CN1089328C - Amino acid granular compound fertilizer and its producing method - Google Patents
Amino acid granular compound fertilizer and its producing method Download PDFInfo
- Publication number
- CN1089328C CN1089328C CN95118478A CN95118478A CN1089328C CN 1089328 C CN1089328 C CN 1089328C CN 95118478 A CN95118478 A CN 95118478A CN 95118478 A CN95118478 A CN 95118478A CN 1089328 C CN1089328 C CN 1089328C
- Authority
- CN
- China
- Prior art keywords
- fertilizer
- compound fertilizer
- granular compound
- amino acid
- mother liquor
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- 239000003337 fertilizer Substances 0.000 title claims abstract description 34
- 150000001875 compounds Chemical class 0.000 title claims abstract description 20
- 150000001413 amino acids Chemical class 0.000 title claims abstract description 18
- 238000000034 method Methods 0.000 title abstract 4
- 239000012452 mother liquor Substances 0.000 claims abstract description 20
- 239000007788 liquid Substances 0.000 claims abstract description 9
- 239000011573 trace mineral Substances 0.000 claims abstract description 9
- 235000013619 trace mineral Nutrition 0.000 claims abstract description 9
- 239000000843 powder Substances 0.000 claims description 11
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims description 8
- 238000005469 granulation Methods 0.000 claims description 8
- 230000003179 granulation Effects 0.000 claims description 8
- 238000004519 manufacturing process Methods 0.000 claims description 6
- 241000195940 Bryophyta Species 0.000 claims description 4
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 claims description 4
- 235000011114 ammonium hydroxide Nutrition 0.000 claims description 4
- 239000003245 coal Substances 0.000 claims description 4
- 239000008103 glucose Substances 0.000 claims description 4
- 239000003415 peat Substances 0.000 claims description 4
- 239000002893 slag Substances 0.000 claims description 4
- 239000004575 stone Substances 0.000 claims description 4
- 230000015572 biosynthetic process Effects 0.000 claims description 3
- 239000002686 phosphate fertilizer Substances 0.000 claims description 3
- 230000007062 hydrolysis Effects 0.000 claims description 2
- 238000006460 hydrolysis reaction Methods 0.000 claims description 2
- 239000000203 mixture Substances 0.000 claims description 2
- 235000015097 nutrients Nutrition 0.000 abstract description 5
- 239000002689 soil Substances 0.000 abstract description 4
- 239000000126 substance Substances 0.000 abstract description 4
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 abstract description 2
- 230000000694 effects Effects 0.000 abstract description 2
- 239000011574 phosphorus Substances 0.000 abstract description 2
- 229910052698 phosphorus Inorganic materials 0.000 abstract description 2
- 238000004321 preservation Methods 0.000 abstract description 2
- QJZYHAIUNVAGQP-UHFFFAOYSA-N 3-nitrobicyclo[2.2.1]hept-5-ene-2,3-dicarboxylic acid Chemical compound C1C2C=CC1C(C(=O)O)C2(C(O)=O)[N+]([O-])=O QJZYHAIUNVAGQP-UHFFFAOYSA-N 0.000 abstract 1
- LEVWYRKDKASIDU-QWWZWVQMSA-N D-cystine Chemical compound OC(=O)[C@H](N)CSSC[C@@H](N)C(O)=O LEVWYRKDKASIDU-QWWZWVQMSA-N 0.000 abstract 1
- 208000035240 Disease Resistance Diseases 0.000 abstract 1
- 229960003067 cystine Drugs 0.000 abstract 1
- 239000004021 humic acid Substances 0.000 abstract 1
- 230000001550 time effect Effects 0.000 abstract 1
- 235000001014 amino acid Nutrition 0.000 description 13
- 241000196324 Embryophyta Species 0.000 description 5
- LEVWYRKDKASIDU-IMJSIDKUSA-N L-cystine Chemical compound [O-]C(=O)[C@@H]([NH3+])CSSC[C@H]([NH3+])C([O-])=O LEVWYRKDKASIDU-IMJSIDKUSA-N 0.000 description 5
- 239000002253 acid Substances 0.000 description 5
- ZOXJGFHDIHLPTG-UHFFFAOYSA-N Boron Chemical compound [B] ZOXJGFHDIHLPTG-UHFFFAOYSA-N 0.000 description 2
- 229910052796 boron Inorganic materials 0.000 description 2
- 238000001035 drying Methods 0.000 description 2
- 238000000605 extraction Methods 0.000 description 2
- 210000003608 fece Anatomy 0.000 description 2
