processing procedures; the sapphire optical fiber Fabry-Perot sensor is sequentially and deeply pushed until the processing depth reaches about 50 mu m, so that the prototype of the sapphire optical fiber Fabry-Perot sensor is processed, and then the section left after half of a cylinder is cut off in the precision etching processing of the optical fiber, namely the first reflecting surface is polished; the sapphire optical fiber is adjusted to rotate by 90 degrees, the end face normal direction is parallel to the emergent light direction of the femtosecond laser, the processing platform is adjusted, a second reflecting surface to be polished is moved to the focal plane of the femtosecond laser, the femtosecond laser is opened, the repetition frequency of the femtosecond laser is set to be 50MHz, the power is set to be 2W, the second reflecting surface processed is polished, the sensor is connected to a demodulation system through an optical fiber jumper, the signal change is observed until interference fringes appear in a signal spectrum, the processing is stopped, and the sensor is manufactured completely.
Compared with the prior art, the sapphire optical fiber high-temperature sensor based on femtosecond laser etching and the manufacturing method thereof have the following positive effects:
1. the invention is manufactured by directly etching the optical fiber by femtosecond laser without other accessories, and has simple structure, reliable performance and economy; the sensor has the characteristics of small size and strong environmental adaptability, and can be used for high-temperature accurate sensing in a narrow measurement environment.
2. The temperature sensing principle of the invention is that the thermo-optic effect and the thermal expansion effect of the optical fiber are utilized to realize the change of the interference optical path difference and realize the conversion from the temperature to the interference optical path difference; compared with the traditional Fabry-Perot or Mach Zehnder temperature sensing, the invention has theoretical innovation.
3. By optimizing the optical path structure of the Fabry-Perot sensor, the invention overcomes the defects of complex mode of the large-numerical-aperture optical fiber and the influence of mode interference, and the structural theory has universal applicability.
Drawings
FIG. 1 is a schematic drawing of a polished microscope (photograph) of the end face of a sapphire fiber at different finenesses;
FIG. 2 is a microscopic (photograph) view of the fusion point of a sapphire fiber and a multimode silica fiber;
FIG. 3 is a fringe pattern etched at different powers in the femtosecond laser etching process of the sapphire optical fiber based on femtosecond laser etching according to the present invention;
FIG. 4 is a schematic structural diagram of a femtosecond laser etching-based sapphire optical fiber high-temperature sensor according to the invention;
FIG. 5 is a schematic diagram of optical path transmission of a femtosecond laser etching-based sapphire optical fiber high-temperature sensor according to the present invention;
FIG. 6 is a schematic view of a sensing system composed of a femtosecond laser etching-based sapphire optical fiber high-temperature sensor according to a first embodiment of the invention;
reference numerals: 1. sapphire optical fiber, 2 Fabry-Perot microcavity, 3, first reflecting surface, 4, second reflecting surface, 5, quartz optical fiber, 6, heterogeneous optical fiber fusion point, 7, optical fiber jumper wire, 8, 2X 1 optical fiber coupler, 9, LED light source, 10, original signal, 11, interference signal, 12 and spectrometer.
Detailed Description
The technical solution of the present invention will be described in further detail with reference to examples.
The first embodiment is as follows:
referring to fig. 4 and 6, an original signal 10 from a 850nm LED broadband light source 9 is guided into the fabry-perot microcavity 2 through an optical fiber jumper 7, a multimode silica fiber 5, a heterogeneous fiber fusion point 6, and a sapphire fiber 1, and light of an interference signal 11 is received by a spectrometer 12 through the sapphire fiber 1, the heterogeneous fiber fusion point 6, the silica fiber 5, and the optical fiber jumper 7 in sequence. The high temperature sensor is arranged in the tubular cavity of the high temperature muffle 13, a temperature variable is applied to the sensor by adjusting the temperature in the muffle cavity, and the measurement range is 100-. The change of the temperature causes the optical refractive index and the material expansion and contraction of the Fabry-Perot microcavity 2, the change of the Fabry-Perot optical path difference is caused, and the optical path difference of the sensor under the measurement environment temperature can be obtained by calculating interference spectrum information received by the spectrometer 12. Since the optical path difference of the sensor has a fixed relation delta 2n (T) L (T) with the refractive index of the sapphire wafer and the thermal expansion length of the wafer, the sensing real-time temperature can be obtained by reverse extrapolation.
A method for manufacturing a sapphire optical fiber Fabry-Perot sensor based on femtosecond laser etching specifically comprises the following steps:
the method comprises the following steps: and preparing a sapphire optical fiber with polished double end faces as a sensor material.
Cutting a sapphire optical fiber with the diameter of 100 micrometers into a section with the length of 15 centimeters, fixing the section by using an optical fiber grinder spindle, exposing one end of the section out of the end face of the fixed ceramic ferrule by 0.2-0.5 millimeter, and adjusting the angle between the central shaft of the optical fiber grinder spindle and the grinding disc to be vertical to each other by 90 degrees. Because the sapphire optical fiber has high hardness, before the sapphire optical fiber is polished, diamond grinding paper with fineness of 10 mu m is selected to carry out shaping processing on the end face of the optical fiber. The grinding disc is wetted by water, and the grinding paper is rotationally adsorbed on the grinding disc. And (5) checking the attaching degree between the grinding paper and the grinding disc, and processing the paper in a smooth and bubble-free manner. And controlling the spindle of the grinding machine to lift and fall through the five-dimensional displacement angle adjusting frame until the end face of the optical fiber is attached to the grinding paper, but the ceramic ferrule is not in contact with the grinding paper. And opening a rotary disc switch of the grinding machine, adjusting the rotating speed to be 50 revolutions per minute, and processing the end face of the optical fiber for the first time. Roughly polishing the end face of the optical fiber to be flat, observing the end face of the optical fiber under a microscope, and finding that the end face is in a nearly circular hexagon and the surface is smooth and free of defects.
Because 10um abrasive paper grinds the precision and is lower, observes under high power microscope after the fiber end face processing, can have multichannel strip arris. Insufficient end face finish can adversely affect both sensor signal quality and fusion quality of the foreign optical fiber. Thus, after obtaining a flat fiber end face by rough grinding, the end face is polished with a higher degree of fineness. And sequentially replacing the polishing paper with 7 mu m, 3 mu m and 1 mu m, and polishing the end face of the optical fiber by the same steps. And after finishing grinding and shaping, finally, carrying out high-precision polishing and grinding on the end face of the optical fiber, and replacing the grinding paper with diamond polishing paper with the fineness of 0.3 mu m. And (3) spraying cleaning water to the contact part of the optical fiber and the grinding paper in the grinding process, keeping the optical fiber wet, adjusting the rotating speed to be 30 revolutions per minute, and grinding for 15 minutes.
Step two: the heterogeneous optical fiber fusion constructs a sensor system.
And manually welding one end of the sapphire optical fiber with the quartz optical fiber through an optical fiber welding machine to form a complete transmission waveguide. And (3) flattening the end face of the quartz optical fiber by using an optical fiber cutter, and adjusting the end face of the quartz optical fiber and the end face of the sapphire optical fiber to be coaxial under a microscope of an optical fiber fusion splicer, wherein the distance between the end faces is controlled to be 10-20 mu m. Adjusting parameters of the fusion splicer for carrying out heterogeneous optical fiber fusion splicing, setting the advancing distance of an optical fiber clamping motor of the fusion splicer to be 30-35 mu m, and carrying out heterogeneous optical fiber fusion splicing. After the welding is finished, one end of the quartz optical fiber is connected with the optical fiber coupler through an optical fiber jumper, the input end of the coupler is connected to the LED light source, and the receiving end of the coupler is connected to the micro spectrometer. So far, a complete sensing system is initially established.
Step three: femtosecond laser calibration and sapphire fiber Fabry-Perot microcavity etching process.