- 239000010871 livestock manure Substances 0.000 description 2
- 235000013599 spices Nutrition 0.000 description 2
- 238000003756 stirring Methods 0.000 description 2
- 241001465754 Metazoa Species 0.000 description 1
- YMKIRWHSXOBLCF-UHFFFAOYSA-N [Mg].[P].[Ca] Chemical compound [Mg].[P].[Ca] YMKIRWHSXOBLCF-UHFFFAOYSA-N 0.000 description 1
- -1 amino-acid compound Chemical class 0.000 description 1
- LFVGISIMTYGQHF-UHFFFAOYSA-N ammonium dihydrogen phosphate Chemical compound [NH4+].OP(O)([O-])=O LFVGISIMTYGQHF-UHFFFAOYSA-N 0.000 description 1
- 229910000387 ammonium dihydrogen phosphate Inorganic materials 0.000 description 1
- 229910021538 borax Inorganic materials 0.000 description 1
- KGBXLFKZBHKPEV-UHFFFAOYSA-N boric acid Chemical compound OB(O)O KGBXLFKZBHKPEV-UHFFFAOYSA-N 0.000 description 1
- 239000004327 boric acid Substances 0.000 description 1
- YYRMJZQKEFZXMX-UHFFFAOYSA-L calcium bis(dihydrogenphosphate) Chemical compound [Ca+2].OP(O)([O-])=O.OP(O)([O-])=O YYRMJZQKEFZXMX-UHFFFAOYSA-L 0.000 description 1
- 229910000389 calcium phosphate Inorganic materials 0.000 description 1
- 230000000536 complexating effect Effects 0.000 description 1
- 239000002131 composite material Substances 0.000 description 1
- 201000010099 disease Diseases 0.000 description 1
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 1
- 239000000284 extract Substances 0.000 description 1
- 235000003891 ferrous sulphate Nutrition 0.000 description 1
- 239000011790 ferrous sulphate Substances 0.000 description 1
- 230000004720 fertilization Effects 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- BAUYGSIQEAFULO-UHFFFAOYSA-L iron(2+) sulfate (anhydrous) Chemical compound [Fe+2].[O-]S([O-])(=O)=O BAUYGSIQEAFULO-UHFFFAOYSA-L 0.000 description 1
- 229910000359 iron(II) sulfate Inorganic materials 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 235000019837 monoammonium phosphate Nutrition 0.000 description 1
- 239000006012 monoammonium phosphate Substances 0.000 description 1
- 235000019691 monocalcium phosphate Nutrition 0.000 description 1
- 238000006386 neutralization reaction Methods 0.000 description 1
- 231100000252 nontoxic Toxicity 0.000 description 1
- 230000003000 nontoxic effect Effects 0.000 description 1
- 239000002367 phosphate rock Substances 0.000 description 1
- 239000004328 sodium tetraborate Substances 0.000 description 1
- 235000010339 sodium tetraborate Nutrition 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
- NWONKYPBYAMBJT-UHFFFAOYSA-L zinc sulfate Chemical compound [Zn+2].[O-]S([O-])(=O)=O NWONKYPBYAMBJT-UHFFFAOYSA-L 0.000 description 1
- 229960001763 zinc sulfate Drugs 0.000 description 1
- 229910000368 zinc sulfate Inorganic materials 0.000 description 1
Classifications
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A40/00—Adaptation technologies in agriculture, forestry, livestock or agroalimentary production
- Y02A40/10—Adaptation technologies in agriculture, forestry, livestock or agroalimentary production in agriculture
- Y02A40/20—Fertilizers of biological origin, e.g. guano or fertilizers made from animal corpses
Landscapes
- Fertilizers (AREA)
Abstract
The present invention discloses amino acid granular compound fertilizer produced by mother liquid after cystine is produced by hair and a preparing process thereof. The present invention is characterized in that phosphorus fertilizer containing humic acid substances and multiple trace elements is added to the mother liquor to make up the product. Compared with liquid fertilizer the amino acid granular compound fertilizer has the advantages of complete nutrients, easy use, long time effect, high fertilizer effect, easy preservation, etc. Compared with chemical fertilizer, the amino acid granular compound fertilizer has the advantages of complete nutrients, soil hardening after the amino acid granular compound fertilizer is used, soil improvement, drought resistance and disease resistance of crops increase, etc. The suggested preparing process has the advantages of simple process and easy operation.
Description
The invention belongs to compound manure, relate to a kind of production method of amino acid granular compound fertilizer.
As everyone knows, amino acid can directly be absorbed by plant, is a kind of fabulous nutrient of plant, can be used for the base manure of various plants and topdresses, and the trend that replaces chemical fertilizer is arranged.Contain multiple (having 18 kinds more than) amino acid in the hair of various animals, mainly produce Gelucystine in the prior art with hair, mother liquor behind the also useful extraction Gelucystine is directly as amino-acid liquid fertilizer, extracts the report that mother liquor production behind the Gelucystine contains the granular compound fertilizer of multiple amino acids, detritus acid and various trace elements but also find no as the present invention's utilization by hair.
The objective of the invention is to disclose the production method of the granular compound fertilizer that hair, the material that contains detritus acid and various trace elements that a kind of usefulness contains multiple amino acids make.The purpose that adds trace element is the fertilization effect that increases this granular compound fertilizer, improves its use value.
The present invention is achieved in that adding in the ammoniacal liquor and the mother liquor of back formation is reprocessed with hair, hydrochloric acid through hydrolysis, (a) phosphate fertilizer and the peat composed of rotten mosses or glucose slag and/or coal stone are pulverized the back and admixed into moistening with mother liquor and mix thoroughly, dry then and be ground into powder again; (b) trace element and mother liquor are made contact to complex liquid, then with the finished product that powder is mixed thoroughly, granulation forms granular compound fertilizer of step (a) gained or directly by the powder of step (a) gained through granulation and granular compound fertilizer.Hair and hydrochloric acid are hydrolyzed, add in the ammoniacal liquor and filtration formation mother liquor, this mother liquor is mainly used to extract Gelucystine in the prior art, and what the mother liquor after the extraction had directly uses as the liquid amino acid fertilizer.This programme is to reprocess with this mother liquor.The first, with phosphate fertilizer and contain the peat composed of rotten mosses (or glucose slag) of a large amount of detritus acid or add coal stone again, be ground into powder together; make contact to moistening shape with mother liquor; stir, dry, be ground into powder then, make granular compound fertilizer through the tablets press granulation.17 seed amino acids and the acid of multiple detritus and a small amount of trace element are contained in this composite fertilizer; In order to improve the fertilizer efficiency of granular compound fertilizer, the second, the powder that trace element and mother liquor is made contact to the complex liquid and first gained is fully mixed thoroughly, forms the granular compound fertilizer that contains multiple amino acids, detritus acid and various trace elements through granulation.
Advantage of the present invention is to compare with the liquid amino-acid compound fertilizer, and it is complete, easy to use to have a required nutrient of the plant of containing, and timeliness is long, easily by plant absorbing, and fertilizer efficiency height, easily advantage such as preservation.Compare with chemical fertilizer, it is complete to have a nutrient, owing to contain multiple amino acids so the crop of increasing sugar part is arranged, increase crop drought resistance, resistance against diseases, use the soil, back not harden, can improve the soil, safe in utilization, nontoxic pollution-free, nuisanceless advantage is a best fertilizer of producing green food.The present invention's production method technology is simple, processing ease.
The embodiment of the invention: with calcium superphosphate 300Kg or contain double superhosphate or monoammonium phosphate or calcium magnesium phosphorus or ground phosphate rock with its equivalent phosphorus, with the peat composed of rotten mosses or glucose slag 150Kg or add coal stone 150Kg again and pulverize, with be hydrolyzed with hair 300Kg and hydrochloric acid, add the ammoniacal liquor neutralization again, filter extracting mother liquor behind the Gelucystine admixes (using the mother liquor about 1/3 approximately) and is moistening and fully mixes thoroughly, drying below 100 ℃ then, making its water ratio below 8%; Add about 1/3 mother liquor again and carry out mixing thoroughly the second time and drying, be ground into powder then; The purpose of carrying out twice spice is for the aminoacid component in the mother liquor that contains q.s in the assurance products obtained therefrom, at this moment is that available tablets press granulation becomes granular compound fertilizer.For the fertilizer efficiency that improves fertilizer can be with zinc sulfate 20Kg, sal epsom 20Kg, ferrous sulfate 35Kg, borax 15Kg boric acid, the boron mud of equivalent boron (or contain), contact with about 1/3 mother liquor, carry out complexing in 1 hour at 40 ℃ of left and right sides stir abouts and form complex liquid, carry out for the third time with aforementioned powder that spice makes evenly then, form the finished product through granulation again.