Sapphire fibers were mounted on a clean glass slide that was mounted on a femtosecond laser processing platform. The processing platform is formed by combining a three-dimensional nanometer electric control displacement control platform and an angle adjusting frame, and can play a role in controlling the position and the angle of the processing platform. Firstly, adjusting the light path collimation of the femtosecond laser, testing the processing precision of the femtosecond laser, and selecting a proper processing focal plane. And controlling the processing platform to enable the focus of the femtosecond laser focusing objective lens to fall on the outer surface of the glass slide close to the objective lens. When the microscope is observed on a visible light microscope with the same optical path, a clear image on the surface of the glass slide can be observed, and the focusing is proved to be aligned. And moving the processing platform in the horizontal and vertical directions, wherein the image planes are clear, so that the processing platform is adjusted vertically, and the outer surface of the glass slide is superposed with the focal plane of the focusing objective of the femtosecond laser. And starting the femtosecond laser, wherein the repetition frequency is 500KHz, the power is 4W, and the starting time is 100ms, and the sample wafer is subjected to trial processing. And (5) shutting down the machine and observing the surface of the sample wafer. If the outer surface of the glass slide is processed with a black hole with the diameter of 10-20 μm, the processing focus position is correctly selected. If the diameter of the processing hole is too large, or no burning black hole appears on the sample wafer, the focal plane needs to be found by fine adjustment again.
After completion of the focusing, we have focused the femtosecond laser onto the slide surface. And controlling the electric control displacement platform to move, displacing the blank glass slide from the position to the end face of the clamped sapphire optical fiber, and adjusting the position to be centered. During the moving process, the sample wafer is ensured to move horizontally on the focal plane of the laser, and the vertical distance between the overload glass slide and the laser is not changed during the whole moving process. After the movement, the focus of the femtosecond laser is still aligned on the outer surface of the glass slide, but the sapphire optical fiber to be processed is added between the objective lens and the glass slide. Due to the near cylindrical structure of the sapphire fiber, a blurred image appears on the observation microscope. At the moment, the electric control displacement platform is adjusted to vertically retreat the sample wafer by the diameter of the sapphire optical fiber, and when the sample wafer under the microscope does not vibrate any more, the position is finely adjusted until the image displayed under the microscope is clear. At the moment, a bright line is arranged at the position, closest to the objective lens, of the sapphire optical fiber, and the processing focal length is aligned to the edge of the outermost edge of the sapphire optical fiber.
And (3) turning on the femtosecond laser, setting the repetition frequency of the femtosecond laser to be 500kHz and the power to be 2W, and starting to process the sapphire optical fiber Fabry-Perot sensor. And arranging a processing platform to vertically displace according to a program, and processing the optical fiber into a strip edge when the optical fiber passes through the focus. And repeatedly processing the strip edges, wherein the width of each strip edge is determined by the diameter of the light spot. In actual processing, the width of the strip edge is slightly smaller than the diameter of the light spot. And after one edge is machined, horizontally moving the machining platform, and continuing machining. Shallow trench processing of 70 μm width was completed. Then, the process was repeated while vertically advancing by 5 μm. And (5) sequentially and deeply propelling until the processing depth reaches about 50 um. So far, the sapphire optical fiber Fabry-Perot sensor prototype is processed, and then two semicircular end faces of the optical fiber are polished. Two semi-circular end faces, one of which is a polished reflecting surface, are cut in half during the machining process, but the remaining half still maintains a smooth finish. The center of gravity of the polishing work is the remaining cross section after half of the cylinder is cut off by the precision etching process, i.e., the second reflecting surface.
The sapphire optical fiber is adjusted to rotate by 90 degrees, and the normal direction of the end face is parallel to the emergent light direction of the femtosecond laser. And adjusting the processing platform, and moving the second reflecting surface to be polished to the focal plane of the femtosecond laser. And (5) turning on the femtosecond laser, setting the repetition frequency of the femtosecond laser to be 50MHz and the power to be 2W, and starting to polish the processed second reflecting surface. Attention is paid to avoid processing many times at two semicircle reflecting surface junctions, prevents to cause the destruction to the first reflecting surface that polishes. And cleaning the scraps produced in the processing process by using an ultrasonic cleaning machine. The sensor is connected to a demodulation system through an optical fiber jumper to observe signal change. And stopping processing until the signal spectrum has interference fringes, and finishing the manufacturing of the sensor.
When the sensor works, the end of the quartz optical fiber 5 is connected with the output end of the 2 x 1 optical fiber coupler 8 through the optical fiber jumper 7, and the spectrometer 12 is connected. The input end of the optical fiber coupler is connected with an 850nm LED light source 9 to provide an original light signal for the sensor, and the return end of the coupler is connected with a micro spectrometer 10. Original Gaussian light source signals 10 emitted from an 850nm LED light source 9 sequentially pass through a 2-1 optical fiber coupler 8, enter an optical fiber jumper 7, a quartz optical fiber 5, a heterogeneous optical fiber fusion point (6) and a sapphire optical fiber 1, enter a Fabry-Perot microcavity 2 processed by femtosecond laser etching, and interfere with each other. The interference signal 11 carries temperature information, passes through the heterogeneous optical fiber fusion point 6, the quartz optical fiber 5, the optical fiber jumper 7 and the 2 x 1 optical fiber coupler 8 in sequence from the sapphire optical fiber 1, and is received by the micro spectrometer 12. When the ambient temperature of the sensor changes, the cavity length and the material refractive index of the Fabry-Perot microcavity 2 change, and the optical path difference between the two beams of reflected light changes, so that the interference signal 11 changes. The Fabry-Perot optical path difference information can be obtained by demodulating the interference signal. And then reversely pushing back the temperature information of the sapphire optical fiber Fabry-Perot sensor.

Claims (1)

1.一种基于飞秒激光刻蚀的蓝宝石光纤法珀传感器的制作方法,该传感器结构包括蓝宝石光纤(1)、石英光纤(5)及连接这两种光纤的异质光纤熔接点(6),所述蓝宝石光纤(1)尾端具有通过飞秒激光刻蚀加工的法珀微腔(2),法珀微腔(2)所具有的第一反射面(3)和第二反射面(4)产生的两束反射光发生干涉且产生干涉信号(11);当所处的环境温度发生变化时,所述法珀微腔(2)的腔长和材料折射率发生变化,两束反射光之间的光程差随之发生变化,从而导致干涉信号(11)的变化;通过解调干涉信号得到法珀光程差,进而得到被测温度;其特征在于,该制作方法具体包括以下步骤:1. A method for manufacturing a sapphire fiber Faber sensor based on femtosecond laser etching, the sensor structure comprising a sapphire fiber (1), a silica fiber (5) and a heterogeneous fiber fusion splicing point (6) connecting the two fibers , the tail end of the sapphire fiber (1) has a Fa-Pere microcavity (2) processed by femtosecond laser etching, and the Fa-Pert microcavity (2) has a first reflection surface (3) and a second reflection surface ( 4) The generated two reflected lights interfere and generate an interference signal (11); when the ambient temperature changes, the cavity length and the material refractive index of the Fa-Per microcavity (2) change, and the two reflected lights change. The optical path difference between them changes accordingly, resulting in the change of the interference signal (11); the Fa-Per optical path difference is obtained by demodulating the interference signal, and then the measured temperature is obtained; it is characterized in that the manufacturing method specifically includes the following steps : 步骤一、制备双端面抛光的蓝宝石光纤作为传感器材料,具体操作包括:Step 1. Prepare double-end polished sapphire fiber as sensor material. The specific operations include: 将直径为100微米的蓝宝石光纤截成15厘米长的一段通过光纤研磨机纺锤固定,将其中的一端露出固定陶瓷插芯端面0.2至0.5毫米,调节光纤研磨机纺锤中轴与研磨盘角度呈90°垂直;在对其抛光之前,选择10um精细度的金刚石研磨纸对光纤端面做定型加工:先用水将研磨盘打湿,将研磨纸旋转吸附到研磨盘上;检查研磨纸与研磨盘之间的贴合度,平整无气泡后进行加工;将研磨机纺锤通过五维位移角度调整架升降控制到光纤端面贴合到研磨纸上,但陶瓷插芯与研磨纸无接触,打开研磨机转盘开关,调整转速为50转/分钟,对光纤端面进行第一次加工;粗略打磨光纤端面至平整,然后在显微镜下观察光纤端面,发现端面呈近圆六边形、表面光滑无缺陷即可;依次将抛光纸换成7μm、3μm、1μm,对光纤端面进行抛光操作,步骤同上;完成研磨定型后,最后要对光纤端面进行高精度的抛光打磨,将研磨纸换成精细度为0.3μm的金刚石抛光纸,研磨过程中对光纤与研磨纸接触处喷清洁水,保持湿润,调节转速为30转/分钟,研磨15分钟;Cut the sapphire fiber with a diameter of 100 microns into a 15 cm long section and fix it with the spindle of the fiber grinder. One end of the fiber grinder is exposed to the end face of the fixed ceramic ferrule by 0.2 to 0.5 mm. °Vertical; before polishing it, select 10um fine diamond abrasive paper to shape the fiber end face: first wet the abrasive disc with water, rotate and adsorb the abrasive paper to the abrasive disc; check the gap between the abrasive paper and the abrasive disc After smoothing and no bubbles, the grinding machine spindle is lifted and controlled through the five-dimensional displacement angle adjustment frame until the end face of the optical fiber is attached to the grinding paper, but the ceramic ferrule is not in contact with the grinding paper, and the switch of the grinding machine dial is turned on. , adjust the rotation speed to 50 rpm, and process the fiber end face for the first time; roughly polish the fiber end face to be flat, and then observe the fiber end face under the microscope, and find that the end face is nearly hexagonal, and the surface is smooth and defect-free; Change the polishing paper to 7μm, 3μm, and 1μm, and polish the fiber end face. The steps are the same as above; after finishing the grinding and shaping, the fiber end face should be polished with high precision, and the polishing paper should be replaced with diamond with a fineness of 0.3μm. Polishing paper. During the grinding process, spray clean water on the contact between the optical fiber and the grinding paper to keep it moist, adjust the speed to 30 rpm, and grind for 15 minutes; 步骤二、利用异质光纤熔接技术构造传感器系统,也就是将双端面抛光的蓝宝石光纤的一端与石英光纤通过光纤熔接机进行手动熔接,构成一个完整的传输波导,具体操作包括:Step 2: Construct the sensor system by using the heterogeneous optical fiber fusion splicing technology, that is, manually splicing one end of the double-end polished sapphire optical fiber and the quartz optical fiber through an optical fiber fusion splicer to form a complete transmission waveguide. The specific operations include: 将石英光纤用光纤切割刀切平端面,在光纤熔接机显微镜下,调节石英光纤端面与蓝宝石光纤端面至同轴,端面间距离控制在10-20μm,设置熔接机光纤夹持电机的前进距离为30-35μm,进行异质光纤熔接;熔接完毕后,石英光纤一端通过光纤跳线与光纤耦合器连接,耦合器的输入端连接到LED光源上,接收端连接到微型光谱仪;Cut the flat end face of the quartz fiber with a fiber cutter, and adjust the end face of the silica fiber and the end face of the sapphire fiber to be coaxial under the microscope of the optical fiber fusion splicer, and the distance between the end faces is controlled at 10-20 μm. 30-35μm, for heterogeneous fiber fusion; after fusion, one end of the quartz fiber is connected to the fiber coupler through a fiber jumper, the input end of the coupler is connected to the LED light source, and the receiving end is connected to the micro-spectrometer; 步骤三、进行飞秒激光器校准及蓝宝石光纤法珀微腔刻蚀,具体操作包括:Step 3. Perform femtosecond laser calibration and sapphire fiber Fa-Per microcavity etching. The specific operations include: 将蓝宝石光纤固定在一片清洁的载玻片上,载玻片固定到飞秒激光加工平台上,加工工序包括:首先调节飞秒激光器光路准直,测试飞秒激光器加工精度,选取加工焦面;控制加工平台,使飞秒激光器聚焦物镜的焦点落在载玻片靠近物镜的外表面上,在同光路可见光显微镜上观察到载玻片表面清晰像,证明焦点对准;水平、竖直方向移动加工平台,直至像面均清晰证明加工平台调垂直完成,载玻片外表面与飞秒激光器聚焦物镜焦面重合,飞秒激光器开机,重复频率选用500KHz、功率选择4W、开机时间选择100ms,对样片进行试加工;关机,观察样片表面:如果载玻片外表面被加工出一个直径10-20μm的黑色小孔,说明加工焦点位置选择正确;如果加工孔直径过大,或者样片上没有出现灼烧的黑孔,说明还需要重新微调位置寻找焦面;完成调焦后,飞秒激光器聚焦到载玻片表面上;这时控制电控位移台移动,由刚才的空白载玻片位置位移到夹持的蓝宝石光纤端面处,调整位置对中放置;移动后,飞秒激光器焦点仍然对准在载玻片外表面上,在物镜与载玻片之间为待加工的蓝宝石光纤,调节电控位移台,使样片垂直后退一个蓝宝石光纤直径的距离,待显微镜下样片不再震动时,微调位置至显微镜下呈现的像清晰;此时蓝宝石光纤最靠近物镜位置处为一条亮线,加工焦距对准在蓝宝石光纤最外缘的边上;打开飞秒激光器,设置飞秒激光器重复频率为500kHz,功率设置为2W,开始加工蓝宝石光纤法珀传感器,设置加工平台按程序竖直位移,光纤在经过焦点时被加工出条棱,重复加工条棱,每个条棱的宽度由光斑直径决定;加工出一个条棱后,水平移动加工平台,继续加工,完成70μm宽度的浅槽加工;然后垂直推进5μm,重复上述加工工序;依次深入推进,直至加工深度达到50μm,至此,蓝宝石光纤法珀传感器雏形已经加工完毕,接下来,对光纤精密刻蚀加工切除半个圆柱后剩下的截面,也就是第一反射面进行抛光处理;蓝宝石光纤调整旋转90°,端面法线方向与飞秒激光器出射光方向平行,调节加工平台,将待抛光的第二反射面移动到飞秒激光器焦面处,打开飞秒激光器,设置飞秒激光器重复频率为50MHz,功率设置为2W,对加工出来的第二反射面进行抛光,将传感器通过光纤跳线连接到解调系统上,观察信号变化,直至信号光谱出现干涉条纹,停止加工,传感器制作完毕。The sapphire fiber is fixed on a clean glass slide, and the glass slide is fixed on the femtosecond laser processing platform. The processing procedure includes: firstly adjust the optical path alignment of the femtosecond laser, test the processing accuracy of the femtosecond laser, and select the processing focal plane; control The processing platform enables the focus of the femtosecond laser focusing objective lens to fall on the outer surface of the glass slide close to the objective lens, and a clear image of the surface of the glass slide is observed on the visible light microscope with the same optical path, which proves that the focus is in alignment; horizontal and vertical movement processing The platform until the image surface clearly proves that the vertical adjustment of the processing platform is completed. The outer surface of the glass slide is coincident with the focal plane of the femtosecond laser focusing objective lens. The femtosecond laser is turned on. Carry out trial processing; turn off the machine and observe the surface of the sample: if a small black hole with a diameter of 10-20 μm is machined on the outer surface of the glass slide, it means that the processing focus position is selected correctly; if the diameter of the processing hole is too large, or there is no burning on the sample If the black hole is displayed, it means that it is necessary to fine-tune the position to find the focal plane; after the focusing is completed, the femtosecond laser is focused on the surface of the slide; at this time, the electronically controlled stage is controlled to move, from the position of the blank slide just now to the clip. At the end face of the sapphire fiber held, adjust the position and place it in the center; after moving, the femtosecond laser focus is still on the outer surface of the glass slide, and the sapphire fiber to be processed is between the objective lens and the glass slide, and the electronically controlled displacement is adjusted. When the sample no longer vibrates under the microscope, fine-tune the position until the image under the microscope is clear; at this time, the position of the sapphire fiber closest to the objective lens is a bright line, and the processing focal length is aligned On the edge of the outermost edge of the sapphire fiber; turn on the femtosecond laser, set the femtosecond laser repetition frequency to 500kHz, and set the power to 2W, start processing the sapphire fiber Faber sensor, set the processing platform to move vertically according to the program, and the fiber passes through the focus At the same time, the strips are processed, and the strips are processed repeatedly, and the width of each strip is determined by the diameter of the light spot; after processing one strip, the processing platform is moved horizontally, and the processing is continued to complete the shallow groove processing with a width of 70μm; and then vertically advance 5μm , repeat the above processing steps; advance in turn until the processing depth reaches 50 μm, so far, the prototype of the sapphire fiber Faber sensor has been processed, and then, the remaining cross-section after cutting half of the cylinder for the optical fiber precision etching process, that is, the first A reflective surface is polished; the sapphire fiber is adjusted and rotated by 90°, the normal direction of the end face is parallel to the direction of the emitted light of the femtosecond laser, the processing platform is adjusted, the second reflective surface to be polished is moved to the focal plane of the femtosecond laser, and the femtosecond laser is turned on. Second laser, set the femtosecond laser repetition frequency to 50MHz and power to 2W, polish the processed second reflective surface, connect the sensor to the demodulation system through the fiber jumper, observe the signal change until the signal spectrum interferes Stripes, stop processing, and the sensor is finished.
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