Claims (1)
1, a kind of production method of amino acid granular compound fertilizer, be to adding in the ammoniacal liquor and the mother liquor of back formation is reprocessed through hydrolysis with hair, hydrochloric acid, it is characterized in that: (a) phosphate fertilizer and the peat composed of rotten mosses or glucose slag and/or coal stone are pulverized the back and admixed into moistening with mother liquor and mix thoroughly, dry then and be ground into powder again; (b) trace element and mother liquor are made contact to complex liquid, then with the finished product that powder is mixed thoroughly, granulation forms granular compound fertilizer of step (a) gained or directly by the powder of step (a) gained through granulation and granular compound fertilizer.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN95118478A CN1089328C (en) | 1995-10-30 | 1995-10-30 | Amino acid granular compound fertilizer and its producing method |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN95118478A CN1089328C (en) | 1995-10-30 | 1995-10-30 | Amino acid granular compound fertilizer and its producing method |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN1149569A CN1149569A (en) | 1997-05-14 |
| CN1089328C true CN1089328C (en) | 2002-08-21 |
Family
ID=5081725
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN95118478A Expired - Fee Related CN1089328C (en) | 1995-10-30 | 1995-10-30 | Amino acid granular compound fertilizer and its producing method |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN1089328C (en) |
Families Citing this family (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP3689302B2 (en) * | 2000-03-15 | 2005-08-31 | 昭博 清野 | Soil solidifying agent, soil solidifying method, and consolidated solidified ground |
| CN101287688B (en) | 2005-10-14 | 2013-01-02 | 阿彻-丹尼尔斯-米德兰公司 | Fertilizer compositions and methods of using |
| RU2394556C1 (en) * | 2008-12-05 | 2010-07-20 | ООО "Фитолон-Наука" | Humic concentrate, containing humic acids, method of obtaining it and composition for head hair and skin care |
| CN102040406B (en) * | 2010-10-12 | 2013-01-02 | 上海绿乐生物科技有限公司 | Method for producing compound microbial fertilizer from amino acid organic granules |
| CN104761313A (en) * | 2015-04-10 | 2015-07-08 | 山东滨州清大科技有限责任公司 | Method for preparing organic nutritional agent for fruit tree in saline-alkali soil |
| CN108530167A (en) * | 2018-05-03 | 2018-09-14 | 嘉施利（应城）化肥有限公司 | A kind of compound fertilizer anticaking agent and preparation method thereof |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1051723A (en) * | 1989-11-17 | 1991-05-29 | 抚顺市露天区新屯街道办事处 | Preparation for organic fertilizer of self-growth alcohol yeast |
| CN1052654A (en) * | 1991-01-08 | 1991-07-03 | 王秀云 | Amino acid fertilizer and its production method |
| CN1058387A (en) * | 1990-07-21 | 1992-02-05 | 北京东城开元新技术公司 | The application of industrial effluent during Gelucystine is produced |
-
1995
- 1995-10-30 CN CN95118478A patent/CN1089328C/en not_active Expired - Fee Related
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1051723A (en) * | 1989-11-17 | 1991-05-29 | 抚顺市露天区新屯街道办事处 | Preparation for organic fertilizer of self-growth alcohol yeast |
| CN1058387A (en) * | 1990-07-21 | 1992-02-05 | 北京东城开元新技术公司 | The application of industrial effluent during Gelucystine is produced |
| CN1052654A (en) * | 1991-01-08 | 1991-07-03 | 王秀云 | Amino acid fertilizer and its production method |
Also Published As
| Publication number | Publication date |
|---|---|
| CN1149569A (en) | 1997-05-14 |
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| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| C57 | Notification of unclear or unknown address | ||
| DD01 | Delivery of document by public notice |
Addressee: Tang Zengyi Document name: payment instructions |
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| C19 | Lapse of patent right due to non-payment of the annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |